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By J. S. Mitchell

Cobalt recovery from arsenical concentrates by pressure leaching and reduction involves special methods and operating problems. Principal steps in the process are auto-oxidation acid leaching under pressure, filtration of the tailings, purification of the solution, hydrogen reduction of the ammoniacal solution, and electrical furnacing for sulfur removal and granulating the metal. Extracting cobalt metal from arsenical ores has presented a major metallurgical problem for many years. In acquiring the Blackbird mine near Salmon City, Idaho in 1943 Calera Mining Co. accepted the challenge to solve this problem.

Nov 1, 1956

Jan 1, 1897

By Robert Carlson, Hugh McMillan

During 1967, the Metropolitan Sanitary District of Greater Chicago adopted a policy of land application as a method of using the solids produced in the wastewater treatment process. Research by the Agronomy Department of the University of Illinois, several demonstrations on farm land, reclamation of acid strip-mine spoils, fertilizing a land fill, and reclamation of an alkaline sand waste pit showed the value of using wastewater solids to reclaim marginal and submarginal lands. To launch the Solids-On-Land Program, 10,000 acres of land in Fulton County, Ill., was purchased, part of it previously strip-mined for coal. The Sanitary District initiated a water monitoring program, constructed holding basins, leveled the land, awarded a liquid fertilizer transportation contract, installed a distribution end application system, and began application and crop production. During 1972, the Sanitary District completed the first year of application and harvested the first corn crop. The corn yielded 60 bu per acre while the previous year in a demonstration field it yielded 56 and 13 bu per acre, respectively, on treated and untreated strip-mined land.

Jan 1, 1976

By William Hamilton Merritt

At the Atlanta Meeting in October, 1895, a short paper was presented by Mr. R. W. Leonard on the " Assay of Auriferous Ores and Gravels by Amalgamation and the Blow-pipe" (Trans., xxv., 645), embodying the results of some very conclusive tests as to the value of the process. His arguments regarding the desirability of the process appear to be indisputable, but the practicability of the field-outfit used by him is open to question. The Province of Ontario, in which Kingston is situated, is still largely unexplored; and at the Kingstoil School of Mining we give much attention to the instruction of prospectors and the testing of ores. To this end, not only is there a small mill (to which Mr. Leonard alludes) attached to the school, but prospectors' classes

Jan 1, 1897

By H. Carroll Weed

By caving a block into the workings of its open pit and using the block as an ore transfer, the Inspiration Consolidated Copper Co. has solved a transportation and sizing problem, making possible a great expansion of open-pit methods as applied to Inspiration ore- bodies.

Jan 9, 1953

By Joseph J. Becker

RECENTLY the "oriented growth" hypothesis of recrystallization textures has been receiving considerable attention. According to this view, "whenever a new generation of grains is growing in a highly oriented matrix . . . one may assume . . . that from among available nuclei of a great variety of orientations those with suitable orientation relationship with respect to the matrix have by far the highest rate of growth (oriented growth) and will, therefore, predominate."' This statement includes primary recrystallization of single crystals and of polycrystalline materials showing strong deformation textures as particular cases. While the phenomenon of oriented growth undoubtedly does operate, and may be of importance in coarsening or secondary recrystallization, the writer feels that its extension to primary recrystallization is a different matter. Several aspects of this phenomenon may be pointed out which are difficult to rationalize on the basis of oriented growth. In recrystallizing deformed single crystals of alpha brass, Maddin, Mathewson, and Hibbard2 found that the twin composition planes of the recrystallized grains were parallel to the three operative slip planes they observed, and not to the fourth octahedral plane. The writer's current work seems to indicate further that when only one or two slip systems can be seen to operate, the recrystallized grains are aligned only with those slip planes actually observed. This behavior could hardly be accounted for by oriented growth, because on the latter basis the recrystallized texture of a deformed single crystal should certainly have the same symmetry as the crystal itself. Growth rates could not be expected to distinguish between crystallogra- phically equivalent directions, unless the presence of a visible slip system vastly increases the growth rate in the appropriate direction. This seems unlikely. These relationships were observed by the writer only when considerable care had been exercised before annealing to etch away the effects of cutting out the centers of tensile specimens with a jeweler's saw and to etch off the ends of compression specimens. When these.precautions were not taken, nu-cleation inevitably appeared to occur at the saw cuts or at the ends, and the resulting orientations never showed a [111] rotation but appeared quite random. The provision of many nuclei of many orientations did not enhance the correlation, but destroyed it. Recrystallization textures are sometimes strongly dependent on annealing temperature, which would imply that the anisotropy of growth rates is a suddenly varying function of temperature. This might be regarded as unlikely. Recrystallization textures can be strongly dependent on the degree of deformation. If textures are to be explained by selective growth from among nuclei of all orientations, it is difficult to see how the recrystallization process could have any dependence whatever on the manner or degree of deformation. It is felt that the above points should be considered before the oriented growth hypothesis is applied to primary recrystallization, with the necessary complete divorce of the mechanism of recrystallization from the details of the deformation process. References 1P. A. Beck and H. Hu: Reply to discussion of their paper on Recrystallization Texture and Coarsening Texture in High Purity Aluminum. Trans. AIME, 188, 1057; Journal oF Metals (Aug. 1950) TP 29083. 'R. Maddin, C. H. Mathewson, and W. R. Hibbard, Jr.: The Origin of Annealing Twins in Brass. Trans. AIME, 185, 655; Journal of Metals (Sept. 1949) TP 26763.

Jan 1, 1952

By Alexander Sutulov

The Western industrial nations are facing today what can be defined as a gradual takeover of their investments in the developing world and more importantly, they are beginning to feel approaching problems with their adequate raw materials supply. This puts them into a strategically hazardous situation, which years ago would probably have been solved by conventional wars. However, the present political and military situation, and particularly the development of nuclear arms, makes such confrontations almost impossible or at least extremely dangerous. Thus other peaceful and more pragmatic solutions should be sought. This is particularly important because the present supply-demand situation in raw materials has a very strong political and ideological background. In the ultimate analysis there are two economic systems, that of free enterprise and the other of the collective or socialistic ownership. Both are competing for world domination, and it seems that both are eager to prove their advantages to the yet uncommitted Third World, which commands the great majority of the human race and a large part of its natural resources.

Jan 7, 1974

ASIDE from the John Fritz Medal, in which the Institute participates through its representation on the John Fritz Medal Board, the Institute itself has five major awards to make annually for excellence in technical papers, as follows: The Robert W. Hunt Medal, The Hadfield Prize, The J. E. Johnson Jr., Award, The Lewisohn Platinum Prize to senior members, and the President's Prize to junior members. ROBERT W. HUNT MEDAL The partners of Robert W. Hunt established a fund which was presented to the Institute at a fitting ceremony on May 27, 1920, to establish an annual medal and a sum of money to be awarded under the following rules: 1. The award shall consist of two prizes; first of a gold medal, second of a sum of money; a certificate to accompany each prize. The money prize shall not be awarded to. a member over 40 years of age, but under unusual circumstances, both prizes may be allotted to one person provided that he is not over 40 years of age. In general it will be understood that the Committee shall award the money prize to the younger men, rather than the medal. 2. The awards shall be made not oftener than once a year to that person or persons contributing to the Institute the best original paper or papers on iron and steel. The scope of the term "iron and steel" shall be determined by the sub-committee considering the awards. In general, papers dealing with the practical side of the subject have preference over those dealing with the theoretical side in recognition of the fact that Captain Hunt's main contributions to the industry have been in the improvement of production and quality of material. 3. A sub-committee of three to five including the Chairman of the Iron and Steel Committee, shall be appointed by the iron and Steel Committee annually to adjudge the award subject to approval. 4. The awarding committee shall submit its report to the Iron and Steel Committee at its October Meeting, and the. award be certified to the Secretary of the Institute in time to permit the presentation to be made at the Annual Meeting of the Institute. 5. The recipient of the award shall be designated "The Hunt Medallist." SIR ROBERT HADFIELD PRIZE Sir Robert Hadfield has offered an Institute prize of $1000 for researches with regard to the different forms of combination of carbon in iron and steel. Until within a few weeks no paper has been submitted which could compete for this prize. If the paper in hand should not meet the requirements, the donor has suggested that the prize be transferred and offered for: (a) the determination of the hardness in metals in connection. with super-hardness, (b) in consideration of questions of fuel economy, (c) in consideration of questions of industrial development and labor. J. E. JOHNSON, JR. AWARD This award is made from the income of a fund of $3000 donated by Mrs. Margaret Hilles Johnson in memory of her husband, J. E. Johnson, Jr., who was a prominent engineer, author of two valuable volumes on iron blast-furnace construction and practise, vice-chairman of the Institute's Iron and Steel Committee, and a frequent contributor of papers to the Institute's TRANSACTIONS.

Jan 1, 1925

By Robert H. Richards

OF the several professions-the chemist, the civil engineer, the mining engineer, the mechanical engineer-the courses of instruction, as arranged at the scientific schools, differ considerably as to the amount of practical information which the student is able to gain. The analytical chemist has facility for a very thorough review of the processes which he will be called upon to perform. The student in civil engineering by his field practice learns the use of his tools and the art of taking field-notes. The mechanical engineering student is in the vicinity of machine-shops, which he can visit, and at which he can work. The student in mining engineering has no such advantages. The mines are at a distance, and the railroad fare to get to them is oftentimes an insuperable difficulty. The aim of these laboratories is essentially to give to the student in mining and metallurgy a chance to study on a small scale the practical parts of his profession. We cannot, in a small laboratory, build a mine to timber, to work, and to survey; we cannot make artificial quicksands and other impediments to mining. In short, we cannot study exploration; but we can study the mechanical preparation and the subsequent smelting of ores. Before presenting the plan of these laboratories it may be interesting to indicate the progress of the idea from its beginning. During the summer of 1870 President Runkle visited the mines of Colorado, and while there, conceived the idea of making an expedition with the mining students to some of the Western mining regions. He talked over the scheme with many railroad and mining men, and everywhere received encouragement. In the summer of 1871 the Institute party visited the mines of Colorado, and spent six weeks in taking notes of them. President Runkle here conceived the idea of building up a mining and metallurgical laboratory ; and by the aid of Booth & Co. of San Francisco, a stamp-mill was obtained, with the Washoe silver-working apparatus. During the year

Jan 1, 1873

By K. J. Reid, H. A. Lex, I. Iwasaki, K. A. Smith

The effects of autogenous grinding and conventional grinding on the floatabilities of copper-nickel sulfides from Duluth gabbro were investigated. At the same mesh-of-grind copper, nickel, and cobalt recoveries were higher and residual sulfur in the flotation tailings was lower with the autogenously ground pulps. With the ball-mill ground pulps the residual sulfur in the tailings could not be lowered to the level attained by the autogenously ground pulps even at increased levels of the collector addition. From mineralogical examinations of concentrate and tailings samples, an electrochemical interaction between grinding media and sulfide minerals was thought to have a greater effect on sulfide mineral flotation behavior than the breakage characteristics of the ore samples in these two types of mills.

Jan 1, 1984

By K. H. Nimerick, B. E. Scott, F. J. Beafore

A unique freeze conditioning agent (FCA) which functions by forming structurally weak ice rather than suppressing the freezing point of water has been successful in alleviating frozen coal problems. Frozen coal treated with FCA has been quickly unloaded at temperatures below -17.8OC (O°F). Other applications of FCA include deicing: conveyor belts, idler, idler arms, and other moving parts that have been impeded by ice.

Jan 1, 1980

By John V. Beall

One Sunday night last month the phone rang and it was George Schenck from Penn State. How would we like to see a big scrap operation, he wanted to know. A few days later we were on the Connecticut turnpike headed for New Haven to visit a large scrap operation, M. Schiavone and Sons. George had a large clam basket in the back which he explained was for collecting trophies. The car shredder, he said, turns out some fancy metal shapes. In fact, they have gained a certain acceptance as objets d’art among George's friends and relatives. He thinks there may be a small, but possibly lucrative secondary market for shredded cars in the art world if the idea is imaginatively promoted. On the way to New Haven we received a briefing on the scrap industry. The scrap business grew from humble beginnings. Mostly it was started by a few immigrant Jews who collected junk in hand- or horse-drawn carts. The fortunate one might even have had a truck. Before proceeding further, we hasten to point out that the word "junk" is strictly taboo among scrap people, who prefer to refer to their industry as the "secondary metals industry."

Jan 1, 1970

Elected Died 1895 *ABBOTT, AI ATTHUR 1908 1882 *ABBOTT, ARTHUR V 1906 1903 * ADAMS, CHARLES C. 1905 1884 *ADDY, MATTHEW 1896 1889 * AKERS, WILLIAMS 1906 1894 *ALLEN R B 1896 1905 * ALLEN, R. SCOTT 1906 1874 *AMIOT, H 1892 1886 *AMSLER, CARL 1894 1895 *ÅNGSTROM, CARL 1901 1900 * ARLETT, GEORGE H 1906 1895 *ARMSTRONG, JOHN F 1898 1882 *ARNOLDS, HUGO 1886 1875 *ASHBURNER, CHARLES A 1889 1872 *ASIIBURNER, WILLIAM 1887 1883 *ATKINS, C M , JR 1885 1905 * AUDTIN, PETER T 1907 1897 *AYERS, WILLIAM 1898 1885 *BABCOCK, GEO H 1893 1884 *BAILEY, EDWARD 1889 1880 *BAILEY, JACKSON 1887 1900 *BALLOU, FRANKLIN 1903

Jan 1, 1910

By R. C. Gifkins

R. C. Gifkins (CSIRO)—In this paper evidence is put forward to support the idea of grain boundary shearing in aluminum at 4.2°K and the phenomenon is explained in terms of a low-temperature "equicohesive temperature". It is stated that these findings show that grain boundary shear cannot be ruled out in any situation by temperature arguments alone. We believe, from our own recent study of "apparent grain boundary sliding'' at temperatures below 0.45 Tm, that it can be ruled out on temperature arguments alone.45 Our experiments were made principally with magnesium and a Ms-A1 alloy ("Magnox A12"). Careful examination of offsets of marker lines or steps at grain boundaries produced by deformation at room temperature (-0.3 Tm) showed many of these to result from curvature over narrow zones along the grain boundaries. A significant residuum did, however, appear as a sharp offset or step. It was found that the mean value of this step rose to a small value during the first 0.5 to 1 pct strain and then remained at this level with further strain. Moreover, exactly the same values were obtained (at the same stress) at 75°C instead of 21°C. That is, in this range of temperature the "apparent sliding" was not temperature-sensitive. At 125°C and above there was sliding which increased with strain and which was temperature-dependent. When this temperature-dependent sliding was used to calculate the sliding to be expected at room temperature, this underestimated the "apparent sliding" by a factor of 104. The conclusion drawn is that the "apparent sliding" consists of shear localized in a zone of a width measured perhaps in microns, whereas it seems that true sliding occurs on the boundary surface.46 A model for such localized shear has been developed in general terms, following a similar model of Urie and Wain.47 Other strong evidence for low-temper- ature sliding has been based on the offsets of marker lines consisting of a substructure seen using the electron microscope to resolve these.48 We have repeated this work and found that the effects can be accounted for in terms of cracks in an oxide film which is produced when the substructure is etched up; these cracks form over zones of shear rather than at actual interfaces. However, in aluminum at room temperature (-0.3 Tm) there is no "apparent sliding" which is optically detectable. We suggest that, when the temperature is much lower (and possibly the rate of strain higher, too), as in the experiments of Chin et al., then aluminum behaves like magnesium at room temperature, and a narrow zone of shear develops to accommodate differences in strain across the grain boundary. Such a zone could well give rise to triple-point cracks. It is hoped to investigate these suggestions further. B. Y. Chin, W. F. Hosford, Jr., and W. A. Backofen (authors' reply)—It is interesting to have Dr. Gif-kin's comments, although it is somewhat difficult to reply in detail without the reference containing the work that he describes. Apparently though, he does find a low-temperature temperature-independent sliding that would seem to be related to the observations reported here. Perhaps some of the difficulty has semantic origins, growing out of the distinction between ('true sliding" and "apparent sliding".

Jan 1, 1965

By F. Lynwood Garrison

The future of the Witwatersrand depends upon the possibility of mining and milling profitably the large tonnage of relatively low-grade gold ores known to exist in that area. The problem must be solved if the existence of the gold-mining industry in South Africa is to be saved and continue. To show that this disaster may be avoided, or at least postponed for another decade or longer, the following official statement is of interest: "There is a fairly large area of possible orebody on the East Rand of whose value and depth from the surface we have some though not very accurate knowledge. There is a far larger area south of the Central Rand which probably carries much payable ore, but at depths that at present appear too great to mine. Finally, there is a narrow strip of country over 100 miles in length stretching south from the Rand to Klerksdorp and beyond, which may contain large ore-bodies. The Witwatersrand rocks outcrop over portions of this ground and in places conglomerates occur in it that carry small bodies of payable ore. There is reason to believe that conglomerates of the Witwatersrand system exist over all this strip, though they are for the most part covered by later sediments. It seems probable also that there are large blocks of payable reef in this belt, at any rate in the area that lies close to the present western limit of the developed mines. The structure in this neighborhood is however very complicated and to prove the orebodies will be both difficult and costly." Ores in the Witwatersrand It should be explained in this connection that the conglomerates mentioned here were originally old gravel beds now consolidated into bedded sedimentary rocks, very hard because strongly cemented with secondary silica. The gold exists in this cement and is rarely found in the pebbles composing the rock or bed called locally reef. It is important to realize that these gold deposits are beds; not veins as generally understood by mining engineers and geologists. In addition to these low-grade ore reserves we have also to consider the ore left behind in the old stopes of the upper levels near the surface,

Jan 1, 1931

By L. S. Reid, R. L. Huntington, Chen Chun Ku

The simultaneous adsorption of water and hydrocarbon vapor from natural gas by three grades of alumina has been studied at atmospheric pressure and temperature. Results of this investigation reveal that the presence of water vapor in the gas inhibits the adsorption of hydrocarbon vapor, although the presence of the latter does not have a pronounced effect upon the adsorption of water vapor. Adsorption of water-hydrocarbon mixtures from gas is divided into three phases. In the first, both water and hydrocarbon vapor are adsorbed; in the second, adsorption of water vapor proceeds while desorption of hydrocarbon takes place; in the third phase, the adsorbyt approaches complete saturation with respect to both water and hydrocarbon vapors. Both theory and experimental data can be applied to design and operation of commercial dehydration plants, and an illustration is presented. Introduction Dehydration of natural gas becomes increasingly important as the operating pressures employed in gas processing and transmission are increased above 500 ib. per sq. in. Gas produced from high-pressure wells is saturated with water vapor when it leaves the reservoir and it continues into the processing plant or transmission system in a saturated condition because of the substantial decrease in temperature due to expansion at the wellhead. Usually this gas is accompanied by liquid water and hydrocarbons that have condensed with the change in temperature and pressure. Without dehydration, gas temperatures must be held at relatively high levels to prevent solidification of gas hydrates. According to Hammerschmidt's data8 on the relationship of pressure to the freezing point of natural-gas hydrates, the minimum safe operating temperatures range from 55' to go°F. for pressures ranging from 500 to 3000 lb. per sq. in., respectively. Often it is difficult to maintain gas temperatures above the hydrate-freezing temperature because of climatic conditions, unless flow-line heaters are installed. Also, in processing gas for its gasoline content at high pressures, it is desirable to employ operating temperatures lower than the hydrate-freezing point. In distributing high-pressure gas, the large pressure drop from line pressure to town-gate pressure often prbduces sufficient cooling to freeze the regulators and disrupt consumer service. Therefore, it is highly essential to dehydrate high-pressure natural gas if smooth and economical operation is to be maintained at all times. Few published data are available on the simultaneous adsorption of water and hydrocarbon vapors. The literature contains many mathematical expressions for rate of adsorption in various systems but a rational correlation of the existing rate

Jan 1, 1944

By R. L. Huntington, L. S. Reid, Chen Chun Ku

The simultaneous adsorption of water and hydrocarbon vapor from natural gas by three grades of alumina has been studied at atmospheric pressure and temperature. Results of this investigation reveal that the presence of water vapor in the gas inhibits the adsorption of hydrocarbon vapor, although the presence of the latter does not have a pronounced effect upon the adsorption of water vapor. Adsorption of water-hydrocarbon mixtures from gas is divided into three phases. In the first, both water and hydrocarbon vapor are adsorbed; in the second, adsorption of water vapor proceeds while desorption of hydrocarbon takes place; in the third phase, the adsorbyt approaches complete saturation with respect to both water and hydrocarbon vapors. Both theory and experimental data can be applied to design and operation of commercial dehydration plants, and an illustration is presented. Introduction Dehydration of natural gas becomes increasingly important as the operating pressures employed in gas processing and transmission are increased above 500 ib. per sq. in. Gas produced from high-pressure wells is saturated with water vapor when it leaves the reservoir and it continues into the processing plant or transmission system in a saturated condition because of the substantial decrease in temperature due to expansion at the wellhead. Usually this gas is accompanied by liquid water and hydrocarbons that have condensed with the change in temperature and pressure. Without dehydration, gas temperatures must be held at relatively high levels to prevent solidification of gas hydrates. According to Hammerschmidt's data8 on the relationship of pressure to the freezing point of natural-gas hydrates, the minimum safe operating temperatures range from 55' to go°F. for pressures ranging from 500 to 3000 lb. per sq. in., respectively. Often it is difficult to maintain gas temperatures above the hydrate-freezing temperature because of climatic conditions, unless flow-line heaters are installed. Also, in processing gas for its gasoline content at high pressures, it is desirable to employ operating temperatures lower than the hydrate-freezing point. In distributing high-pressure gas, the large pressure drop from line pressure to town-gate pressure often prbduces sufficient cooling to freeze the regulators and disrupt consumer service. Therefore, it is highly essential to dehydrate high-pressure natural gas if smooth and economical operation is to be maintained at all times. Few published data are available on the simultaneous adsorption of water and hydrocarbon vapors. The literature contains many mathematical expressions for rate of adsorption in various systems but a rational correlation of the existing rate

Jan 1, 1944

By Kelvin K. Wu, Daniel S. Mazzei

As a result of the 1972 Buffalo Creek disaster, the Mining Enforcement and Safety Administration (MESA), now the Mine Safety and Health Administration (MSHA) initiated the draft of new federal regulations to deal with the mine waste impoundment and refuse pile problems. Public hearings were held and finally promulgated in October, 1976. As stated in 30 Code of Federal Regulations 77.214-216, the complete engineering design plan which is mandated by the regulations has to be approved by a coal mine health and safety district manager. During the past 18 months MSHA has gained considerable experience through the submission, review, and approval process. This report indicates the procedures, general design criteria and inspection requirements for submission of engineering plans to be approved. In particular, problem areas encountered most frequently by both operators and MSHA will be discussed. Only through diligent efforts by the operators, consultants and government, can we hope to accomplish the common goal to improve the safety of operations.

Jan 1, 1982

By George C. Toland, Ronald E. Versaw

Most existing impoundment ponds and dams leak effluent into the soil or rock upon which they are constructed. However, proposed environmental legislation will require very stringent control of the release of toxic effluents such as cyanide. More exacting investigation, design, and construction techniques than have been used in the past will be required to satisfy these new regulations. The types of field and laboratory investigations required to develop the data for the design of an impoundment system containing toxic effluent are discussed, together with the technical considerations necessary to design this system. Design topics include reservoir sealing with natural and man-made materials; embankment sealing; embankment design considering stability, surface hydrology, capacity, and downstream catchment basins; and special implications of cyanide effluents.

Jan 1, 1977

By John K. Hammes, Stanley D. Michaelson

Generally, the mining costs reported for the large open-pit operations in the United States and South America lie within the range of $0.20 to $0.30 per ton of material moved. (These operations have strip- ping ratios ranging from 1.5 to 4.0.) Productivities for the larger North American properties are in excess of 200 tons of material per man shift, while those for the South American operations are less than 200 tons per man shift. The most significant variations in cost are in the categories of haulage and general mine cost. Haulage costs vary, as expected, according to the mine elevation, pit profile, crusher location, and accessibility of a dump area, and general cost variations depend largely on the overhead cost items included in this category. Drilling and Blasting Practice The majority of open-pit copper mine production drilling is performed by rotary drills. Hole diameter varies from 6 in. to 12 in., with 9-in. holes being most common, and penetration rates vary from 35 ft to 60 ft per hour.

Jan 1, 1968