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By Diego Pacheco Wermuth

Micrometric surgical components typically have high geometric complexity and stringent regulatory specifications. These components need to have excellent mechanical properties and a high demand of products. Besides these factors, it is necessary to maintain a low manufacturing cost, performing essential research on new manufacturing technologies. Metal Injection Molding (MIM) is a process that has been explored , providing an interesting alternative for making medical devices. The research in the production of microcomponents obtained for MIM is gaining momentum and prominence, due to low cost and high productivity of this process. This paper is a study and development of feedstocks with AISI 316L alloy , which is known for its biocompatibility. Four feedstocks with 61%vol. of metal powder were analyzed by capillary rheometry and DSC/TGA.

Aug 16, 2017

By Samuel Filgueiras Rodrigues, Clodualdo Aranas Jr., Gedeon Silva Reis, Eden Santos Silva, Fulvio Siciliano

When austenite is deformed above the Ae3 temperature, partial amount of it transforms dynamically into ferrite by a displacive mechanism. After unloading, it retransforms back into the stable austenite by a diffusional process. This influences the rolling load which decreases under isothermal condition or does not increase with decreasing temperature as rapidly as expected under cooling. Plate rolling simulations under isothermal and continuous cooling conditions were carried out on a 0.09 wt.% Nb X-70 steel. Pass strains of 0.2 were employed together with interpass times of 10 s, and 30 s for the cooling conditions and 0.3 with interval of 10 s at 900 °C for the isothermal experiments; strain rate of 1 s-1 was used during the simulations. The mean-flow-stress (MFS`s) behavior of both conditions indicates that dynamic transformation and dynamic recrystallization were taking place during straining. The critical strains for the initiation of dynamic transformation fell around 0.06 while the critical strain for DRX was 0.12. It has been shown that ferrite is formed due to the applied deformation of roughing passes and increases its volume fraction throughout the finishing rolling stage. Under cooling conditions, the ferrite formation is also favored as the temperature approaches the Ae3 line. Such ferrite forms when the driving force for dynamic transformation is higher than the total free energy barrier preventing its formation. This obstacle consists of the free energy difference between austenite and ferrite as well as the lattice dilatation work and shear accommodation work. The addition of Nb retards the retransformation of the ferrite into austenite. Moreover, holding times after rolling increases the amount of austenite available for microstructure control on subsequent stages. The dynamic transformation (DT) mechanism can be used to design improved rolling schedules

Oct 1, 2019

By Antônio Augusto Gorni, Fabio Adriano da Silva, Emanuelle Garcia Reis, Afrânio Márcio Costa

Gerdau Ouro Branco´s plate mill started the operation in 2016 with high level technology. Stands out the capacity to produce different thicknesses in a same plate, therefore allowing special service for sectors such as building structures, bridges, shipbuilding and mechanical applications. The purpose of this study is to present the first results obtained in this innovative product in Brazil. Some slabs of EN10025-2 S355JR+AR steel were rolled and were evaluated the dimensional tolerances, mechanical properties uniformity, grain size, surface and internal qualities. In addition, a correlation was observed between slab and plate thickness reduction and internal plate quality. The results show that this technology can be used with adequate performance for these steel grades in the current market.

Oct 1, 2019

By Edmar de Souza Silva, Antonio Augusto Gorni, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Controlled rolling followed by accelerated cooling, known worldwide as TMCP, aims to increase mechanical properties without toughness deterioration. The process principle is to promote the plate cooling with water jets along the range of the austenite transformation temperatures. The accelerated cooling process is only fully effective when controlled in an integrated manner, as it alone cannot ensure significant improvements in the final properties of steels. Plate surface quality depends on some parameters that must be controlled before the start of the plate accelerated cooling. Good flatness is essential to avoid irregular water accumulations during cooling. After the reheating process, the slab should have uniform temperature, uniform austenitic grain size and easily removable scale. The slab thermal and microstructural heterogeneities are inherited by the rolled plate and tend to increase further during the accelerated cooling. This results in flatness problems, high level of internal stresses and mechanical property variations. The descaling strategy is an extremely important factor and must be determined with great caution. It is important that scale thickness and distribution is uniform to ensure homogeneous cooling over the entire plate surface. Otherwise, there will be an uneven temperature distribution, which can cause serious problems of flatness, surface quality and mechanical properties.

Oct 1, 2019

By Franco de Castro Bubani

Cu-base alloys (Cu-Zn-Al, Cu-Al-Be, Cu-Al-Ni), depending on their composition, have martensitic transformations that can be thermally or mechanically induced between a metastable structure called austenite and one or more metastable structures called martensites. In single crystals, depending on the specific composition of the alloy and the crystallographic orientation of the tensile axis, martensite-martensite transformations can be mechanically induced. The hysteresis associated to these martensite-martensite transitions is usually much greater than the one associated to the austenite-martensite transformation. Thus, martensite-martensite transitions are potential candidates for energy dissipation in a mechanical damper. Possible applications that would benefit from high hysteresis include seismic damping devices, dampers for satellites and the aerospace industry, defense and others. We present pseudoelastic cycling results of alloys submitted to different thermal treatments. Our conclusions highlight the fact that, under certain conditions, Cu-base alloys deliver better damping performance than commercially available SMAs and even the new Fe-base SMAs.

Aug 7, 2018

By Rodrigo Ribeiro de Andrade, Túlio César Nogueira, Ed Juarez Mendes Taiss, Nilton José Lucinda de Oliveira

The objective of this study was to determine the effects of an eventual slab central macro-segregation in microalloyed steels with low Mn content (0.80%) and high Nb content (0.08 to 0.10%) on the kinetics of recrystallization of austenite during its rolling, on its critical temperatures, that is, of non-recrystallization (Tnr), start Ar3 and finish Ar1 of ferrite transformation and its response to a simulated industrial thermomechanical processing. The determination of the austenite recrystallization kinetics was made through isothermal double compression tests using a dilatometer, while the critical temperatures were determined through hot torsion tests in a Gleeble® 3800. It was found that austenite recrystallization kinetics, Ar3 and Ar1 temperatures did not present significant changes for the samples extracted both at ¼ of the thickness and at the core of the plate, indicating that, as expected, the central segregation in this type of steel was not intense to the point of affecting this phenomenon. The Tnr values determined for the samples extracted in the core of the plate were, on average, 30°C lower than those obtained from specimens extracted at ¼ thickness, which suggests that a significant portion of the carbonitrides present in the core of the slab are eutectic and coarse, not having completely dissolved during the reheating of the specimens. This occurred despite the fact that the austenitization temperature adopted in this treatment theoretically leads to the total dissolution of Nb, as seems to have occurred in the case of specimens extracted at ¼ of thickness, where carbonitrides have a finer size.

Oct 1, 2019

By Lucia Vieira

Kelvin probe force microscopy (KPFM) can be used to monitor electrostatic charges on the surfaces of materials. In this paper, we describe the use of KPFM to evaluate the electrostatic effect induced by silver nanoparticles incorporated as clusters in diamond-like carbon (DLC) films, before and after scratching. The results are compared to those obtained for DLC films without silver nanoparticles. Raman spectroscopy was used to identify the DLC signature, and energy dispersive X-ray spectroscopy (EDX) was used to confirm the presence of silver in the film. The morphology of the DLC film containing silver was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings suggest that the incorporation of silver nanoparticles in amorphous materials could offer new options for electrostatic energy storage on the surfaces of these materials.

Jul 31, 2018

By Nicola Santangelo

The current economic crisis and growing environmental issues have led the steel industry to face the simultaneous effects of low demand and production overcapacity in a globalized steel market, whilst confronting high energy prices and the need to comply with the green economy. Heat Recovery from waste gas of the Electric Arc Furnace (EAF) represents one of the greatest opportunities to reduce the consumption of primary energy and reduce the CO2 emissions in steel industry. The heat of the off-gas, if recovered and converted into electrical power, can make the whole Fumes Treatment Plant autonomous from the electric point of view, thus making it a “Zero-Energy FTP”. The concept is to substitute the Cooling Components (Water Cooled Panels and Air Cooler) are substituted with Heat Recovery Components (Hot Water Cooled Panels and Heat Exchanger). The recovered heat can be converted into power by using an Organic Rankine Cycle (ORC) turbine. The heat recovered by the HWCP and the Heat Exchanger is characterized by a variable thermal power, which affects the efficiency of the downstream ORC System. Danieli, in collaboration with the University of Udine, has developed the Thermal Stabilizer Unit (TSU). Danieli has realized the first step towards Zero Energy FTP at ABS steelmaking plant (Italy) by installing a CHR® - Clean Heat Recovery. This plant has been started up on 17th October 2014. The HMI of the CHR® is integrated in the HMI of the furnace, so all the process could be kept under control by the furnace operator. At ABS recovered thermal power reaches 5.5 MW. The max power production reached with CHR plant in ABS (over 1MW of electric power) consents an annual saving of approx. 500,000 EUR.

Aug 16, 2017

By Marco Antonio Meggiolaro

Notches are preferential sites for fatigue and for environmentally assisted cracking (EAC) initiation. Semi-empirical notch sensitivity factors have been used for a long time to quantify notch effects on fatigue design. Recently, this concept has been mechanically modeled using techniques which properly consider the notch tip stress gradient influence on the fatigue behavior of mechanically short cracks. This model properly calculates such values from the basic fatigue resistances of the material, its fatigue limit and crack growth threshold, considering the characteristics of the notch geometry and of the loading, without the need for any adjustable parameter. Such criteria to estimate notch sensitivity and tolerable short cracks on fatigue have been extended to EAC conditions and verified by proper tests. In its simplest version, the criterion for the maximum tolerable stress under EAC conditions uses the resistances to crack initiation and to large crack propagation and the characteristic short crack size under EAC, considering the crack size and stress intensity factor. Moreover, the tolerance to short cracks under fatigue and under EAC conditions can be unified in an extended Kitagawa-Takahashi diagram, a new and potentially very useful tool for material selection tasks.

Aug 8, 2018

By Yuechang Wang

A new method of manufacturing the wavy-tilt-dam(WTD) mechanical seal has been mentioned. In this method, the special equipment is designed to provide a predetermined force to external and inner circular surface of the ring. After milling the end face of the seal by grinding miller and releasing the preload, the wavy-tilt-dam can be done on the seal surface. In this paper, a prediction model is built up to investigate the relationship between the predetermined force and the deformation on the surface of the ring by using ANSYS software. A WTD ring is manufactured by this method which approves that the prediction model is in accord with the real process and this manufacturing method of the WTD mechanical seal is a proper choice.

Jul 31, 2018

By Guilherme Corrêa Soares

Deeper understanding about the strain hardening behavior of steels has become necessary due to its importance in industrial processes such as mechanical cold forming, rolling and drawing. In this work, the strain hardening behavior of AISI 304, non-grain oriented electrical (NGO) and dual phase steels was investigated. Tensile tests were performed and the strain hardening behavior of each steel was studied by the Hollomon’s equation. X-ray diffraction measurements and hardness tests were also carried out in order to characterize the specimens. Different work hardening stages were observed in each steel during the deformation process. The results obtained are discussed in terms of the relationship among the instantaneous strain hardening coefficient, hardness and eventual phase transformations. The instantaneous strain hardening coefficient of dual phase and NGO increases after the yield point, rapidly reaching its maximum and then steadily decreases until tensile strength is reached. In AISI 304’s case, the strain hardening coefficient keeps raising to high values in response to a large strain and then rapidly decreases before reaching the tensile strength. In comparison to the other steels, AISI 304 shows higher instantaneous strain hardening coefficient value, which persists even in large strains. This is a consequence of its strain hardening mechanism based on stress-induced martensite transformation.

Aug 16, 2017

By Jari Larkiola, Aarne Pohjonen, Juha Jokisaari, Oskari Seppälä, Joonas Ilmola

Finite element method (FEM) is widely used to model the hot strip rolling process. Flatness defects e.g. front-end bending in multipass hot strip rolling is studied by authors using a finite element (FE) model with interactively operating automated controlling logic (ACL) [1]. However, industrial corresponding grade of accuracy in strip thickness subsequent to the rolling pass is not easily accessible in FE-model without separate calculation of significant rolling parameters and integrated roll gap control. In order to study flatness defects and optimize pass schedules the controlling and physics of the FE-model must correspond to the industrial process. For this need the automated controlling logic is upgraded by setup calculations to predicting roll force and work roll flattening. These predictions are utilized in setup positioning of a work rolls. Reliable setup calculation enables smooth multi stand rolling process without significant additional adjustment of roll gap clearance. State of art rolling technology requires above-mentioned setup controlling for the FE simulations to simulate different pass schedules without time consuming preparations. Operational setup calculations together with automated controlling logic of hot strip rolling enable simulation of new pass schedules and efficient problem solving.

Oct 1, 2019

By Rafael Abreu Fraga, Carlos Noberto Paula da Silva, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Since 2016 Gerdau Ouro Branco has been producing steel plates of various qualities and grades. However, it was not until 2018 that the first plates produced by accelerated cooling process were made available for external testing, in this case for large diameter UOE pipes manufacturing. Recent line pipe and OCTG specifications are showing that the oil and gas market still consumes regular API grades, such as X60, X65 and X70, however with increasing wall thicknesses, reaching values up to 1.5 inches. These specifications also demand longitudinal and transverse tensile guarantees and drop weight tear tests in temperatures as low as -40°C. Projects with these types of mechanical properties present process requirements as challenging as those necessary for higher API grades in lower thicknesses. This paper shows the steel design concepts and rolling routes for achieving the necessary properties for X70 steel plates in 28.15 mm. The microstructural features were also investigated and associated with the production process and the tensile and toughness results. Finally, challenges such as tensile anisotropy and DWTT abnormal fracture are presented.

Oct 1, 2019

By Jesús A. Carlos Cornelio

Since their discovery in 1991 Carbon nanotubes (CNTs) have attracted much interest due to their remarkable mechanical, thermal, electrical, chemical and optical properties. In connection with their mechanical properties, CNTs have been studied in various forms for tribological applications including their use as lubricant additives for oil and water. In this paper the tribological properties of CNTs (SWCNTs and MWCNTs) when used as lubricant additives are studied under rolling-sliding conditions in a twin-disc testing machine. The tests were performed using 5% of creepage and pressures of 0.8 GPa and 1.1 GPa. Used functionalized nanotubes were modified with carboxylic acid ultrasonically dispersed at different concentrations (0.01, 0.05%). The results indicated that the presence of carbon nanotubes leads to a decrease in both friction coefficient and wear rate for both systems studied (oil and water).

Jul 31, 2018

By Jose M. Rodriguez-Ibabe, Beatriz Pereda, Beatriz Lopez, Felipe Bastos

The modeling of austenite evolution during the hot rolling of steels is covered in the literature for a wide range of chemical compositions, although mainly for carbon contents below 0.20%. In addition, most research on this topic is oriented for processes that are characteristic of flat products. Compared to those processes, the hot rolling of bars for structural applications presents considerable particularities concerning mainly deformation, rolling speed and rolling temperature profile. Those particularities result in considerable changes on process parameters that affect the austenite microstructure evolution, both in the softening and hardening mechanisms if microalloying elements such as Nb is present. The aim of this work was to develop a model to predict the evolution of austenite microstructure that is suitable for the hot rolling of structural reinforcing bars. Different torsion tests simulating industrial schedules particular from those type of processes were performed. The tests showed the need to investigate Nb strain-induced precipitation interaction with softening mechanisms that can occur during the deformation schedule. At the end, the new proposed kinetics and routines were introduced to a program, MicroSim-Bars®, that is able to model austenite evolution under structural bar hot rolling conditions.

Oct 1, 2019

By Samuel F. Rodrigues, Clodualdo Aranas Jr., Fulvio Siciliano

The application of thermo-mechanical control processing (TMCP) in hot rolling of steels has become a common routine since the last 60 years. The understanding of the physical metallurgy behind TMCP played a major role in the early developments. Physical and numerical simulation works are performed firstly to derive the fundamental metallurgical knowledge and secondly to conceive existing TMCP practices. In this paper, a summary TMCP techniques is presented. The occurrence of dynamic transformation of ferrite in the austenite region is shown by means of synchrotron light diffraction methods. This phase transformation mechanism is taken into consideration and its effects on TMCP are proposed in an exploratory way.

Oct 1, 2019

By Woo, Hur, Kim, Ki Nam, Seung Min, Kyoung Sik

Tandem cold mill (TCM) is a process to obtain flatness as well as thickness desired by the customer by rolling hot-rolled coils continuously. The final stand of the TCM plays the most important role of flatness control, which usually uses the real-time measurement at the exit. However, as the material property increases, it is not easy to handle flatness with only the final stand. In order to overcome such a limitation, we propose a feedback control method to strengthen flatness control for non-final stands. The proposed method was tested in an actual production line, and the effect is proved for 45K or less steel grade.

Oct 1, 2019

By Dong Maolin

A great amount of high temperature off-gas, whose maximum temperature is up to 2100?, is generated during the smelting process of electric arc furnace (EAF). The dust content, which is mainly iron oxide, of the off-gas is high and worthy of industrial recovery. The heat carried by the high temperature off-gas with dust is about 11% of the total energy input of EAF, and some even is as high as 20%. The high-temperature off-gas not only takes away a lot of heat but also places a huge burden to de-dusting system of EAF. It not only reduces the iron oxide dust recovery ratio, but also causes serious pollution problems. With the development of the iron and steel industry, the proportion of molten iron for EAF gradually increases, and even more than 30% in some cases. The increase of molten iron causes increases in the amount of EAF off-gas and heat waste. As a result the problem of dust removal is worsening [1-2]. How to sufficiently recover the sensible heat of the high temperature off-gas, create conditions for efficient dust removal, thus reduce operating costs of dust removal system and the production costs is a problem which EAF steel making companies must pay attention to.

Oct 30, 2017

By Xihuai Gong, Hongshuang Di, Jianping Li, Ning Yan

In this work, we investigated the effect of the rolling process (warm-rolled or cold-rolled) on microstructure evolution and mechanical properties of 9Mn steel. After intercritical annealing at 670°C for 10min, both cold-rolled and warm-rolled microstructures are composed of ultra-fined austenite and intercritical ferrite. The austenite in warm-rolled sample includes two types of morphology, namely equiaxed and lamellar, which exhibits a wide distribution of grain-size. The incomplete recrystallization or recovery behavior of ferrite in warm-rolled and annealed sample results in higher yield strength and shorter yield point elongation. Moreover, the warm-rolled and annealed sample extends the TRIP-related work hardening over a broad strain range, resulting in a better combination of ultimate tensile strength and total elongation.

Oct 1, 2019

By Hongshuang Di, Tianyu Zhang, Huiqiang Huang

A CMnSiAl transformation induced plasticity (TRIP) steel was used to study the effect of retained austenite on room-temperature mechanical properties. The steel plates with retained austenite were obtained by hot rolling, cold rolling and subsequent continuous annealing. The starting and finishing temperature of hot rolling are between Ac1 and Ac3. Reduction ratio of cold rolling is 75%. The continuous annealing is carried out at different intercritical temperatures. The relationship between work hardening exponent and retained austenite was discussed. The results show that, the Ac1 and Ac3 were much high because of the alloy elements, and the temperature range between them was wide. Due to the high hot rolling temperature, the grains was hereditarily refined as a result of dynamic recrystallization. Annealing at intercritical temperature of 930 ºC, retained austenite with relatively high stability reached a maximum volume fraction of 25%, a maximum total elongation of 30.2% and a best ultimate tensile strength × total elongation of 20.1 GPa·%. Instantaneous work hardening exponent reflects strengthening mechanisms at different strain stages. The TRIP effect of retained austenite is the main mechanism during deformation. With retained austenite of sufficient amount and high stability, continuous work hardening was observed in the tensile specimen of 930 ºC.

Oct 1, 2019