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By Giselle de Mattos Araújo

A autorredução é afetada por características das matérias-primas tais como granulometria, porosidade, tipo e teor da fonte carbonácea, e também por características do ciclo de processamento imposto, taxas de aquecimento, tipo de atmosfera gasosa, temperatura média de processo. No presente trabalho objetiva-se, através de testes de termogravimetria, avaliar a cinética de autorredução e também o fluxo térmico associado, durante o processamento de diversas associações de finos de minério e fonte carbonácea. Com os resultados obtidos identificam-se condições que otimizam tanto a mistura autorredutora quanto o processamento, observando-se que em uma mesma faixa granulométrica, o maior conteúdo de Cfixo da fonte carbonácea e materiais mais reativos otimizam a cinética, em detrimento da maior quantidade volumétrica de partículas carbonáceas observada em amostras contendo carvões mais pobres em Cfixo. Taxas adequadamente controladas permitem a definição de instantes distintos para as diversas etapas fenomenológicas envolvidas no processamento da autorredução.

Aug 2, 2018

By Severino Albani Junior

A crise econômica mundial de 2008 obrigou as empresas a se recriarem para atender um mercado mais cauteloso e conservador. Isso demandou uma reformulação na maneira de executar as atividades e estruturar os preços dos produtos. Nesse contexto a ArcelorMittal Tubarão iniciou os trabalhos na área de gestão de ativos focada em manutenção, desenvolvendo um programa para melhoria da confiabilidade dos equipamentos. Dentro desse programa, foi identificada a oportunidade de revisar os planos de manutenção da planta. Essa revisão contempla ajustes no cadastro, criticidade dos equipamentos e revisão dos planos de manutenção no Sistema da Manutenção da Planta. Esse trabalho abordará a metodologia adotada para realização dessas revisões, considerando a formação das equipes de trabalho centralizadas, sua interação com as áreas de manutenção das unidades produtivas, critérios utilizados para revisão dos cadastros/criticidades, a utilização da Manutenção Centrada em Confiabilidade (MCC) para revisão dos planos de manutenção e resultados obtidos.

Aug 16, 2017

By André de Albuquerque Vicente

Foram estudadas as camadas de óxidos formadas nas superfícies de um aço inoxidável austenítico laminado do tipo 22.12, após oxidação ao ar a 800, 900, 1000 e 1100 °C, dentro de um projeto que visava uma melhor compreensão da oxidação a altas temperaturas ao ar de aços inoxidáveis resistentes a altas temperaturas. Utilizou-se o aço inoxidável austenítico microligado ao cério (253 MA®), que é um aço projetado para trabalhos a altas temperaturas. Várias técnicas complementares de análise microestrutural foram utilizadas, tais como difração de raios X e microscopia eletrônica de varredura com EDS acoplado. Observou-se a formação de uma camada não protetora de óxidos de ferro (Fe2O3, Fe3O4 e FeO) e posterior formação de uma camada protetora mais espessa de crômia (Cr2O3). Mais internamente observou-se a formação de SiO2.

Oct 30, 2017

By Rodrigo Perito Cardoso

Low-temperature nitriding of stainless steels is applied to obtain wear resistant surfaces without losing its corrosion resistance. The treatment consists in introducing nitrogen into the steel surface avoiding chromium nitride precipitation. The corrosion resistance of martensitic stainless steels is expected to be improved if the treatment parameters are correctly selected. It can be related to ?Fe2-3N and a'N phase formation on the treated surface. In the present work the influence of the pretreatment and treatment temperature on corrosion resistance of plasma nitrided AISI 420 steel samples is studied. Annealed, as-quenched and 400ºC-tempered samples were nitrided at 300, 350, 400, 450 and 500°C, for 6 h at 600 V. The pressure was 3 Torr and the gas mixture was composed of 70%N2, 20%H2 and 10%Ar, at a gas flow rate of 3.34×106 Nm3s-1. Plasma was generated using a square-wave pulsed DC power supply and the sample temperature was controlled by the duty cycle. The modified layers were characterized by optical microscopy, X-ray diffraction and microhardness measurement. The corrosion resistance was studied by electrochemical characterization, by means of Open circuit potential and Anodic polarization curves. The maximum surface hardness was achieved at 400°C. This temperature seems to be near the limit temperature for low-temperature treatment aiming to improve or at least to keep unaltered the corrosion resistance in relation to that verified for non-treated steel samples. Results confirm that the pretreatment and treatment temperature significantly affects the corrosion resistance of the treated surface.

Aug 8, 2018

By Humberto Tronconi Coelho

The use of friction dampers are wide proposed for a variety of mechanical systems for which it is not possible to apply viscoelastic materials, fluid based dampers or others viscous dampers. An important example is the application of friction dampers in aircraft engines to reduce the blades vibration amplitudes. In most cases, friction dampers have been studied in a passive way, however, a significant improvement can be achieved by controlling the normal force in the contact region. The aim of this paper is to study four control strategies for friction dampers based on three different hysteresis cycles. The first control strategy maximizes the energy removal in each harmonic oscillation cycle, by calculating the optimum normal force based on the last displacement peak. The second control strategy combines the first one with the maximum energy removal strategy used in the smart spring devices. Finally, is presented the strategy which homogenously modulates the friction force. Numerical studies were performed with these four strategies defining the performance metrics. The best control strategy was applied experimentally. The experimental test rig was fully identified and its parameters were used for numerical simulations. The obtained results have shown the good performance for the friction damper and selected strategy, also, the agreement between numerical and experimental results.

Jul 31, 2018

By Dilermando Nagle Travessa

High strength-light weight materials are very attractive for the transportation sector, particularly to the aerospace industry. High strength-age hardenable aluminium alloys are widely used in airframes due to their unique combination of strength, density, toughness, corrosion resistance, cost and easy processing. However, the hardening capacity of such alloys is somehow saturated due to thermodynamic issues related to the conventional processing. The production of aluminum-matrix composites is a promising strategy to overcome this limitation, resulting in strength levels that cannot be reached by actual commercial aluminum alloys. In the present work, multiwall carbon nanotubes were used to reinforce the AA6061 aluminium alloy. 1 and 2% weight percent of MWCNT were mixed to the alloy powder by high-energy ball-milling process. The blended powder was consolidated by hot extrusion. The obtained composite bars were submitted to heat treatment for the T6 condition in order to combine both CNT dispersion and precipitation hardening effects. Optical and scanning electron microscopy, as well as hardeness testing, was used to characterize the bars. Typical wrought microstructure, free of defects, was observed on the extruded bars. Hardness of the composites was observed to increase by 20, 28 and 68% for 1% MWCNT 6 h milling, 2% MWCNT 6 h milling and 2% MWCNT 10 h milling, respectively, in the as-extruded condition. The better performance for the composites blended at higher milling time was attributed to a better nanotubes dispersion. Subsequent heat treatment to the T6 condition did not result in additional hardening.

Aug 8, 2018

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the ex-service condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 52 to 224 MPa producing rupture times varying from 5 to about 3950h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results obtained on a similar plate of the same material in the virgin condition.

Aug 16, 2017

By Diego José Inforzato

Hot tensile data were correlated with creep data, in Aluminum Alloy AL7475-T7351, as part of a broader research program, aiming at the validation of a methodology that proposes an equivalence between the two kind of results, for metallic materials in general. The methodology is based on a criterion that establishes correlation among the following parameters from each test: the strain rate, ultimate tensile stress, and time to reach the ultimate tensile stress, in tensile tests, are equivalent respectively to the: minimum strain rate, applied stress and rupture time, in creep tests, for a given test temperature. The present material was tested at 3 temperatures: 133,166 and 193ºC, using 3 nominal tensile strain rates in the hot tensile tests: 3.2x10-6, 1.6x10-4 and 6.4x10-3 s-1 and 9 applied stress levels in the creep tests, varying from 140 to 400 MPa. The conversion of the hot tensile data to creep-like data allowed performing the analysis of all the results together according to the traditional creep relations proposed by different authors, namely: Norton, Arrhenius, Zener-Hollomon and Monkman-Grant, with the determination of the corresponding parameters in each case. The equivalence between hot tensile and creep data is also confirmed for this aluminum alloy.

Aug 8, 2018

By Leandro Rigo Ramos, Marcelo Lucas Pereira Machado, Lumena Gloria de Souza Nunes, Mariana Valinhos Barcelos

The aim of this work was to study the influence of temperature on the grain refining process from severe plastic deformations through the simulation of Accumulative Roll Bonding (ARB) by torsion tests. The assays were performed to simulate the ARB at three different temperatures of 550 ° C, 625 ° C and 700 ° C with 5 torsion cycles with equivalent strain of 0.8 per cycle at a rate of 0.1−1 , totalizing an accumulated deformation of 4.0. Grain refining was obtained with an average size of 2μm, 5μm and 6μm for the temperatures of 550 ° C, 625 ° C and 700 ° C respectively. There was a rise in Vickers hardness by 68%, from 119HV in the annealed sample to 175HV in the deformed sample at 550 ° C. In the deformations at 625 ° C and 700 ° C the value of 130HV E and 150HV respectively was obtained. Based on the obtained results, it can be stated that the severe plastic deformations in microliged steel, carried out at temperatures lower than the end of the austenite-ferrite transformation, produce refined grains of the order of 2μm and, consequently, increase the mechanical strength of the material.

Oct 1, 2019

By Fernando Velazquez Guzman

Titanium is an alloying element used to refine grain size in steel and improve its physical and mechanical properties. In some stainless steels it is used to increase the resistance to corrosion by the precipitation of titanium carbides or carbonitrides. Its alloying performance is highly variable and depends largely on the stage of the secondary metallurgy process when it is added. Furthermore, the addition method (wire injection or direct addition) has a remarkable influence in secondary refining. This paper describes the tests performed in vacuum degasser (VD), with a highly compacted and encapsulated Ferrotitanium wire (FeTi HC). The yield of titanium in steel increased from 52% to 89%. Moreover, the consumption of the highly compacted Ferrotitanium was optimized.

Oct 30, 2017

By Wujian jun

In the process of wire rod production, the rolled wire products must be cooled from the red-hot state to the normal temperature state. How to cool the wire rod after rolling is one of the key links of product quality control in the whole wire rod production process. In this paper, combined with the closed-loop transformation project of controlled cooling temperature of Xuanhuan iron and steel group co., LTD., the closed-loop related controlled cooling equipment (including water cooler, valve table, etc.), nozzle layout and process layout of water tank, and closed-loop software control system of controlled cooling temperature of high-line are analyzed and designed. Closed-loop system design USES temperature of cooling water cooling and water cooling two temperature closed loop regulating circuit, through temperature feedback and feedforward to achieve the uniformity of temperature adjustment, in order to prevent occur due to temperature closed loop control function with the phenomenon of a steel before and after the temperature difference is bigger, system Settings have "absolute temperature regulation" and "relative temperature regulation" selection mode. The system has a self-learning mode, which can modify the temperature feed forward formula. In addition, this paper takes the hard wire 82B rod as the test object, and studies the process parameters and the comprehensive mechanical properties of the rod before and after the water cooling system reform. The research results show that the temperature closed loop system, can ensure the rolled piece temperature control precision of plus or minus 10℃, enhances the stability of wire rod cleaner performance. It can reduce water consumption by about 186m3/h and improve the utilization rate of cooling water.

Oct 1, 2019

By Ananda Moreira Vaz Ourique de Avila

Ferritic stainless steels have been used in the making of high and intermediate temperature operation solid oxide fuel cells (SOFC) interconnects, replacing the ceramic materials. However, at high temperatures, on the order of 700-850 0C, these steels can present significant oxidation and degradation processes, promoting increased electrical resistivity and corrosion losses that result in contamination of the electrodes and reducing the performance and the useful life of the SOFC. Thus, the knowledge on kinetics of oxidation/corrosion of these steels and their relationship with the microstructural transformations are of great importance. In this study, samples of ferritic stainless steels AISI 430, AISI 441 and Crofer22APU® were tested for oxidation at high temperature (800 0C) for long periods of time (up to 3,600 hours) and mass gains were monitored allowing the determination of the oxidation behaviors of these steels. Additionally, the microstructural characteristics of the samples before aging (corrosion-oxidation test) and after various oxidation times were evaluated by optical (OM) and scanning electron microscopy (SEM), as well as by micro chemical elemental analysis (EDS) and X-ray diffraction (XRD) phase analysis. Electrical characterization allowed determination of electrical area-specific resistances (ASR) characteristics of the systems studied, thus relating the electrical and oxidative behaviors of steels evaluated.

Aug 7, 2018

By Mühlböck Marlene

Increasingly stringent global environmental regulations are forcing steel producers to continually improve the efficiency of sinter waste gas treatment. With the Selective Waste Gas Recirculation (SWGR) system from Primetals Technologies, lower production costs can be achieved and the size of downstream waste gas cleaning units can be reduced for investment savings. SWGR features the extraction and reuse of hot sinter off gas from selected wind boxes along the sinter strand, which contributes to improved energy efficiency and off gas treatment in the sintering process. With the next generation of SWGR, Primetals Technologies can provide an energy optimized, emission optimized and environmentally friendly solution that meet customer requirements and country specific regulations. This paper demonstrates the latest developments in selective waste gas recirculation, especially results from pot grate tests and comparison from lab to real plant data. Furthermore theoretical finding and mathematical modelling is presented.

Aug 16, 2017

By Mingyu Ma, Lingling Liu, Liqing Chen, Houlong Liu

In this article, a 444-type heat-resistant ferritic stainless steel containing 0.05wt% Ce and 2wt% (Mo+W) was used as an experimental material and a study was carried out on the effect of rolling processes on the microstructures and texture evolution as well as on the mechanical properties and formability. The rolling processes contain hot rolling at different hot rolling finish temperatures, annealing after hot rolling, cold rolling and subsequent annealing. As for the hot rolling process, two hot rolling finish temperatures, 860 C and 770 C, were adopted, and their influence on the microstructures and mechanical properties was comparatively studied. The results showed that the microstructures after hot rolling and subsequent annealing could be refined by lowering the hot rolling finish temperature. The resultant microstructures after cold rolling and annealing were hereditarily refined. Lowering the hot rolling finish temperature can weaken the -fiber texture in hot rolled or cold rolled ferritic stainless steel strip. However, the -fiber texture was homogeneously strengthened by annealing the cold rolled ferritic stainless steel strip. Enhanced mechanical property and formability in terms of strength and average plastic strain ratio could be obtained by lowering the hot rolling finish temperature of ferritic stainless steel.

Oct 1, 2019

By Nicolás Ariel Zabala

During the make-up and break-out of the connections, threaded joints are exposed to intense mechanical and tribological solicitations. The connection performance is influenced by its geometry, material properties, surface treatments and thread compound. The aim of this work is to evaluate and characterize the tribological behavior of different thread compounds applied on manganese phosphated carbon steel under low speed and high pressure sliding contact. Four thread compounds were evaluated: one containing lead, zinc and graphite; other lead-free, containing copper and finally, the last two lead-free and containing non-metallic solids. The tribological behavior was analyzed by a block-on-ring tribotest. During the test, load varied linearly between 250 N and 7000 N; loading and unloading lasted 14 sec and were performed in opposite directions of rotation to simulate the make-up and break-out operations. Friction force and load as a function of time were registered. Upon completion of the test, wear surfaces were analyzed by SEM, optical microscopy and energy dispersive spectroscopy. The obtained results show that the lead and zinc containing thread compound displayed the best behavior, showing a wear reduction of approximately 20%. These results are in line with previously known oilfield experience. Average COF values around 0.15 were measured and no significant differences between dopes were observed; indicating that the wear behavior was influenced by the additive package.

Jul 31, 2018

By Charles Sóstenes Assunção

A mathematical model of heat transfer and solidification for a continuous casting of round billets was developed. The water flux density of the secondary cooling zone was experimentally measured, using an apparatus in industrial scale with two types of nozzles, flat jet and full cone jet. The profiles of water distribution were applied on the mathematical model. The results showed that the water distribution is not uniform in both longitudinal and angular directions owing to the unevenness of the spray and to the curvature effect of the round billet. This non-uniformity causes important variation of the heat transfer coefficients and superficial temperature of the billet, especially in the first cooling zones, where the temperature is higher. The mathematical model was used to simulate a change of nozzle type in the first cooling zone. The results showed that the heat flux and superficial temperature variations were reduced with a full cone jet nozzle in comparison with the flat jet nozzles.

Aug 16, 2017

By Marcus Vinicius Laudares Mendonça

SMS calculates and improves tooth and flank profiles individually to realise a homogeneous pressure distribution over the complete load flank. With a tooth profile and flank profile according to AGMA, ISO or DIN standard the contact pressure varies along the load flank. To realize a homogeneous distribution of the contact pressure and to avoid a premature mesh, SMS improves the tooth profile and flank profile in three steps. First SMS is doing a preliminary calculation and design according ISO, DIN or AGMA standard, with safety factors based on more than 125 years of experience. Second SMS calculates and checks the local contact pressure at the load flank under consideration of shaft, gearing and housing deformation, as well as the bearing behaviour. Finally SMS calculates and designs an improved tooth profile and flank profile to receive a homogeneous contact pressure at the load flank. The result is an increase of the torque transmitting capacity of up to 30% of the SMS advanced gears with the same outer dimensions than traditional gears.

Aug 17, 2017

By Débora Ribeiro Lopes

A descoberta das grandes reservas de petróleo e gás ao longo da costa sudeste do Brasil representou um novo desafio tecnológico na história da indústria brasileira de petróleo. Entre as principais dificuldades pode-se citar: água ultra profunda, espesso leito de sal, alta pressão, baixa temperatura, ambiente muito corrosivo contendo contaminantes como o gás carbônico (CO2) e o sulfeto de hidrogênio (H2S). O objetivo deste trabalho é o estudo do comportamento eletroquímico de um aço inoxidável supermartensítico contendo cerca de 14% de cromo (Cr), em meio contendo 115.000 ppm de íons cloreto, 10 ppb de oxigênio dissolvido, com adição de 10-2 mol/L e 10-3 mol/L de tiossulfato de sódio. Para tal foram empregadas as técnicas de polarização anódica potenciodinâmica cíclica e microscopia ótica. Os resultados experimentais mostraram que ocorreu uma variação significativa na extensão da região de passivação quando tiossulfato de sódio foi adicionado ao meio, aumentando a susceptibilidade à corrosão por pites do material.

Jan 16, 2018

By Alex Alves

No cenário econômico atual as organizações estão focadas na maximização de resultados para manter a competitividade e posicionamento frente aos acionistas. Isso exige uma busca minuciosa de alternativas logísticas que envolvem toda a cadeia produtiva, desde a aquisição com o menor custo até uma gestão racional dos recursos materiais, consequentemente se exige cada vez mais controle nos processos. Nesse sentido, destaca-se a atividade de recebimento e inspeção de materiais como uma função da administração de materiais, que tem a missão de garantir o abastecimento dos recursos materiais ao usuário na qualidade e tempo necessário. O presente trabalho tem por objetivo apresentar a sistemática de recebimento, controle e liberação de materiais da Companhia Siderúrgica Nacional, partindo de técnicas de recebimento de materiais e inspeção de qualidade, controle de processo através do SAP, lay-out e fluxos para melhoria da qualidade e produtividade do armazém central de recebimento, garantindo a melhoria contínua no processo e níveis de serviço no atendimento ao usuário.

Jul 29, 2018

By Maria Cecília Junqueira Murta

A espectrometria de emissão óptica é uma metodologia de análise de amostras sólidas utilizada pelas indústrias no controle da composição química de seus materiais. Nesta técnica, uma centelha é direcionada à amostra a ser analisada provocando a excitação dos elétrons de seus elementos, seguida pela emissão de radiação que é convertida em concentração química. Um recente avanço obtido nesta área analítica foi o desenvolvimento do sistema PDA/OES (análise de discriminação de pulsos). Esta ferramenta complementa a espectrometria de emissão óptica, permitindo que ela forneça além da composição química da amostra, o seu conteúdo de inclusões não metálicas. Trata-se de um progresso na investigação de inclusões, que atualmente é desempenhada principalmente pelos métodos de microscopia óptica e eletrônica de varredura. O propósito deste trabalho foi desenvolver uma metodologia de análise de inclusões através da espectrometria de emissão óptica e comparar os resultados obtidos com as técnicas clássicas de microscopia para, assim, possibilitar sua utilização no controle de inclusões durante a fabricação do aço.

Jul 30, 2018