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By N. Lilienberg

The success of European experiments in melting iron and steel with gases resulting from the decomposition of steam by incandescent coal, has encouraged me to design, with the valuable assistance of Mr. George S. Dwight, a plan for producing and burning these gases in a manner economical and efficient for metallurgical purposes. That this direction is the right one, is demonstrated by the repeated efforts made in practice, to introduce as much steam as possible with the blast in ordinary producers, thus displacing a certain amount of nitrogen. Such attempts, however, must always be limited by the cooling influence of the steam. The accompanying drawings represent the producers and the steel-melting furnace, arranged according to our first ideas which may be susceptible of improvement in details when put into practical

Jan 1, 1885

By Henry C. Freeman

The writer spent the month of November last in the La Plata mountains, Colorado, and the material portion of his observations, so far as they may be of general interest, is here recorded. The La Plata mountains lie northwest of the town of Durango. The California mining district is co-extensive with the mountains. They appear on the map as an isolated group; but an examination on the ground shows that they are the continuation of the great

Jan 1, 1885

By P. Barnes

It cannot be said that this whole subject is a new one in respect to its presentation to the Institute, but the minute discussion of it has been looked upon as lying more strictly within the field of study of the societies which have to do chiefly with the construction and management of machinery as such. It must be true that the importance of close limits in steam-economy is as fully recognized among the members of this Institute as by any body of men who have to do with steam-machinery. In all directions, nevertheless, among manufacturers as well as among metallurgists, there may still be found those who do not give the same attention to exact methods in fuel-consumption as devoted to steam, as to other technical uses which, to say the least, are not more important. The study of the most efficient methods of use of fuel in operations which are more strictly metallurgical has been long-continued, and in some directions nearly or quite exhaustive. This has led to a rather close bringing-up, in those particulars, all along the line of technical work, of the establishments (and their managers) which had lagged behind. Yet, in the steam-departments of those works, there are too many reasons for believing that the name may still be legion of those whose methods and results are far from the best. If there be room in any given case to suspect any imperfect working or waste of fuel in the steam-supply, the search for the evil, the clear fixing of its cause, and the application of the remedy are, or certainly ought to be, too obvious in their pressure for attention upon a manager to call for even so scanty a mention of them as can be accorded in this paper. It is natural that men should be incredulous as to imperfections which may be noted as existing in their machinery or methods. Still more are they likely to be altogether disinclined to admit that there may be thus an actual and palpable leakage in the compartment of their money-drawer devoted to coalsupplies. But the laws which govern the combustion of fuel, the

Jan 1, 1885

Jan 1, 1885

By Arthur F. Wendt

In the manufacture of charcoal-blooms, washing or cleansing of the ore from adhering gangue has been practiced for many years. A sluice-box is even to-day used for that purpose in the Southern Appalachian Mountains. For the Lake Champlain bloomaries hard magnetic ores are crushed with stamps and then sluiced or jigged in hand-jigs. The stamps used in the Lake Champlain region are of the most primitive kind. They consist of a trip-hammer, dropping on a perforated cast-iron plate, through which the crushed ore escapes. Only friable rock can thus be successfully treated. To render the raw ore friable, a calcining or burning in piles on a bed of cordwood is resorted to. An expense of 35 cents per ton of crude rock treated is thus incurred. The crushed ore is shovelled or otherwise fed into jigs without previous sizing, except such as is incidental to crushing through the perforated bottom of the stamping-machine. In jigging this ore, it is allowed to pass through the bedding into the "hutch." The tailings are scraped off and wasted. They contain a large percentage of fine ore. In many instances, this is regained by subsequent sluicing. Such was the condition of the industry, when the writer's attention was first called to it in 1882. No attempt had been made to introduce into thiS branch of ore-dressing the notable improvements adopted in concentrating the ores of other metals. The result of the writer's investigations was the building in 1882 of the "Crown Point Separator." At the Crown Point Mines, N. Y., lean ore unfit for the blastfurnace (containing less than 331/3 per cent. of iron), was concentrated and used in the bloomary connected with the mines. The ore was burned here as elsewhere, and treated as described. The plant designed by the writer for Crown Point, is nearly a counterpart of that since erected by Messrs. Copeland and Bacon, contractors, for the Theal mine, Putnam County, New York, which is illustrated by the accompanying plate. The only difference is in

Jan 1, 1885

By James P. Kimball

Jan 1, 1885

By George W. Maynard

In the Journal of the Iron and Steel Institute for the year 1878, in the account of the proceedings of the annual meeting in March of that year, when Mr. Bell read his paper On the Separation of Phosphorus from Pig-Iron, occurs the following statement, as part of the reported discussion of that paper: " Mr. Sidney Thomas stated that he had succeeded in effecting the almost complete removal of phosphorus in the Bessemer process. Experiments had been carried on at Blaenavon, with the co-operation of Mr. Martin, on quantities varying between 6 lbs. and 10 cwt., and some hundred analyses made by Mr. Gilchrist (who had the conduct of the experiments from the first) showing the removal of from 20 per cent. to 99.9 per cent. of phosphorus in the converter. He believed the practical difficulties in the way had been overcome, and that Cleveland pig might be made into good steel without any intermediate process. He hoped on a future occasion to lay full details before the Institute." I was present at that meeting, and I doubt if any one in the hall knew, either by sight or name, the young man who had dared to rise in that august body and claim that he had accomplished that after which the great metallurgists of Europe had been unsuccessfully striving ever since Mr. Bessemer's great discovery. I remember distinctly the pitying smile of derision and the stony stare

Jan 1, 1885

By W. H. Adams

Among the persistent experimenters of the present century no one man is more widely and favorably known in the metallurgical world than the late Peter Spence of Manchester, England, to whom we are indebted for many of the successful processes in the manufac ture of acids and alkalies, and for much of that perfection in me chanical detail which goes so far towards insuring success. For the past twenty-five years—a period covering the greatest changes in soda-processes and a revolution in acid-manufactures ef fected by the substitution of pyrites for brimstone—Mr. Spence was constantly engaged in perfecting the plant for the economical treat ment of pyritous ores; and no text-book has been complete without reference to his many inventions, patented or otherwise. The results of his labors for the past six years were not given to the public, by reason of the active competition existing among man ufacturers on the continent of Europe and in Great Britain ; but it was well known and conceded that the crowning triumph of his .life had been achieved in the successful working of his automatic desulphurizing furnace, which mechanically calcined "smalls" or finely crushed pyrites—the bugbear of all chemical manufacturers. That he was met by many delays and disappointments, and that

Jan 1, 1885

By Josef Westesson

No question in the metallurgical chemistry of the present day seems to be so difficult to agree upon as the determination of phosphorus in iron and steel. To my knowledge, there are at present at least three different methods in use in the iron laboratories of the United States, viz.: The citric acid method, the molybdate-magnesia method, and the direct molybdate method,—the last-named method having been lately adopted. Each of these methods has its advocates, who take every pains to prove its advantages, and the incorrectness of the others; and much has been written for the purpose of securing the use of a standard method—as yet, however, without any result. There is no doubt, or ought to be none, that each of these methods gives correct results, when it is carefully conducted and every precaution is taken. But it is not only correct results that we want nowa-days. The demand is great, also, for getting results in the shortest possible time. I think it has been sufficiently proved that the direct molybdate method, the weighing of the precipitate, answers well in both respects. Being a pupil of Prof. Eggertz, I have myself used his method for years until quite recently, as it is described by Mr. Troilius in our Transactions, vol. x., p. 166 (but with some slight modifications), and I can safely say that the results of this method agree well with those of the molybdate-magnesia method. I have, moreover, been checked, in a few instances, by some of the

Jan 1, 1885

By Henry M. Howe

Preparing the Metals.—Ordinary silver wire was hard-drawn to No. 23 Brown and Sharp gauge; it was cut in two, and one piece was carefully annealed in the ordinary way. The wire was prepared by Messrs. Guild and Delano, jewelers, Boston. The Ansonia Brass and Copper Co., Ansonia, Conn., kindly furnished me with some hard-drawn copper wire No. 31, A. W. G., and some of the same wire after annealing in the ordinary way.

Jan 1, 1885

By J. P. Witherow

The Clapp and Griffiths steel-process may be considered a pneumatic system, similar to the Bessemer, with the difference that the converter is fixed or non-tilting, and that the blast is introduced around the lower section of the converter instead of through its bottom. Mr. Griffiths was engineer-in-chief of the Gilchrist & Thomas basic dephosphorizing process during all the time those gentlemen were experimenting and working up their system, as Mr. G. communicated to me. After separating from these gentlemen, he began developing the present Clapp and Griffiths type of converter. Dr. Clapp, of Nantyglow, Monmouthshire, was a prominent physician in a large iron district. Previous to his association with Mr. Griffiths, he took out some patents on a process of his own for the manufacture of steel, which patents stood in Mr. Griffiths' way; hence the consolidation. Early in the summer of 1883, my attention was called to the experiments of Messrs. Clapp & Griffiths in Great Britain by a friend who had just returned from England. Later in that summer I went to Newport, on the border of Wales, where I met Messrs. Clapp and Griffiths and their friends. After visiting two small converters of their type which were in operation at different works, and spending a few days in the iron-districts of Wales, I went to London, where I met my friend Henry W. Oliver, Jr., who had already heard of the new steel-process. We decided to revisit Wales and examine more fully the process, more especially that Mr. Oliver might have the opportunity of coming practically in contact with the men and die process himself, so that his judgment might not be influenced by my sanguine feelings. On

Jan 1, 1885

By John Fulton

The Connellsville coal-field is a separate strip of the upper coal measures, flanking the Chestnut Ridge along its western side. It extends from a point a few miles south of Uniontown, in Fayette County, following a northeasterly course parallel to the trend of Chestnut Ridge, through Fayette and Westmoreland counties, with its terminal prongs resting 011 the southern portion of Indiana County, north of the town of Blairsville. This belt of coking coal will average about three miles in width and over sixty miles in length, affording nearly, if not quite, two hundred square miles of this large coal-bed.

Jan 1, 1885

By N. Lilienberg

Refractory materials play much the same part in the producion of metals as houses and shelter for men, and it therefore seems useful to discuss sometimes the ways of manufacturing them. In fact, it appears to me that too little has been said on this important matter, probably because the manufacturers of fire-brick do not care to publish details for the benefit of competitors, but perhaps, also, by reason of the indulgent indifference of consumers. Judging from the revolutions in the manafacture of iron and steel caused by using calcareous materials for the furnace-bottoms, it does not seem improbable that in the future basic bricks may be produced suffciently strong for building also side-walls and arches, and perhaps, also, for use in blast-furnaces. But the existence of the present difficulties of great shrinkage in burning and small strength against compression, which limit the possibility of using basic bricks to Bessemer converters and such open-hearth furnaces as permit the bottom to be separated from the superstructure, seems to indicate still a long and extensive use of silica fire-bricks. I am not prepared to say anything about American fire-brick making, but knowing that industries abroad are watched with increasing interest by American manufacturers, I have imagined that this association would like to hear some facts about the way firebricks arc made in my country—Sweden. Well-known as it is that Sweden produces a high quality of iron, it is perhaps not so universally known that the same country produces a very high grade of silica fire-brick, whereby most of its own wants are supplied. In giving the following sketch I can, of course, not claim that all the facts are entirely new, but shall consider my object attained if American manufacturers can derive some benefit from the comparison of the following methods with their own, and if some discussion on this important subject can be aroused which will contribute to further progress. In order to show the extensive use of domestic fire-bricks in Sweden, where English bricks are easily obtainable, I mention the fact that about twelve millions of all kinds of fire-bricks (reduced to

Jan 1, 1885

By Byron W. Cheever

In working up the process which I described at the Chicago Meeting, May, 1884 (p. 163 of the present volume), for the estimation of phosphorus in iron and steel, I employed samples of steel obtained from one works only, and of a given brand. Since then I have had frequent occasion to test the process on other steels, and find that it works equally well. But some steels present certain colors which may mislead the operator; and I therefore propose a slight change in the directions formerly given. On the second page of my paper, in the second paragraph, I would substitute the following modified directions: Place the flask under the hydrant, till the solution is perfectly cold ; then add, gradually, strong ammonia, with constant stirring, till the solution is changed into a pasty mass and the ammonia is in slight excess; then add cautiously HNO3 (1.40 specific gravity)

Jan 1, 1885

By Robert W. Hunt

HAVING devoted considerable time to the investigation of the Clapp-Griffiths converter and the metal produced in it, it may perhaps be of interest to the Institute to learn the conclusions which I have formed. Of course, it is well known that the stationary converter of small size is the very oldest type of vessel used in the pneumatic process. Hence it will be only necessary to call your attention to the points which are special features of the Clapp-Griffiths. This converter has a slag tap-hole, situated at such a height in relation to the metal under treatment that, when the cinder is formed and boils up as the blow progresses, it can run off and thus be removed from contact with the iron, and will also be out of the way when the decarbonized metal is tapped into the casting ladle and the manganiferous alloy added. The manner of shutting off the blast, when the process is completed and the metal is being tapped, is another distinctive feature. The tuyeres are situated around the sides of the vessel, and enter the interior some little distance above the bottom; they are provided with plugs through the centers of which there are small openings. When the blow is completed, these plugs are forced forward into the outer orifices of the tuyeres, thus shutting off the blast, excepting the small quantity' entering through the passages named. While this is sufficient to keep the metal from running into the tuyeres, it reduces to the minimum the action of the blast while the metal is being tapped. Of course, this is of great importance, as in an ordinary stationary converter any delay in getting open the tap-hole means overblowing, and even while the first part of the charge is running out the oxidation is in frill force. Duplicate or movable bottoms are used, thus more than doubling the possible output of the plant. The pressure of' blast is quite light, never ex-

Jan 1, 1885

By F. H. McDowell

For more than two hundred years Mexico has been enriching the world from her inexhaustible wealth of precious metals. From this source alone, over three thousand five hundred millions of dollars have been poured into the coffers of Europe and America. During these centuries the wants of the country in manufactured goods have been supplied from the mills and machine-shop of the Old World. English, French and German merchants in Mexico have vied with each other in their efforts to control the importing of these goods from their respective countries. The overthrow of Maximilian, the departure of the French and the restoration of the Republic, largely influenced by the strong stand taken by the United States Government during our own civil war, established a new order of things. Americans were encouraged to visit the sister republic, examine into the needs of the country, as well as its resources, and interest themselves in the work of development. More recently, under Presidents Diaz and Gonzales, liberal inducements have been extended to American capitalists to build railroads, open mines, erect reduction-works, raise cattle and improve the crude systems of agriculture. The Mexican Central Railway has been pushed south from the Rio Grande to the Capital, and, by its branches and connections, makes the whole mineral belt of the country accessible.

Jan 1, 1885

Jan 1, 1885

By Oswald J. Heinrich

SINCE my communication to the Institute at the Baltimore meeting in 1879,* in which I took the lead in emphasizing the importance of a new method in the manufacture of soda, already practiced to some extent in England and on the Continent of Europe, five years have passed. I.then referred particularly to the advantages offered in the United States for this peculiar method, by the ammonia process, namely: 1. At the present time, at least, we have but one mine in this country where rock-salt is mined, namely, at New Iberia, La. On the other hand, we have many localities where brine of various degrees of strength, up to that of cold saturation, is obtained in large quantities. 2. We have excellent fuel, in close proximity to most of the brinecenters. 3. Our supplies of pyrites, to use in the manufacture of sulphuric acid, for use in the manufacture of soda by the Leblanc process, are mostly too far from the brine-centers to permit competition in that line with the more favorable conditions existing in England. 4. Unlike our foreign rivals, we have no large and costly plants, erected on the Leblanc plan, which must be abandoned and exchanged for new but cheaper plants, before the ammonia-soda process can be adopted. 5. We have a constantly increasing demand for soda, which is almost entirely supplied by importation. If slow progress has been made hitherto in this country in the extension of this manufacture (only one plant at Syracuse, erected . under the Solvay patent, having as yet been placed in operation), I still feel gratified in saying that developments in England, and particularly on the Continent of Europe, give ample proof of the

Jan 1, 1885

By W. McDermott

It is well known that many so-called free-milling silver arcs are so classed more from their value necessitating a cheap process than from a real adaptability to raw amalgamation. Such low--grade ores, carrying more or less sulphurets, are more profitably treated by a cheap rapid process than by the more effective but costly process of roasting arid amalgamation. The tailings are sometimes crudely concentrated, or, after lying and becoming partially oxidized, are again worked in pans. Of late years, by the use of improved methods of concentration, many old low-grade tailings-piles have been reworked to a good profit; and in some improved mills arrangements are made to concentrate before or after amalgamation, thus making a single treatment in mill suffice. It is self-evident that on a low-grade ore a small increase in percentage saved is of no commercial advantage if accompanied by a material increase in cost, and therefore a cheap and continuous system of work is the real necessity, if a fair saving be effected. As an illustration of the possibilities of combined concentration and amalgamation on some ores, the following results of a working test at the New York Ore-Milling and Testing Works will be of some interest. The ore treated was a hard white quartz from Mexico, carrying a very small percentage of finely divided sulphurets, chiefly iron

Jan 1, 1885

By W. J. Taylor

FURNACE-MEN who have not taken advantage of the use of dynamite in certain blast-furnace troubles, as explained by Mr. Witherbee in his valuable papers read before the Institute some years since, cannot appreciate the quick relief and great advantage that may be derived at times from its judicious employment. Before giving my experience in the use of high explosives in blastfurnace troubles of certain kinds, I will record a method I have used with marked success in " blowing down." Had I not understood, however, the use of powder, I would have " salamandered " effectually the first time I tried it. Early in my straight-furnace experiments, last summer, at the Chester, N. J., Furnace, I wanted to blow down to within 3 or 4 feet of the tuyeres. To do this with a down-comer not lined, and without putting in any limestone to keep the gases cool enough to do no harm, was not an easy task. We could keep the bell and hopper cool by filling them with water, say 12 inches deep; but before we got the stock down 15 or 20 feet the pyrometer in the gas-flue on top mas up to 1300°, and the clowncomer was red-hot, with the heat still rising. In this emergency my assistant, Mr. N. M. Langdon, urged the trial of a plan lie had often advocated, viz., the introduction of water in some way under the bell in the proper quantity, in order that its evaporation might absorb and reduce the heat of the escaping gases to a point where it would not do any harm. He thought the bell

Jan 1, 1885