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By Paul Hammond

Abstract The Allard Lake ilmenite deposits, which are currently being developed on a large scale, occur as a series of dykes or lenticular, flat-lying bodies within the northeastern part of a large, oval shaped anorthosire mass of Precarnbrian age which lies with its long axis paralleling the gulf of St. Lawrence. The Lac Tio deposit, discovered by Kennco Explorations, Limited, in 1946, is the largest body of titanium ore of its type now known in the world. It contains upwards of 112,000,000 short tons of ilmenite ore averaging 32 per cent TiO2 and 36 per cent Fe. The ore is an aggregate of ilmenite with oriented microscopic blades of hematite. The deposits appear to be high temperature, late magmatic injections containing only a small amount of volatiles, and bear a genetic relationship to the anorthosite rocks in which they occur. * * * Introduction Recent developments on the ilmenite deposits in the Allard Lake district of Quebec indicate the probability of a major industry, and one which may make Canada the world's greatest producer of titanium pigments and, ultimately, of titanium metal. The presence of ilmenite in this district was first reported by the Quebec Department of Mines following a reconnaissance shore-line geological survey in the year 1941. The ensuing report by Retty describes the occurrence of a number of small ilmenite lenses about the shore of Allard lake and' along two smaller lakes in the vicinity. These showings were later staked by Toronto and Montreal interests who carried out a certain amount of development work, and were described in more detail by Longley for the Quebec Department of Mines. The claim groups were later optioned by Kennco Explorations, Limited, Canadian subsidiary of Kennecott Copper. None of the deposits in themselves constituted a sufficiently large body of ore to warrant the major construction expenditures necessary for their exploitation on a profitable basis. The surrounding anorthosite areas, however, were considered favourable for the possible occurrence of other ilmenite deposits

Jan 1, 1949

By Robert W. Geehan

A preliminary examination of the Dayton iron deposit was made in 1941 and 1942 by Paul E. Pesonen and O. H. Metzger, engineers of the Bureau of Nines. Trenching and sampling were recommended, to be followed by core drilling if favorable results were obtained. The Bureau of Mines conducted a project at the property from June to December 1942. The deposit is in sec. 6, T. 17 N., R. 23 E.; sec. 31, T. 18 N., R. 23 E.; sec. 36, T. 18 N., R. 22 E.; and sec. 1, T. 17 N., R. 22 E., M. D. B. & M., about 15 miles west of Lahontan Reservoir in Lyon and Storey Counties, Nev. It lies at an altitude of about 4,500 feet north of the Carson Plains, in the foothill section of mountains that rise to about 7,000 feet to the north of the property. The deposit may be reached by driving 12.5 miles northeast of Dayton over U. S. Highway 50, thence northerly 2.7 miles over a dirt road to the property. The climate is hot and dry in summer, with occasional thunderstorms some of cloudburst variety, and frequent high winds. Winters are usually moderate, with light snowfall and some subfreezing temperature.

Jan 1, 1949

INDEX OF CONTENTSIntroductionChemical compositionsNormally Cooled MattesPort Kembla mattesMount Lyell matteMount Morgan matteGranulated MattesConclusionsIllustrationsINTRODUCTIONIn a previous paper in these Proceedings(l) an account was given of the composition of some copper-lead mattes from the Port Pirie Smelters. The research programme of the Mineragraphic Section of the Commonwealth Scientific and Industrial Research organization has since been extended to copper-iron mattes from Port Kembla (The Electrolytic Refining ana Smelting Co. of Australia), Mount Lyell (The Mount Lyell Mining and Railway Co.) and Mouilt Morgan (Mount Morga:p. Ltd.).Chemical Composition of the Mattes.The mattes examined have a considerable range in chemical composition, as is shown by their analyses (Table 1).

Jan 1, 1949

By Graham W. Marks

This report is the fourth of a series concerning the development of spectrochemical methods for the analysis of ore samples and related Metallurgical materials by the total-energy method. In this report, the application of this method to the determination of thallium is discussed. This element lies in group III of the periodic tale; one other Clement of this group; indium, has already been investigated.

Jan 1, 1949

By Cyril Stanley Smith

Jan 1, 1949

Jan 1, 1949

By Louis A. Panek

The purpose of this paper is to present a method of designing safe and economical arch structures that are to be constructed of concrete or directly of original earth materials. The experimental data used to illustrate the design method are taken from Bucky and Fen tress,1,2 and the application of the ideas presented by them is extended by obtaining an additional set of curves from which arch structures may be designed. This design method is based upon the following principles of similitude: A scalar model made of the same material as that of the full sized structure will behave similarly to its prototype if the density of the model is increased in the same proportion as its linear scale is decreased. Let R represent the scale or model ratio, namely, the ratio of a prototype linear dimension to the corresponding model linear dimension. The effect of increased density may be obtained by rotating the model in a centrifuge at a speed such that the centrifugal held exerts on the model an accelerative force R times the accelerative force of gravity. Under these conditions; (I) model unit stresses are equal to corresponding prototype unit stresses, (2) the ratio of the prototype deformation at a given point to the model deformation at a similar point is equal to the scale ratio, R, and (3) the model and the prototype will behave similarly within and beyond the elastic limits of strain. According to the above relations, such models can be used to solve the following problems: I. The dimensions of the most economical safe arch structure for a given load. 2. The miaximum safe roof span underground for given geologic conditions. The procedure is described briefly as follows. Tests are made by rotating in a centrifuge a number of models that repiesent a variety of prototype loads and dimensions. From the experimental data, curves are plotted to show the relations between these loads and dimensions. The curves are used to solve directly the problems stated above. Structural design is based upon the working (safe) stress of the material of construction, which is established by applying a factor of safety to the experimentally determined ultimate strength of the material. In conformity with this principle, each model is gradually loaded until failure occurs. A safety factor is then applied to the results. If a safety factor of 4 is used, a given model at failure represents a safe prototype, the linear dimensions of which are equal to one-fourth the model ratio at failure times the corresponding model dimensions. The safe model ratio is computed from the following formula: Safe R =(1/4)4p2n2r/g=p2n2r/g [I] in which: n = centrifuge revolutions per second at model failure; r = radius of rotation of the model in feet; g = 32.2 ft/sec2.

Jan 1, 1949

By G. Richards Gwinn

THE mineral graphite has been known for hundreds of years and was first used commercially as a coloring agent. Its true identity, however, was not recognized until the end of the eighteenth century and its commercial development did not become extensive until near the close of the nineteenth century. The common names for this mineral are graphite, plumbago, and black lead; others less frequently used are potelot, crayon noir, carbo mineralis, and kish. Graphite was named by Johann Gottlieb Werner in 1789 from the Greek word graphein, to write, and this name was applied primarily to the large crystalline, flake variety. Plumbago is a trade term used primarily for massive graphite as found in Ceylon. Black lead is also a trade term and, like plumbago, is based upon the idea that prevailed throughout the Middle Ages that graphite was a form of lead, or at least contained that metal. Graphite is a soft, black, unctuous form of carbon that crystallizes in the hexagonal system with rhombohedra1 symmetry. It occurs occasionally in six-sided tabular crystals but usually is found in foliated masses, minute disseminated scales, or earthy lumps. It has perfect basal cleavage, is gray to black, has a metallic luster and a gray streak. The specific gravity is 2.1 and hardness is 1 to 2. It is opaque even in finest particles; extremely resistant to the action of acid or heat; and a good conductor of both heat and electricity. Graphite may be separated into three classes: ( ) natural, (2) manufactured (which is sometime called artificial), and (3) colloidal. Natural graphite is divided into two classes, "crystalline" and "amorphous." Crystalline graphite may occur as flake, lump, chip or dust. Amorphous graphite is a commercial term only, as all graphite is crystalline, but grades in which the individual grains cannot be distinguished are classified by the trade as amorphous. Natural mixtures of crystalline and amorphous occur in all proportions. The term "artificial graphite" is a misnomer; "manufactured graphite" is a better term, because it actually is pure crystalline graphite,

Jan 1, 1949

By A. Sutherland Brown

"The Red Rose Mine is in the Rocher Deboule Range, 8 miles south of Hazelton. The mill camp (elevation 4,000 feet) is on Red Rose Creek, 11 miles by road from Skeena Crossing. The mine camp is one mile northeast and 1,600 feet above the mill camp on a spur of Red Rose Peak.The Red Rose mine was described in the Jubilee Volume, Structural Geology of Canadian Ore Deposits (Davis, pp. 129-131), but regional geology and mine development have progressed to a stage at which a more complete description is possible.The property was first located in 1912, and for the next 7 years was prospected actively for gold and copper on the southern extension of the Red Rose shear. Scheelite was first discovered in the vein in the northern part of the shear in 1923. The Consolidated Mining and Smelting Company of Canada, Limited optioned the property in 1939, and after a drilling program in 1940 the present mine development was initiated in the vein in the northern part of the shear. A 75-ton-per-day mill started operating early in 1942 and continued until 1943. The property was inactive until 195 l, when Western Tungsten Copper Mines Limited leased the property from The Consolidated Mining and Smelting Company of Canada, Limited. A mill, which later was enlarged to 140 tons per day, started operations at the end of 1951. The mine and mill were closed in December, 1954.The mine has twelve levels and sub1evels, and most of the workings are in the plane of the vein (see Figure 2a). The level interval is not constant, but between the lower four levels is 87 feet (100 feet in the plane of the vein). Access is provided by four adits; the 800 (elevation 5,659 feet), 600 (5,920 feet), 300 (6, 133 feet) and 200 levels (6,237 feet). The 600 level is the main haulage, and from it the ore is transported to the mill by aerial tram. From this level an inclined shaft extends in the vein to the lowest level (I, 100)."

Jan 1, 1949

By F. W. McQuiston

Idarado Mining Company's mill and surface plant are at the portal of the Treasury tunnel at elevation 10,625 ft, 12 miles south of Ouray, Colo. In 1943 and 1944 this tunnel was extended in a westerly direction to tap the Black Bear vein, and, together with the recently completed 1100-ft inclined Treasury raise, provides access to the Black Bear mine. In 1945 a 250-ton mill was placed in operation to process development ores containing much needed copper, lead and zinc for war requirements, and to serve as a pilot testing unit for larger scale milling operations. In the years 1902 to 1927 some 329,000 tons of ore were produced from mine workings on the Black Bear vein that extended downward from elevation I2,325 ft at the Black Bear tunnel portal to elevation 11,618 ft, the lowest level of the mine. The ores were taken to the Cascade and Smuggler-Union mills near Telluride over two aerial tramways. Gold bullion, a copper-lead concentrate, and a zinc concentrate were produced. Ores The Black Bear is a compound fissure vein that has undergone several stages of mineralization. The first important stage is represented by complex ores of copper. lead and zinc in a quartz gangue. Precious metal content in this stage is low. The galenn is argentiferous and varying amounts of tetrahedrite, freibergite and bornite tend to increase the normal copper content represented in chalcopyrite. The zinc occurs as a true sphalerite with little or no iron. Later re-openings of the fissure took place more or less co-extensively with the successive introduction of (I) abundant quartz gangue containing minor amounts of chalcopyrite, galena and sphalerite; (2) free gold in a fluoritic quartz gangue; and (3) barren, low-grade quartz with minor amounts of pyrite as the only important sulphide. The sulphides show practically no oxidation and little mineralogic inter-growth. Because of the common overlapping of these successive stages of mineralization within a given mining area, considerable dilution of the base-metal content takes place, thus lowering the average mill-head grade. Plant Practice Metallurgical testing was started shortly after the Black Bear vein was encountered on Treasury tunnel level in 1944. Laboratory tests showed good flotability of the minerals in the ore and indicated an economic separation could be made of the copper, lead and zinc minerals into their respective concentrates. The success of the separation is close reagent control to maintain a balance between promotion and depression of the sulphides. To maintain this balance reagent consumption for the three metal separation is considerably higher than in ordinary lead-zinc flotation.

Jan 1, 1949

By T. W. Guy

The increased moisture due to water-spraying for coal dust control is of interest even for mines from which the coal is to be wet-washed before screening, because in many cases wet coal dust materially de- 20-mesh X 0 sizes as pct ROM average ............................... 6.3 pct Range 2.3 to 9.5 pct 20-mesh X 0 sizes as pct 3/8 X 0 sizes average........'...................... 18.9 pct Range 12.7. to 23.9 pct creases the loading efficiency of men and equipment at the faces. It also causes a serious increase in the normal wear and deterioration of all equipment with which it comes in contact. It is important to the consumer if it increases his as-received moisture. No attempt will be made in this paper to cover the entire subject of water-spraying of coal for dust control. It will be confined to discussion and data on (I) percentages of dust in bituminous coals, (2) moisture increases due to spraying for dust control in mines or plants by methods which have proved satisfactory for periods of one to five or more years, and (3) a few suggestions for research. Size and Percentage or Coal Dust The U. S. Bureau of Mines1 classifies as coal dust all bituminous coal passing a 20-mesh sieve (0.0328 in. square opening). The percentage of such dust to be found in ROM coal, of course, varies widely with the characteristics of the seam, and with the methods used in the mining and in the preparation of the coal. ROM screen analyses of 12 U. S. coals selected at random from personal files given in Table I show: A few other screen analyses examined indicating 40 pct or more of 20-mesh X 0 dust in 3/8 in. X 0 sizes were not included because of uncertainty that they were representative. The number of results in Table I is not sufficient to give a reliable estimate of the average, or of the range to be expected, but it indicates that in every case the coal dust is a relatively large percentage of the total ROM coal, and, of course, a progressively larger percentage of resultants as the larger sizes are separated for marketing.

Jan 1, 1949

Jan 1, 1949

Jan 1, 1949

By Robert B. McCormick

THE major use for quartz crystal is in the manufacture of radio oscillator plates and telephone resonator and filter crystals. Quartz crystal is also cut and polished as a semiprecious gem stone, particularly in the colored varieties (amethyst, Brazilian topaz, and others), and often is carved into various objects of art. Prisms, wedges, lenses and other optical parts often are made of quartz crystal, usually for special- purpose instruments. Chips and small clear crystals below 100 grams in weight, called “lascas” by the trade, are the raw material for fused quartz products. HISTORICAL BACKGROUND The Greeks believed quartz to be permanently frozen water and therefore called it krustallos, which, literally translated, means clear ice; but ages before their civilization, prehistoric man had crudely cut and polished crystals for rough charms and ornaments. About 2000 B.C., the Egyptians brought the art of cutting quartz to a high level. While there are earlier examples of crystal art that have great value, working in crystal during that period became a means of artistic and religious expression that has endured through the ages. Art museums and private collections throughout the world contain many priceless pieces. They include findings from the tombs of the earliest Egyptian rulers, as well as magnificent art objects in both clear and colored crystal encrusted with silver, gold, enamel, and precious gems of oriental and European workmanship. Pierre Curie first measured the piezoelectric effect of quartz, in 188 1, by placing a weight on the surface of a quartz crystal and measuring the resulting electrical charge, which he found was proportional to the weight applied. The following year the inverse piezoelectric effect was proved by the Curies. By applying a voltage to a piece of quartz, a measurable physical displacement occurs. The first practical application of this effect was the construction of a bimorph unit to measure voltage by measuring the amount of the displacement of the end of the bimorph. The piezoelectric properties of quartz crystal remained largely a laboratory curiosity until World War I, when a supersonic device for

Jan 1, 1949

By A. D. Mufch, G. P. Mitchell

"THE HARDY MINE of Falconbridge Nickel Mines Limited is located in Lot 9, Concession 1, Levack Township, Sudbury District, Ontario, 20 miles northwest of the city of Sudbury, and a mile west of the town of Levack. The ore deposit is one of the many nickel-copper sulphide bodies found on, or near, the lower contact of the well-known Sudbury norite-micropegmatite irruptive, and is one of a family of ore deposits which occur on the northwest rim of the irruptive.The property was acquired by purchase in 1935. In the same year a magnetometer survey along the footwall contact of the norite, which is covered by about 150 feet of glacial sands and clays, first indicated the location of the orebody. Drilling from 1935 to 1942 outlined the extent of the ore. Shaft sinking was commenced in the fall of 1951, and the mine is now approaching full production at a rate of about 300,000 tons per year.There are several major differences between the geology of the Levack area and the Falcon bridge area, which lies at the opposite extremity of the irruptive, 28 miles to the east. The purpose of this paper is to describe the essential features of the geology of the Levack area as seen in the Hardy mine, and to supplement the recent papers on other properties in the Sudbury area by Davidson (1), Lochhead (2), and Yates (3).General GeologyA recent review of the regional geology and an extensive bibliography of the Sudbury area can be found in the two papers by H. C. Cooke (4, 5). Some of the recent related references are: Jas. E. Thomson (6), E. M. Abraham (7), Franc. R. Joubin (8), W. G. Q. Johnstone (9)."

Jan 1, 1949

By Wesley A. Grosh

The Vest nickel prospect, in Floyd County, Va., was discovered about 25 years ago. Limited exploration of the deposit had indicated some appreciable nickel mineralization in the sulfide ore. The property was examined on March 9, 1943, by an engineer of the Bureau of Mines in company with C. W. Vest, owner of the property. A limited exploration program was recommended. Two holes totaling 320 feet were diamond-drilled in January 1944. Drilling indicated the sulfides are sparsely disseminated. The only nickel values of interest were at the old prospect shaft.

Jan 1, 1949

By E. A. Gulbransen, W. S. Wysong, K. Andrew

The reaction of carbon in solid solution in a metal with the surface oxide fim on many metals may be inferred from thermo-dynamic calculations for high vacua and high temperature conditions. Holm has recently shown that oxide films may be removed from ferrous materials by heating in a vacuum at high temperatures and that carbon is the essential element in the reaction. considerable work has been described in the literature on the de-carburization reaction. Several general references may been 2,3,4 However, the nature of the mechanism involved in the decarburization is not well understood. Our interest in this reaction resulted from many attempts to degas and to reduce by pure and dry hydrogen the surface oxides on strips of various types Of chrome-nickel alloys. Some of the early experiments On the behavior Of '3 pct chrome-iron in vacua of the order of 5 X lo' mm and at a temperature Of 600°C have been reported.5 These experi-merits showed a 'low reaction with the residual Oxygen Or water vapor in the system and no reaction with hydrogen. This is in accord with thermodynamic data which would lead to the prediction that it is extremely difficult to maintain a hydrogen atmosphere at 600' C pure enough to reduce Crz03 formed On the surface. The crystal structure of the superficial oxide film formed on 13 pct chrome- iron and Nichrome V has been investigated in the thin film range by Gulbransenr Phelps and Hickman,' and shown to be "203. It Was surprising to us to note that when a specimen of Nichrome V containing approximately 80 pet nicke1 and 20 pet chromium was heated to 850°C in a high vacuum, the specimen lost weight. The rate Of weight loss was very temperature sensitive. A study of this reaction in vacua and in a hydrogen atmosphere is the subject of this communication. Type Reactions Let us consider the various reactions which may occur when a metal is heated in vacua, in a hydrogen atmosphere, or in an oxygen atmosphere. The number and kind of reactions will depend upon the chemical nature of the metal, its alloying constituents and the location of the alloying constituents. The metals used in this study are chrome-nickel alloys of the heater type, They consist essentially of chromium, nickel and iron, small amounts of carbon, silicon and manganese and traces of zirconium, calcium, aluminum and magnesium. The trace elements are added to improve the lifetime and other characteristics of the alloy when used as a heater. Seven of the more important reactions with which we are going to be concerned here are as follows: 1. Metal . (gas) F? metal + gas — degassing of the metal 2. zM(s) + y }i Oi(g) M MIOu(s) -oxidation

Jan 1, 1949

By F. S. Wartman

This paper gives an account of the production of ductile-grade titanium powder in 100-pound batches by reduction of purified titanic Chloride with magnesium, grinding, leaching, and magnetic-separation of the reaction product. Apparatus, technique, and methods of controlling product quality are described and some data on operating costs are given.

Jan 1, 1949

Jan 1, 1949

By Edward Sampson

Bases of National Power At a time when the economy of the world is in a particularly troubled state it is appropriate to examine some problems of the distribution of natural resources. I should like particularly to call attention to the remarkable increasing demand for natural resources, to give an analysis of the demand for certain mineral resources, and to direct attention to some problems in satisfying this demand. All industrial power is based on natural resources and the most basic of these are soils, energy resources, and mineral resources. There is a strong interrelation of these resources, more than is obvious, and I shall take up certain aspects from the point of view of a geologist. Few nations are well endowed with all three of the kinds of natural resources I have mentioned and much has been done by some small countries whose peoples are industrious and enterprising and where conditions for free world trade have been favourable. However, major industrial power is dependent on a substantial endowment of all three classes.

Jan 1, 1949