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By R. L. Hopkins, H. T. Rall, H. J. Coleman, C. J. Thompson

Two methods were tested for separating sulfur compounds in certain petroleum fractions into types . Such separation is preliminary to identifying the compounds . Each method involved extraction of sulfides from petroleum sulfur concentrates . In the first method , the sulfur concentrate was reacted with methyl - ptoluenesulfonate to form sulfonium compounds from which unreacted portions of the sample were removed by washing with solvent . The sulfides then were recovered by heating the sulfonium compounds with anhydrous triethanolamine . The second method consisted of passing anhydrous hydrogen iodide into a n-butane solution of the sample cooled in dry ice , whereupon the hydrogen iodide adducted with the sulfides to form sulfonium compounds . These adducts separated as crystalline solids or , more frequently , as glassy viscous liquids . The sulfide was regenerated by adding water to the filtered sulfonium compound and was recovered by steam distillation or by extraction with pentane . These methods have been evaluated , using individual pure sulfur compounds and blends of sulfur compounds . They also have been applied successfully to separating sulfides from sulfur concentrates derived from petroleum fractions .

Jan 1, 1964

By Oliver Bowles

It is noteworthy that 80 to 95 per cent of the gross production of all slate quarries in the United States is discarded as waste . In view of the loss involved in handling so much waste , and the consequent added cost of the finished product , the Bureau of Mines has undertaken a study of the slate industry for the purpose of devising the best means of reducing the proportion of waste , and of utilizing the unavoidable waste . The utilization of waste has received special attention , and the cooperation of many prospective purchasers of waste slate has been enlisted in testing its adaptability for various uses .

Mar 1, 1921

By Boyd Guthrie

The current use of Mid - Continent crude oil for the manufacture of war products , such as aviation gasoline and lubricating cil , has caused an acute shortage of available supply from established sources . Therefore , refiners who heretofore have had no reason to use West Texas crude oils now are considering them as charging stock and need more information concerning their characteristics . The Bureau of Mines has published several reports3/ giving analyses of the most important of these crude oils . However, to make the applicable data in these publications readily available to refiners , the present compilation of analyses of West Texas crude oils has been prepared . Data showing the effect of catalytic desulfurization of naphthas from West Texas crude oils have been presented in a restricted Bureau of Mines Report of Investigations . These analyses were made under the general supervision of R. A. Cattell , chief, Petroleum and Natural Gas Division, Bureau of Mines , Washington, D. C. , and N. A. C. Smith, supervising engineer , Fetroleum Experiment Station, Bureau of Mines , Bartlesville, Okla . , and under the direct supervision of Harold M. Smith, senior petroleum chemist, Bartlesville , Okla .

Jan 1, 1944

By H. P. Greenwald, H. C. Howarth

There was reported in Bureau of Mines Technical Paper 5754/ a series of tests to determine the compressibility and bearing strength of specimens prepared from blocks of potash salt obtained from a mine near Carlsbad , N. Mex . The events leading up to the investigation were sketched in a foreword by George S. Rice , then chief mining engineer of the Bureau ( retired September 30 , 1937 ) ; this foreword also gives a discussion of the possibility of increasing the ultimate total recovery of the potash salt by " second mining" of pillars or by use of a longwall system . In June 1936 , Rice and the senior author visited Carlsbad with H. I. Smith , chief of the mining division of the Geological Survey , to observe mining then in progress and to discuss with the management of one of the mines records of convergence of roof and floor which they were obtaining . It developed that serious thought was being given to the possibility of roof failure resulting from shear at the faces of pillars . There was envisioned the danger of such cracks extending upward to water - bearing strata . Obviously , the simple compression tests of the potash salt then being made would throw no light on this question , and tests of assemblies of potash and roof salts would have to be made . In this connection it is to be remembered that in the mine no sharp division exists between the potash salt being recovered and the nearly pure halite which forms the roof . The interlocked crystalline structure is continuous , and there is merely a very rapid decrease in the proportion of sylvite in a short distance vertically . Figure 2 of Technical Paper 575 shows that two samples near the top of the salt being mined contained , respectively , 51 and 65 percent potassium chloride . Contrasted with this is an analysis of the roof salt given on page 24 of that publication , which showed only 3.6 percent potassium chloride . As the data given in Technical Paper 575 show , the roof salt is much less plastic than the potash salt . The immediate roof may then be thought of as a more rigid stratum of indefinite extent resting on and continuous with yielding supports and loaded uniformly at the rate of 900 to 950 pounds per square inch . Just what thickness of the salt should be considered as immediate roof is uncertain .

Feb 1, 1938

By J. S. Kennedy, R. G. Omeara

Beryllium is a strategic metal of ever-increasing peacetime importance because of the unusual properties of beryllium-copper alloys. These unusual characteristics are the combination of high strength and hardness, high fatigue resistance, and high wear resistance in alloys that have the corrosion resistance of copper. The principal industrial source of beryllium is the mineral beryl, a beryllium-aluminum silicate that occurs in pegmatites associated with quartz, feldspar, mica, and smaller amounts of various accessory minerals. The beryl is usually recovered in processing the pegmatites for the recovery of some of the other mineral constituents. Pegmatite deposits are found in various parts of the United States, but those in the Black Hills of South Dakota are the source of most of domestic production. The beryl marketed from the South Dakota pegmatite deposits occurs as coarse crystals, which are obtained by hand sorting. These pegmatites also contain other valuable minerals.

Jan 1, 1948

By J. E. Tiffany, N. A. Tolch

The Pittsburgh Experiment Station has made a survey of the properties and characteristics of the brands of fuse manufactured in the United States ; 25 samples were procured from 4 manufacturers representing the different brands offered on the market when the investigation was begun . It is believed that the field was completely covered except for special fuse made to order for a particular job .

Jun 1, 1934

By C. E. Armantrout, H. Kato, M. I. Copeland

The data collected during this investigation indicate that the chromiumgadolinium system has extensive liquid immiscibility and one eutectic point . Liquid immiscibility occurred at temperatures above the monotectic isotherm , 1,830 ° C , which extended from less than 0.25 to about 85 weight - percent gadolinium . The eutectic was at 96 percent gadolinium and 1,170 ° C. Gadolinium and chromium were the only phases in this system . There was a solid solubility of less than 0.25 percent gadolinium in chromium at 1,730 ° C and less than 0.10 percent chromium in gadolinium at 1,160 ° C. The alloys were prepared by nonconsumable - electrode arc - melting , and the alloy system was investigated by heat treatment , metallography , thermal analysis , and X- ray diffraction . All the melting , heat treatments , and thermal analyses were conducted in a vacuum or in helium because of the reactivity of chromium and gadolinium with the components present in the atmosphere at elevated temperatures .

Jan 1, 1964

By F. D. Osgood, A. C. Fieldner, W. A. Selvig

In connection with investigations being conducted by the Bureau of Mines regarding pulmonary disease which is prevalent among metal miners in certain districts , a large number of rock- dust samples have been collected , and have been examined in the Bureau's laboratories . The earlier work has been described in Bureau of Mines Technical Paper 105 , " Pulmonary disease among miners in the Joplin district , Missouri , and its relation to rock dust in mines " by A. J. Lanza and Edwin Higgins , 1915 , and in Bureau of Mines Bulletin 132 , " Siliceous dust in relation to pulmonary disease among miners in the Joplin district , Missouri , " by Edwin Higgins , A.J. Lanza , F.B.Laney , and Geo . S. Rice , 1919. The methods of collecting and examining dust samples have been greatly improved during the investigation , much valuable information having been made available by similar investigations conducted by the Miners ! Phthisis Prevention Committee , Union of South Africa . The latter are described in the " General report of the Miners ' Phthisis Prevention Committee , Johannesburg, Union of South Africa , 1916 " , and " Final report of the Miners ' Phthisis Prevention Committee , Johannesburg, Union of South Africa , 1919. " The investigations by the Bureau of Mines and the South African committee show that by prolonged inhalation of air containing minute particles of sharp and insoluble rock dust , the lungs retain sufficient dust particles to cause decided injury to the lung tissue , the injured lung becoming very susceptible to the development of tuberculosis .

May 1, 1920

By W. W. Adams

Fatal accidents at coal mines throughout the United States numbered 170 during May , 1923 , according to reports received by the Bureau of Mines of the Department of the Interior from State mine inspectors . The production of coal during the month was 54,649,000 tons ; hence , the fatality rate was 3.11 per million tons . In May last year the fatality rate was 4.22 , based upon an output of 20,636,000 tons , including 35,000 tons of anthracite . Because of the miners ' suspension of work last year, the production of fresh-mined anthracite in May 1922 was completely stopped ; in May 1923 the anthracite output was 9,573,000 tons . For bituminous mines alone , the fatality rate in May 1923 was 2.67 per million tons as compared with 4.17 in May a year ago . During the first five months of the present year , the fatality rate for bituminous mines was 3.55 per million tons , based on 809 deaths , as against a rate of 3.70 for the corresponding months last year, based on 611 deaths . The rate for 1923 represents a reduction of 4 per cent . For anthracite mines alone the five-month fatality rate for 1923 was 5.36 per million tons , based on 228 fatalities , as against a rate of 6.72 for the first five months of 1922 based on 147 fatalities . The rate for 1923 represents a reduction of 20 per cent . The average fatality rate for May during the past ten years ( 1913-1922 ) is 3.37 per million tons for bituminous coal mines and 6.02 per million tons for anthracite mines . A gas explosion , due to open light , occurred on May 6 at Aguila , Colorado , and resulted in the death of ten men . This explosion brought the number of "major disasters " in 1923 to 4 , with a loss of 145 lives . During the first five months of last year, there were 7 similar disasters with a loss of 82 lives . The year's record to date for all fatalities from all causes shows a reduction in the fatality rates per million tons from haulage accidents and from falls of roof and coal , an increase in explosions of gas and dust and in accidents due to electricity , and no change in the fatality rate from explosives . The reductions in haulage accidents and in falls of roof and coal are particularly gratifying, because these two classes of accidents usually cause about 65 per cent of all fatalities in the coal-mining industry . Reports of Investigations , Department of the Interior , Bureau of Mines .

Jun 1, 1923

By Raymond W. Hiteshue, Henry H. Ginsberg, Paul S. Lewis

Coal was gasified in the presence of up to 3.57 million roentgens of gamma rays by the Bureau of Mines to determine whether the irradiation increased the gasification rate or yields of methane and hydrogen . High volatile A bituminous coal was gasified with steam at 500 and 1,500 psig and temperatures of 1,400 ° and 1,800 ° F ; five other coals ranging in rank from lignite to anthracite were gasified at 500 psig and 1,800 ° F. The average results of replicate experiments with and without radiation were compared for possible effects of radiation from 40,000 curies of radioactive cobalt . The irradiation had no gross effect on the gasification rate or on the yield and distribution of methane and hydrogen . It was concluded that gammaray irradiation produced no improvement in the technology or economics of coal gasification .

Jan 1, 1964

By Raymond B. Ladoo

The Bureau of Mines frequently receives requests for information on the mining , preparation and marketing of epsomite or Epsom salt , and in order to answer such inquiries the following information has been compiled . While it is probable that few people have considered epsonate as a mineral product , it will be noted that it should be so regarded and its production forms an important industry .

Mar 1, 1922

By Andrew Dobson

The assessment and control of environmental noise from mines has become increasingly important in recent years, due to urbanization and population growth, increased regulation of environmental factors, and overall awareness and sensitivities to noise exposure. Minimizing adverse effects on communities and achieving compliance with local ordinances is now commonplace, and consideration of noise during the design and/or operation of a mine cannot be ignored. Ventilation equipment can represent the loudest and most bothersome equpiment at mines, however there are complexities when attempting to control the assocaited noise, due to the acoustical nature of mine vent fans. In fact, the utilization of traditional and/or industry standard methods can intensify the noise impact, or simply not work as intended. This paper provides recommendations on specific noise control methods that are suitable for mine ventilation equipment, based on recent assessment work and field experience.

Oct 1, 2024

By Karl Dufresne

Blasting in geothermally high temperature ground and/or extremely reactive ground is an increasing common challenge for surface and underground mines. Many current PETN based non-electric and electronic detonators have manufacturer published in-hole temperature limits ranging from 55°C to 65°C (131°F to 150°F). When confronting blasthole temperatures above the manufacturer published limits, operations may request site-specific guidance and qualification for use. The advised safe loading window for in-hole PETN based detonators is often too short to be practicable for production blasting. To overcome limitations of PETN based initiation systems, surface mines with high temperature ground and/or reactive ground are known to load blastholes with a qualified high temperature bulk emulsion that are top primed with a cartridge of temperature qualified detonator sensitive emulsion plus an RDX detonating cord downline. As there is no in-hole delay detonator in this system, blasthole timing is accomplished with surface delays. Although this system is safe, top priming and surface delaying does influence floor quality and top size fragmentation, and safe loading windows times reduce blast block size and increase blasting frequency. A mining company with a site characterized by geothermally high temperature ground plus highly reactive ground employed a blasting system like the one described above. The site desires to improve blasting performance by moving to an in-hole delay initiation system that can withstand the site ground conditions. At the request of the mining house, DynaEnergetics developed an electronic initiation system for application in geothermally high temperature ground and/or extremely reactive ground conditions. The DynaEnergetics IGNEO high temperature electronic initiation system is rated for in-hole use in ground up to 150C (302°F) for 48 hours. The detonator consists of a high strength detonator with an HMX base charge and thermally resistant downline. To make up a primer, the detonator is inserted into a booster charge assembly that is fitted with a small HMX shape charge. This high energy primer is designed to be compatible and reliable for firing bulk emulsions, including those with high percentages of urea inhibition to combat reactive ground. Up to 1000 detonators may be programmed in 1ms increments up to 1500ms. The system is controlled by a digital firing panel that can be used with either a wired or wireless trigger.  The system enables high temperature and/or reactive ground sites to utilize in-hole delay initiation and realize the associated performance benefits. Conclusions and Future Work 1] The HMX based electronic initiation system permits bottom in-hole delaying in ground temperatures above 80°C (175°F). As compared to top priming and surface delaying, in-hole bottom delaying is known to improve floor quality, muckpile fragmentation uniformity and reduce oversize. 2] Field evaluation of the HMX initiation system at the Lihir Mine is continuing. 3] Work on the next generation of the HMX initiation system is underway and will bring with it expanded application range and flexibility. 

Oct 1, 2024

By Jeanie Wills, Theresa Nyabeze, Samantha Espley, Donna Beneteau

This presentation reports survey findings that aim to modernize the definition and understanding of the term 'mining.' The survey, conducted via LinkedIn in Winter 2024, garnered responses from a diverse group of individuals, including current or former employees of mining or exploration companies, mining consulting firms, service providers, supplier firms, as well as students and retirees with industry experience. The data, ethically approved by the University of Saskatchewan, offers valuable insights into satisfaction levels within the mining sector and suggests an expansion of the identifying characteristics of definitions of mining. This marks the third CIM gaining insights paper by Beneteau, Espley, and Nyabeze, following previous works on 'Career Satisfaction for Women in Mining' (2010) and 'Mentorship Initiatives in the Canadian Mining Industry' (2018*)."

Oct 1, 2024

By Muhammad Usman Siddiqui

Managing and analysing the vast amounts of data collected in a mining project effectively is crucial for enhancing the project's economic feasibility. The efficient utilization of this data is critical to minimising the time spent on projects and increasing project value. Process engineers can effectively integrate geometallurgical data into plant operations by employing analytical tools like Python, significantly optimizing the mine-to-mill process. This practical approach is a game-changer in the mining industry. Classifying a geomet dataset into units of similar characteristics (properties of the ore) is an important outcome of a geomet study. This approach simplifies data classification, allowing for class-by-class process modelling, which improves the decision-making process in mine planning and development. Classifying a geomet dataset involves using grade, lithology, and test work data (if available) to create blocks of similar characteristics, known as ‘geomet units.’ Compared to conventional methodologies, these units provide context and empirical evidence that can be more accurately mapped onto block-by-block process flowsheet development and net present value (NPV) estimation. This robust classification method reduces a project's technical risks and influences the initial mine planning sequence to maximise profitability. Defining robust geomet units with data sets with similar material is challenging due to the vast amounts of data available and the database's high heterogeneity. The methodology's purpose is to minimise time-consuming low-value-adding aspects of geometallurgy. The approach is different for a greenfield and a brownfield study, as all the valuable data in a brownfield process can be utilised to define the geomet units. Python has various libraries providing multiple machine-learning algorithms to assist in classification. The k-means algorithm is used for clustering, and the SHapley Additive exPlanations (SHAP) method is used to quantify the effect of each feature on the clustering results. However, even with automation, the methodology still requires a keen eye to account for the nuances that appear from project to project.

Oct 1, 2024

By Amir Karami, Derek Kinakin, Catherine Schmid

The Mathews Stability Graph Method (Mathews et al., 1981) has been used by geotechnical engineers and mining engineers for over 40 years to estimate the performance of longhole open stopes in underground mines. The method is widely used and accepted by practitioners because it is relatively simple to use and can be modified to account for observed performance at a given mining operation. While the simplicity of the method increases its accessibility and utilization, it does not intrinsically account for variability in the various inputs, including rockmass quality, structure, stress, or stope orientation. This paper presents a modified approach for the Stability Graph Method, whereby Python scripts are used to process available geotechnical datasets and combine them with actual or potential distributions of Q parameters, induced stress, structure, or stope orientation. The resulting Stability Numbers are then plotted as a contoured distribution on the Stability Graph.  This allows the practitioner to quickly incorporate large datasets into the analyses, while also developing an understanding of how variability in rockmass quality, induced stress, structure, or stope orientation could affect stope stability.  This paper presents the fundamental principles of the Stability Graph method, the Python script and workflow, and two case studies to demonstrate the utility of the tool.

Oct 1, 2024

By Cesar Carrasco

Mine reconciliation is the art and science of comparing predictions and real-world outcomes with the intent of revealing the true quality of performance of models, planning, mining, and mineral processing. When mine reconciliation is conducted in a systematic, transparent and sustainable way it can play a central role in the governance of Mineral Resource and Mineral Reserve (MRMR) estimation and reporting. The core processes of modelling, planning, mining, and processing need to be transparent to be able to demonstrate that MRMR are reliable predictors of mine performance and value. Transparency is also necessary for mine technical staff to generate meaningful analyses, conclusions, and business improvement actions that demonstrably maximise value for all stakeholders. Most mines have some form of mine reconciliation practice, however because there is no agreed industry standard, and because mine reconciliation is difficult for a variety of reasons, it is often unsustained and/or ineffective at delivering the required transparency of performance. To deliver true governance of MRMR and business value, mine reconciliation must be sustainable. There are two categories of issues that combine to make mine reconciliation extremely difficult to sustain, these are technical, and people related. Technical issues include defining standard terms, accurately tracking material flows, data availability/adequacy/quality, calculation of key performance indicators and tolerance limits, analysis, and interpretation of results, understanding limitations of modelling techniques, and defining appropriate actions that can deliver value. These technical challenges are non-trivial, however compounding these are a range of people issues that include personal agendas, scepticism, lack of knowledge and experience, poor teamwork, absent leadership, toxic workplace culture, staff turnover, ineffective communication, siloed organisational structure, and lack of deliberate change management. All these problems can be solved with clarity of purpose, definition of the process of mine reconciliation, discipline in following the process, appropriate resourcing, and commitment to success across the entire organisation. Outlined in this paper is a management system that delivers sustainable mine reconciliation by addressing both the technical and people issues described above. This approach can deliver significant value for a mine and adds a robust, defensible governance over MRMR estimation and reporting.

Oct 1, 2024

By Gurupraveen Ramanathan

Slot raises are relief holes within a stope in longhole stoping methods, designed to provide a free face that facilitates the expansion of the blasted rock during blasting, ultimately achieving the desired fragmentation. Various methods are employed to produce these slot raises, like conventional drop raise drilling, raisebore & V30 drilling. However, slot drilling is generally characterized by high costs and limitations in precision, resulting in unplanned ore losses and dilution. This paper introduces a novel alternative to slot drilling referred to as the "paste slot", designed specifically for paste backfill operations in underground mining. This new method emphasizes considerations in cured paste strength, paste wall removal, and stope dimensions and employs modified drop raises or dumped rings to optimize blast gas effectiveness and material flow. The paste slot method eliminates the need for reamers and reduces the total slot drill meters an average from 650m to only 300m for narrow stopes (3-4m wide). This significantly reduces the stope cycle time, leading to substantial cost savings and increased productivity. This new method was successfully implemented at the underground mines in Canada and Australia, resulting in a 20% reduction in stope cycle time and cost savings of 53,000 USD per slot compared to the conventional slot. This paper discusses the design and execution strategy of the paste slot method in underground paste backfill operations. It highlights the advantages of the method, shares operational insights gained during implementation, and showcases its potential applicability to other mines across Canada and globally.

Oct 1, 2024

By G R Ryan

Recent events have raised the issue of whether, and if so when and how, an explorer may gather data from a mining tenement or permit which is held under the relevant mining Act by another party. Two situations arise: that of the small operator who wishes to prospect, and if successful mark off, ground held by others by virtue of the local form of exploration permit; and that of a regional explorer who may wish to enter on to some one else's existing mining tenement within the region of interest. The legal situation varies from state to state. At present the broad consensus seems to be that, provided consent is given, small-scale prospecting on another's exploration permit is at least tolerated if not actually provided for by the relevant Act. Entry onto a granted tenement to carry out any form of exploration is, however, prohibited in all jurisdictions unless consent is given. Furthermore it would appear that the proposal and conclusion of a joint venture agreement places certain obligations upon the party proposing to carry out exploration. These conclusions apply where ground surveys are proposed. Where data acquisition is by aerial survey the situation is much less clear, principally it would appear, because up to now little thought has been given to it. If trespass applies at ground level, at what height does it cease to apply? Can aerial magnetometry or photography be classified as prospecting? Is there an obligation upon public authorities who carry out remote sensing to make data available to the holders of mining tenements within the surveyed areas? Moves are now afoot to address these and other considerations, and it would be in the interests of everyone if a national approach to the problem could be adopted from the beginning. Certain suggestions in this respect are put forward.

Jan 1, 1994

By JOHN G. RAYNER

An examination was made of the filtration characteristics of a haematite slurry using a range of polyacrylamide based flocculants in solutions containing up to 3 per cent sodium chloride. The polymers used were "high" and "Iow" molecular weight and had from 0 to 40 per cent charged groups.Increasing charge density tends to reduce the dose required to achieve optimum performance measured by filtration rate and by cake moisture. In general increased salt addition tends to increase the dosage required to achieve these optima. Both these observations result from the change in polymer extension and accord well with the bridging theory of flocculation.The dose required for optimal cake moisture is up to three times greater than that required for optimal filtration rate. This effect is reasonably consistent for all polymers studied and appears to be non-linearly dependent on salt concentration, with the difference being small at 0 and 3 per cent but quite significant at 1 per cent.

Jan 1, 1987