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By Carlos Alberto Perim

Devido à obstrução no distribuidor, os aços ultra baixo carbono estabilizados ao titânio apresentavam baixo sequencial de lingotamento na ArcelorMittal Tubarão (AMT). Foram identificadas práticas utilizadas na redução de obstrução nestes aços, que foram adotadas para a produção na AMT. Uma das práticas foi estabelecer uma relação entre alumínio e titânio com menor propensão à formação de compostos de alumina e óxido de titânio que se aglomeram na região da válvula superior do distribuidor. Também foram introduzidas melhorias no processo visando a melhorar a condição de fluxo na região próxima da saída do aço no distribuidor. Neste projeto, um aço UBC de maior volume de produção foi escolhido e novas práticas foram adotadas para sua produção. Amostras de aço foram retiradas de corridas produzidas nesta condição e foram enviadas para análise na ArcelorMittal Research USA. Os resultados mostraram melhorias nos índices de qualidade tanto em laminados a quente como em laminados a frio. Neste trabalho será apresentado um resumo das ações adotadas na AMT, que resultaram em um aumento do sequencial médio de distribuidor, permitindo atingir um máximo de 18 corridas. Os níveis de esfoliação com esta nova prática atingiram também nível mínimo histórico.

Aug 16, 2017

By Nicolás Lugo

The electric steel industry has reached a level of maturity in its relative participation in the world’s steel production. As the industry has grown and matured, EAF steel producers have participated in an ever more competitive market. This competition has led to a continuous search for lower cost alternatives for energy and input materials. Over the years, the Electric Steel Furnace community of operators has developed a variety of technological improvements geared to increasing EAF productivity. Operators have emphasized lowering operating costs and improving the quality of steels produced. Depending on market conditions, the EAF operators may run with different goals and priorities. In times of low demand, the goal may be to operate with an emphasis on cost and the goal of maximizing cost effective use of resources. When the market demand is high the goal may be to maximize EAF throughput. The objective of this work is to list some of the EAF operating best practices observed by our team in the electric arc furnace operations around the world. EAF operators can consider and possibly implement these practices depending on the specifics of each EAF operating reality.

Jul 29, 2018

By Antonio Adel dos Santos

Visando elucidar o comportamento da carepa terciária durante a laminação de tiras a quente, em um aço produzido como laminado a quente e com rigorosa exigência de qualidade superficial, foi realizada uma parada forçada do laminador, impondo-se, imediatamente, um resfriamento rápido da superfície da tira. Amostras coletadas na região do arco de contato mostraram que a carepa possui espessura na faixa de 10 ?m a 14 ?m na entrada das cadeiras, sendo reduzida para 7 ?m com a deformação, sem ocorrência de ruptura. Tais características indicam que, do ponto de vista do comportamento no trem acabador, a carepa apresenta espessura e plasticidade adequadas para evitar defeitos nos produtos laminados. A carepa foi constituída predominantemente por Fe3O4, óxido plástico na temperatura de laminação. Foi desenvolvido e aplicado um modelo de crescimento da carepa, que forneceu valores de espessura muito próximos dos medidos, se tornando uma ferramenta útil para análise da influência de condições de processo na carepa.

Oct 30, 2017

By Ricardo Thomé da Cruz

O conhecimento sobre o comportamento do revestimento refratário dolomítico durante a etapa do refino de aço é fundamental para se atender às exigências técnicas de qualidade e o aumento da produção de aço. É particularmente importante que os mecanismos de corrosão dos refratários dolomíticos sejam bem compreendidos, principalmente, em operações de exceção, nas quais as exigências metalúrgicas causem forte dano ao revestimento, prejudicando não somente o desempenho do mesmo, mas também gerando um risco à segurança operacional. Este trabalho visa à caracterização técnica da camada protetora (coating) de silicato dicálcico (C2S), a qual se origina da reação entre as escórias silicosas e os refratários dolomíticos. As amostras de coating foram caracterizadas quanto à composição química, fases formadas e microestrutura. Estudou-se uma panela retirada de operação, por dano aos refratários, retirando-se amostras de diferentes regiões. Em duas amostras, juntamente com o C2S e o periclásio, foi observado à presença de fases à base de silicato de baixa fusibilidade como a cuspidina, indicando que o coating foi atacado por uma escória com elevado teor de fluorita.

Jul 30, 2018

By Elaine Carballo Siqueira Corrêa

Os aços rápidos são aços ferramentas de alta liga capazes de usinar metais a altas velocidades. Dentre estes, o aço rápido AISI M2 é um dos mais empregados, em função das boas propriedades alcançadas mediante a combinação de composição química e parâmetros de tratamentos térmicos. Neste contexto, o objetivo deste trabalho foi avaliar os efeitos da temperatura de aquecimento na têmpera sobre a microestrutura e dureza do aço AISI M2 após revenimento em diversas temperaturas. Para tal, duas temperaturas de têmpera e cinco temperaturas de revenimento foram definidas. As transformações microestruturais foram analisadas por meio de microscopia eletrônica de varredura e difratometria de raios-X. A dureza foi obtida por ensaios Rockwell C. Foi observado que, de modo geral, o aumento da temperatura de aquecimento promoveu elevação nos valores de dureza do aço, sendo que, para a maior temperatura utilizada, notou-se a ocorrência do fenômeno de endurecimento secundário. As análises microestruturais revelaram a presença de maior quantidade de carbonetos nas amostras temperadas à menor temperatura.

Oct 30, 2017

By Alberto Tremea

The eddy current system is universally recognized as a most suitable method to point out discontinuities or modifications on the roll surface. The automation of the controls through the implementation of sophisticated equipments on the grinding machine has favoured its employment in the roll shop. A big effort is still going on to clarify the best way to promptly identify situations that could be really unsafe for the roll life. The results presented in this paper have been obtained through an intensive activity conducted in field by Innse Cilindri on work rolls of finishing stands of hot strip mills. The correct interpretation of the eddy current signals and a good calibration of the automatic system have allowed, in many cases, a substantial optimisation of regrinding practices.

Aug 16, 2017

By Evandro Tolentino

As fibras vêm sendo empregadas nos materiais de construção civil desde o início da humanidade. No começo da década de 50 houve o início da utilização de fibras de aço no reforço de matrizes de cimento. Com isso foram notadas alterações no comportamento do material, sendo detectado o aumento da tenacidade pós-fissuração. Esta é uma pesquisa experimental que teve como objetivo a definição de parâmetros de ensaios para a produção de argamassas de cimento Portland, que utilizem fibras de sisal nas suas composições, tratadas quimicamente por acetilização com intuito de reduzir a absorção de água. O sisal (Agave Sisalana) apresenta boas propriedades físicas e mecânicas. As fibras foram cortadas manualmente nos comprimentos de 20 mm. As diferentes composições de argamassas foram produzidas com 0,2% e 0,4% de fibra de sisal, em relação ao volume total da argamassa. Estudou-se o comportamento mecânico dos compósitos com ensaios de resistência à tração na flexão. Os resultados mostraram uma melhoria na resistência à tração na flexão para argamassas com fibras tratadas quimicamente por acetilização.

Oct 30, 2017

By David A. Collins

Red Dome Gold Mine classifies ore types within the pit by gold and copper grades. Copper grades are further distinguished by total copper and cyanide soluble copper levels. At present, Cyanide Soluble Copper samples take six hours of agitating before they can be assayed. This agitation time produces results which are a proportion of the total cyanide amenable copper. This relates to our plant's performance. Frequently the total copper result is needed before we can begin the cyanide soluble copper analysis. This caused a protracted tum around time. Mennetech Pty. Ltd has produced a catalyst proven by David Martin Menne to accelerate the cyanidation of gold. David said that the information at hand indicated that Leach WELL TM also accelerates the leaching of cyanidable copper substantially. Test work was undertaken on-site at Red Dome Gold Mine to investigate the potential of Leach WELL TM to reduce the leaching period and therefore, the overall tum around time required for cyanide soluble copper determinations.

Jan 1, 1995

By Darryl J. Butcher

The Akjoujt Project is operated by MORAK SA, a company incorporated in the Islamic Republic of Mauritania. MORAK is jointly owned by General Gold International SA (A wholly owned subsidiary of General Gold Resources NL.), SAMIN, and the International Finance Corporation. The project was devel­oped to treat approximately 2.1 million tonnes of TORCO (Treatment of Refractory Copper Ores) tailings containing an average 3.2gAu/t, and 0.75%Cu/t. The process involves the use of ammoniacal cyanidation for gold extraction, and conventional carbon adsorption, and eventual desorption, of gold values. This is believed to be only the second commercial application of this leach chemistry in the world. The other being a small vat leach operation on the Paris Mine Dumps. (This operation was described by Mr M Ruane in a paper to a previous Randol Forum.) Initial work on the process, and the Akjoujt process design assumed that the reaction involved was anaerobic. This paper describes the operating experience, plant trial, and eventual installation which has lead MORAK to the conclusion that the process is not anaerobic, but requires oxygen, or an oxidant to proceed.

Jan 1, 1995

By Marc E. Orman, Todd V. Ramey, Mark E. Smith

Heap leaching in certain parts of the world, such as Chile's Atacama Desert, brings unique design problems in the form of possible large differential settlements of the foundation soils due to the dissolution of salts. In northern Chile the soils often c?ntain very high concentrations of soluble salts (nitrates, potas­smm, magnesium, and common sodium). When a leak in the liner occurs, the escaping solution dissolves these salts and trig­gers differential settlement. If the settlement is great enough, the geomembrane tears, the leakage increases, triggering more dif­ferential settlement. The nitrate plants have experienced many occurrences of this phenomenon where a brine pond will under­go a sudden and complete loss of the impounded liquors. The authors present a simplified technique to quantify the differential settlement resulting from dissolution and provide a method which can be used to select a geomembrane with suit­able flexibility under axi-symmetric (multi-axial) load condi­tions to tolerate the predicted settlement.

Jan 1, 1996

By M. T. Errington, P. C. Miller, W. E. Hardwick

Paper discusses in general terms the techno economic merits of various types of aerated biological reaction systems. The current status of the technology leaves many questions unanswered and hence the choice of the best system to employ is open to discussion. Reasons are given for the choice of the reactor system to be built and operated by Davy McKee. The pilot plant has been designed to provide answers to a number of the questions posed by this technology.

Jan 1, 1998

By Robert S. MacPhail, Bret G. Cousins

Many copper-bearing ores with associated gold use Sodium Isopropyl Xanthate (SIPX) as a flotation agent. In general, SIPX will float to some extent other minerals that may not be desirable, such as pyrite. FLEX 31 is a chemically enhanced SIPX product with many of the same properties as SIPX. But FLEX 31 has the ability to reject more pyrite from concentrates and improves copper recovery when using up to 50% less FLEX 31 than is required if using SIPX. Copper activated minerals such as sphalerite and arsenopyrite show increased recoveries as well using FLEX 31. Tests have been performed on copper/zinc ores and an arsenopyrite/pyrite ore.

Jan 1, 1995

By Gary Jobson

The Mt Todd Gold Mine is owned and operated by Zapopan NL, and is located 300km south of Darwin near the town of Katherine. The crushing plant and heap leach facility, which has operated since November 1993, has recently been expanded to treat 6 Mtpa with 1995 budget gold production reaching 120,000 oz from a head grade of 1.12 git. The process flowsheet and equipment are described, with innovative key features including:

Jan 1, 1995

By J G. Dunn, S M. Thurgate, A C. Chamberlain, P Franzmann, M Jeffrey, L J. Warren, G E. Poinen, T Williams

Gold has always fascinated mankind. From Tutankhamen's mask to the huge nuggets that have been found in the Australian outback, gold has quickened the pulse and fevered the eye. But in recent years, governments around the western world have shown a singular lack of interest in research into gold processing, with many programs being cut. There are some notable exceptions, fortunately, and this paper summarizes a large research effort that is well supported by the Australian government and the Australian gold industry. The AJ Parker Cooperative Research Centre for Hydrometallurgy is an unincorporated joint venture between the CSIRO Division of Minerals, Murdoch University, Curtin University of Technology and the Western Australian Department of Minerals and Energy. The Australian Mineral Industry Research Association (AMIRA) is the Parker Centre's broker for generic R&D contracts with industry. Each of the partners makes available staff, students and equipment to further the work of the Parker Centre, and the Australian Government provides additional funding. The Parker Centre is nearly five years old and has grown spectacularly in that time. There are now about 30 full-time-equivalents of effort from 50 scientists and engineers, as well as about 40 postgraduate and honours students. The fundamentals of the key operations in hydrometallurgy are studied in three programs: leaching (which includes pretreatment by roasting etc), precipitation (or crystallisation), and surface processes (which includes solid/liquid separation, adsorption, solvent extraction, etc). A large part of the Parker Centre's R&D is directed towards gold processing technology. In Australia, a dramatic increase in gold production, from about 30 to nearly 300 tonnes per year (1977-1997), has been made possible largely as a result of a brilliant metallurgical innovation, the carbon-in-pulp process. However, falling head grades eg 2.56 to 1.84 g(Au)/t over the last 10 years, and environmental concerns, are squeezing profit margins. There is increasing pressure to reduce costs, and the Parker Centre program is focussed on providing the scientific understanding required to do this. A selection of research highlights will be given, to indicate the depth and breadth of the R&D at the Parker Centre.

Jan 1, 1997

By James L. Whitlock, Amy E. James

During the past twenty years, numerous advances have been made in the technologies used to pretreat sulfidic refractory gold ores. These advances have included improved equipment design, increased gold recoveries, and reduced operating and capital costs. More recently, treatment of refractory gold ores has primarily been accomplished by pressure oxidation (POX), roasting, chlorine oxidation, or biooxidation. In addition to improving the time-proven processes of pressure oxidation and roasting, new and innovative approaches to biooxidation pretreatment of both concentrates and whole ores have been developed. Selecting the appropriate biooxidation technology depends on the nature of the refractoriness in the ore, economic gold recovery, plant design operating parameters (such as desired tonnage), site climatic conditions, and operating and capital costs, as well as several other deciding factors. The objective of this paper is to outline the biooxidation processes and technologies currently available for the recovery of gold from refractory sulfidic ores, to discuss the critical factors that affect plant design and operation, and to provide the metallurgist with a practical guide to choosing the appropriate biooxidation technology for a particular ore or concentrate.

Jan 1, 1999

By G. Deschenes, M. Fulton

The New Britannia Mine processes a qumtz-carbonate gold ore containing 4.63 git Au at a rate of 2,200 tpd. The ore contains approximately 3 .0% arsenopyrite, 2. 7% pyrite and the rest is gangue minerals. Eight to ten percent of the gold is refractory to leaching. Two years ago, New Britannia Mine experienced cyanidation problems. Gold extraction was not stable and occasionally decreased significantly. Preliminary test work, at laboratory scale and in the plant, indicated that lead nitrate addition was beneficial. A laboratory study was initiated to evaluate the level of control of the parmneters (grinding size, dissolved oxygen, pH, free cyanide and lead nitrate) to optimize the efficiency of the process. It was found that lead nitrate addition is required to alleviate the effect of metallic sulphides. This addition causes a significant increase in the gold leaching kinetics and a reduction in the cyanide consumption. The optimum system appeared to be: leaching for 24-30 hours at pH 11.8, 50 git lead nitrate, 250 ppm NaCN and 8 ppm 02. The gold extraction was 89.8% with grinding at 89%-74Fm (leached tail at 0.48 git). Cyanide and lime consumption are 0.40 kglt NaCN and 1.9 kglt respectively. Following the incorporation of lead nitrate, overall gold extraction was increased from 89.2% to 91.1 % but no change was noticed in cyanide consumption. The gross profit is $CDN 988,000 per year.

Jan 1, 1999

By Denis McDermott

This paper describes the process used at three mines to devel­op safety and training programs. The mines are located in Australia, New Zealand and the United States of America. The aims of the programs were to promote and reinforce safe and healthy behaviour, increase productivity and efficiency and to provide a fair and objective basis for the payment of wages. There were common aspects to each of the projects: • mandatory legislation required employers to provide employ­ee training in work performance • employees had little previous involvement in the design and development of the training provided • training had been unstructured with employees relying on the "buddy system" to acquire new skills; the degree of skill acquired by an employee depended on the knowledge and teach­ing capacity of the worker to whom the novice was assigned • appointments and promotions had been based on judgements by supervisors and these were not generally understood by employees • employment conditions for employees were covered by an industrial agreement between management, unions and employ­ees. The degree of sophistication of the industrial agreements varied however none provided a description of work performed in each classification, nor the career or promotional path for an individual • supervisors with the responsibility to train, develop, motivate and reward employees expressed concern that there were no structured processes ( eg work standards or wage progression cri­teria) to support their role.

Jan 1, 1998

By D. L. Slyter

Coeur d'Alene Mines Corporation's Thunder Mountain project in Valley County, Idaho, is one of the most remote active mining operations in the US. High altitude, heavy snows, and proximity to wilderness complicate operations in this environmentally sensitive area. Mining is conducted by conventional open pit techniques while processing utilizes on-off heap leaching and Merrill-Crowe zinc precipitation. The project is one of a few similar operations which detoxify the leached ore prior to its removal from the leach pads. Both leaching and neutralizing ( detoxifying) circuits are closed and independent loops. After leaching, alkaline chlorine solutions destroy residual cyanide in the heaps. Calcium hypochlorite solution for the cyanide destruction is prepared by injecting chlorine gas into milk of lime solution.

Jan 1, 1998

By Norbert Patzelt, Johann Knecht, Wolfgang Baum

The principle of high-pressure interparticulate comminution has been used very successfully since the mid 1980's for grinding a wide range of different materials. A number of reports about operating experience have already been published. High-pressure grinding rolls (HPGRs) are currently making their debut in the mining industry. Experience is being gained with test machines, particularly for the comminution of hard rock. In the grinding of diamond-bearing ore, (Fig 1) interparticulate comminution has already become the standard for liberating the diamonds from the matrix. The advantages of interparticulate comminution are also recognized for the grinding of concentrates (chrome ore, iron ore). Numerous HPGRs are being used very successfully in this field. A testing plant for first-time industrial grinding of coarse, very hard and highly abrasive copper ore was built at Cyprus Amax's plant in Sieretta, Arizona (Fig. 2). The operating experience gained here showed that the grinding of very hard ores places particularly high mechanical demands on the mill. While the machine itself meets the high availability requirements, the wear-protection system proves to be the most sensitive point. Naturally, the properties of the ore to be ground exert a considerable influence on the lifetime of the grinding rolls. This paper describes the wear mechanisms and the wear­protection systems designed to combat these.

Jan 1, 1997

By Mike D. Adams

Testwork was conducted on loaded carbon samples from a small gold mine in South Africa. It was shown that a 75% saving in reagent consumption in the Zadra elution circuit could be achieved by adopting a cyanide-free elution approach, i.e. by cutting back the NaCN level from 1 % to nil, and the NaOH level from 3% to 1 %. This process change was also shown to result in a 20% improvement in the elution kinetics. Furthermore, it was also shown that a 50% enhancement in elution rate over the current situation could be achieved by use of an eluant containing 0.5% NaOH and 0.15% NaCN, corresponding to an 84% saving in reagent consumption. A further improvement in elution kinetics was found to occur by increasing the NaCN level to 3%, but this would lead to a concomitant increase in reagent consumption, due to the decomposition of cyanide at high temperatures. The presence of base metals loaded onto the carbon was also found to have a significant effect on the elution. Copper tends to adsorb as Cu(CN)2- during the adsorption stage, and acid washing converts this species to CuCN. Copper in this form is not eluted during cyanide-free elution, whereas it is eluted during a conventional cyanide elution, consuming the initial cyanide in the process. The elution data was analysed and the fit to a simple model was verified.

Jan 1, 1995