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By John C. Calhoun, Frank T. Bethel

Glass beads have been surface treated with Dri-film to render them oil wet by n-octane to varying degrees, and capillary desaturation curves have been determined by the restored state method. The desaturation curves show a regularity of increasing displacement pressures as the oil wetness increases. This has been used to compute apparent contact angles between n-octane and water on glass. The family of desaturation curves also shows a regular crossover, such that the residual wetting liquid saturation values are in reverse order to the displacement pressures. A semi-logarithmic variation is shown between the apparent contact angle and the residual saturation. The desaturation data are interpreted to mean that the wetting liquid ceases to be a continuous phase within individual pores before the capillary pressure can be raised sufficiently to force out the wetting phase completely. The saturation of wetting liquid at which this break in liquid continuity occurs is higher as the oil wetness decreases. INTRODUCTION The petroleum industry has for some time been using measurements of capillary pressures on porous media for research correlations and engineering calculations. It has been generally recognized that the capillary desaturation curve reflects the character and arrangement of the pores within the media and the distribution of fluids within the pores. Methods have been proposed for computing pore size distributions, tortuosity factors. and relative permeabilities from capillary desaturation data.' There is little doubt that the interactions between porous rocks and their contained fluids resulting from surface forces play a dominant role in determining the magnitude and direction of capillary pressure measurements. There have been attempts to introduce as variables two quantities — inter-facial tension and contact angle — generally used to char- acterize surface forces, but in spile of the wide interest in these quantities as important variables, few definite conclusions have been drawn concerning their qualitative or quantitative significance. INTERFACIAL TENSION The interfacial tension appears in a capillary pressure function given by Leverett for correlating capillary desaturation type curves. Use of the interfacial tension in this function seems to be justified by other experiments reported. Apparently, interfacial tensions have little bearing on wetting phase residual by desaturation. CONTACT ANGLE The contact angle was utilized as a variable by Bartell and co-workers"." in tests on displacement pressures, later recognized as the initial point of capillary desaturation. Although Leverett did not include contact angle in his original formulation of the capillary pressure function, later workers suggested its addition. Few reports are available to show variation of residual liquid with contact angle as a result of capillary desaturation.' The problems attendant to measuring contact angle within a porous medium are great. As a consequence of the lack of a concrete approach to a measurement. the workers in this area of research have adopted the general expression of "wettability" to indicate the relative position of two liquids saturating a porous body. It has been shown that gross measurements on porous systems, including capillary desatura-tions, are sensitive to wettability. Attempts at giving a scale to wettability in terms of contact angle through capillary desaturation curves have been made and these apparently are steps in the right direction. In these attempts presence of many other variables precludes attainment of exactness. Also, as a result of other variables, it has been impossible to correlate changes in apparent contact angle with changes in other physical measurements of the systems in question. The present work is an attempt to eliminate as many variables as possible in measuring capillary desaturations resulting from changes in contact angle within a porous medium.

Jan 1, 1953

By W. J. D. Stone

Many of the common valuable minerals have a magnetic susceptibility which is sufficiently high to render them amenable to magnetic separation. In addition,, many minerals which form the unwanted constituents of an ore can be removed by magnetic means. Magnetic separation in general has suffered seriously from, the lack of a high intensity wet separator. It is only recently that such a separator has become available to the industry. Prior to this, high intensity magnetic separation has been limited to the use of the dry techniques. Since the introduction of the Jones Wet High Intensity Magnetic Separator, extensive test work has been conducted to investigate possible applications. From the investigations conducted and the discussions that have taken place in the industry, it is apparent that the important mineral characteristic of magnetic susceptibility is not receiving the attention that it deserves. Applications for high intensity wet separation are being found in areas hitherto not considered.

Jan 1, 1963

By E. J. Duggan

THE mine and mill of the Climax Molybdenum Co. are at Climax, Colorado. Climax is on Fremont pass directly on the Continental Divide, at an elevation of 11,400 feet. DESCRIPTION OF ORE The Climax ore-bearing rock is essentially an altered and highly silicified granite, fully half of the gangue being quartz. Molybdenite is the only mineral of economic consequence and most of it is intimately associated with quartz in the form of fine veinlets and stringers. Other minerals are molybdite, pyrite, and chalcopyrite. While the molybdite may be readily extracted by hydrometallurgical methods, its content is too low to make such operations profitable. The pyrite content ranges from 2 to 5 per cent and that of the chalcopyrite from 0.03 to 0.05 per cent. There is not enough copper to make its recovery attractive and one of the metallurgical problems is the elimination of it and the pyrite from the product. On account of the close association of the molybdenite with the quartz and the necessity of eliminating the pyrite and chalcopyrite from the final product, fine grinding followed by flotation is the only feasible method of concentration. HISTORY Construction of the first milling unit was started in 1017 and it was operated during parts of 1918 and 1910. In the postwar years, there was almost no demand for the product and production was at a standstill until 1024. The Company's research campaign to develop the use of the metal began to show results in that year. From 1926 to 1932 production ranged from 500 to 1200 tons per day. In 1931 an additional mill section was built and production was gradually increased until in 1934 and 1935 about 3000 to 4000 tons was milled per day. This tonnage overtaxed the milling facilities, and as the demand for molybdenum was growing constantly, additional milling equipment was needed. In 1936 and 1937 another crushing plant, six additional mill sections and the necessary auxiliary plants were constructed and brought into operation. This plant was designed to mill I0,000 tons per day, but it was not long before 12,500 tons was being treated during periods of peak demands. During the summer of 1941, to meet defense needs, the mill has been required to treat 15,500 tons per day. This has been accomplished with little plant expansion and at no loss in recovery, as will be described later. To increase capacity still further, one more primary section is now being built. This will bring capacity to 18,000 tons per day, which can be stretched to 20,000 tons at a small sacrifice in recovery. CRUSHING There are two crushing plants: No. I, of 5000 tons capacity (flowsheet in Fig. I) and No. 2, of 15,000 tons capacity (Fig. 2).

Jan 1, 1942

Jan 1, 1883

Jan 1, 1951

By Frank R. (Original by) Barnako

Coal mining historically has been a hazardous occupation but, in recent years, tremendous progress has been made in reducing accidental coal mine deaths and injuries. The purpose of this chapter is to discuss the basic principles of accident prevention as they are related to coal mining. Accident prevention fundamentals are no different for coal mining than for any other type of work. The fundamentals apply to all industries. Construction workers may be struck by falling tools and materials, and miners may be struck by falling slate and coal. Sailors may be trapped by shipboard fires, and miners may be trapped by mine fires. Railroad brakemen may lose hands and fingers positioning couplers, and miners may lose hands and fingers positioning couplers. Many other examples could be cited, but the point is that accidents that happen in coal mines are basically similar to accidents that happen in other industries. Thus, the basic principles for preventing accidents apply in coal mining as they do in any other type of work.

Jan 1, 1981

By James H. Taylor

"Titanium is a widely distributed, dark grey metal1ic element found in small quantities in many minerals. It has no important uses." Happily, this early quotation proved to be wrung; titanium has, on the contrary, found a large number of very important uses. The error in the 1926 quotation illustrates the problems associated with forecasting the future development of any metal. 'The paper will nevertheless attempt to estimate what will happen to the European titanium industry over the coming decade with slightly more accuracy. It was not until 1955 that anything other than pilot plant facilities were installed in Europe. In 1955 IMI's plant in England, two plants in Germany, one in France and one in Sweden came into operation. All the companies associated with titanium installed melting furnaces but only IMI Titanium has forging and rolling facilities devoted solely to the production of titanium. The other firms rely on the use of equipment of their parent steel companies for processing the me1 ted titanium ingots.

Jan 1, 1982

By F. B. Henderson III

Since the "end" of the Cold War, revolutionary new research and commercial remote sensing capabilities are being developed that will dramatically change the way we map the earth and address its environmental problems. The technology challenge is not the growth of new environmental remote sensing technologies themselves. It is, rather, how these new innovative observing systems can be accepted and used to the benefit of both the regulatory and the mining communities in the light of present concerns about unknown risks of discovery and liability. The basis for this paper is an unpublished technology primer prepared for the industry-government Workshop on Advanced Measurement and Site Characterization for Mining Impacts held at Colorado School of Mines, Golden, Colorado, July 14-17, 1997

Jan 1, 1999

Jan 1, 1946

By Kevin M. Connor, Malcolm J. McPhersqn

Examples are presented in which Time Domain Reflectometry (TDR) was employed to locate deformation of rock masses induced by mining. The first example involved motoring the propagation of overburden fractures above a longwall coal panel and the second example involved the we of a)R to monitor rock mass deformation in the vicinity of a strip mine highwall. Bock mass deformation, strata separation and large block movement generated strains and failure along coaxial cables which were installed in drill holes and the TDR reflections generated by these strains and failures were monitored. Analysis of field data and a preliminary laboratory test indicate that it may be possible not only to locate rock mass movements but also to quantify these movements with TDR data.

Jan 1, 1984

Discussion of the paper of HOWLAND BANCROFT, presented at the Salt Lake meeting, August, 1914, and printed in Bulletin No. 91, July, 1914, pp. 1767 to 1769. THEODORE SIMONS, Butte, Mont. (communication to the Secretary*). -While preparing maps and models for use in mining litigations the writer was frequently confronted with the problem referred to in Mr. Bancroft's paper. His chart gives the apparent angle of dip with which a vein should be plotted on a vertical section not at right angles to the strike of the vein. For a quick determination of this apparent angle the writer has used an exceedingly simple graphical method, which he believes may prove helpful to engineers engaged in practical work. It is submitted, not as a criticism of Mr. Bancroft's paper, but as a means of solving the same problem when no chart is available and when calculations would consume too much time. The writer's method requires merely a few lines marked off on a piece of tracing cloth, as shown in Fig. 1: Draw line be on any convenient scale. At b erect a perpendicular, ba. By means of a protractor cut off on ba a number of angles within the probable range of variation of dip, so that a line connecting a and c, for instance, forms an angle of 60° with be, etc. With b as a center and be as a radius, draw a circle through c. This completes the tool for solving the problem. Fig. 2 represents the line of strike of the vein and db the trace of the vertical plane on which the vein is to be plotted with the apparent angle of dip. A° is the angle which this plane makes with the strike. Fig. 3 shows the application of the method: Place line cb of tracing over line db of Fig. 2 and move fore and back until line of strike becomes tangent to the circle. Connect d with the point (a) that marks the true angle of dip as found by measurement in the mine (60° in the case illustrated). The angle adb is the apparent angle of dip (C°) to be used in the vertical section. Proof.-As stated in Mr. Bancroft's paper, the apparent angle of dip is: tan C° = sin A° tan B° (1)

Jan 12, 1914

Jan 1, 1879

By R Kerrich

Early-Archaean (3.26 Ga) volcanogenic massive sulphide (VMS) deposits located within the low strain and sub-prehnite-pumpellyite metamorphic-grade Strelley greenstone belt, East Pilbara, Western Australia, contain exceptionally well preserved sulphide textures which are directly analogous to those of sulphide chimneys formed by black smokers at present day submarine hydrothermal vents. The VMS deposits are associated with seafloor alteration zones in and below silica-carbonate laminites, at the top of tholeiitic to calc-alkaline intermediate and felsic rocks. VMS mineralisation comprises stratabound Zn-rich sulphide lenses with significant Cu and barite, and variable Pb and Ag, above Cu-rich stringer zones, all of which are similar to Phanerozoic polymetallic or Kuroko VMS deposits. Sulphide-sulphate mineralisation implicates hydrothermal discharge into sulphate-bearing ocean waters, ruling out a globally anoxic Archaean hydrosphere. The volcanic rocks and co-magmatic sub-volcanic intrusion hosting the VMS deposits are characterised by the conjunction of LILE>LREE>HREE, and Phanerozoic La/Yb with negative normalised anomalies of Nb, P and Ti, consistent with derivation via subduction zone hydrous metasomatism fusing the mantle lithosphere.

Jan 1, 1995

A. Sutherland Brown (ed.). Porphyry deposits of the Canadian Cordillera. The Canadian Institute of Mining and Metallurgy, Special Volume 17, 1976. C. G. Down and J. Stocks. Environmental impact of mining. G. B. Rothenberg. Refractory minerals. Park Ridge (V.S.A.), Noyes Data Corporation, 1976. Geology, mining and extractive processing of uranium. London, Institution of Mining and Metallurgy, 1977.

Jan 1, 1978

1. Book reviews Mill Operators' Conference. Parkville (Australia), Australasian Institute of Mining and Metallurgy, 1982. 425 pp. Reviewer: B. K. Loveday Off highway truck haulage. Newman Combined Group, the Australian Institute of Mining and Metallurgy and the Institute of Engineers in Australia. Sep. 1982. Reviewer: B. J. Vorster Environmental engineering in South African mines.Johannesburg, Mine Ventilation Society of South Africa, 1982. 974 pp. Reviewer: A. N. Brown Underground Operators Conference. West Coast Tasmania Branch. Australasian Institute of Mining and Metallurgy. Reviewer: D. R. Aspeling 2. New publications Electric steelimaking in the eighties: challenges and opportunities. Rotterdam, Balkema, 1982. 362 pp. $50.00 or £33. Tungsten: a review, by P. M. Harris and D. S. C. Humphreys. London, Institution of Mining and Metallurgy (Occasional Paper 2), 1983. Members: £3, nonmembers £6. The platinum industry - prospects in recovery. London, Shearson{American Express Ltd (St. Alphage House, Fore Street, London EC2Y 5DA), 1983. £75. The best of E&MJ mining and processing idea book' New York, Engineering and Mining Journal, 1983. 128 pp. Free with subscription to Engineering and Mining Journal. Mining 1983. Harlow (U.K.), Longman Group Limited, 1983. 500 pp. £39.50. Ooncise guide to world coalfields. London, World Coal Resources and Reserves Data Bank Service (14/15 Lower Grosvenor Place, London SW1W OEX), 1983. 380 pp. £45. 3. Canadian publications Asbestos, by G. O. Vagt, 9 pp. Ooal and Coke, by J. A. Aylsworth, 16 pp. Orude oil and natural gas, by R. L. Thomas, 12 pp. Phosphate, by G. S. Barry, 8 pp. Rhenium, by S. A. Hamilton, 3 pp. 4. Mintek reports Report 2102D The recovery of magnesite from dump fines from the Strathmore Mine. (First issued Feb. 1981.) Report 2106D The evaluation of drill cores and a bulk sample from a deposit of andalusite near Thabazimbi. (First issued Mar., 1981.) Report 2108D Evaluation of a grinding aid in batch grinding, classification, and gravity concentration. (First issued Jul. 1981.) Report 2109D The evaluation of an andalusite deposit from Kleinfontein, Groot Marico. (First issued Apr. 1981.) Report M7D The beneficiation of chromite ore from the Ma-l seam near Marikana. (First issued Nov. 1981.) Report M62 A preliminary investigation into the extraction of zinc by direct oxidative leaching of high-manganese sphalerite. Report M76 A mineralogical investigation of a refractory gold ore, and of a sulphide concentrate and calcined tailing from that ore. Report M85 List of unrestricted Mintek publications issued from 1966 to 1982. Report M97 Reduction in metal consumption by the use of alternating lines of higher and lower lifter bars in a rod mill. Report M98 Multivariable control and optimization of the operation of a milling circuit at East Driefontein Gold Mine. Report M101 The potentiality of heat-treated balls in the grinding of gold ores. X-ray diffraction The Southern Transvaal Section of the South Mrican Chemical Institute is to present a mini-course on 'X-ray Diffraction: Theory and Application' in Johannesburg on 18th and 19th October, 1983.

Jan 1, 1983

By M. Karmis, C. Haycocks

Geographic Information Systems (GIS) are becoming a more commonly used tool for resource estimation as they provide not only a database management platform, but also the graphical capabilities to visualize resource characteristics. Interpolation methods used commonly in these resource studies do not typically provide a quantitative answer to the question: "How accurate is the estimate?" By comparing localized measurements at several locations to the interpolated thickness distribution used in a resource estimate, a quantitative analysis of accuracy can be obtained. The technique is demonstrated with a case study from Central Appalachia.

Jan 1, 1999

By P. Rusin

Toxic substances in On solutions can retard biological leaching of copper sulfide dump ores. On solutions were analyzed for metals, organics, and chloride, and showed inhibitory concentrations of aluminum, manganese, and chloride. Inhibition of bacterial activity by the solid fraction of On solution, with and without the organic constituents, was evaluated. Toxicity to bacterial species was evaluated by monitoring bacterial numbers, pH, Eh, and rates of iron oxidation. The On solution solids were toxic at 50 -60% of their field concentration. Most of the toxicity of the On solution was due to the organic fraction. Different SX reagents show varying degrees of inhibition of T. ferrooxidans. Bacterial inhibitory effects of carriers and lixiviants used in the SX plant should be determined so that entrained SX reagents do not retard biological dump leach systems. The reagents used should be the most cost effective and the least toxic.

Jan 1, 1994

By Nagy El-Kaddah

"One of the emerging technologies for the production of ultra-clean metals is electromagnetic filtration. The theory and the mechanism of electromagnetic separation of inclusions from molten metal are briefly reviewed along with basic electromagnetic separation systems. This paper focuses on inclusion removal in the induced current separators, with specific reference to a new separator developed at the University of Alabama. A simple analytical model is presented for the analysis of particle separation in such a system. The role of the applied magnetic field on inclusion removal will be discussed. It is shown that particle velocity increases exponentially with increasing magnetic field strength. At moderate field strengths, the velocity of 50 to 100 u. inclusions· are an order of magnitude larger than those achieved by buoyancy. The separator developed at the University of Alabama is described together with experimental results of laboratory and large scale experiments on purification of molten aluminum. These results demonstrate the capability of the system for producing super-clean metals.IntroductionThe nature of extraction, refining and processing of metals is such that oxides and other non-metallic particles will always be present. This is due to the highly reactive nature of metals with oxygen and other non-metallic elements. The presence of these type inclusions in metals, even in minute amounts, can seriously flaw the reliability and performance of the final product. They not only reduce the strength and the stiffness of the metal/1/, they are the reason behind many of manufacturing defects such as porosity in castings, surface and internal cracks in continuously cast ingots and rolled products, etc., which act to cause premature failure of manufactured parts. In fact, for critical applications such as turbine blades, there is virtually no tolerance for inclusions above ten microns in size /2/. Therefore, removal of inclusions from the liquid metal is an essential processing step.The demand for cleaner metals has brought major changes in the technology and practice of metal refining and casting. Inclusion removal from the melt is currently achieved by passing the melt through a series of melt treatment systems, including induction stirring furnaces, argon-stirred ladle, and ceramic foam and deep-bed filters /3,4/. These systems are generally capable of removing all inclusion particles above 50 microns in diameter, which meets current cleanliness requirements for most applications. However, they may not be able to meet the projected cleanliness levels for critical applications due to kinetic and operational limitations of these systems in removing smaller particles /5/."

Jan 1, 1996

Meeting of June 4, 1915.-The President announced the appointment of the following Committee on National Reserve Corps of Engineers: Dr. Henry S. Drinker, Chairman; Arthur S. Dwight, and Warren A. Wilbur; also, the appointment of Arthur F. L. Bell as Chairman of the Committee on Petroleum and Gas, and of James F. hemp as Chairman of the Committee on Mining Geology. All of these appointments were approved. It was voted that the following minute be, placed on record and a copy sent, by order of the Board of Directors, to the family of John Birkinbine: "The Board of Directors of the American Institute of Mining Engineers hereby records its sense of sorrow and loss in the death of John Birkinbine, a former President, and for many years an active member of the Institute, and contributor to its Transactions. "Mr. Birkinbine's eminence as an engineer, author and editor, intimately connected with the industrial progress of the United States, brought him into contact With the leaders of science and the captains of industry, among whom his genial and estimable personal character won for him many friends; and his departure in the prime of Strength and usefulness is mourned by a wide circle."

Jan 7, 1915

1. New books Extractionmetallurgy'81. London, Institution of Mining and Metallurgy, 1981. 441 pp. $40. Structures and properties of engineering alloys, by W. F. Smith. London, McGraw-Hill, 1981. 512 pp. R89,65. Rock and mineral analysis, by W. M. Johnson and J. A. Maxwell (editors). 2nd ed. New York, Wiley, 1981. 424 pp. $40. Mining methods and equipment, by Mining Information Services. London, McGraw-Hill, 1981. 218 pp. International directory of acronyms in library, information and computer sciences, by P. M. Vaillancourt. New York, Bowker Publishing Co., 1980.516 pp. 2. New journals Trends in analytical chemistry (TRAC), Amsterdam, Elsevier, 12 issues per year. Subs. for Volume I (16 issues) D.H 95.50. Engineering management international, Amsterdam, Elsevier, 4 issues per year. V.S. $32.50, D.H. 70.00. 3. Mineral policy sector publications Mineral Bulletin MR 188. Vanadium: an imported mineral commodity. $3.60. Mineral Bulletin MR 190. Canadian mines: 1980 perspective. $3.00. Canadian mineral survey 1980, by the staff of Mineral Policy and Energy Sectors. $1.00. 4. NIM reports Report 2090 Observations made during the dig-out of a 48 MV A ferrochromium furnace. Report 2110 The investigation of a fracture on one side of a skip bridle in a mine shaft. Report 2111 Pilot-plant tests for the recovery of chromite and the noble metals from the UG-2 Reef at Maandagshoek. Report 2112 The behaviour of UG-2 chromite concentrates during smeUing. Report 2113 M uUivariable control of a milling circuit at East Driefontein Gold Mine. Report 2115 Estimation of material variation in powdered materials Report 2116 Optimum operation of a direct-reading spectrometer with excitation by a 5 kW inductively coupled plasma torch. Report 2121 Five robust indicators of central value. Report 2124 The direct determination, by differential pulse anodicstripping voUammetry at the thin mercury-film electrode,of cadmium, lead, and copper. Report 2127 The preparation of a reference material of South African zirconium concentrate from Richards Bay. Report 2128 The determination, by differential pulse anodic-stripping voltammetry at the thin mercury-film electrode, of cadmium and thallium in six NIMROC reference materials Report 2130 The organizing of conferences. Research grant The Board of Directors of International Precious Metals Institute in conjunction with Gemini Industries, Inc., a California-based refiner of precious metals, recently announced a Gemini Research Grant of $3000 will be awarded annually to a graduate student who is pursuing studies in metallurgy, chemical processes as it pertains to precious metals, or materials sciences, and who is performing or planning research studies in the precious metals. Accidents and diseases The Third International Colloquium for the Prevention of Occupational Accidents and Diseases in the Iron and Metal Industry is to be held on 15th and 16th June, 1982, in Palma de Mallorca, Spain.

Jan 1, 1981