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By D. J. MacDonald

The Bureau of Mines investigated two alternative methods for treating a zirconium-bearing chloride-sulfate strip liquor to obtain reactor-grade Zr02. One method involves neutralization with NH3 and the other hydrothermal precipitation. The strip liquor was derived from zircon sand by a Bureau of Mines method for separating zirconium and hafnium via solvent extraction with a tertiary amine. Neutralization with NH3 to precipitate hydrous zirconium oxide required 0.9 to 1.1 g NH3 per gram of zirconium. The NH3 can be recovered for recycle. Zr02 that met reactor-grade specifications was produced by precipitation with NH3? Hydrothermal precipitation of Zr02 from strip liquor required that the solution be maintained at 2600 C and 680 psi for 10 min and in a non-corrodible pressure vessel. In bench-scale experiments both methods gave-zirconium recoveries greater than 99 pct.

Jan 1, 1984

By R. L. Armstrong, C. I. Godwin, V. M. Kruan

"The Scheelite Dome tungsten-bearing skarn property, central Yukon Territory, is in metasediments in contact with a quartz monzonite intrusion. Contact metamorphism to biotite-muscovite- andalusite hornfels and calc-silicate hornfels is superimposed on low-grade regionally metamorphosed rocks represented by quartz-mica pelitic schist and muscovite-biotite pelitic schist.Metasediments are likely Precambrian in age, even though Rb-Sr whole-rock analyses indicate an early Paleozoic age (511±41 Ma); this apparently too young radiometric age is due to partial loss of radiogenic strontium during regional metamorphism. The minimum age of the quartz monzonite intrusion is Cretaceous at 90.4±2.6 Ma (K-Ar on biotite) and its initial 87Sr/86Sr ratio is 0.7121. The high initial ratio of the intrusion is due to the addition of radiogenic strontium from the metasedimentary country rocks and perhaps an underlying older basement.Scheelite-pyrrhotite-chalcopyrite mineralization occurs in diopside-zoisite skarn pods within the calc-silicate hornfels near the quartz monzonite intrusion. The source for lithophile tungsten is probably the same as for the granitic magma, namely Precambrian sialic basement.IntroductionThe Scheelite Dome tungsten skarn property is within the Mc-Questen map-area (NTS: 115P/16),28 km northwest of Mayo, Y.T., at latitude 63°47' north and longitude 136°15' west. The property can be reached by helicopter or by four-wheel- drive vehicle from Mayo.This paper summarizes the geology of the Scheelite Dome property, which has been described in a general way by Little (1959) and Cathro (1969). Geological mapping and sampling were done by the first author (nee Steffler) during June 1979. Field work was supplemented with detailed work at the Department of Geological Sciences of The University of British Columbia during 1979 and 1980 (Steffler, 1980). Whole-rock chemical analyses were done by Cominco Ltd."

Jan 1, 1982

A visitor to the Republic of South Africa might profitably make his first sightseeing objective the Voortrekker's Monument at the administrative capital, Pretoria. Here he will find memorialized in sculptured stone the epic of the migrations of Dutch colonists from the Cape in search of new pastures and to escape British rule. He will see depicted the battles with the Bantus who were coming south also in search of habitable land, the peace treaties with great chiefs and the rise of Afrikaaner leaders. An American will be struck by similarities in events with his own history as well as in clothes and in type of covered wagons of the colonists. Before the latter half of the 19th century, little that transpired in South Africa was of any great international moment. The country had not attracted a great many settlers (about 15,000 Europeans in 1800 compared to about 2 million in the American colonies in 1776). Although some gold was being mined the majority of population was engaged in trade or subsistence farming.

Jan 12, 1962

By W. G. Miller, J. D. Scott, D. C. Sego

ABSTRACT The influence of using different extraction processes (caustic versus non-caustic) on thethixotropic strength of oil sands fine tailings is examined, as is the influence of adding a coagulant tocaustic fine tailings. The thixotropic strength of fine tailings at large void ratios manifests itself as a bonding or gel strength that has been widely noted both in the laboratory and in the field. This gel strength has a significant influence on preventing the initial consolidation or settlement of fine tailings. Differences between the fine tailings’ thixotropic strength development are explained based on their physical and chemical characteristics.

Jan 1, 2010

By A. MacG. Robertson

INTRODUCTION The tailings, or solid waste, remaining after uranium has been extracted from an ore and the liquid wastes associated with it contain both radioactive and other substances which, if released to the environment, may have a detrimental impact on man and his environment. Although the radioactivity of the waste is of natural origin, the mining and milling process results in bringing the radioactive ore to the surface, changing its chemical and physical form, increasing its mobility and, therefore, enhancing the potential radiological exposure to man. Exposure to radionuclides released from a tailings impoundment, while small as applied to any one generation, can be made large by counting far into the future, large enough to be the dominant source of exposure from the nuclear fuel cycle, Cunningham (1978). Increasingly it is being found that where the prime concern was initially the radionuclide releases, the release of other pollutants and contaminants may be of equal or greater concern. While there is a definite benefit, at least to present generations, resulting from the recovery of uranium, current and long-term concerns require that consequential present and future releases be kept as low as is reasonably achievable. Design practice, to minimize this release, is currently passing through a technical revolution; precipitated by public and institutional concerns. New techniques and methods are, therefore, being actively sought and continuously implemented. Because of the complexity of the pollutant release mechanisms and the sitespecific nature of each impoundment site and tailings product, a wide variety of site selection and design options have been implemented or considered. It is often possible to design a number of satisfactory tailings disposal schemes which differ widely in nature and cost. This paper outlines the principal areas in which options are available and discusses some of these options. Both operating and post-decommissioning conditions are consi-

Jan 1, 1980

By D. E. Shanks

As part of its program to lessen dependence on foreign bauxite as the Nation's primary source of cell-grade alumina, the Bureau of Mines is investigating sulfuric acid (H2S04) leaching procedures for the recovery of alumina from domestic aluminous materials. The successful application of a H2S04 leaching process depends on the recovery of the aluminum values in an easily washed and filtered form, containing a minimum of water to be driven off in the subsequent calcination step. This goal was met by the high-temperature hydrolysis of simulated aluminum sulfate [A12(S04)3] leach liquor. Crystalline, insoluble aluminum hydroxy sulfate [A1(OH)S04], which had a water-to-alumina mole ratio of 1:1, was produced. Eighty-six percent of a solution containing 127 g of A12(S04)3 per liter and 76 pct of a solution containing 336 g of A12(S04)3 per liter were hydrolyzed to insoluble aluminum hydroxy sulfate by autoclaving for 1 hr at 320° C and rapidly quenching to room temperature. Higher operating temperatures were precluded by corrosion of the autoclave. The yield of aluminum in the hydrolysis product increased with increasing hydrolysis temperature and decreasing A12(S04)3 concentration.

Jan 1, 1981

By J. E. JR. Johnson

AT the Cleveland meeting of the Institute in October, 1912, I had the honor to present a paper outlining the conditions surrounding the charcoal iron industry, and giving some of the results of an investigation started about three years ago for the purpose of determining the reason for the poor reputation of the Lake Superior charcoal irons as compared with the Southern and Eastern irons. In that paper I explained the effect of high carbon on quality, and tried to make clear that that paper was a preliminary one, as we felt convinced that we should eventually discover other factors affecting quality. The progress of the investigation has brought out facts that seem to us of the utmost importance practically and theoretically, and the purpose of the present paper is to present these facts with the proofs which seem to us to establish them. The closing year of the nineteenth century saw the publication of the first definite and connected statement of the relationship between the cast irons and the steels.' The metallurgical world was ready to accept the fundamental unity of these two series, acceptance being greatly hastened by Professor Howe's classic paper, The Constitution of Cast Iron, presented at the Richmond meeting of the Institute, February, 1901.

Jan 1, 1914

Sampling systems are never perfect. They all have some bias and give variable sampling errors. The ways of thinking about bias and precision should be different before and after construction (or reconstruction) of a sampling system. Before a sampling system is constructed, the fundamental error variance can be estimated using GyÆs formula or by doing test work on the material to be sampled. The component of sampling variance which varies with the number of sample increments can be computed for the expected patterns of grade variation. The smallness of the bias can be checked using discrete element modelling, by checking that the proposed design complies with clauses in standards, or by copying an existing sampling system that performs well for similar material. After a system has been constructed, sampling precision can and should be monitored directly. Anyone claiming to take responsibility for a sampling system should know its precision. Bias could be checked by comparison to a more accurate sampling system, such as stopped-belt sampling, under conditions where bias seems most likely. However, it is more practical to conduct regular checks that the system is still operating as designed, that the design is still appropriate despite any changes to material flows, and that sample masses are consistent with the correct operation of the sampling system. If precision is not regularly assessed then it should be assumed to be very poor. If a sampling system is not regularly inspected then it should be assumed to be biased.

Jan 1, 2008

By L. J. Erck, T. E. Ban

A discussion of laboratory procedures used to determine pellet quality and to simulate handling and firing conditions. Strength- temperature relationships in pelletizing; effect of chemical additives on agglomeration; and crushing, abrasion, and impact resistance of the pelletized products are discussed with respect to five different iron ore concentrates.

Jan 8, 1953

By W. Irwin

As a consequence of the oil crisis of the 70?s, the commercial value of coal increased very sharply and an upward trend in coal prices although now less pronounced, continues today. The graph shown in figure 1 illustrates the trend in the F.O.B. price of U.S. metallurgical coal. This trend occurs during a time when mechanized mining is firmly established as a means of production throughout the coal mining world. With modem methods of mining, mechanical cleaning is a necessity and quality control is no longer entirely dependant upon coal face practice. The efficiency of fine coal recovery is of vital economic importance to present day operations and good practice in this field contributes significantly to improving profitability. Numerous processes are available for the duty and this paper discusses one such system, namely the practice of froth flotation.

Jan 1, 1980

As this district is so far distant from the other mining centres and its mode of approach so circuitous, I am afraid that many residents of other portions of the Commonwealth never think of paying this" Australia's Silver City" a visit, to learn personally the many and various lessons everywhere available, and to become familiar with the really wonderful and interesting features and deposits (which pature has so lavishly bestowed in the mineralogical world) yet seemed to almost ignore or overlook when disposing of topogr,aphical beauties of landscape and vegetation) unless professional or business duties require their presence here. So it is to those whose life is necessarily spent in other parts of the States where they answer their call of duty, and yet feel an interest, either for business or other reasons, that my paper is specially addressed and prepared, and for that reason I witl endeavour to make my remarks more of an explanatory than a dictatorial nature. I feel sure that there. are many members of our Institute who are much more familiar, and have had many more years' experience in the various methods of timbering, filling, and ore extraction, etc., than myself, but I hope that over I6 years' experience in connection with mines and engineering works, the last six of which have been spent in Broken Hill, where, I have been very closely connected.

Jan 1, 1903

By Mehrotra G. M, Frohberg M. G

Based on the concepts of statistical thermodynamics of athermal mixtures, an approach is developed which is capable of quantitatively explaining the thermodynamic properties of binary silicate systems. Expressions for the ionic fractions of various anionic linear and nonlinear chain polymers are derived. The developed expressions for free energy of mixing are tested by applying these to the system PbO-SiO2. The ionic fractions of various chain polymers in this system are calculated. The two cases, namely, of linear and nonlinear chain polymers are compared with each other.Limitations of earlier models are pointed out.

Jan 1, 1975

By J. Lui

Inco Copper Cliff Smelter commissioned two new Inco flash furnaces in 1991/1993 as part of its S02 abatement program. Each flash furnace is equipped with a fluid bed dryer. The ~ 12 wt% water content in the concentrate filter cake, flux, reverts and sludge is removed in the fluid bed dryer. The dry solids are discharged from the dryer together with exhaust gases into the baghouses where they are separated. The dry solids are transferred to four storage bins. In September 2003, for the first time since startup in 1991/1993, a large amount of elemental sulfur accumulation was discovered on the walls, roofs and floors of the outlet side of the baghouse chambers. Several baghouse fires were experienced during cleaning and conducting maintenance work in the elemental sulfur contaminated baghouses. Laboratory scale test work at the Inco research lab was conducted to understand the mechanism. A plant solution to minimize elemental sulfur formation was implemented with success. This paper summarizes the efforts to understand and minimize elemental sulfur formation in the baghouse chambers.

Jan 1, 2007

By W. E. Lamont

As part of its program to minimize mineral and metal needs, the Federal Bureau of Mines conducted investigations to determine the feasibility of producing foundry-sand-grade olivine concentrates from low-grade sources. Using a Bureau-patented attrition-grinding technique, concentrates meeting Steel Founder's Society of America (SFSA) specifications for loss on ignition (LOI) were prepared. Studies showed that green strengths and tensile strengths of the attrition-ground olivine were equivalent or superior to those of commercial materials. Metal-casting studies showed that molds of attrition-ground olivine produced better surface finishes. The improved surface finishes were attributed in part to increased grain sphericity.

Jan 1, 1977

By A. M. Ouchi

Existing empirical design tools have been developed from fair-to-good quality rock masses (RMR76 >50). This paper presents a focus of ground control research presently being conducted by the Rock Mechanics Group in the UBC Mining Department in incorporating weak rock masses (RMR76 <50) into existing empirical design relationships. An emphasis is being placed upon the updated span design curve/critical span graph originally developed at UBC. The original database has been augmented with over 450 weak rock data points from mines such as the Stillwater mine (Montana), the Eskay Creek Mine (BC) and several mines in the Carlin Trend and other parts of Nevada. The original database is comprised of spans supported with ?traditional? mechanical bolting. In weak rock environments however, this type of support has been found for the most part, ineffective. This paper presents the span and weak rock RMR76 relationship for four different support categories. This work attempts to provide rock mechanic tools that will enable a mine operator to make economic decisions that will also ensure a safe working environment.

Jan 1, 2008

By D. Lelinski, R. Bokotko, J. D. Miller, J. Hupka

Air-sparged hydrocyclone (ASH) flotation is a new, promising technology, and, since its conception, numerous applications have been successfully tested. Nevertheless, research and development efforts have continued to improve the technology with respect to operating conditions and design considerations. Results, from experimental studies on bubble generation in the ASH system are presented in this paper. Bubble size distributions generated during ASH operation were determined using a high-speed photographic technique. The influence of many factors, including surfactant concentration, water flow rate, and porous-tube pore size have been studied. Test results indicate that these process variables have a profound effect on the bubble size distribution. With an increase in surfactant concentration or water flow rate (shear field), the bubble size distributions become narrower and shift toward smaller average bubble diameters. However, the influence of pore size is more complicated. Depending on the experimental conditions, the average bubble size was found to range from about 100 to 300 µm in diameter.

Jan 1, 1997

By Zhang Y. D, Zhang R. X

A new decision-making approach of artificial neural network system with hierarchic structure is presented. The fundamentals of network topology, node functions and network training are introduced. A neural network system with hierarchic struct

Jan 1, 1998

By T. J. Joiner

A critical demand exists to develop new mineral resources, and the need for exploration techniques to supplement costly test drilling is becoming; more acute. In the past few years more industries have begun experimenting with geophysical methods to locate and define mineral deposits and delineate reserves. The new techniques have proven profitable in many instances. As a part of a broad long range program to study the mineral resources of Alabama, and in response to requests from land owners and mining companies, the Geological Survey of Alabama is investi¬gating the occurrence of bauxite and kaolin deposits in the Eufeula area. This project is supported by special funds appropriated for this purpose by the Alabama Legislature.

Jan 1, 1966

By R. S. Simkus, J. R. Egan

"Changes have recently been applied to the Sullivan Concentrator lead and zinc circuits to treat fine-grained ores which make-up the majority of ore reserves in the mine. Pilot plant test work conducted in 1990-91 indicated that concentrate grades would be substantially improved by reducing the particle size (P,0) of the lead from 38 to 15 µm and the zinc from 45 to 24 µm.Circuit revisions involved installation of major new equipment including: two GUO kilowatt Vertimills for regrinding, a 4 metre diameter column flotation cell and a 4 metre diameter hyperbaric pressure filter for dewatering. Duties of the existing regrind mills were reassigned.IntroductionThe Sullivan ore body is a massive sulphide deposit consisting of fine grained mixtures of sulphides, sometimes inter-banded with country rock and varying widely in their content of lead, zinc, iron and silicates. Principal economic minerals are marmatite and galena. Iron is mainly present as pyrrhotite (85%), and to a lesser extent as pyrite (15%) .The orebody has been actively mined since 1923, with 1992 ore reserves estimated at 15,800,000 tonnes with an average grade of 4. 7% lead and 7. 9% zinc. Current plans call for treatment of 1,600,000 tonnes/year, (7,000 tonnes per operating day), with flotation feed grades of 5.9% lead, 10.1% zinc, and 22.0% iron."

Jan 1, 1994

The Report on the Manufacture of Coke for the year 1880 by J. D. Weeks1 includes an historical account of the early days of coke-making that is very complete and accurate, and but little can be added to it to fully cover the period prior to 1885. The few additional references that have been found follow. The earliest suggestion found about making coke in this country is in a letter from D. M. Randolph to Harry Heth, dated August 22, 1808. Heth was then operating the mines in the Richmond, Virginia coal field and had sent Randolph to England to investigate steam engines for hoisting and pumping and other conditions in the coal industry there. The letter was written in London and said: "I shall explain to you, how, by turning Deep Run fine coal in Coak, to make great profit from what has heretofore been useless. You will do well to ascertain the price and amount of demand for this article throughout the U. States among brewers and manufacturers. I know how also to make every bushel of such fine slaty coal, fetch as much as any of the best grate coal, by turning it into Coak: and that too, after paying all expenses of the process."2 His interest was to use the slack more for domestic purposes than otherwise, probably, although what the interest of brewers would be in coke as fuel does not appear. Nothing ever came of this suggestion, and so far as known, no coal from this field was coked excepting in gas-making. The Plumpsock Iron Works, mentioned by Weeks as having used coke, was advertised for sale in June 1818.3 It was stated that stone coal was the only fuel used at the works, the pit being within 100 yards of the forge. "Three men with a horse and cart are sufficient to raise coke, and haul to the forge all the coal necessary for keeping the works in full operation." The coke, of course, was made in ricks, or heaps, and not in ovens. The first real coke oven in this country was probably built in Connellsville, the coal coming from a mine nearby on Mounts Creek. L. L. Norton operated an iron foundry and was persuaded by his foreman, one Nichols, who came from Durham, England to build a coke oven. The oven was 12 feet square, and the first coke was produced in 1833. Later

Jan 1, 1942