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By Charles S. Barrett

THIS paper is a progress report covering metallographic applications of the electron microscope that have been made during the past year at Carnegie Institute of Technology. An account is presented of the techniques that have been most satisfactory, the difficulties encountered, the resolution obtained, and the peculiarities that have been noted in the microstructures. About 12m exposures have been made during the year on the instrument, which is an RCA type B2 transmission microscope,1 and a number of these have been selected to illustrate the results obtained. Prints are also included showing the common types of falsities-to borrow a term from the biological field, the "artifacts." In brief, the paper is a record of our attempt to determine the value of the electron microscope in the study of the structure of metals and alloys. n addition to comments on techniques and the quality of photomicrographs obtainable with them, the paper discusses the nature of the etch attack on a few metals, and the possible relation between the fine structure revealed by etching and the mosaic block structure of the grains. Since numerous papers and reviews are available on the subject of imperfection in crystals, the comments here may be very brief; in fact, are restricted almost entirely to points having to do with recent theories relating the strength of metals to imperfections and to spacings of slip lines. SPECIMEN PREPARATION AND PHOTOGRAPHS Mechanical polishing by hand was used throughout this work. Precautions that must be taken in microscopy at high magnification, which have been well explained by Vilella in his book on Metallographic Technique for Steel, are likewise important with the electron microscope. This applies particularly to the need for repeated polishing and etching (each successive polish becoming less severe and each etch lighter), since the final etch should in general be no heavier than is used for oil-immersion optical microscopy and in many instances should be much lighter (compare Figs. 6a and 7a, 6d and 7b). An extremely light etch, of course, is incapable of cutting through a flowed layer of appreciable thickness. Unquestionably it would be very advantageous in each instance to compare the structures obtained by electrolytic polishing with those obtained by mechanical polishing, but difficulties with the electrolytic method have prevented this in the following collection of prints. The choice of etchant is important, of course; for example, picral proved superior to nital for tempered martensite. With the exception of Figs. Ib and IC, the replicas used were of silica, deposited up0n polystyrene and floated from the polystyrene in ethyl bromide according to polystyrene in ethyl bromide according to the method of Heidenreich and Peck.2 The samples were mounted in Bakelite, polished and etched, then the polished Bakelite

Jan 1, 1943

By Roy A. Grancher

CYCLING WITH CEMENT "THE WHEEL IS COME FULL CIRCLE" Shakespeare's King Lear Act V, Scene 3, Line 176 The time clock of the cement industry has been turned back to the early 1950s. After the trials and tribulations of the decade of the Sixties, the hands now stand where they did just over twenty years ago. Cement shipments have steadily increased, with a record 419 million barrel level (78.8 million tons) being reached last year. Plants are operating at average utilization rates in excess of 85 percent of rated capacity. The spread between supply and demand has narrowed to where a definite shortage of cement now exists within the industry. The notable and unfortunate difference between the two periods however is that, back then, cement's returns were a respectable 14 to 18 percent, whereas today they stand at less than half those levels. Insufficient return forms the present foundation of the U.S. cement industry. This lack is destined to have a cumulative effect. Just as the industry's balance between supply and demand is returning to favorable proportions, promising a period that has historically and now should generate those profit levels required to modernize and provide for capacity addition, cement instead finds itself frozen by federal price controls into the semi-depressed condition that has existed for over a decade and from which it was just starting to emerge. Capital is not attracted to continued low returns, and increasingly restrictive pollution control measures are necessitating great non-productive expenditures be made as definite costs to stay in business. Even a clouded crystal ball would reveal that additional cement plant closings can be expected.

Jan 1, 1972

By Edgar L. Newhouse

The lead smeltery at East Helena, Mont., controlled by the American Smelting & Refining Co. since 1899, has been in continuous operation for the past 25 years. Most of the old smelting and roasting practices have been superseded by newer and more modern methods, but on account of the difficulties involved in changing the original construction, some of the methods in use of handling materials are not the most modern. This plant, however, is particularly interesting as being one of the few essentially lead smelteries in the United States. At Federal, Ill., Collins-ville, Herculaneum, and possibly other places, similar work is being done, but it is doubtful whether any of them produces as much lead as the East Helena plant, whose monthly production averages 6,500 tons. The situation, 5 miles east of Helena, is convenient to both the Great Northern and Northern Pacific railroads, while the electric power is obtained from Canyon Ferry, 12 miles east on the Missouri river. Local quarries supply the requisite amount of lime rock, which the contracts require to be crushed to 5 in. Of the 450 men on the monthly pay roll, a census showed 200 Austrians, 110 Americans, and 30 Italians, the balance being made up of miscellaneous nationalities. The ore supply is mainly derived from the Coeur d'Alene mines in Idaho, and consists of crude ore, coarse and fine concentrates, middlings, and slimes. About one-half of the total output of the Coeur d'Alene camp is sent to East Helena. An average analysis of these ores gives approximately 40 per cent. lead and 11 per cent. sulphur. Local shipments, varying from month to month, are mostly highly siliceous gold and silver ores carrying little lead. Small shippers, leasers of old mines, and prospectors are very numerous throughout Montana, and it is the policy of the company to encourage these men by every possible means, including the free sampling and analysis of their ores and aid in the development of their mines and prospects, whenever their results show promise.

Jan 1, 1915

By Carl H. Beal

DURING the latter part of 1915 and the first half of 1916, the writer held the position of geologist in connection with the conservation work instituted by the U. S. Bureau of Mines, on oil and gas land belonging to the Indians of the Five Civilized Tribes in Oklahoma. The duty of the geologist was to correlate formations containing oil, gas, and water, and to determine the relations of these substances in the different formations so that the conservation agents might carry on their work most intelligently. On account of the rapid development of the Cushing field, which lies in the western part of the Creek Nation, much work was done there by the inspection force. In the course of the geologic studies a large amount of information was collected, which, on analysis, has disclosed some interesting facts worthy of publication. The report, of which the following remarks are an abstract, has been prepared and submitted to the U. S. Geological Survey for publication. This report is now (June, 1917) in the press and will doubtless be issued in a few weeks. Methods Used In addition to the structure maps showing the folding of the Pawhuska limestone, which crops out in several places in the Cushing field, separate structure maps of the three most important productive sands—the Lay-ton (Fig. 2)) Wheeler, and Bartlesville—have been prepared. These structure maps were prepared by obtaining the logs of nearly all the wells

Jan 1, 1918

By A. Ahmadieh, J. E. Dorn, Jack Mitchell

A detailed investigation of the disloccrtion mechanisms controlling prismatic, slip in a solid solutions of magnesium containing up to 15.9 at. pel Li revealed that low-temperature prismatic slip is controlled by the Peicrl's mechanism for all alloy compositions. At higher temperatures slip in the 7.9 at. pet Li alloy was found to follow the diclates of the cross-slip mechanism from basal to prism planes, while the higlier-lilhium alloys exhibited an athermal dejormation process which might be due COARSE-GRAINED polycrystalline aggregates of distilled magnesium exhibit very limited ductility at low temperatures.' The ductility of polycrystalline magnesium, however, is much improved by solid-solution additions in excess of about 8 at. pct to shot-range ordering. The major effect of lithium additions on the low-temperature Shear] stress. for prismatic slip appears to be due to its efftct in lowering the Peierl's stress whereas (1 increase in the shear stress with increased lithium conlent at higher temperatures might he due to short-range order strengthening. Additions rip to 7.9 (at. pel Li appear to have only minor effects on the slackiug-jaidt energy. Li.2 Although the relative amounts of basal slip and twinning are not materially altered by such alloying, a substantial change takes place in the relative amounts of prismatic slip. Whereas prismatic slip is negligible and limited to regions of high stress concentrations in the vicinity of the grain boundaries in pure magnesium, extensive prismatic slip over entire grains occurs in the higher lithium content alloys. Furthermore, as the lithium content is increased above 8 at. pct, the flow stress for polycrystalline aggregates decreases. Comparison of the single-crystal data on pure magnesium for basal slip by Sheely and Nash3 and those for prismatic slip by Flynn, Mote, and Dorn4 indicates that the critical resolved shear stress for prismatic slip is much above that for basal slip.

Jan 1, 1965

By T. K. Mukcherjee

The importance of the processing of secondary resources such as solid industrial wastes and liquid effluents as well as byroducts for the recovery of the associated metal values hardly needs any elaboration. Such processing contributes in no small measure.towards the augmentation of the availability and the supply position of resources. As an added benefit, it leads to a reduction in environmental pollution caused by the undesirable waste materials. As some typical examples of secondary resources in the Indian scenario, mention' can be made of spent catalysts, metal/alloy scrap, ash, consumed batteries, flue dust, slag, sludge and slime, pickling solutions, spent acids; plating rinse solutions, spent etchants, waste water from synthetic fibre manufacture and from tanneries etc. These wastes constitute a source of a variety of non ferrous metals. In the processing of secondary resources like these, the techniques of hydrometallurgy such as solvent extraction play a pivotal role. This paper outlines the efforts made to use solvent extraction to recover(1) base metals. such as copper, zinc, nickel and cobalt from a number of secondary resources like cake, and sludge(2) refractory metals like molybdenum and vanadium from sulphidic byproducts and spent catalyst and (3:) nuclear metal like uranium from phosphoric acid. In the case of base metals, process flowsheet involving the use of acidic extractants such as DEHPA and PC88A have been optimised. The problem of iron removal from the leach liquor, "which influences the metal recovery process significantly, has drawn a special emphasis. hi the case of refractory metals, basic extractants .like Alamine 336 has been pressed into service to produce kilogramme. quantities of pure salts of molybdenum and vanadium, Finally, the paper gives a brief account of plant experience in recovering uranium from phosphoric acid, using 'a solvent system comosed of DEHPA and TOPO.

Jan 1, 1996

By Tim O’Neil

Dressed in black tie and Victorian attire, some 200 people came to Leadville, CO, for a September weekend featuring a National Mining Hall of Fame and Museum (NMHF&M) induction banquet and a scenic mountain train trip to Fremont Pass and the Climax Mine. The 18th annual induction banquet on Sept. 17 began with cocktails and a open house. It was a chance for visitors to tour the National Mining Museum including the new Hennebach Wing, opened in February. The new wing is named in honor of Ralph Hennebach, retired chairman of Asarco. Formerly Leadville Junior High School, the Hennebach Wing encompasses more than1,440 m2 (15,500 sq ft) of floor space in two stories. One prominent feature is a 1923 Wills Sainte Claire touring sedan. Climax Molybdenum donated this first all-molybdenum steel motorcar. Docents were available throughout the museum to give banquet attendees directions and answer questions.

Jan 1, 2005

By William D. Gallant, Thomas M. Barczak, Carol Tasillo

"This paper describes the results of full-scale testing of several multi-layered wood crib configurations that were tested in the Bureau of Mines mine roof simulator in cooperation with the Cape Breton Coal Research Laboratory and Cape Breton Development Corporation of Sydney, Nova Scotia. Nine different crib configurations currently being used as wood packwall supports for advancing longwall applications in Canada were evaluated. Configuration parameters understudy included the aspect ratio (height-to-width relationship) and percentage of solid material used in the crib construction. Test results and generalized wood crib behaviour are discussed in detail. Recommendations are made concerning crib constructions to maximize strength and stability. A cost benefit analysis of multi-layered wood crib configurations is made. A comparison of laboratory results and underground observations of several wood packwall supports in the Sydney coalfield suggest in situ load capacity is less than that measured in laboratory testing. Reasons for the apparent decrease of in situ load bearing capability are described.IntroductionA cooperative effort was undertaken by the U.S. Bureau of Mines with the Cape Breton Development Corporation (CBDC) and the Cape Breton Coal Research Laboratory (CBCRL) to evaluate the behaviour of gateside packing materials used in advancing longwall mining applications in the Sydney coalfield. As part of this effort, full-scale tests were conducted on wood packwall supports in the Bureau's 3-million pound (13.3 MN) active load frame.Nine different pack configurations were evaluated as part of this study. The wood packwall supports were multi-layered crib constructions from 6 in. (0.15 m) by 6 in. (0.15 m) cross section timbers using timber s 30 in. (0.75 m) and 60 in. (1.5 m) in length . The percentage of solid material in the crib constructions varied as illustrated in Figures 1 and 2. A summary of crib constructions is provided in Table 1."

Jan 1, 1991

By David J. T. Carson

"The metalliferous deposits of Vancouver Island have generally been assigned to the Mesozoic ""Coast Range Orogeny."" However, a metallogenic study by the writer has revealed that several important classes are early or middle Tertiary. Included are porphyry coppers, and gold-quartz, arsenic and copper-arsenic veins.The porphyry coppers and many gold-quartz veins are within and adjacent to Oligocene-Eocene quartz diorite intrusive complexes. Arsenic and copper-arsenic veins have a close spatial relationship to sills and laccoliths of Oligocene dacite porphyry which intrude the late Cretaceous Nanaimo Group.Other deposits of demonstrable Tertiary age include a molybdenum stockwork related to a relatively potassic Eocene plug and a few small copper-skarn occurrences. Some copper stockworks and a mercury deposit are probably also Tertiary.The copper deposits of previously recognized Tertiary age are those of the Sooke area that occur in Eocene basalts and Oligocene gabbros."

Jan 1, 1969

By Leahy GJ, Wright DJ, Player RI

The operation of a one tonne submerged combustion pilot plant for the recovery of copper from anode furnace and converter slags is described and the effects of variables discussed. Using coal as reductant, copper levels of anode furnace slag were lowered to 1% or less, with batch times of approximately 120 minutes. Fluxing with limestone was required to produce a fluid slag at temperatures of 1200 - 1300¦C. For converter slags, reduction to 0.5% Cu or less was achieved in batch times of 35 minutes. The chemistry of the pyrometallurg- ical recovery of copper is briefly reviewed in relation.to copper recovery methods.

Jan 1, 1978

By Kohei Yajima

The dusts and fly ash generated from the steelmaking processes and municipal solid waste incineration processes contain metallic elements such as Fe, Zn, Pb and Cd with considerable amount of halogens. In Japan, zinc in dusts is recovered by Waelz kiln or MF process, etc. However, the presence of halogen in the dust affects the evaporation and condensation behavior of zinc and other metals, and disturbs the direct recycling of dust to steelmaking processes, because alkali or heavy metals reacted with halogen vaporize easily as halides and/or oxyhalide compounds in pyrometallurgical process. Recently, the formation mechanism of zinc oxychloride vapor was investigated and the formation of zinc oxychloride such as ZnOCl was proposed. However, considering the practical operation, the effect of water vapor on the evaporation behavior of oxychloride is not fully clarified yet. This study is focused on the investigation of evaporation behavior of ZnO with Ar- O2-HCl-H2O atmosphere.

Jan 1, 2008

Salt Lake City was founded July 24, 1847, by Mormons under the leadership of Brigham Young. It had a population of 1 18.1 10, according to the United States census of 1920, and of 15 1,968, according to a civic survey, January 1, 1925. The Salt Lake metropolitan district is estimated to have 180.079 inhabitants. The city's area is 5 1.8 square miles. Its altitude is 4,354 feet. It has 514 miles of streets, of which 91 miles are paved. The streets in the main portion of the city are 132 feet wide and the blocks are 660 feet long. It has 144 miles of street railway and 2,200 electric street lights. It has fifteen parks and playgrounds, forty public schools and six private schools. It has eighty-nine church edifices, of which forty-nine are devoted to denominations other than the Mormon church.

Jan 1, 1925

By Shoji Higashi, Nobuhiro Honda, Takeo Asanuma, Tatsuo Nagatsu, Masaki Kitazume, Sachihiko Tokunaga, Shigeru Kubo, Hidenori Takahashi, Tsuneyasu Onishi, Yoshiyuki Morikawa

"Various kinds of civil engineering structures and facilities were seriously damaged in the earthquake in Tohoku and Kanto regions of Japan on 11 March 2011 due to the greatness of its magnitude. In contrast, many structures resisted the large seismic force having been reinforced by the CDM (Cement Deep Mixing) method, which is often used for increasing the bearing capacity of ground and improving seismic performance. This paper summarizes the field survey undertaken to investigate damage to structures and facilities reinforced by the CDM method. Several prefectures and metropolitan areas were selected for the survey, based on the occurrence of strong seismic motions. A total of 847 structures and facilities were studied, in the survey using a questionnaire, which mainly inquired about the appearance of structures and facilities. Of the respondents to the questionnaire, 789 replied that there were no seriously damaged structures. The paper presents the damaged and non-damaged sites of CDM-technique sites and non-CDM-techniques sites. It can be concluded from the field survey that the CDM Method demonstrates high efficacy and durability against a strong seismic motions.INTRODUCTIONDuring the afternoon of 11 March, 2011, a huge magnitude-9.0 Mw (Category 9.0 on the Richter scale) earthquake occurred about 25 kilometers below the Pacific Ocean’s surface off the coast of Tohoku. This massive earthquake, now called the 2011 Off the Pacific Coast of Tohoku Earthquake was the largest earthquake ever observed in Japan. The seismic intensity of this earthquake was measured 7, the maximum on the Japanese intensity scale, as observed 7 in northern Miyagi Prefecture. The earthquake caused severe damage over a wide area from Tohoku to Kanto, and triggered large tsunamis that struck the Pacific coast of Hokkaido, Tohoku, and Kanto. The number of missing and fatalities caused by this earthquake exceeded 18,000 persons, making this an unparalleled earthquake disaster with a cost-in-life toll not experienced by Japan in recent years. Because of the scale of its seismic motions, the earthquake damaged facilities and structures of many kinds. In the years prior to this earthquake, the CDM method was used extensively to increase the bearing capacity of the ground as an anti-seismic countermeasure and to prevent liquefaction. Immediately after the earthquake, the CDM Association visually surveyed the state of damage to about 800 facilities in the Tohoku and Kanto regions where a seismic intensity of 5 or higher was observed. This report summarizes the survey of damage to facilities and structures constructed applying the CDM method in order to confirm the durability and performance of the method against seismic motions."

Jan 1, 2015

By S. Whinery

In these times of sharp rivalry, both as to price and quality, among the makers and venders of engineering explosives, it is often desirable to be able to determine the relative energy or value of the various explosives offered for sale, in order to purchase intelligently ; or, having contracted for a large amount of an explosive of a certain standard quality, to be able to ascertain if the manufacturer keeps his product up to the specified standard. The simple and inexpensive apparatus described below was devised by the writer while engaged on the improvement of the Tennessee River, at MuscleShoals, under the direction of' Major W. R. King, U. S. Engineers, in the summer of 1879. It answered the purpose so well that it is thought that a brief account of it may be of interest to other engineers. It consisted, essentially, of an old blacksmith's anvil and a common striking hammer, such as is used for driving rock-drills. The anvil was placed face downward on solid, level ground. In what was then the top of it, a vertical hole, one and one-fourth inch in diameter and about one arid three-fourths inch deep, was made with a ratchetdrill. The surface of the anvil immediately around the drill-hole was made as true and smooth as possible with a file. Next, a new striking-hammer, weighing nine pounds, with a turned and true face, was selected ; and a handle, eleven feet long and about one and a half inches in diameter, was fitted into it so that it

Jan 1, 1886

By Carlos Pineda

El presente trabajo describe la integración de las herramientas Whittle. 4X en la planificación a largo plazo de la mina Pierina. El uso de la informática en las etapas de planeamiento se realiza a través de software especializados con aplicaciones CAD y comunes: Kedit, excel, access, etc. Asimismo, la planificación a largo plazo se vincula a las fases del minado, cuyo objetivo es la optimización los recursos conocidos de la mina, así como los resultados economicos de la explotación del yacimiento a través de la optimización del límite final.

Aug 25, 2002

By Holliday RJ

The Imperial Smelting Furnace (ISF) was developed in Britain during the 1950's as a process which could produce zinc from a blast furnace. Since then it has evolved into an efficient means of producing zinc and lead from lower grade raw materials, both of primary and secondary origin. These changes have been in response to the need to improve the cost competitive position of the ISF in a climate of decreasing metal prices. The improvements at the Cockle Creek smelter of Sulphide Corporation Pty Limited have resulted from work undertaken in four main areas: 1. Changes in plant design and operating practice to give more stable furnace operation. 2. Improvements to the quality of sinter being charged to the furnace. 3. Improved monitoring of process variables and the formulation of control strategies based on the improved data. 4. Increased understanding of the processes occuring within the furnace shaft to allow predictive modelling to be undertaken. Work in these areas is still progressing but the work to date has resulted in a significant improvement in the production rate and efficiency of operation.

Jan 1, 1984

Furnace Builder. Engineer with extensive experience in furnace building. Position with well-established firm, branching into new fields. Location Ohio. 11-1343. Erecting and Operating Engineer to take charge of erection of gas-producer equipment and to teach customers how to operate such equipment. Location Ohio. Salary $250 per month. R-1339. Assistant Professor in Mining School, for instruction work; must have had experience in ore dressing and metallurgy. Location Missouri. Salary $1500-$2100 per school year (8 mo.). R-1332. Consulting Engineer, familiar with construction of artesian wells to act in a consulting capacity. Location New York City. R-1324. Mining Engineer and Investigator to do non-metallic mineral investigations in both field and office for United States Government. Position will last at least a year, and may become permanent. Location Washington, D. C. Salary $1800-$2700 depending on qualifications of appointee. R.-1317. Crushing Plant Superintendent, cement mill and construction experience essential. Prefer man who has had limestone crushing experience. Location New York. R-1314. Assistant Professor of Coal Mining, must be a graduate of mining engineering and have had some coal mining experience. Location Philadelphia.. Salary $2200 for school year of 10 months. R-1312.

Jan 9, 1919

By C Hall, P Hazell, C Wilson

Every mine is situated within a water catchment – a catchment with potentially many other land uses. A mine may take up a relatively small area in that catchment, but its operations have the potential to affect the whole catchment and long after that mine has ceased to operate. Therefore, the residents of any given catchment have the right to feel secure in the knowledge that their catchment, and indeed the wider environment, will not be degraded by mining activities. Much conflict can arise when this confidence does not exist.But, imagine if a community not only felt confident that their catchment would not be degraded by mining activities, but was also confident that their catchment would be left in a better and continuously improving condition – with improving water quality, biodiversity and soil - and a strengthening, more resilient economy. CITATION:Hazell, P, Wilson, C and Hall, C, 2018. Landscape regeneration lessons learned from Mulloon Creek, in Proceedings Life-of-Mine 2018, pp 125–126 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 25, 2018

By Y. Wang, E. Forssberg

Wet magnetic separation methods for the recovery of hematite and chromite fines and ultrafines were investigated. These methods included wet high-intensity and high-gradient magnetic separation, carrier or "piggy-hack" magnetic separation, magnetic field-induced aggregation and magnetic seeding. This investigation indicated that wet magnetic separation is more efficient for fines and ultrafines. This investigation also indicated that other methods can be used to enhance the particle aggregation and/or the magnetic response. The magnetic behavior of these minerals with respect to the magnetizing field, temperature and particle size is also presented.

Jan 1, 1995

By Olaf Hondrum

CHURN drilling equipment at Bagdad consists of two Bucyrus Erie 27-T model drills and one 22-T drill with gasoline engines. The drilling tools weigh approximately 1600 lb. The holes are drilled with 7-in. bits which are heated in an oil burning furnace and sharpened in an electrically powered bit sharpener. A service truck brings the bits to the drills and takes the dull bits back to the shop. The bits weigh around 250 lb. when new and are handled by drill crews without any mechanical handling device.

Jan 10, 1950