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By T. H. Watkins

COAL is the basis upon which the activities of the industrial nations of the world rest today. In order that the coal industry may bee restored to a reasonably healthy condition, it is essential that both the operator and the miner should understand that they are directly concerned and that their selfish interests demand that they take an active, intelligent, self-sacrificing view of the entire situation and do their part in restoring and repairing the economic structure. Foreign credits, foreign debts, unstable exchanges, destroyed markets, and inability through lack of credit to carry on as before, all require our attention and cooperation. DEEP CONCERN AS TO FUTURE There is deep concern as to the future and a realiza-tion on the part of some of these leaders of industry that they will have to sacrifice their personal time, away from their desks and the details of business, in order to cooperate with other groups in studying the situation and endeavoring to find the best method of utilizing their knowledge in improving conditions and averting further disaster. It is most unfortunate for the country and for labor itself that the labor chiefs are blind to these necessities, and hostile to every effort to secure their cooperation in rebuilding prosperity.

Jan 2, 1922

Jan 1, 1888

By Joseph Richards

THERE are two essentially different types of case-hardening processes; that using a dry mixture in which the object to be case-hardened is packed and kept for the necessary time at the necessary temperature, and the "liquid" process, employing a bath of fused, salts into which the object- is immersed and which by immediate contact case-hardens the surface of the article. The Shimer process belongs to the second class, and was a war emergency invention. Of the liquid melts used as baths, the most effective and most fre¬quently used are melted potassium cyanide and melted sodium cyanide. These may be used either pure, or mixed with salts that reduce the melting point and the percentage of cyanide present. The use of these baths since 1914 has met many commercial difficulties because of the high price and frequent commercial scarcity of the cyanide salts; at present sodium cyanide has practically entirely displaced potassium cyanide. Another trouble is the danger to the workmen handling the cyanide salts, which are extremely poisonous, and the annoying and poisonous vapors or gases given off in the workshop, unless an effective system of hoods and ventilation is provided, so as to prevent the gases from the baths mixing with the air of the room. Porter W. Shimer, of Easton, Pa., has invented a substitute for the bath of melted cyanides which case-hardens with equal or greater facility and effectiveness, gives off no poisonous vapors, and costs for chemicals materially less than the cyanide costs in the previously used baths. The process has been in use over a year in a large American works and the following statement embodies the results of practical experience in the use and operation of the process. The Shinier liquid or melted bath consists of a mixture of easily fusible salts that do not possess case-hardening properties, into which is immersed fresh calcium cyanamide, which imparts to the bath case-hardening properties. The composition of the non-case-hardening-,salts appears rather immaterial. Good results have been obtained by using a mixture of sodium chloride, calcium chloride, and barium chloride in

Jan 2, 1919

By A. J. Hudson, M. R. Yenchek

Faulty insulators on mine trolley/track haulageways may allow the flow of leakage currents into the mine roof and ultimately result in combustion of the local roof material. The National Institute for Occupational Safety and Health (NIOSH), Pittsburgh Research Laboratory (PRL), has devised a passive means to detect overheating insulators on direct current systems. The detector consists of a spring-loaded cartridge that ejects a reflective streamer of white Teflon tape when subjected to elevated temperatures. The cartridge assembly can be easily installed over the outer metallic shell of an existing trolley line insulator. If an insulator overheats due to ground leakage currents, the visible streamer alerts mine personnel traveling on the haulageway.

By A. J. Lyon

THE stability and permanence of any structural material used in aircraft are of paramount importance. The spontaneous hardening, or age-hardening; which takes place in some of the aluminum alloys under ordinary conditions of temperature and atmosphere, is accompanied by an increase in tensile strength and proportional limit and a decrease in elongation or ductility. Within the last few years the introduction of a number of strong and ductile casting alloys led to a study by the Materiel Division, Air Corps, of the permanence of the physical properties in several of these alloys. It has been found that even though some alloys have good properties directly after casting or heat treatment, they are not satisfactory for stressed parts that require a combination of strength and ductility. It has also led to the conclusion that all alloys that can be hardened by artificial aging-heating in a temperature range below 170° C. (340° F.)-will harden spontaneously if allowed to stand for a sufficient length of time. It follows that, in aircraft work where the factors of safety are limited on account of the necessity of keeping the weight of the structures as low as possible consistent with their safe operation, the properties of the alloys in the stable or final condition should be used as a basis for design rather than the properties obtained on the material directly after casting. The work of Wilm in Germany, Hanson and Gayler at the National Physical Laboratory in England, and Merica, Jeffries, and others in the United States, has shown that the spontaneous hardening is characteristic to a greater or less extent in all aluminum-base alloys in which the solubility in the solid state of the alloying constituents decreases with the temperature. It has been shown that, by heating to a temperature as near as possible to the melting point of the material and soaking at that temperature for a sufficient length of time and then quenching or cooling rapidly, a maximum amount of the soluble constituents can be retained in solution and the condition of maximum hardening effect upon aging can be obtained. Also, in ordinary sand and chill castings, without heat treatment, a sufficient amount of the alloying constituents is held in solution to cause important changes in the final physical properties.

Jan 1, 1928

By H. E. Stauss, E. I. Salkovitz, F. W. von Batchelder

EXISTING information regarding the structure of a spherulite in nodular cast iron is based on optical studies. According to these data, a nodule consists of an aggregate of graphite crystallites radiating from the center, with the closely packed basal planes at right angles to the radii. The c axes lie along the radii. This view faces some uncertainty in the fact that the c axis does not represent the accepted direction of fastest growth in graphite. To supplement the optical information, X-ray studies have now been made. The principle used was to screen the nodule in greater part from the X-ray beam and expose only a minor cap. As successively larger portions of the nodule were introduced into the X-ray beam, any differences in the X-ray patterns could be observed. Such photographs have been taken with chromium radiation and a Laue camera. The graphite nodule itself, about 0.010 to 0.025 in. in diam, was mounted with vaseline on a micrometer screw for control of the linear motion. The nodule rotated about 45" each time that it was translated linearly. The nodules were obtained from magnesium-treated hypereutectic iron by electrolytic solution of the iron in hydrochloric acid. In Fig. la is shown the pattern of the thinnest cap examined. In Fig. lb is shown the pattern of the same nodule moved 0.003 in. farther into the X-ray beam, and rotated 45" at the same time. Figs, la and lb indicate incomplete circles for graphite (the two outer circles arise from graphite) with the side arcs much weaker than the top and bottom ones. The arcs obtained are themselves not continuous in intensity but vary with maxima of intensity some 15" and 30" apart. The structure of the nodule that would give rise to such a pattern can be explained as follows. Basically the nodule consisted of small crystallites. The discontinuous character of the diffraction rings demonstrates that the nodule was not composed of randomly oriented crystallites. The strong vertical reflections and the weak lateral reflections show that the reflecting planes were roughly normal to the radii. The absence of sharp reflection spots suggests that the nodule did not contain large crystals. The sharpness of the diffraction rings in their radial direction shows that the variations in intensity along the arcs were not the result of line broadening resulting from extremely small crystals. In the diffraction patterns two rings corresponding to graphite were found. The third and inner ring in the figures originated in the vaseline. The graphite rings correspond to the a and ß lines reflected from the basal planes, showing that the radii of the nodules are the [0001] direction normal to the basal planes of graphite. The picture of the structure that is formed is, therefore, one of aggregates of crystallites. Within each aggregate the c axes of the crystallites tend to align themselves in the radial direction of the nodule, although these axes deviate somewhat in direction by a continuous variation of angle. Correspondingly the basal planes of the graphite crystallites are generally normal to the radii. It is a pleasure to acknowledge the assistance of M. C. Bloom and R. P. Dunphy of this laboratory.

Jan 1, 1952

By P. H. Royster

For a number of years the Bureau of Mines has been investigating certain problems relating to the blast furnace. In the course of these investigations it was desirable to measure, with the optical pyrometer, the temperatures occurring in the hearth of the furnace. Since no systematic measurements of these temperatures have been published a statement of the results may be of interest. The data given in this paper were obtained it thirty-two blast furnaces operated by seventeen companies; twenty of these furnaces were making iron, eight ferromanganese, and five spiegeleisen. The collection of this information was made possible by the cooperation of the American Manganese Co., Bethlehem Steel Corpn., Brier Hill Steel Co., Buffalo Union Furnace Co., Clinton Iron & Steel Co., Donner Steel Co., John B. Guernsey & Co., Jones & Laughlin Steel Co., E. E. Marshall, the McKinney Steel Co., National Tube Co., New Jersey Zinc Co., Republic Iron & Steel Co., Seaboard Steel & Manganese Corpn., Southeastern Iron Corpn., the Youngstown Sheet & Tube Co., and the Wharton Steel Co.

Jan 9, 1919

By H. Kandemir

An experimental study of the bacterial oxidation of naturally occurring high-purity sulphide minerals (FeS2, Fe1-xS, Cu5FeS4, ZnS) is presented using a mesophilic strain of T. ferrooxidans. As well as metal analyses and solution pH, partitioning of sulphide sulphur into elemental sulphur and sulphate has been monitored as a function of leach time. Partially oxidized sulphide substrates have been characterized, at regular time intervals, by X-ray diffraction methods and extracellular organic compounds reporting into leach solution .have been identified by thin layer -chromatography.

Jan 1, 1985

By J. Drenda

The model for methane removal from the workings directly behind an advancing longwall as presented in this paper may be used for U-ventilated cross or length-wise systems of longwall advance, starting from the boundaries of the extraction field. In mines with high methane concentrations, Uventilated longwall extraction from the boundary of the extraction field produces a methane risk. The risk is manifested by a higher methane concentration at the end of the longwall, upper gate and incline. The methane in increasing concentrations, which is emitted mainly from the workings with caved areas, appears towards the end of the longwall and in the upper gate. The graphical model of the longwall provided includes both the workspace of the longwall and the caved area. Based upon a model of the rock distribution in the cave, a ventilation model comprising two standard air splits and large number of crosswise air splits has been constructed. Simulations indicate that if the shearer is not present in the longwall, the air distribution in the caved area is symmetrical. The presence of the shearer, both at the bottom and the top of the longwall, causes an asymmetrical air distribution in the cave, that is the asymmetrical flows in the goaf and longwall workspace and in the inflows and outflow between those regions. This phenomenon causes an increase in methane concentration at the end of the wall and at the upper gate. The methane removal method proposed for workings with a caved area directly behind the advancing U-ventilated longwall, starting from the boundary of the field, consists of the removal of methane-air mixtures from the caved area with the boom pipes. These booms may be of several meters long and may be extended if necessary. The insertion of the boom pipes into the cave towards the end of the longwall and connecting them with the general methane removal system creates negative pressure causing a change in the depression field, which is the aerodynamic potential field in the goaf area around the ends of the boom pipes. This will promote the extraction of the methane-air mixture from voids and the goaf cracks, and the area from which methane is being extracted may extend to the side of the cave. This is a positive phenomenon, which could result in the methane flow from the goaf into the airflow in the longwall workspace decreasing or even stopping. A reduction in the methane flow into the longwall workspace with extractions booms will be advantageous for the production continuity. Based on the floor load model for the rocks in the cave and the methane-removal boom load model, the value of the force required to move the boom behind the advancing wall has been calculated. Strength calculations for the pipe were performed using a finite elements method. The analysis results, as well as the comparison of the pipe material effort to the strength parameters of steel, which can serve as piping material (for the assumed load conditions), lead to a belief that the proposed boom construction satisfies the strength requirements.

Aug 1, 2013

By Robert J-M Ethier

"Sequential blasting has been introduced at Mines Gaspe to reduce the harmful effects associated with the instantaneously primed blasting method. Three stages of modifications had been tried to improve this method: trials of a rectangular pattern instead of the square one, trials of lengthened hole collars at the perimeter of the blast and trials of increased inter-row delay intervals from 35 to 50 ms. Results showed that improvements to the instantaneously primed blasting method were limited by the probability of increasing the number of bootlegs.Doing these modifications allowed the definition of a general approach to improvements before the sequential blasting method was introduced. This general approach included: planning of the mining sequence, following up on the drilling, loading and tying-in of each blast, compiling and evaluating blast results, comparing results from one bench to the other and moving along with one change at a time. This approach has permitted the successful introduction of the sequential blasting method in two steps: trials of blast by rows of delayed holes and trials of hole-by-hole blasts. The optimum result has been analyzed by high-speed camera and by computer blast simulations, The actual optimum sequential blast is obtained with a CORDLINE priming system using period 15, permitted in a large drilling pattern, with an intersequences delay interval of 230 ms and an inner-sequences delay interval of 50 ms.While these modifications were being introduced, a careful study of the drilling and blasting costs was made, which showed a sharp reduction of drilling cost per tonne. Even though there was an increased use of packaged slurry the blasting cost per tonne also dropped. The reduction in cost per tonne was explained by the fact that the average energy factor was maintained while the blasting pattern was expanded.The sequential blasting method, successfully introduced at Mines Gaspe, permits blasts of better quality, reduces the drilling requirements by more than 30% and helps to achieve improved productivity while minimizing costs."

Jan 1, 1984

By P. D. Ferro

The direct oxide reduction (DOR) of plutonium oxide generates significant amounts of contaminated waste. This waste primarily consists of calcium oxide-saturated calcium chloride salt. This investigation explores the possibility of recycling the salt, by the electroreduction of the calcium oxide. Fused salt electrolysis of a simulated salt mix (CaC12 + ~10 wt. pct. CaO) is being carried out to electrowin calcium, and the process is being optimized in terms of the calcium solubility, cell temperature, current density and cell design to maximize the current efficiency. This work identifies the major concerns in the development of a process to electrowin calcium from this simulated salt mix.

Jan 1, 1992

It is not often that mines have as much warning of the approach of bad ground conditions as was the case at the Western Mining Corporation, Kambalda Nickel Operations Lafranchi/Schmitz Decline. Most aspects of this operation are in fact quite unique and like the best solutions, the answer to the problem of weak and foliated ground conditions was relatively simple; requiring the use of readily available explosives although the idea of using it in this manner may not be the most obvious.The use of high shock energy POWERGEL 2131 cartridges proved to be the correct answer, in conjunction with small changes in drill pattern design. The resulting lack of overbreak bears testimony to the success of the concept and the commitment of the miners to achieving a safe working environment.

Jan 1, 1992

By A. M. Cummings

During August 1943, the Bureau of Mines undertook sampling and measuring of the Kennedy zinc tailing pile near Hazel Green, Lafayette County, south-western Wisconsin, as part of a general investigation of this lead-and zinc-producing area at a time when it was extremely important to increase the production of metals for the Nation's War program. The tailing pile was the residue from old jigging plants that treated ore from the Kennedy mine, one of the oldest and. largest mines in the district. Because retreatment of tailing by modern milling methods was proving economically successful at other sites in the southwestern Wisconsin field, the Bureau?s investigation was designed to assist the potential operators in evaluating the feasibility of a retreatment operation at this site. The study involved measurement of the tailing pile and sampling by means of auger to determine the average metal content within the narrowest possible limits. A total of 46 auger holes ranging in depths up to 40 feet and aggregating 886.5 feet of bore were drilled in the tailing pile, and weighted samples from each hole were analyzed and averaged to determine the zinc and iron content of the tailing.

Jan 1, 1949

By R. B. Casault, J. D. Boyd, D. R. Bell

"Full-scale sections of three different types of Grade 483 line pipe have been evaluated extensively. The variations in chemical composition, optical microstructure, tensile properties, hardness and Charpy impact toughness with specimen orientation and location were determined. Significant variations in several properties, notably Charpy shelf energy, impact transition temperature, inclusion content and ferrite grain size, were observed for different locations in the pipes. The results indicate that current specifications call for test samples for the most conservative locations, except for impact tests. Minimum Charpy impact values generally occur at the II2-width location, which may be a more appropriate specified test location than the present I/4-width location. The anisotropy of impact toughness, and the importance of low sulphur content and inclusion shape control for adequate toughness in the transverse/rolling-direction orientation were demonstrated. The orientation of impact specimens is critical for spiral-weld pipe, and the current specification test is non-conservative in that it can give results which are two to three times higher than the minimum value for the steel.IntroductionThis report presents the results of an extensive metallurgical evaluation of three different Grade 483 line-pipe steels. The sample material came from full-scale sections of line pipe, which represented current commercial practice at the time of manufacture (1975-1977). Since then, significant improvements have been made in the manufacturers' procedures for producing skelp and pipe, and the line-pipe specifications have been revised. Hence, the information in this report is dated in terms of current design, but it is unique and significant in several respects:"

Jan 1, 1982

By Jae-Chun Lee

Di-2-ethylhexyl phosphoric acid (D2EHPA) is widely used for separating rare-earth elements. In commercial plants, rare-earths are usually stripped from loaded extractant streams using mineral acid, then precipitated as oxalates. Many rare-earth uses demand specific powder characteristics, which are obtained by secondary processing. This paper demonstrates the feasibility of combining the stripping, precipitation and powder processing stages, thereby achieving considerable savings. MEHPA solutions were loaded with yttrium, then emulsified with oxalic acid-HC1 solutions to precipitate yttrium oxalate, which was readily calcined to yttrium oxide. The precipitation kinetics and yield were sensitive to process conditions. The morphology and size of the yttrium oxalate powders varied with the concentrations of D2EHPA and oxalic acid, and the presence of SPAN 60, which affected nucleation, growth, and the emulsion characteristics.

Jan 1, 1992

By L. S. Pratt

In 1910 the author was engaged in a qualitative study of the radioactivity of several chemical substances and a few minerals. In the course of the work he studied the mineral allanite (obtained from granite ledges at Topsham, Maine), and found it to be appreciably radio-active. Recently the fact was brought to his attention that the radio-activity of allanite is not well known, although Hon. R. J. Strutt in 1905 published a list of radio-active minerals with their analyses, including allanite from Amherst County, Virginia.' In the work done, a standard type of electroscope was used, and the readings were made with a telescope, fitted with a scale, by means of which the rate of discharge could be readily determined. The natural "leak" of the instrument was carefully determined, and all results corrected accordingly. The method of study was as follows: The material to be tested was finely powdered, and spread over the bottom of a small, inactive pan. The electroscope was then charged, and the pan placed in position. The door of the instrument was closed, and the rate of discharge carefully determined. All results were reduced to common form to permit of comparison. It is to be noted that the materials tested were not used in strictly comparable quantities, such as if 1 g. of each had been used, but about the same quantity of powder was used (in the cases of the solid substances), so that the results are qualitatively accurate. The results obtained were the following, reduced to common form and corrected for the natural "leak" of the instrument used: Mm. in 6 Min. (on Scale) "Leak1'...................................... 1 Radium residue (in pan)....................... 720 Thorianite.................................... 62 Nernst mantle................................ 17 Uranium nitrate............................... 11 Allanite ...................................... 3

Jan 1, 1917

By R. J. Mechin

IN the early part of 1934, the St. Joseph Lead Co. purchased from the Kadco Corporation three dust-removal units, two suitable for raise work, and the other for drifting operations. The equipment was installed at the Balmat mine, in St. Lawrence County, New York. The Kadco dust-control system can be briefly described as one in which hoods, through which the drill steel is drawn, control the dust at the drill hole, the dust is conveyed through rubber hose or pipe to a collector, where it is removed from the air stream, and the air is then available for recircula-tion in the working place. As during the last few years a number of studies had been completed for the purpose of determining whether or not the dust was effectively removed by the Kadco system, and as the dust counts taken in these tests apparently indicate that it was, the St. Joseph Lead Co. was only inter-ested in obtaining data to show the efficiency of drilling, expressed in terms of minutes per foot drilled, when -using Kadco equipment, in comparison with the former method of drilling dry in a raise and drilling wet in a drift. Comparative dust counts were taken at Balmat, however, by the Metropolitan Life Insurance Co. to show the difference in the dust content of the air in which the operators worked when drilling dry, wet, or with the Kadco equipment.

Jan 1, 1935

By Óscar Cantorín

El presente texto describe las ventajas del sistema de relleno utilizado en la compañía minera Ares de Arequipa. La metodología del relleno se inicia en el tajo de una chimenea, la cual contiene las tuberías bicapa. Luego se conecta mediante un niple las tuberías de una sola chapa, y se instalan hacia el tope del ala del tajo que entrará en relleno. Entonces, se prepara una barrera con tablas y puntales en el límite señalado para rellenar, y la parte interior se forra con tela prolipropileno. Al estar preparado el tajo, se comunica al personal de Planta de Relleno el inicio de la operación, donde se hace una mezcla de agua y cemento para lubricar la tubería. Luego se procede a bombear la mezcla con las proporciones de diseño y un slump promedio de 8 pulgadas. El tajo de 60 m de longitud, se rellena hasta en 3 etapas, ya que las tuberías son recuperadas en su totalidad y finalmente el relleno queda a 0.5 m del techo de la labor. Entre los principales beneficios de este tipo de relleno tenemos que: no tiene excedente de agua, no necesita sistema de drenaje, permite la continuidad del minado ya que no es necesario esperar más de un día para reiniciar las operaciones, recuce el costo del relleno con la disminución de cemento y prolonga la vida de la cancha de relaves.

Sep 13, 2001

By W. Randolph Van Lewis

In determilling the relative rate and in fi~lding the point where different inlpurities containecl in copper-matte are eliminated during the process of a converter-blow, the follo~ving results were obtainecl : A converter was selected which was starting on its sccolld charge. The first charge after lining had finished its copper " hot," and conseqaently no copper was adhering to the sides of the lining. All the copper and granulated slag from the previous charpc mcrc dumped, thus removing ally possibility of " salting " the matte to be tested. The coliverter worked fast and well during the entire test. Periods of ten minutes were selected. The converter mas brought from the stack to secure each sanlple of matte to be

Jan 1, 1904

By R. N. Lambert

This chapter discusses the evolution of high-speed shaft sinking in the South African goldfields. Whether we are talking of an additional shaft at an existing mine or the opening of a new mine, the increasing depth of the ore-bearing reef and the unremitting inflation of costs have provided the compelling incentive to shorten the time taken to sink a shaft and start earning revenue. The high costs of sinking a modern shaft system in South Africa are indicated by the recent example of a deep-level mine in the Orange Free State where the cost was nearly $22!42 million. This was for a single large shaft of 33 ft 6 in. diam (in all cases, shaft diameters refer to the finished diameter of the shaft, e.g., inside the concrete) and 7600 ft deep with a prestressed concrete brattice wall dividing the shaft into upcast and downcast compartments. Higher costs and the consequent demand for increased tonnages, deeper shafts with higher rock temperatures, which necessitate highly sophisticaled ventilation and refrigeration requirements, have all accentuated the importance of time in a shaft-sinking operation. Rectangular shafts with their simple design and comparatively reasonable sinking speeds remained popular for many years until greater mining depths combined with a host of the other allied problems inevitably led to changes in shaft design. Circular shafts appeared to offer many advantages, particularly when considering ventilation, strength, mechanization, and sinking through bad ground and heavily watered zones. However, these advantages were largely offset by the slow rate of advance necessitated by the need to stop sinking in order to line the shaft. The development of the curb ring which enabled lining to take place above the bottom of the shaft and the use of multideck stages allowing sinking and lining to be carried out concurrently resulted in a major break- through. Rectangular shafts, which are still popular elsewhere, have been superseded in South Africa by circular shafts which are almost without exception the only shafts sunk in our goldfields today.

Jan 1, 1970