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The present study refers to passive systems for the treatment of acidic liquid effluents emanating from mixed-sulphide mines by means of an-aerobic compost wetlands. An effort was made for the thermodynamic study of the chemical systems that are involved in the reactions during the simulation of this specific system using laboratory columns and a pilot scale application. The substrate used was a mixture of cow manure, a high alkalinity organic substrate and chestnut woodchips, while the synthetic solutions prepared for the laboratory experiments contained the three basic metal contaminants i.e. Fe, Zn and Mn. The precipitation mechanism of the contained metals and the form in which these are precipitated was therefore investigated by constructing the equilibrium phase diagrams (Eh-pH diagrams) of the Me-S-C-H2O systems. Based on the experimental results from laboratory and pilot scale tests the stability conditions of the chemical species taking part in the aqueous solutions were also determined and verified with the thermodynamic data available. The thermodynamic analysis of the system was performed for ambient temperature, which is the prevailing temperature on field constructed compost wetlands. Results were further validated with the results obtained by the application of a five step sequential extraction procedure in the remaining substrate in order to determine the form in which the metals were precipitated.

Jan 1, 2006

By Masahiro Lnoue, Kenichi Uchino

Airflow velocity vectors by a forcing auxiliary fan at a heading face were measured in an actual size model gallery and an actual mine. The location of an outlet of ventilation duct gives significant effects on the airflow at the heading in the gallery. It was also found that there were several stagnated regions which may have danger of methane accumulation. The flow were also examined using the visualization technique by laser light in a reduced scale model. The flow in reduced scale model showed similar behavior to those observed in actual size galleries. The air velocity at the outlet has no significant effect on the airflow. It was found that a region to be ventilated by the direct flow of the exhaust fan is limited to a relatively short distance but a secondary flow region is generated near the heading face. CFD ( Computational Fluid Dynamics ) method was also developed to examine the airflow. The calculated results coincides with those measured by actual and reduced scale models. It is concluded that the CFD is useful tool for the analysis of ventilation at the headings.

Jan 1, 1997

Improve the performance of waterjet nozzles used for water-jet-assisted cutting to optimize rock cutting efficiency. Approach The performance of a longwall shearer equipped for water-jet-assisted cutting was evaluated during an earlier study (Tech News No. 277). Waterjet nozzles were used to direct the solid streams of water that impacted the rock near the tip bits. The maximum water pressure that could be delivered to the nozzles was about 6,000 psi. Due to the "break up" of the solid stream of water, some of this pressure was lost before the water reached the rock. The pressure could have been increased by moving the nozzle closer to the bit tip but) moving the nozzle too close increases the possibility of damage to the nozzle. Study Results A test apparatus was built to measure water pressure at the location of water jet impact (see illustration). The target, a tungsten carbide plate with a 0.013 inch diameter orifice, was placed at the location of water jet impact. A pressure transducer, used to monitor impact water pressure, was positioned under the plate. Water pressure at the nozzle was maintained at 6,000 psi. The distance between the nozzle and target was varied from 2 to 5 inches.

Jan 1, 1988

By K. O. Bennington

Thermodynamic properties were determined by the Federal Bureau of Mines for lithium metasilicate (Li2Si03) and lithium disilicate (Li2Si205). Their enthalpies of formation were investigated by hydrofluoric acid solution calorimetry. The standard values are ?Hf°298 -393.8 ± 0.8 kcal/mole for Li2Si03, and ?Hf°298 -611.8 ± 1.0 kcal/mole for LiSi205. Enthalpy increments above 298 K were measured by copper-block drop calorimetry from 298 to 1,404 K for Li2Si03, and from 298 to 1,281 K for Li2Si205. Low-temperature heat capacities were determined adiabatically from 6 to 305 K for Li2Si205 only. The derived standard entropy is S°298 = 29.20 ± 0.10 cal/deg-mole. The various experimental data were combined with other data from the literature, and resulting properties of ?Hf°, ?Gf°, and log Kf were tabulated as a function of temperature.

Jan 1, 1976

By Robert D. Saltsman

Two modes of seal application were identified, and promising state-of-the-art seals of both types -shaft and drum -were selected for initial rating by non-destructive testing. Only one shaft seal survived the initial test, and a search was made for other candidate seals including new seals. One new type of seal was found that gave promising enough operation, as both a shaft and drum seal, to be recommended for installation in prototype wet-head machines.

Jan 1, 1975

By V. A. Ivanova

Modification of hydrophobic part of carboxylic collector molecule is an upcoming trend for producing new reagents and changing its flotation properties such as activity, selectivity, sensitivity to hardness salts that inevitably present in the pulp liquid phase in the processing of ores containing calcium minerals. A wide range of apatite collectors ? monoalkyl ethers and monoalkylamides of dicarboxylic acids ? succinic, o-phthalic and maleinic acids have been synthesized by the addition of aliphatic alcohols and amines with various hydrocarbon radical value (from ?11 to ?16) to anhydride of the corresponding acid. Using computer modeling based on ChemBio 3D program of specialized complex Chem?ffice the calculation was carried out of charge distribution on atoms, energy parameters of molecules for investigated compounds. Calculated values of absolute hardness (?=6.75 ? 12.36) and absolute electronegativity (?= 5.67 ? 8.90) of the reagents showed that monoderivatives of dicarboxylic acids refer to the ?hard? type of bases. The degree of a charge transfer during calcium compounds formation of considered collecting agents (?N=0.009 ? 0.143) has been computed. Dissociations, micelle formation in solutions of these reagents and its hydrophobic and collecting properties were investigated in respect to apatite. Dependence of bulk, surface and collector properties on collector molecule architecture (double bond or benzene ring and non-ionogenic functional group in the structure of hydrocarbon radical) has been established. It is shown that experimentally determined dissociation constants (??a=5.16 ? 5.60 for succinic acid derivatives and ??a=3.32-3.78 for maleinic and o-phthalic acid derivatives) perfectly correspond to acidic properties predicted by computer calculations. Compounds of monoalkylderivative dicarboxilic acid have been determined optimum in composition and structure. The results of apatite flotation from apatite-nepheline ores of the Khibiny deposit (the Kola Peninsula) are presented here and show benefits of selected reagents. Keywords: monoalkylderivatives, dicarboxylic acids, reagents, microflotation

Sep 1, 2012

By L. B. Pankratz

High-temperature heat contents were measured for two praseodymium oxides and three terbium oxides. There were: Pr2O3 (298° to 1,600° K), PrO1.833 (298° to 1,050° K), Tb2O3 (298° to 1,600° K), TbO1.719 (298° to 880° K), and TbO1.812 (298° to 850° K). With the exception of PrOl.833, all results were regular. PrO1.833 had a small thermal anomaly at 760° K with an extra absorption of 380 cal/mole. The measured heat content values, tabulated smooth heat contents, and entropy increments are reported. Heat content equations were derived.

Jan 1, 1966

By Henry J. Welge

Laboortory apparatus has been devised which permits study of the displacement of oil from cores by water and by gas. The cores used contained interstitial brine as well as oil. Experiments were run to determine the comparative effect of varying the properties of the fluids used. No great effect was noted on the maximum displacement achieved. This observation made it unnecessary in initial work to use fluids in their exact reservoir conditions. Consequently, the displacements were run at near-atmospheric pressure in Pyrex glass equipment, using stripped crude oils. Introduction and Theory The chief object of this work has been to determine the efficiency of gas and water as primary agents for displacing oil from reservoir rock under laboratory conditions in which capillary phenomena were predominant. To this end the maximum displacement of oil from cores has been ascertained. This maximum displacement may not be equal to the maximum displacement from a reservoir; but it will be a close approxirnation to it sometimes, and other times the laboratory information will be useful in reservoir engineering predictions. It is] believed that the laboratory experimental maximum represents the upper limit for the reservoir recovery. The experiments were carried out by obtaining cores of interest from the reservoir, and filling the pores with interstitial brine and oil with the restored state tech- nique.1 Then the oil was displaced from the core as described later, either by brine from below, or by gas from above. The former type of displacement suggests analogy to production by water drive, but not to water flooding, for reasons discussed below. The latter type of displacement is believed to simulate production by gas cap displacement. The displacements were performed by what may be termed the capillary-pressure method. The cores are placed in capillary contact with an oil-wetted membrane which has very small pores (about I micron in diameter). Pores of this size will transmit oil but Prevent the Passage of gas or water, unless the Pressures used are higher than the capillary Pressures employed in this work. Accordingly, use of the membrane makes it possible to apply a capillary pressure differential between the displacing phase and the oil in the core. AS in the displacement of brine toward that condition of oil and water distribution existing originally in the reservoir,' it may not always be desirable to reduce the oil saturation in this experiment to an absolute minimum. With reservoirs having small productive closure, it is preferable to evaluate and use a displacing pressure no higher than the capillary pressure, Ap, which will ultimately become available for displacement in the reservoir. This pressure may be calculated from a knowledge of the density of the oil-in-place, do, the density of the displacing phase, dl, and Ah, the vertical distance between the section of the

Jan 1, 1949

By Seth C. Schaefer

The Bureau of Mines has determined the standard Gibbs energies (AGf°) of CoS1.035 (cobalt sulfide) and Ni2.515S2 (nickel sulfide) with high-temperature galvanic cells using stabilized Zr02 (zirconia) as the electrolyte. Potential measurements were obtained for the cell Pt, CoS1.035, CoO, S02(g, 1 atm)//Zr02//02(g, 0.0114 atm), Pt, with the overall cell reaction C0S1.035(c) + 1.535 02(g, 0.0114 atm) = CoO(c) + 1.035 S02(g)¬ These results, combined with the best available data for ?Gf° of CoO and S02 from the literature, give the standard Gibbs energy of formation of CoS1.035 for the reaction Co(c) + 0 5175 S2(g) = CoS1.035(c) ?Gf° = -38.890 + 18.87 x 10-3T ± 0.185 kcal/mole (866.0 - 1,104.9 K), where temperature (T) is expressed in kelvins. Similar measurements were obtained for the cell Pt, N12.515S2, NiO, S02(g, 1 atm)//Zr02//02(g, 0.0122 atm), Pt, with the overall cell reaction Ni2.515S2(c) + 3.2575 02(g, 0.0122 atm) = 2.515 NiO(c) + 2 S02(g). Combination of these results with data for ?Gfo of NiO and S02 from the literature yields the standard Gibbs energy of formation of Ni2.515S2 for the reaction 2.515 Ni(c) + S2(g) = Ni2.S1SS2(c) ?Gf° -65.377 + 24.67 x 10-3T ± 0.541 kcal/mole (968.6 -1,053.7 K).

Jan 1, 1981

By T. H. Yang, K. K. Lee, Z. Z. Liang, C. A. Tang, L. C. Li, Y. Tsui, L. G. Tham

Abstract: A series of numerical tests of hydraulic fracturing in heterogeneous rocks were performed to investigate the influence of pore pressure magnitude and gradient on initiation and propagation of tensile fractures. The numerical tests were run with a Rock Failure Process Analysis code, F-RFPA2D, incorporated with a Flow-Stress-Damage coupling model (FSD). To investigate the influence of pore pressure magnitude on fracture behaviour, “pinch-off” breaking tests, originally employed by Bridgeman to investigate the effective stress law for tensile fracture in a uniform pore pressure field, were numerically modelled. In another numerical test, a double-notched sample, with fluid pressure in one notch while keeping the other one open to the atmosphere, is numerically extended to investigate how the fluid flow direction or the pore pressure gradient will influence the fracture behaviour. The simulation results show that fracture is strongly influenced by both pore pressure magnitude and pore pressure gradient. Keywords: seepage mechanics; heterogeneous; pore pressure; numerical simulation; failure process ZUSAMMENFASSUNG: Um den Einfluss der Wasserdruckgroesse der Oeffnung und der Porisitaet auf den Bruchentstanden und Verbreiten der Tension von Gebirgen zu beurteilen, wurde viele nummerische Pruefungen auf den hydraulischen Bruch in dem Gebirgen aufgenommen. Diese Pruefungen wurden mittels der Analyse- Software F-RFPA2D und Flow-stress-Damage Coupling model ( FSD) durchgefuehrt. Um den Einfluess der Wasserdruckgroesse der Oeffnung auf den Bruch zu beurteilen, wurden auch Bruchpruefung und nummerische Analogexperimenten gemacht, und dadurch wurde die ganze Phase der Bruchentstanden und Verbreiten wiedergezeigt, und die Ergebnissen ergeben sich, dass die Wasserdruckgroesse der Oeffnung und der Porisitaet sehr viel auf den Bruchentstanden und Verbreiten der Tension von Gebirgen beeinfluessen. Schluesselwoerter: Durchlaessigkeit , ungeleichmaessig, Wasserdruck der Oeffnung, nummerische Analog, Zerstoerungspahse Résumé : Une série de simulations numériques a été ménée pour analyser l’influence de la grandeur de la pression de pore et du gradient sur la naissance et la propagation des fractures de tensions par le biais de la simulation numérique des fractures hydroliques dans des rochers hétérogènes . Le logiciel F-RFPA (Rock Failure Process Analysis code ) intégrant FSD ( Flow-Stress-Damage coupling model ) y a été employé. Les résultats des simultations montrent tout le processus de la naissance et de la propagation des fractures sous la pression de pore. Ces résultats nous ont permis de constater que la grandeur de la pression de pore et le gradient exercent une influence importante sur la naissance des fractures dans les rochers et sur leur mode de propagation . Mots de clé : le mécanisme de transfusion ; l’hétéogénéité ; la pression de pore ; la simultation numérique ; le processus destructif

Jan 1, 2003

By B. M. Larsen

AN increasing amount of attention is being paid to the possible influence of oxygen, in its several modes of occurrence in steel, upon some of the properties of the metal; but clearly investigations along this line are unlikely to yield significant results until reliable analytical methods for the determination of oxygen have been established. This paper presents some results of a study of an improved Ledebur method which aims to determine a definite portion of the oxygen; namely; that which presumably is present in diffusible form in the. solid steel. These more or less preliminary results lead us to believe that the oxygen so determined has some significance; their presentation at this time will, we hope, stimulate discussion of, and focus attention upon, certain rather neglected aspects of the problem. Considerable work has been done recently on methods of estimating inclusions and on the vacuum-fusion method for oxygen; with results which, however, are of somewhat questionable significance. It is commonly presumed that the oxygen in a bath of molten steel in a furnace is present partly as a separate phase consisting of suspended particles of oxides or silicates, partly in solution, the latter being probably the more important. Upon addition of a deoxidizer, it reacts with some portion of the dissolved oxygen and precipitates it as additional suspended particles; the oxygen not eliminated in this way, which remains in solution in the liquid steel, may be regarded indifferently either as dissolved oxygen or as dissolved FeO. When the steel is poured, some of the suspended particles rise towards the surface, others remain trapped in the finished steel, appearing as nonmetallic inclusions in amounts corresponding usually to about 0.01 to 0.03 per cent 02 in the steel. The dissolved oxygen may be partly eliminated as CO during freezing of the ingot, but some remains either in solution or in part precipitated as FeO. Finished steels may thus contain oxygen in several forms: (1) In non-metallic inclusions which are probably quite insoluble in the solid metal at all temperatures; (2) in solid solution which at lower temperatures may be supersaturated; (3) in FeO particles produced by relief of this

Jan 1, 1932

By T. E. Watkins, M. D. Nelson

A method of determining the lime content of drilling muds proposed by Battle and Chaney* has been examined both in the Field Research Laboratories of Magnolia Petroleum Co. and in field drilling operations. This proposed analytical method is condensed as follows: Titrate one ml of mud and one ml of mud filtrate, each with 0.02 N H2SO4, to the end point with phenolphthalein. The volume of acid in ml required for the mud titration is recorded as Pm and that of the mud filtrate titration as Pf Calculation of the lb lime/bbl mud is accomplished by use of the formula, lb lime/bbl mud = 0.6 (Pm - 1.3Pf) - 0.6 The analytical procedure outlined by Battle and Chaney was found to be quite satisfactory when reasonable precautions are used in mud sampling technique. Calculation of lime concentration by the method proposed in the above publication, however, has given values that varied as much as 100 per cent from the known lime content, for muds of either high or low solids concentration. By use of a formula, lb lime/bbl mud = 0.26 (Pm-F1.Pf), based on chemical equivalents of acid required for titration, both laboratory and field data have been satisfactorily correlated with the known amounts of lime present in the muds. In this formula a correction, F1, or volume fraction of liquid in the mud, is made for the solid content of the mud. Pm and Pf * Paper on "Lime Base Muds," presented by J. L. Battle (Humble Oil and Refining Co., Houston, Tex., and P. E. Chaney (Sun Oil Co., Beaumont Tex.), at the 1949 Spring Meeting of the Southwestern District API Division of Production, Dallas, Tex. The analytical procedure has also had wide distribution in a trade journal, Kembreak, published by the Accuracy Rig and Tool Co., Houston, Tex, †Derivation of equation lb/bbl — grams/350 ml 1 ml 0,02 N acid = 0.000741 grams of lime 1 ml 0.02 N acid/ml lime suspension = 0.26 lb of lime bbl lb of lime/bbl = 0.26 (Pm -F1, Pf ) have the same significance as in the Battle and Chaney equation. Table I shows typical data employing both formulas in calculating the lime content of various lime muds. This suggested procedure ignores lime which is in solution in the mud. The solubility of lime in water, normally about 0.5 lb per bbl, is greatly decreased by the addition of caustic soda, and, in a lime mud, it is probable that the concentration of dissolved lime is of the order of 0.1 lb per bbl. Such an amount of lime can be ignored, since it is within the range of accuracy of the method.

Jan 1, 1950

By J. Yue

"Mount Milligan mine is located in northern British Columbia. The concentrator employs conventional SABC grinding circuit with bulk sulphide flotation processes. Commissioning started in September of 2013 and nameplate production of 60,000 TPD was reached in the fourth quarter of 2015. As is typical with many mill ramp ups, bottlenecks developed as throughput increased. Since then, plant modifications and new control philosophies in the comminution and flotation circuits have been implemented and evaluated. The mine-to-mill collaboration played a key role in reaching target throughput rates by improving blast fragmentation and implementing temporary pre-crushing. Results of the projects as well as ongoing challenges/bottlenecks and solutions will be discussed.IntroductionMount Milligan Mine is a copper-gold producer located approximately 253 km northwest of Prince George in British Columbia. Production commenced in September 2013 and reached nameplate capacity of 60,000 TPD in December 2015. Average head grades for the mine life average 0.18% Cu and 0.39 g/t Au.Circuit DesignOriginal process design began with run-of-mine ore from the pit crushed through a 60-110 gyratory crusher, conveyed to a live ore stockpile and fed to the mill via four variable apron feeders. The concentrator circuit employs SAG mill - Ball mill - Pebble Crusher (SABC) grinding configuration to grind the ore down to a target P80 of ~200µm. It is then fed to two parallel trains of flotation tanks, each consisting of five 200 m3 tank cells with the first two being roughers and last three being scavengers. Concentrate streams from roughers and scavengers are separately reground with a closed circuit Tower mill and two open circuit ISA mills operating in parallel, respectively.Three stages of cleaners upgrade roughers/scavenger products to 25% Cu followed by a cleaner scavenger stage. The final concentrate is then thickened and filtered to approximately 9% moisture and shipped off site (Figure 1)."

Jan 1, 2017

By Charolett Hayes, A. L. Russell, Anthony J. Bednar, Jared Smith, Valentine A. Nzengung, Stephen L. Pilcher

The manufacture of Energetics Materials (EM), including maintenance and demilitarization of munitions causes dangerously high levels of explosives residues to be harbored in building features. The two commonly approved methods of decontaminating energetics contaminated equipment and building features are thermal treatment and steam washing. The current regulatory environment is generally becoming more stringent and unfavorable to thermal and steam decontamination because of their adverse impact on air, soil, and water and their ineffectiveness to completely remove accumulated energetics from foundation cracks, internal and external piping, voids in walls and ventilation systems, and internal cavities of fixed equipment. However, chemical destruction of energetics, especially high explosives, is gaining acceptance as a safer, cost-effective and environmental friendly alternative to thermal and steam decontamination. Organic explosives, including nitramines and nitrate esters are oxidized organic compounds that are susceptible to chemical oxidation and reduction reactions. Under suitable conditions, a chemical reagent consisting of sulfur-based bulk reductants (neutralent) commercialized as MuniRem generates highly reactive free radicals that very rapidly degrade many energetic compounds to innocuous end products while stabilizing metals as the insoluble metal sulfides.

Jan 1, 2016

By Ricardo Huancaya

El presente texto describe el plan estratégico desarrollado por La Cia Minera Coimolache para mejorar su sistema de producción, rentabilidad, aceptación social y manejo ambiental. Para ello, se desarrollan tres áreas: asuntos sociales, medio ambiente y planeamiento mina, generando la sinergia necesaria y así tener un proyecto minero sostenible.

Oct 21, 2015

By Ken Musgrave

"What Most Effective Management Does?It must satisfy the demands, of three groups of people: owners, employees and the public.OwnersOwners want profitable operations that will pay them a return on their investment, plus operations managed for long life. Many owners are also concerned with employee's well being and their company's public image.EmployeesJob security and a good income are probably still the most important demands, however, as time goes by, employees are also demanding more involvement in safety issues, working conditions, and even how work is done.The PublicThe public requires acceptable environmental standards, as well as enjoying the prosperity supplied by a successful operation.How are Mines Managed?Most mines are managed very traditionally. The basic credo is that the managers make the decisions, and the hourly, and junior salaried employees do what they are told. Clearly this is the extreme case, epitomized by the long service shift boss who might say ""It took twenty-years to become a shift boss, and no miner is going to tell me what to do"" .There are some exceptions, two notable ones being Campbell-Chibougamau, and T.G.S. (now Kidd Creek Mines) which, in very different circumstances, decided on a more participative style.Campbell-Chibougamau, having closed down due to unprofitable operations, reopened, using a team structure with working leaders, and a system for sharing gains against cost targets with employees. Although the system has some problems, and development miners are bonused conventionally, this has been a basically successful program.Texasgulf Sulphur, a company with a history of non-union operations, and a participative management style, made a corporate decision to operate their Kidd Creek Mine in the same way. The orebody was rich enough to allow them the luxury to do this, but they have never had a strike, so perhaps they have more than saved the cost of the benefits and salaries they needed to pay. They also reward employees with a stock distribution scheme based on service and earnings."

Jan 1, 1985

The Coal Corporation of New Zealand Ltd (CoalCorp) is the largest coal producer in New Zealand, with extensive properties in both the North and South Islands. CoalCorp's North Island operations are kilcmetres to the south of Auckland. opencasts, are located in the catchment wildlife, historical and scenic values. in this catchment is the single most mining operations. centred on Huntly, a town some 80 Five coal mines, four of which are of Lake Waahi, a lake with significant The discharges of mine lodgement water important environmental constraint on Throughout New Zealand the use of water is controlled by a statute called the Water and Soil Conservation Act 1967. All industrial water users are required to hold Water Rights, which are in effect licences to take, use, dam, divert or discharge water. Water Rights are obtained through a legally defined process and any potentially affected party has the per to object to their granting. A special tribunal hears the evidence for and against an application, and issues its decision, which is reviewable in a higher court on Appeal. Rights, if granted, are issued subject to conditions and, in the case of mining discharges, limits would be set on flaw rate, suspended solids concentrations, turbidity, pH and the concentrations of any potential toxicants. This paper presents a case study of an integrated, catchment wide water management plan for Lake Waahi, that was prepared by the author, and others while the author was in the employ of CoalCorp, and its predecessor, State Coal Mines. The author is grateful to CoalCorp for their permission to submit this paper.

Jan 1, 1988

By D. A. Stanley

The Bureau of Mines has developed a simple titration technique for determining the points of zero charge (PZC) on minerals. The technique consists of titrating a mineral slurry with the potassium salt of polyvinyl sulfuric acid (PVSK) in the presence of an indicatory dye and a positively charged polymer. Values obtained by this simple method are in good agreement with values found in the literature.

Jan 1, 1982

By H. H. Schrenk, W. P. Yant, P. H. Mautz

"In a study of the chemistry and pathology of chronic benzene poisoning, which was conducted cooperatively by the United. States Bureau of Mines, the Barrett Co., and the producers of benzene, it was necessary to make quantitative determinatious of the abzorption, distribution, and: fate of benzene in the organism. Although methods for determining benzene in relatively large amounts were available no satisfactory method was found for removing and determining the small amounts that are present in the tissues or excretions after exposure to conditions which ultimately cause chronic poisoning. This no doubt accounts for the lack of information in the literature on this particular phase of benzene poisoning.The writers have found in work that will be described in a subsequent publication that the amounts of benzene present in the tissues and excretions under conditions of exposure which produce chronic benzene poisoning arc of the order of a fraction to a few milligrams per 100 grams of tissue. This report describes a method developed and found satisfactory for these determina¬tions.RÉSUMÉ OF PERVIOUS METHODSA method for the determination of benzene in tissue was developed by Joachimoglu. 5 In the Joachimoglu procedure the ground organs are mixed with water and acidified with diluted sulphuzic acid, and the benzene is distilled into a receiver containing carbon tetrachloride. The benzene is nitrated in the carbon tetrachloride, the carbon tetrachloride evaporated, the acid mix¬ture neutralized, and the dinitrobenzene extracted with ether. After removal of the ether the dinitrobeuzene is determined gravimetrically. Joachimoglu reports that this method is about 55 to 60 percent quantitative."

Aug 1, 1935

By Lawrence F. Johnsen

Six case histories are presented in which tall, slender high rises are supported on high capacity minicaissons. The recent development of a high strength rebar cage has resulted in compressive loads of up to 3400 kips on 24 inch diameter minicaissons. Provisions in the pending NYC building code will allow borehole video inspection in lieu of load testing. The ?new? technology results from the marriage of several well established methods: rotary duplex well drilling, high capacity micropiles and high capacity reinforced concrete building columns.

Jan 1, 2007