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A novel pressure leaching process for platinum group metal (PGM) feedstocks is described. The process is particularly well suited for treatment of ores or concentrates that are too low grade for economic processing by the conventional smelting/leaching process. Operating conditions have been identified under which gold, the PGM's and the base metals dissolve simultaneously in a pressure leaching autoclave. The product of this leaching process can then be treated by one of several flowsheets, of which the preferred will likely involve solid/liquid separation, followed by precipitation (or adsorption on activated carbon) of gold and the PGM's, followed by copper solvent extraction/electrowinning. Depending on the concentrations of nickel and cobalt, the copper raffinate would either be partially recycled to the autoclave to allow NilCo concentrations to build up, or it would proceed directly to a Ni/Co refinery. This paper deals with the pressure leaching process and the recovery of gold and the PGM's from the pressure leach product.

Jan 1, 2000

By A. Lawson

"Continued and expanded use of underground diesel-powered equipment is considered desirable in order to achieve necessary production capability, particularly when coal becomes increasingly in demand as an energy source. Although diesel engines are derated for underground use, concern has been expressed in many quarters regarding the health effects of worker exposure to diesel-generated particulate and NOx emissions. This concern will increase as Canadian diesel fuel quality becomes heavier and with higher sulphur content. This could result in a requirement to increase ventilation rates by 50%.This paper describes the results of studies of various approaches designed to reduce diesel emissions. Two major approaches have been followed: fuel modification, and emission control hardware development. The results of progress in the development of these approaches will be described.Fuel modification includes the application of water/diesel and methanol/diesel fuel emulsions to the engine. Details of the techniques employed in this approach will be described, together with the effects on diesel emissions. (The paper is concerned with the emission aspects only, not the possible major engine modifications and/ or substitute materials of construction for 100070 methanol.) Use of methanol has the added advantage of acting as a diesel fuel substitute and extender, and there are expectations that underground diesel engines could eventually operate on close to 100% methanol fuel, thereby eliminating particulate emissions. The results of emission control hardware development will also be presented and will include the effects of catalysts, water scrubbers, exhaust filters and exhaust gas recirculation techniques on emissions. A combined systems approach employing a number of these components appears to be the most viable method of controlling the complete array of diesel emissions.This work should culminate in a better understanding of the costs involved in employing fuel modification or emission control hardware relative to the costs of increased ventilation which mpy be necessary to maintain a safe working environment for the underground worker."

Jan 1, 1981

By R. W. Van Dolah

The Bureau of Mines t.ced its investigations into sympathetic detonation of ammonium nitrate (AN) and ammonium nitrate-fuel oil (AN-FO) to define the scaling law for safe separation from detonating AN-FO. Both missile- and non-missile-producing AN-FO donors, weighing up to 5,400 pounds, were employed with acceptors of the same size. The usual cube-root scaling law was not confirmed; exponents for the relationship S = f(Wx) for AN were 0.51 with non¬missile-producing donors and 0.61 for missile-producing donors. For AN-FO an exponent of 0.80 was indicated in the missile-producing case. AN-F0 in polyethylene bags appeared somewhat more easily initiated than bulk AN-FO. The efficacy of barricades in protecting AN charges was investigated. detonation distances were reduced from one-third to one-seventh when filled barricades were employed. The investigation was extended to dynamite with both types of donors. With 1,600-pound missile-producing donors and an equivalent weight of dynamite, initiation would be expected in 50 percent of the trials at 167 feet. The corresponding value in the non-missile case was 67 feet. The data developed in this program of sympathetic detonation will allow the development of a rational set of safe separation distances for AN, AN-FO, and explosives.

Jan 1, 1966

By P. Chris Pistorius

"Ilmenite smelting involves partial reduction of iron oxide from a slag consisting mainly of T1O2, T12O3 and FeO, yielding as products iron (with approximately 2% carbon) and titanium slag. Slag purity requirements preclude any fluxing additions, and the aggressive nature of the slag necessitates a furnace freeze lining. Large departures from thermal and chemical equilibrium hold in the smelter, with possible implications for process stability. The slag is approximately 150K. hotter than the metal, which means that the metal temperature is below the slag melting point; this difference in temperature has been shown to lead to formation of a solid TisOs-rich layer between the slag and metal. Recent equilibrium measurements have confirmed that the slag and metal are not in chemical equilibrium either, with significantly more reducing conditions in the metal than in the slag. After solidification, the pseudobrookite slag structure is metastable below approximately 1400K, and may transform upon slight oxidation.IntroductionThe natural mineral ilmenite is the main source of titanium, which is mainly used to produce Ti02-based pigments. Ilmenite has the ideal formula FeTiC>3, but natural minerals can be partially oxidized (to contain some Fe3+), and typically contain MnO and MgO as well, together with associated silicate minerals. Smelting is one of the methods to upgrade ilmenite for subsequent T1O2 pigment production; smelting involves partial reduction of FeO to form metallic iron as a byproduct and titanium slag as the main product. Reduction is typically controlled to yield a slag which contains around 10% FeO, 85% (Ti02+Tij03) and 5% impurity oxides (mainly MnO, AI2O3 and S1O2). An example of a typical average slag composition from reduction of South African ilmenite is shown in Table I. As this indicates, a significant side reaction is reduction of some T1O2 to T12O3. The relative extents of reduction of FeO to Fe and of Ti02 to T12O3 are such that the slag stoichiometry is close to that of the pseudobrookite phase [1]. Pseudobrookite has the structure AB2O5 (where ""A"" and ""B"" are different cation sites); the phase which makes up the bulk of solidified titanium slag has the AB2O5 structure and stoichiometry [2], and can be viewed as a solid solution of FeTi20s, T13O5, ÌçÔÀ2è5, MgTi20s, AI2T1O5 and C^TiOs [1]. This solid-solution phase is referred to as ""pseudobrookite"" or ""M3O5"" in this paper."

Jan 1, 2012

By M. Gaft, G. Panczer, R. Reisfeld, L. Nagli

Laser-induced luminescence and breakdown spectroscopy methods appear to be a good tool for real-time evaluation of dolomite content on moving belt. The distinctive feature for time- resolved luminescence is Dy3+ emission in apatite, which is excited by 251 nm laser light and detected with delay time of 5 ms and gate width of 1 ms. The distinctive features for breakdown spectroscopy are 604 nm line of F and P in apatite and 518 nm line of Mg in dolomite. The representative sampling of more than 200 pebbles has been studied by both methods. By luminescence method 100% of dolomite will be identified, while approximately 15-20% of apatite with extremely week Dy3+ luminescence may be mistakenly counted as dolomite. By breakdown spectroscopy the identification is 100% correct both for dolomite and for apatite.

Jan 1, 2002

The National Institute for Occupational Safety and Health (NIOSH) conducratory and field tests to evaluate the effectiveness of dust collector bags for reducing dust liberation and operator exposure from a roof bolter?s dust collection system. The laboratory tests evaluated the bag?s effectiveness to contain dust and the effect on canister filter loading in both a bag and bagless condition. The dust emissions from the collector?s exhaust were also measured in each condition during laboratory testing and show that nearly 100% of the test dust fed into the collector was captured by the dust bags. Loading and pressure drop on the dust collector?s canister filter is greatly decreased when using the bags, enabling longer periods of drilling without filter removal/cleaning. The field results showed that, even though dust standards were met, respirable dust in exhausted emissions was reduced around the bolter. Laboratory and field results show that benefits from use of the bags are realized in all areas of operator exposure.

Jan 1, 2008

This brief resume of events, transpiring in Mexico, culled front the daily New York newspapers, since the last Bulletin-went to press, does not indicate any degree of improvement in the situation. RECORDS OF 217 MEXICO KILLINGS SUBMITTED BY AMBASSADOR FLETCHER Henry P. Fletcher, the American Ambassador to Mexico, called as the first witness before the Rules Committee of the House which has begun a preliminary inquiry into conditions in Mexico, which, it, is believed, will lead to a thorough and far-reaching investigation by a joint Senate and House Committee of the entire Mexican problem, submitted a list of the names of Americans officially known to have been killed in Mexico, a majority of them murdered in cold blood, since the overthrow of Porfirio Diaz by Maderoin 1911. The list contains 217 names and in comparatively few instances do the records show that arrests were made by the particular Mexican faction that happened to be in power where the crime was committed. In only one instance, that of John B. McManus, who was killed in March, 1915, was reparation made. It is significant that McManus was killed by Zapatistas, and Zapata officials apologized for the crime and paid to Mrs. McManus a voluntary indemnity of $20,000 in gold. Of the 217 persons listed as victims of the Mexicans, .137 perished since Carranza came into power. The list, it was admitted, is not complete. It was evident, says the New York Times, that the Ambassador considered the situation very serious.

Jan 9, 1919

By W. S. Sanner

A High Splint coal was carbonized in a low-temperature, fluidized-bed sys-tem to study the effects of thermal cracking on the products of decomposition. The coal was fluidized in recycle gas at 485° to 600° C, and the products were cracked at 600°, 700°, and 800° C in a bed of fluidized coke. Yields of tar, pitch, paraffins, and olefins decreased as carbonization temperature increased. Thermal cracking of the tar vapors produced the highest tar yields at 600° C, and light oil yield increased at cracking temperatures up to 700° C. At an 800° C cracking temperature, the yield of light oil decreased.

Jan 1, 1969

By A. D. Pienaar

The aqueous chemistry of niobium and tantalum compounds with hydrofluoric acid is a mature field of investigation. In contrast, very little attention has been paid to reactions of these compounds in non-aqueous environments. Similarly, reactions of elemental fluorine with niobium and tantalum compounds have received little more than cursory attention in literature. This work discusses the isothermal reaction kinetics derived from thermogravimetry, using a less redundant approach than is currently the standard. We also discuss the most likely kinetic models for this reaction.

Jan 1, 2012

By Frederick Laist

(Butte Meeting, August, 1913.) WHILE remodeling No. 1 section of the concentrator at the Washoe Reduction Works of the Anaconda Copper Mining Co. during the summer of 1912, for the purpose of ascertaining what additional metal recoveries could be made by improvements in concentration practice which had been developed by the staff of the Boston & Montana Reduction Department, at Great Falls, it was deemed advisable to carry on some experiments on the treatment of the regular mill tailings by roasting and leaching, to see whether the losses of metal values might not be still further decreased. In the course of these experiments about 5,000 tons of tailings were roasted, and of the resulting calcine about 200 tons were leached. The results were so satisfactory that it was decided to continue the work on a larger scale, particularly as regards the leaching end of the process, and construction work on an 80-ton roasting and leaching plant was accordingly commenced during the latter part of February, 1913, and is being pushed as rapidly as possible. 80-Ton Leaching Plant. This plant will consist of one 20-ft. roasting furnace of the MacDougall type, specially adapted to the work of roasting for leaching; two leaching tanks, .32 ft. in diameter by 12 ft, deep, together with the necessary solution tanks, air lifts, precipitating launders, etc. It has been decided to precipitate the copper from solution on scrap iron, so as not to hamper the roasting and leaching departments by any weakness that might develop in the precipitating department. It is, however, the intention to experiment with a number of different methods of precipitation ; for example, by electrolysis and by hydrogen sulphide.

Jan 7, 1913

By Gerald S. Cole

It used to be that a science/engineering presentation on "light weight" at a metallurgy conference, would relate to the materials science, processing, component fabrication and applications of aluminum, magnesium and titanium. Within the automotive industry, light weight now includes how to "lighten up", how to lightweight, or how to mass reduce vehicle components and systems. Increasingly stringent global emissions-reduction requirements require increasing vehicle fuel efficiency; mass reduction is an enabler to achieve this. While light metals certainly are the basis, a host of other materials can be used to optimize mass reduction while meeting vehicle performance, safety and cost requirements. New grades of ultrahigh strength steels and even nanosteels can be thinned down and save over 1/3 the mass vs conventional mild steels. A compacted graphite cast iron engine can be made lighter than an aluminum one. Aluminum components in vehicles were only castings; now aluminum stampings, forgings and extrusions are becoming more visible components of mass reduction. Lower mass high temperature polymers, and carbon fiber polymer composites now replace aluminum and steel. These materials often require specialized processing and manufacturing techniques to produce a component, including superplastically formed twin roll cast sheet aluminum and magnesium, and hot stamped/in-mold quenched steels. The assembly of hybrid structures requires unique joining/bonding, and corrosion-inhibiting techniques that might include sophisticated structural adhesives. This thinking "light" presentation, will conclude with a discussion of U.S. and Canadian government engineering and research support for mass reduction, including the proposed $148 M American Lightweight Materials Manufacturing Innovation Institute.

Jan 1, 2014

By M Phil Schwarz

"A CFD model for the gas-side of an impinging jet iron bath reactor has been developed to assist in the interpretation and design of oxidizing gas-melt reaction rate experiments. Heat transfer and reaction at the surface have been included. A free surface model, which solves for the liquid motion within the bath as well as the gas motion above the bath, has also been developed. This model also predicts extent and shape of the dimple formed on the liquid surface by the impinging jet. Both models have been run for conditions typical of jet impingement experiments using CO2 , H2O and O2• The main conclusions are• Results from the model for gas-side mass transport are in good agreement with the empirical correlation of Belton and Belton (1980)• Experimentally determined rates of decarburization by CO2 should be corrected for mass transfer because the experiments are often carried out under mixed rate control, eg for gas flow rate 10 L/min when the sulphur concentration is lower than 0.045• If the rate constant for oxygen reaction is greater than about 5 mol/m2.s.atm, it cannot be determined using a gas flow rate of 10 L/min or lower because of mass transfer control.• A cavity of depth 4.5 mm is predicted for a gas flow rate of 10 L/min and this substantially changes the flow field (and hence reaction rate) compared with a simulation in which the surface is assumed to be flat."

Jan 1, 1999

In presenting the paper, Mr. Davey quoted subsequent work which yielded k, at miscibility gap composition, of about 50.We can confirm the authors' findings for k j 300 for nearly pure tin to k 2 about 50 (average 47) from our own experience and from repeat experiments on materials described by the authors, at 1150°C.During laboratory-scale trials we also found confirmation of the authors' view that it is more difficult to reach equilibrium from the high-iron (in slag) side than from the low-iron (high-tin) side. Working from the high-iron side tends to yield results that point to a high k, leading to optimistic values of iron/tin ratio in final slags. In practice the smelting of a tin concentrate, unless it is exceptionally low in tin and high in iron, must yield initially a tin-rich slag and therefore equilibrium can only be reached from the "tinny" side.

Jan 1, 1967

Copper and gangue mineralogy constitute the most critical parameters for the hydrometallurgical processing and cost-efficient extraction of copper. Minor changes in copper-, rock-, or alteration mineralogy can severely impact the comminution efficiency, curing, agglomeration, acid consumption, copper extraction and PLS impurity loading. Further, copper leach operations, particularly in the southwestern United States, are increasingly challenged by a combination of low grades and semi-refractory copper. This paper discusses the metallurgical and economical benefits of continuous mineralogical analyses in order to establish and operate a mineralogical data base in copper leach operations. Troubleshooting for copper extraction, integration of process mineralogy into production forecasting, and process optimization will be illustrated with operational experiences from Chile and the United States.

Jan 1, 1999

By Don Conrad, Tom Friend, Bill Wiehagen, Lynn Rethi

On-the-job training (OJT) is a very common method of teaching job skills. Much of the training is done by experienced workers. This paper discusses small investments that can help improve the effectiveness of OJT. Effective OJT involves some structure and planning in the transfer of responsibility for task performance from the trainer to the novice. Assisting the OJT trainer could involve helping develop up-to-date job analyses and offering strategies for teaching and evaluating job skills. The scope of this paper addresses (1) organizational considerations supporting structured OJT, (2) general strategies for structuring OJT, (3) a typical approach for conducting OJT, (4) characteristics and duties of OJT trainers, and (5) limitations of OJT as a teaching method. Health, safety, and operational skills can be connected through training. Haul truck operator training is used to illustrate some of the concepts discussed in this paper.

Jan 1, 2002

By A. N. Brown

The importance of the minerals industry in the economy of the country is discussed, and the tremendous changes that have taken place over the past two decades, including the widespread application of computers and the use of mechanization, are outlined. A discussion of the future of the minerals industry points out that, with the rise in the price of gold, the life of the gold-mining industry can be expected to extend beyond that previously predicted, and that the demand for uranium, which has been depressed, is uncertain. As a result of the oil crisis, the demand for coal has increased and large expansion programmes are planned. These involve coal exports and the use of coal for the generation of electric power, for the production of liquid fuels, and for the smelting of metals. Technical challenges face engineers in every avenue of the minerals industry: in deep gold mines, underground coal mines, strip coal mines, and open-pit mines. Studies indicate that only one-third of the demand for trained mining and metallurgical engineers is being met and that the position is worsening. However, there are indications that the industry is succeeding in attracting more engineering students, and the supply is expected to improve. These efforts should be co-ordinated, expanded, and intensified. There is a need to ensure that sufficient teaching staff of the right calibre and experience are attracted to universities and technikons. The first degree course is comprehensive and basic, and specialization through post-graduate study should be encouraged. The influence of national service on the education and training of engineers is discussed.

Jan 1, 1982

By J. H. Douglas, A. F. Matheson

"The Hard Rock is the most easterly producing mine in the Little Long Lac area. The Company was formed in 1934 to develop a surface showing of gold in quartz made by a prospector, W. W. Smith, in 1931. Although some ore was eventually produced from this discovery, the principal orebody, hidden below 10 feet of muskeg, was found about 1,000 feet to the north by exploratory diamond drilling early in 1938 from the No. 2 shaft workings at the 250-foot level.Production started in 1938 and to January 1, 1947, 201,000 oz. gold had been obtained from 1,165,282 tons of ore mined and 869,397 tons milled. Of this ore about 15 per cent came from the development and mining of the original orebodies discovered at the surface. The remainder came from the ore found by the underground diamond drilling done in 1938. Of the latter ore, the Company estimated, at January 1st, 1947, only 140,000 tons remained. The orebody, therefore, contained approximately 1,100,000 tons.OREBODIES AND GENERAL GEOLOGYThe orebodies of the Hard Rock mine are of two main types: the quartz ore of the south and No. 1 shaft zones, and the sulphide ore of the north zone. The quartz ore consists of white quartz veins mineralized with sparse, fine, light-coloured pyrite, or, less commonly, nests of coarse, crystalline, light pyrite. A little tourmaline, scheelite, pyrrhotite, chalcopyrite, arsenopyrite, and native gold are also present. Native gold occurs in a few places in quartz veins in exceedingly rich cemcentrations, apparently where there are large, light-coloured, pyrite crystals of imperfect form. The ore of the north zone is massive pyrite with arsenopyrite and in places pyrrhotite. Many short irregular quartz veins, from a few inches to 2 feet in width, are also present, but the quartz forms a very small percentage of the whole. The veins may be flat to vertical, and sulphides on one or both sides replace the host rocks. The gold is closely associated with the sulphides . The quartz is commonly barren except where it contains sulphides or along the borders of the sulphide ore zone where native gold is not uncommon in quartz stringers."

Jan 1, 1954

By R E. McIvor, K M. Bartholomew

Classification system efficiency (CSE) is a simple, powerful metric that provides a comprehensive measure of classification system performance. CSE directly quantifies the amount of coarse solids in the mill, and as a result, also directly quantifies the percentage of mill power being used effectively. In this manner, it is an effective, practical grinding energy efficiency metric.Three independent variables drive CSE: circulating load ratio, sharpness of classification, and classifier bypass. Due to practical downstream constrains on per cent solids, improvements realised by increasing circulating load reach diminishing returns as sharpness of classification and bypass deteriorate in the most commonly used classification device, the hydrocyclone. This combination of effects leads to the use of CSE, and its relationship to operational economics, as an objective circuit optimisation criterion.Its simplicity in measurement makes CSE a useful tool for the plant metallurgist, and it is not subject to a great amount of experimental error. CSE provides the plant operator a fast, simple, and effective means to evaluate the performance of the plant classification system. Improvements in CSE relate directly to circuit throughput and energy efficiency. This paper, through description and plant case studies demonstrates the power and utility of this emerging grinding system optimisation metric.CITATION:Bartholomew, K M and McIvor, R E, 2013. Classification system efficiency - a comprehensive closed-circuit grinding optimisation metric, in Proceedings World Gold 2013 , pp 389-394 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Sep 26, 2013

Load transfer capacity and failure mechanism of a fully grouted bolt installed across joints in shear is evaluated both experimentally and numerically in five types of bolts (low strength steel, rebar bolt and high strength steel). The strength of the concrete, bolt profile configuration, bolt mechanical properties and bolt pretension load play significant influence on the shear resistance, shear displacement and failure mechanism of the reinforced medium. Failure location moves towards the bolt joint intersection due to the increasing shear load, shear displacement and axial load developed along the bolt. Finally bolt failure occurs as a result of the induced axial and shear stresses acting between hinge points on either sides of the shear joint plane.

Jan 1, 2006

By A. A. Paoli

The selection of a mining plant for carrying on development work presents many problems distinct in themselves, and affected by various local factors. In this paper, the writer proposes outlining and discussing in some detail the chief factors governing the economic selection of such plants. This will be followed by an enumeration of the underground and surface plant required for carrying on several hypothetical exploratory and mining operations. Where it is impossible or not convenient to obtain hydro-electric power, and where wood for fuel is scarce, we now find oil engines being used. A 100 h.p. oil engine, such as would be required to operate a three-drill air compressor, consumes approximately five Imperial gallons of fuel-oil per hour at full load. On the basis of a 60 per cent load factor, this gives, for eight hours' operation, a probable actual consumption of twenty-four Imperial gallons.

Jan 1, 1929