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By Walter V. Knopp, Laurence Delisle

INTRODUCTION THE aim of this work was the preparation of nickel-steels from elemental metal powders by powder metallurgy techniques. It was known that plain carbon steels could be made from a mixture of iron powder and graphite and that the effect of carbon on iron in powder form was of the same nature as that produced in fusion metallurgy. The problem in making nickel steels from elemental powders consisted therefore in finding out whether sufficient diffusion of the nickel and other incidental metals normally present in such steels could be induced in the solid state to modify the properties of plain carbon steels made from powders and produce the beneficial effect of alloying. The composition selected originally was that of an S.A.E. 2330 steel. Metal powders, in the proportion corresponding to that composition, were mixed with graphite, pressed, and heated at different temperatures for different periods of time, to produce bonding of the metal particles and mutual diffusion of the various elements without melting. Temperatures up to 1325°C and sintering periods as long as 6 hr were first investigated because it was expected that such conditions would produce maximum diffusion with an accompanying improvement in the properties of the alloy. It was found that, although diffusion proceeded to a large extent under the conditions investigated, it would not be complete unless sintering were carried out at a high temperature for much longer than 6 hr. Relatively high temperatures and long sintering times are objectionable from a practical point of view, particularly when a low cost material is to be produced, because they necessitate the use of special, costly equipment. Work could be done to improve the diffusion of iron and nickel by changing conditions other than the sintering temperature and time, i.e., finer primary or alloy powders could be used. However, a marked change in the properties of the steel had been observed even with only partial diffusion. It was thought, therefore, that instead of trying to improve the diffusion, advantage might be taken of its incompleteness to produce a special structure consisting, in the unquenched condition, of a hard constituent, rich in nickel, dispersed in a tough pearlitic matrix. Steels with such a structure, not readily obtainable by fusion, should have desirable mechanical properties. Besides, it should be possible to prepare them from elemental powders under economical conditions. This latter alternative was therefore adopted for the second phase of this work. This report is divided into four parts: 1. General Procedure. 2. Effect of Sintering Temperature. 3. Effect of Varying the Nickel Content. 4. Effect of Alloying Elements. GENERAL PROCEDURE The general technique of cold pressing as used in powder metallurgy was applied.

Jan 1, 1948

By L. A. Melis, A. R. Marchbank, S. A. Webster

"Certain northern Saskatchewan uranium ores have a high content of nickel and cobalt which offer the potential for recovery as a by-product to uranium. A nickel/cobalt recovery process has been developed as a viable method of recovering a marketable concentrate from typical uranium raffinate solution.Impurities are first removed from the raffinate and the pure solution is then treated with sodium carbonate to recover a bulk nickel/cobalt carbonate precipitate for sale to a primary nickel producer. All contaminants of concern are removed to very low levels and the product is free of radioactive contamination with gamma emissions significantly below natural background. Cost estimates have shown that installation of a nickel/cobalt recovery circuit within a uranium process plant is economically feasible.The testwork that led up to the selected process is described along with recommendations for further investigations such as additional testing of hydroxide precipitation as a possible viable alternative to carbonate. The selected process is described and project economics are briefly reviewed.PROCESS TEST PROGRAMBackgroundExtensive metallurgical research has been performed over the years to develop a process for recovering uranium from the Midwest deposit in northern Saskatchewan. During the course of this research, a certain amount of information became available which suggested that recovery of nickel and cobalt from uranium raffinate could be economically feasible. It was decided to undertake a test program which would investigate methods of separating nickel and cobalt from radioactive and other metal contamination to permit production of a saleable product.Available technology suggested that three general approaches could be taken to recover nickel and cobalt. The first and simplest approach would be to selectively precipitate the impurities of concern, primarily arsenic, iron and radium, and then recover a bulk concentrate from the purified raffinate. The second approach would be to purify the raffinate and then remove cobalt from solution by solvent extraction producing pure nickel and cobalt solutions for further treatment. The third approach would be to precipitate all metals from solution and then selectively re-dissolve nickel and cobalt in ammoniac solution which would be further treated by solvent extraction for nickel recovery, leaving cobalt for further treatment."

Jan 1, 1993

By K. Hajmrle

The production of nickel coated mica composite powder by hydrogen reduction of a nickel ammine sulphate solution, followed by the production of molded plastic samples containing Ni/Mica is described. Sample preparation by injection or compression molding is outlined and the better results in compression molding are explained by the combination of better particle-to-particle contact, less particle breakage during processing, and more random particle distribution in the plastic. Three volume resistivity measurement techniques are described and compared. Two of them (conductive paint and silver-rubber electrodes) are found reliable and are used throughout the work. The influence of nickel content and particle size of Ni/Mica on volume resistivity is evaluated and the optimum product defined. One of the most important assets of Ni/Mica, its ease of injection molding, is demonstrated by the good electrical properties obtained with little optimization of the injection molding process. Surface roughness of molded plastics with and without Ni/Mica is briefly discussed. Shielding effectiveness of Ni/Mica in four plastics (PP, ABS, PBT and PC) is presented and correlated to volume resistivity data for the same materials. The addition of 15 to 50 weight % Ni/Mica (3 to 16 volume %) to plastics and subsequent injection or compression molding produces composite materials having low volume resistivities (0.03 to 1 ohm.cm) and high shielding effectiveness (40 to 70 dB).

Jan 1, 1988

By J. P. Golightly

The structure and occurrence of nickeliferous laterite profiles are described and explained in terms of mineral solubility and drainage conditions. Complete profiles, from top to bottom, include: limonite zone; nontronite or silica zone; and saprolite zone. The middle zone is present only where drainage is sufficiently slow to allow saturation conditions to build up with resulting quartz or smectite precipitation. This precipitation may occur in any climate at a water table or in tropical climates with a long dry season. The degree of serpentinization of the laterite parent rock is important in determining the nature of the saprolite zone. Unserpentinized peridotite produces saprolite ores with hard residual rock cores, nontronitic or amorphous saprolitic rims, and fracture fillings of garnierite and quartz. Ser-pentinites yield relatively homogeneous serpentine saprolite, with minimal quartz or garnierite.

Jan 1, 1979

By H. L. Paterson, R. R. Keays, M. J. Donaldson, D. J. Boyack, M. F. Smith, J. J. Gresham

"Albite-rich sedimentary rocks that contain abundant Fe sulphides occur in the lower portion of the ultramafic sequence at Kambalda and their broadly antipathetic relationship to most of the nickel orebodies is well documented. These sediments generally contain less than 0.1% Ni, but nickeliferous equivalents with 0.3 to >6% Ni occur locally in close spatial association with more typical volcanic peridotite-associated massive, matrix and disseminated ores. Nickeliferous sediments have been mined at several locations at Kambalda but, collectively, they constitute less than 2% of the total Kambalda nickel reserve. The nickeliferous sediments occur both on the ultramafic-footwall basalt contact and within the lower part of the ultramafic sequence, and are usually less than 5 m thick. They are commonly finely laminated rocks with a cherty appearance, composed essentially of layers of albite+quartz±amphibole, alternating with pyrrhotite+pentlandite±pyrite layers. Some contain a minor amount of carbon. The sediments are only of ore grade (> 1% Ni) immediately adjacent to massive Fe-Ni-Cu sulphides, which are interpreted as normal magmatic ores on the basis of geochemistry and the presence of distinctive ferrochromites. The nickel content of the sediments decreases to background levels (<0.1%) within about 20 m of the massive sulphides. In most locations the massive sulphides clearly have been emplaced tectonically within or adjacent to the sediments, which are commonly highly deformed. Typical nickeliferous sediments contain about 1% Ni, 0.1% Cu, 0.1% Zn, 400 ppb Pd, <0.2 ppb Ir and 10-200 ppb Au. They have lower Ni/Cu (average 10), higher S/Ni (average 6) and higher S/Se (average 11 200) than associated massive sulphides (average 40, 4.8 and 7400, respectively). The Pd/Ir ratio of the nickeliferous sediments (typically > 1000) contrasts markedly with that of associated massive sulphides (average ca 16).The high Pd/Ir values are similar to those which have been reported for hydrothermal Fe-Ni sulphides and barren sulphidic sediments of probable volcanic exhalative origin. They preclude a direct magmatic origin for the sulphides in the nickeliferous sediments, though S/Se and S isotope data indicate a magmatic source for the sulphur. The restriction of nickeliferous sediments to within about 20 m of normal magmatic sulphides and the lack of a widespread Ni dispersion halo suggest local redistribution of originally magmatic Ni. This probably occurred by diffusion and hydrothermal mobilization during deformation and amphibolite-facies metamorphism. Although not totally ruled out, a volcanic exhalative origin for the Ni seems unlikely."

Jan 1, 1984

By Cristián Araya L.

A dynamic agglomeration, heap leaching, solvent extraction and electrowinning software, called NICO, has been developed in order to either design or simulate copper ore recovery plants. NICO contains a library of routines, each representing a unit operation or piece of equipment, which are assembled like a meccano to match almost any wet plant configuration. Routines include agglomeration or curing either in drums or belts, belt conveyors, heap stacking and reclaiming, heap leaching of oxide, sulfide or mixed copper ores, heap irrigation, drainage, ponds, mixer-settlers, filters, columns, coalescers, tanks, electrowinning cells, pumps, and all connections and related piping. All models are semi- phenomenological, i.e., they include all physical-chemical, mass, thermal, transport equations, which are required to represent as closely as possible the equipment or unit operation. However, operating experience has been incorporated into the model in order to make it simpler, faster and reliable. This experience has been tested in several plants in Chile since 1992. Site meteorological data is simulated also; in this way the model is responsive to weather conditions (temperature, solar radiation, ambient humidity, atmospheric pressure, wind velocity, etc). NICO has been used recently for design and optimization studies in copper plants in Chile like Radomiro Tomic, Collahuasi and Zaldivar. A user-friendly interface allows fast and comprehensive simulations. The entire plant is shown in a single graphic screen, so the user can see all the relevant information, and soft-keys are provided in order to change parameters on-line and watch their effect in final copper production in cathodes. Model also calculates and reports operating parameters, as well as estimated investments and operating costs.

Jan 1, 1999

By M Csar

The Nicolsons Find gold project is located 35 km southwest of Halls Creek in the east Kimberley. It was discovered in the late 1980s by John Nicolson and Stuart Skoglund, when high grade gold mineralisation within outcropping gossanous quartz reefs was found. The area has produced a modest 28 150 ounces of gold over two brief mining periods in 1996 and 2002 - 2003. Indicated and inferred resources as of September 2011 stand at 1 384 000 t at 5.58 g/t Au for 248 500 ounces of gold.The project is situated within the Halls Creek Orogen. Principal host units are metasediments and volcaniclastic sediments of the Koongie Park Formation. Minor mafic units are also recognised. Immediately east of these units, emplacement of the loadstone granite is believed to have provided the structural setting for the later gold mineralising event.Mineralisation is hosted within a broad, brittle-ductile arcuate shear zone about the western contact of the Loadstone granite. In the Nicolsons Find area, the shear zone strikes north-northeast and within the shear zone, gold is hosted in a series of narrow, quartz rich veins up to 200 m in strike length, plunging moderately to the north-northeast. To date, mineralisation has been drilled to a depth of 360 m below the surface. The veins are stepped or en-echelon in nature with low gold values towards the quartz vein limits where compression is inferred and higher grades present in the dilational body of the quartz veins. Gold is fine grained and can be present with or without associated sulfides. Sulfides are generally minor and consist mainly of arsenopyrite with traces of chalcopyrite, pyrite and sphalerite. Where present, sulfides are generally indicative of higher gold values.CITATION:Csar, M, 2012. NicolsonÆs Find gold project, East Kimberley, Western Australia, in Proceedings Narrow Vein Mining 2012 , pp 31-36 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Mar 26, 2012

By Connor J. W

Nifty Copper Operations was established to treat a copper orebody situated in the East Pilbara area of North West WA, located approximately 70 km west of Telfer in the Great Sandy Desert. The plant was designed to treat the oxidised portion of the orebody with underground development following at a later date. Nifty was designed to produce 16 500 tpa of copper cathode. This will increase with treatment of the chalcopyrite ore (underground resource). Ore processing is similar to other operations of this type but has its unique challenges. Problems discussed are: fine clay minerals which hinder percolation; oxidation of organic by manganese in the electrolyte; crud formation by clays; third phase emulsions; and organic carryover into the electrowinning tankhouse. As the orebody utilisation progresses, some sulphide material will require leaching and further investigations into liquor chemistry.

Jan 1, 1996

Mineral Industries education as an entity, again and again has sought recognition, always to be turned aside or ignored.1 The incident mentioned in Lost Chapter was only the first of a series of disappointments. The Land-Grant Act is camouflaged here and there in the name of progressive education. A new interpretation may be in the best interests of society in so far as the goose is not killed that lays the golden egg. The primary objective of the act is still "agriculture and mechanic arts" but mechanic arts is not alone mechanical arts or engineering. Mechanic arts was used in a broad sense as a symbol of creative effort in locating and winning the fundamentals of existence - plants, animals, and minerals - from Mother Earth, their primary processing and treatment into foodstuffs and raw materials of industry, their manufacture into useful articles of commerce, and, last, their distribution and utilization. Significantly the great agricultural industry is now at least half mechanic arts. The Association of Land-Grant Colleges and Universities has neglected the mineral kingdom shamefully. The Association embraces Divisions of Agriculture, Arts and Sciences, Engineering, Home Economics, and Veterinary Medicine but has no division relating to the mineral industries.

Jan 1, 1950

The mining industry, like most other industries, has had a difficult couple of years. What are your thoughts on the industry?s direction in the next few years? I am bullish on our industry. There is no question in my mind that the quality of life we enjoy today is largely a result of our past successes in the minerals and mining sector. I am equally certain that the sustainability of that quality of life and the aspirations of the rest of the world to attain that same level of lifestyle will depend hugely on our future successes and will be the driver for our industry to continue to excel and prosper. Surely, there are going to be challenges along the way. These challenges are not only from the public, regulators and various governing bodies, but also from our industry?s own self regulating efforts. However, we have demonstrated throughout the past several decades that we have the capability to meet these challenges head on and come out ahead.

Jan 3, 2010

NIM Reports Report No. 1563 Neutron activation analysis of samples from the Kimberley Reef Conglomerate. Report No. 1569 The use of DDTU as an analytical reagent for the noble metals. Special general meeting A Special General Meeting of the Institute was held in Kelvin House, Johannesburg, on Wednesday, 14th November, 1973. The President, Mr P. W. J. van Rensburg, opened the meeting at 9 a.m. and read the notice of the meeting, which was as follows: Colloquium and general meeting CONSTRUCTION OF SLIMES DAMS A General Meeting and Colloiquum on the above topic was held on November 14th and 15th, 1973, at Kelvin House, Johannesburg. Mr P. W. J. van Rensburg (President) was in the chair. The Colloquium was attended by 135 delegates and was opened by the President at 9.10 a.m. Orange Free State Branch PROCEEDINGS OF THE ANNUAL GENERAL MEETING The Annual General Meeting of the Branch was held in the Western Holdings Cant,een on Tuesday, 11th September, 1973, at 7.00 p.m. Book Review Westwood, W., and Cooper, B. S. Analytical methods in use in non-ferrous minin~ and metallur~ y: a selective review. London, Institute of Mining and Metallurgy, July 1973. 54 pp. £3.50.

Jan 12, 1973

NIM reports Report no. 1845 The composition and mode of occurrence of gold in Witwatersrand ores and leach residues", Report no. 1861 The determination of some impurities in zirconium metal by instrumental neutronactivation analysis. Report no. 12 Exploratory tests on the concentration of tin ore from Kuils River, C.P. (29th Apr., 1966; re-issued Aug. 1976). Report no. 286 A mineralogical and petrographic study of the pre- Transvaal rocks in Borehole K.l, Koster district, western Transvaal. (15th Feb., 1966; re-issued Jun. 1976). Report no. 938 Life test on IRA 400 resin during the recovery of zinc chloride. (27th Mar., 1970; reissued Aug. 1976). Report no. 1010 The leaching, with hydrofluoric acid, of materials containing tantalum and niobium. (8th Jul., 1970; reissued Aug. 1976).

Jan 12, 1976

NIM Reports Report no. 1549 Thermodynamic and related physicochemical factors pertaining to the production of ferromanganese. A literature survey. Report no. 1568 A computer programme for the estimation of parameters in flotation. Report no. 1571 The commissioning of a directreading spectrometer for the analysis of silicate rocks by use of the graphitepellet technique. Report no. 1582 The construction and testing of a precision calorimeter. Report no. 1587 A preliminary investigation of the flotation of copper-activated sphalerite without the use of collectors.

Jan 2, 1974

NIM Reports Report No. 1647 The industrial application of KEGOLD electrodes. Report No. 1665 The determination of minor amounts of antimony in ores and concentrates by atomic absorption spectrophotometry.

Jan 1, 1975

NIM reports Report No. 1615 Fluorspar pellets. A survey of the world market and an assessment of future South African production. Report No. 1621 Correction for matrix effects in the analysis of solutions by X-ray-fiuorescence spectrometry. Notices Questionnaire on Technicians The Department of National Education&apos;s committee of enquiry into the education, training, utilization, and status of engineering technicians in the Republic of South Africa was established as a result of Resolution 6.3 taken at the Sixth Conference on Engineering Education: The Education and Training of Engineering Technicians. Vraelys oor Tegnici Die Departement van Nasionale Opvoeding se komitee wat ondersoek instel na die opleiding, gebruik en status van ingenieurstegnici in die Republiek van Suid-Afrika is gestig as gevolg van Besluit 6.3 wat geneem is tydens die Sesde Konferensie oor Ingenieursopleiding: Die Opleiding van Ingenieurstegnici. Competition for Student Members of the South African Institute of Mining and Metallurgy Each year the Institute offers a prize (or prizes should the entries warrant it) of up to R100 for the best paper or dissertation on a topic appropriate to the interests of the Institute. The competition is open to all Student Members of the Institute.

Jan 8, 1974

By Pengfu Tan

NiModel, a thermodynamic model, database and computer program, has been developed to predict the distribution behavior of Ni, Cu, Co, Fe, S, O, As, Sb and Bi, and heat balance in the nickel pyrometallurgical processes such as Outokumpu flash smelting, Outokumpu direct high-grade matte smelting, INCO flash smelting, and Peirce-Smith converting processes. In this model, as much as 16 elements (Ni, Cu, Co, Fe, As, Sb, Bi, S, O, Al, Ca, Mg, Si, N, C and H) are considered. The compositions of matte, slag and gaseous phases, and heat balance are calculated using the thermodynamic data and the activity coefficients of the components derived from the experimental data. The model predictions were compared with the known industrial data from Kalgoorlie Nickel Smelter in Australia, Outokumpu Harjavalta Nickel Smelter in Finland and INCO Metals Company in Canada, and an excellent agreement was obtained. In this paper, the applications of NiModel in the nickel pyrometallurgical industries have been presented. NiModel has been used by Jinchuan Group Limited in China.

Jan 1, 2004

By AIME AIME

N OW THAT the war is over it is possible to release data and correct some erroneous statements and impressions relative to the use of manganese-steel armor and helmets, which heretofore have been carefully guarded. The material of the helmets furnished to the English, American, and Belgian armies was invented by Sir Robert Hadfield, Bart., F.R.S., and was described in a paper read by him at the International Engineering Congress in August, 1893. The French helmet was 2 oz. lighter than the English but had a greatly inferior resistance. Tests showed that it was perforable at as low a velocity as 350 ft.- sec. impact of the standard shrapnel bullets. Helmets made of the Hadfield "Era" manganese steel kept out standard shrapnel bullets of the same quality at no less than from 750 to 950 ft.-sec. impact velocity. The respective energies were, in the case of the French helmet, only 0.021 ft.-tons, 46 ft.-lb., and in the British 0.095 ft.-tons, 213 ft.-lb. The German helmet was made of nickel-chromium steel and, although 12 oz. heavier and 12 per cent. thicker than the Hadfield, was not only perforate

Jan 1, 1920

By Claude Cunningham

AEL has been developing electronic detonators continuously since 1986. It launched its first system for opencast mining in 1993, and now has two distinct product lines. The path has not been without great difficulty, but the determination to persevere was always buoyed by the strong encouragement of customers who experienced the transformed blasting results, as well as a clear vision of the enormous intrinsic value of the concept. The path of growth to dominant global supplier is traced through the separate application channels of coal stripping, quarrying, massive mining, opencast mining and narrow reef mining, to the first allelectronic detonator demolition blast in June 2001. Reasons for the slow coming to market of this highly desirable concept, which often coincide with reasons for the demise of various other systems, include the difficulty of safely mating electronics and explosives in a low cost environment; the extreme difficulties of achieving proper connection under mining conditions; the rapid rate of evolution of the technology, and the safety concerns raised by various accidents and incidents along the way. ED.s are now established as the way forward and are set to displace other systems in all serious applications. There is place for both programmable and pre-set delay systems.

Jan 1, 2002

The past year has been a difficult one for the mining industry in this country, but an active and successful one for the Branch. Membership has continued to increase, albeit at a slower rate than last year, and with the increase almost all from student membership. I dwelt at some length last year on the continued increase in student membership, which I ascribed largely to deliberate policies adopted by the Branch to foster this area of membership. I don&apos;t propose to reiterate these, suffice it to say that as usual, the Otago School of Mines has been a prolific source of student members, and it will be a pity if this source dries up û more on this subject later. In fact, students form just on 29 per cent of the Branch&apos;s total membership û a far higher percentage than for any other Branch in the Institute, whose membership as a whole comprises only ten per cent students.

Jan 1, 1985

By P. E. Weidmark

"CANMET InformationPART 1-Published PapersAsmis, H. W., ""The dynamic response of caverns in discontinuous rock""; Proc 22nd U.S. Symposium on Rock Mechanics, Cambridge, Mass, June 1981, 272-277; 1981.Austin , M.W., Bray, J.W. and Crawford, A.M., ""A comparison of two indirect boundary element formulations incorporating planes of weakness"" ; Technical Note; Int J Rock Mech Min Sci Geomech Abstr; 19:339-344; 1982.Barrett, J. R., ""Applying geotechnical theory to underground metalliferous mining""; Proc 1st Intnl Conf on Stability in Underground Mining; Vancouver, BC, August 1982; SME of AIMMPE; 210-222; 1983.Barron, K., Wright, P.L. and Smales, T., ""Guideline s for the design of coal pillars in the No .4 seam at Mclntyre Mines Ltd ., Grande Cache, Alberta""; Proc 1st Intnl Conf on Stability in Underground Mining; Vancouver, BC, August 1982; SME of A IMMPE; 559-578; 1983.Bauer, A., ""Wall control blasting in open pit mines""; Mining Engng; 34:155-158; 1982.Bieniawski, Z.T., "" Improved design o f room-and-pillar coal mines for U.S. conditions""; Proc 1st Intnl Conf on Stability in Underground Mining; Vancouver, BC, August 1982; SME of AIMMPE; 19-51; 1982.Blackwell, G.H. and Calder, P.N., ""Practical aspects of wall stability at Brenda Mines Ltd., Peachland, BC""; 3rd Intnl Conf on Stability in Surface Mining; Vancouver, BC, June 1981; SME-A1ME; 3:573-608; 1982.Blake, W., ""Microseismic monitoring for underground stability "" ; Proc 1st Intnl Cont on Stability in Underground Mining; Vancouver , BC, August 1982; SME of AIMMPE; 272-294; 1983.Brawner, C.O., ""Stabilization of rock slopes"" ; 3rd Intnl Conf on Stability in Surface Mining; Vancouver, BC, June 1981; SME-AIME; 3:289-310; 1982.Bridges, M.C., ""Review of open stope mining in Australia""; Proc 1st lntnl Conf on Stability in Underground Mining; Vancouver, BC, August 1982; SME of AIMMPE; 813-828: 1983."

Jan 1, 1983