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Both drilling and production in Rumania showed increases in 1934 over 1933. The drilling totaled 1,138,000 ft. and production 63,500,-000 bbl., being increases of 50 and 15 per cent, respectively. During the year production gradually increased from 155,000 bbl. per day in January to 180,000 bbl. in September, and then declined slightly to the end of the year. The increases were largely due to competitive drilling in the Gura Ocnitei field (including west extension to Viforata). Wells completed during the year totaled 238, of which 215 were oil producers. The outstanding development of the year was the discovery by Steaua Romana of what appears to be a major field at Bucsani. Other important discoveries were a three-mile west extension of the Gura Ocnitei fault to Viforata and a five-mile east extension of the Moreni field to Calinesti. Strictly speaking, the latter cannot as yet be called an extension. Oil sands have been corded in the Meotic, and in all probability production will be established in 1935. The Calinesti discovery greatly restricts the unproved area between Moreni and Baicoi, and the probabilities of

Jan 1, 1935

By Takahide Wakamatsu, Douglas W. Fuerstenau

Contact angles on alumina are related directly to the adsorption of alkyl sulfonates at the solid-water interface and thus are strongly controlled by the pH of the solution, the concentration of surfactant, and the number of carbon atoms in the alkyl chain. As the pH of the solution is increased above the point of zero charge, sulfonate adsorption ceases and alumina remains hydrophilic. However, in neutral and acidic solutions, contact angles increase markedly in magnitude when the adsorbed sulfonate ions form hemimicelles at the solid-water interface. Under a wide variety of solution conditions, a limiting value of the contact angle is attained at the point of reversal of the zeta potential. Finally, contact angle phenomena are empirically correlated with the sulfonate adsorption density through the work of adhesion.

Jan 1, 1974

JEROME ALEXANDER.-All of you undoubtedly know that a microscopic examination of metals will reveal many things; but we should go further than just simply using a low- or medium-powered- microscope and seek the reason why grain size varies under different conditions. When we get below the limits of the ordinary microscope, we enter the so-called colloidal field, which means that we are dealing with aggregations of matter that approximate, say, 100 millimicrons. The colloidal dimensions average approximately 50 millionths of a millimeter and extend down to about 3 µµ. This, of course, is beyond the range of visibility in the ordinary microscope. Just to give you an idea of this matter, if 1 cu. in. of platinum is reduced to a sheet five molecules thick, it will cover 7 acres; you can imagine the amount of surface involved when metal, or anything else, is subdivided to so high a degree. Of course five molecules thick is a little below the limits of the colloidal dimensions. The statement is made in the paper that "metals and alloys might be

Jan 4, 1919

By R. Taggart, G. R. Purdy

DURING a study of the tempering of ß-quenched alloys of cobalt in titanium, parallel lines were observed crossing certain faces of retained-ß crystals in the early stages of tempering, Fig. 1. The lines closely resemble stress-induced martensite' or substructures attributed to clusters of faults in titanium-nickel2 and copper-silicon3 alloys. The markings were observed only in intensely etched quenched and tempered alloys having compositions ranging from 4.5 pct* Co (the composi- formed by the lines was reproduced upon repolishing and reetching. Close metallographic examination indicated that the markings were troughs, Fig. 2, and that the characteristic surface substructure persisted within the troughs. The occurrence of the troughs was associated with the age hardening reaction due to the metastable u) phase (previously reported in titanium-cobalt alloys by Raub and Beeskow4 and indicated in this work by the broadening of 0 diffraction peaks and by hardnesses approaching 600 Dph). The troughs

Jan 1, 1961

WILLIAM YOUNG WESTERVELT, Chairman, Representing A. T. M. E. and M. and M. Soc. of Am. ALFRED G. WHITE, Secretary, Representing U. S. Bureau of Mines. W. 0. HOTCHKISS, Representing Association of American State Geologists. DAVID WHITE, Representing U. S. Geological Survey. The organization and purpose of the War Minerals Committee was explained in a special war notice in the-August Bulletin. The first work of this Committee is to secure and condense information as to the relative importance of different properties from the standpoint of domestic mineral production. When the possibilities of ore deposits are known, involving, in some cases, further examination through the voluntary services of, Engineers and Geologists, then the necessary policy required to stimulate such development can be determined. Proper recommendation has been and will be made to .the various agencies controlling the situation during the war. This will insure a complete presentation of the needs of the situation. Every legitimate effort will be made to stimulate the production of domestic minerals and to put the industries on a permanent basis. The following information forms indicate the type of information required by the Committee. Engineers and Geologists can assist in one of several ways in furnishing information to the War Minerals Committee:

Jan 10, 1917

The following is an incomplete list of members and guests who called at Institute headquarters during the period Apr. 10, 1918 to May 10, 1915. Robert H. Chapman, Washington, D. C. Francis Nicholson, Charlotte Court House, G. A. Collins, Seattle, Wash. Va. W. N. Cummings, Orange, Cal. F. S. Platt, Australian Imperial Force. W. A. Deane, Summitville, N. Y. H. Rabling, Melbourne, Australia. H. W. Edmondson, Camp Lee, Va. James C. Ray, Palo Alto, Cal. H. F. E. Gamm, Rutherford, N. J. Jasper T. Robertson, Chicago, Ill. A. L. Gholz, Minneapolis, Minn. John A. Root, Kings Mills, Ohio. H. H. Hodgkinson, Dover, N. J. Robert H. Seip, Franklin, N. J. Norman L. Jenks, Marmato, Colombia, Trevor B. Simon, Morristown, N. J. South America. H. N. Stronck, Chicago, 111. Paul S. King, Wilmington, Del. Benjamin F. Tillson, Franklin, N. J. Ray G. Knickerbocker, Rolla, Mo. J. R. Underwood, Granby, Mo. Carl A. Lewis, Habana. Thor Warner, Phoenix, Ariz. Robert S. Lewis, Salt Lake City, Utah. G. B. Waterhouse, Buffalo, N. Y. Edmund Newton, Minneapolis, Minn. W. M. Weigel, Renfrew,. Ont., Canada. Alexander Nicholas, Australian Imperial Chas. F. Willis, Tucson, Ariz. Force. Ralph Arnold is devoting a part of his time to work as a member of the Board of Tax Reviewers in connection with the administration of the War Revenue Act.

Jan 6, 1918

(Under this heading will be published notes sent to the Secretary of the Institute by members or other persons introduced by members.) Milling or Smelting. Graduate Missouri School of Mines desires position in milling or smelting department of responsible non-ferrous mining company. Twenty-eight years of age, married, 4 1/2 years in milling, smelting, and experimental work with large copper company. Refererences. A-3326. Technical Graduate, B. S., E. M., 1909, age 34, single, desires position with prospects of advancement. General engineering experience in, mining, development and exploration work, estimating, mining methods, mapping, mine accounting, and drafting. Can furnish complete .record of experience. A-3327. Superintendent or Engineer. Civil engineer, technical graduate, age 29, seven years varied experience, municipal, drainage, mining of iron ores in Virginia, desires position as superintendent or engineer; available immediately; references. Salary expected $2000 to $3000. A-3131. Engineer or Executive. Graduate mining engineer, age 31, married, eight years' experience in mine operation, exploration and reporting, desires engineering or executive position of responsibility. Now employed. Highest credentials. A-3422. Mine Manager or Superintendent, technical, education, married, desires opening. First class references. Wide experience in mine development and operation; milling and general construction as executive. A-3496.

Jan 8, 1919

By A. G. Metcalfe

THE failure to detect any change in the thermal properties of cobalt at the Curie point would appear to indicate that the apparatus may have a limited sensitivity. The Curie temperature has been determined by direct methods to be 1121+3°CP and 1131°C.3 The specific heat has been determined many times'.' and weighted values are given in Table I. The allotropic transformations in iron and titanium, used by the authors to test the experiment method, involved a volume change of the order of 3 pct on going from the close-packed to the body-centered-cubic lattice. These energy changes are likely to be much larger than those involved in a diffusionless transformation from a hexagonal to a cubic-close-packed lattice. However, it has been pointed out that thermal observations are unreliable in the detection of phase changes when these are near a Curie point.' James 0. McCaldin and Pol Duwez (authors' reply)—The sensitivity of the present technique is limited to first-order transformations, so that gradual changes in specific heat, e.g., in the vicinity of Curie points, are not detected. Furthermore, the existence of first-order transformations with latent heats much smaller than those occurring in the known allotropic transformations of iron and titanium is, we agree, still pending.

Jan 1, 1956

By Nicholas J. Grant, Ulf Kalling, John Chipman

D. E. Babcock (Republic Steel Corp., Youngstown, Ohio)—I would like to know what evidence you have to prove the MnO was pure MnO. I would also like to know whether you might not explain it on the basis of a temperature reversion; and, was it due to the oxidizing power of MnO? N. J. Grant (authors' reply)—Briefly, we have no proof that pure MnO was used. The manganese oxide was added as chemically pure MnO,. MnO is assumed as the oxide in the reacted slag following standard molecular slag theories, especially under the reducing conditions of these experiments. The noted sulphur reversion cannot by any means be explained on the basis of a temperature reversion since the temperature effect is shown in this paper to be very small. Until a more logical explanation can be offered, backed I hope by some experimental proof, we propose to explain this sulphur reversion as stated in the paper, namely, that it is due to the oxidizing effect of the added manganese oxide. Member—How did the oxygen in the slag give you a reversion of sulphur? What was the mechanism there?

Jan 1, 1952

By J. B. Hiskey, G. Ramadorai

This paper presents the kinetics of leaching pure wulfenite (PbMoO,) with sodium sulfide solutions. Wulfenite dissolves in the presence of sulfide ion according to the following reaction: PbMoO , + S= PbS + MOO;. Synthetic galena is formed and molybdenum is released to solution as molybdate ion. The reaction follows the shrinking core model and the leaching mechanism involves mixed kinetics where both diffusion and chemical reaction are rate controlling. Molybdenum extraction is explained in terms of temperature, particle size, and sodium sulfide concentration.

Jan 1, 1977

By L. S. Pratt

IN 1910 the author was engaged in a qualitative study of the radio-activity of several chemical substances and a few minerals. In the course of the work he studied the mineral allanite (obtained from granite ledges at Topsham, Maine), and found it to be appreciably radio-active. Recently the fact was brought to his attention that the radio-activity of allanite is not well known, although Hon. R. J. Strutt in 1905 published a list of radio-active minerals with their analyses, including allanite from Amherst County, Virginia. In the work done, a standard ,type of electroscope was used, and the readings were made with a telescope, fitted with a scale, by means of which the rate of discharge could be readily determined. The natural "leak" of the instrument was carefully determined, and all results corrected accordingly. The method of study was as follows: The material to be tested was finely powdered, and spread over the bottom of a small, inactive pan. The electroscope was then charged, and the pan placed in position. The door of the instrument was closed, and the rate. of discharge carefully determined. All results were reduced to common form to permit of comparison. It is to be noted that the materials tested were not used in strictly comparable quantities, such as if 1 g. of. each had been used, but about the same quantity of powder was used (in the cases of the solid substances), so that the results are qualitatively accurate.

Jan 5, 1916

By A. E. Weissenborn

Current knowledge of the substantial resources of zinc that exist in northwestern Washington is reviewed. These zinc-lead deposits are all associated with the Kootenay Arc, a narrow arcuate belt of folded and faulted rocks that dominates the regional structure of Stevens and Pend Oreille Counties and adjacent parts of British Columbia. The deposits of the Arc are only part of a major lead-zinc silver metallogenic province that includes the deposits of the Coeur d'Alene district and the famed Sullivan ore body of Kimberly, British Columbia. Most, but by no means all the zinc-lead deposits of the Kootenay Arc are in carbonate rocks. They occur in several stratigraphic units, and in different parts of the Arc are quite diverse in character. The deposits appear to have undergone a complex geologic history and have not necessarily all been formed at the same time or by the same geologic processes.

Jan 1, 1976

By Magnus Troilius

The method of using the bromine process of determining sulphur in steel, described below, is in successful use at the Midvale Steel Works. Ten grams of drillings are weighed out and put into the 1/2-liter flask A, with long neck. The flask is connected with a wide glass tube C', which, in its turn, is connected with the absorption bulbs B, containing HCI, 1.12 specific gravity, and ahout 5 C.C. of bromine. The wide tnbe C causes the vapor to condense and flow back into the flask A during boiling. The bulbs B connect with a long glass tnbe, which may be made to carry off the bromine fumes through a hole in a window, or, better still, through a flue with powerful draught. The connections being made, 100 C.C. of boiling water are run in through the thistle tube T. The air is thus completely driven out of the flask. 100 C.C. of HC1 (about 1.19 specific gravity) are then run in. When the gas begins to run rattler slowly through B, heat is applied until boiling gradually ensues. The steel being completely dissolved, the apparatus is disconnected, and the contents of B rinsed out into a beaker of 100 C.C. capacity, into which a few C.C. of a concentrated solution of BaCI, have been previously introduced. Heat is then applied (best by means of the hot iron plate) until the bromine is completely driven off and the BaSO, has settled nicely to the bottom. The BaSO4, is then filtered off on a small

Jan 1, 1884

By A. A. Venghiattis

This paper is discussed not because of its intrinsic value but because it has been related by its authors to the oilwell gun perforators. It is well known that conditions almost ever present in oilwell perforations are the overburden and the presence of the casing. Because of the lack of information in the paper on the dimensions or confinement of the target rocks, one is led to guess that they were not confined at all and, particularly, that no steel front plates were used on the impact face of the rocks to materialize the presence of the cemented casing. This situation, plus the fact that small steel balls have been used as projectiles instead of actual bullets, makes the whole thing unapplicable to oilwell perforation. When shooting is performed against target rocks confined (as shown on Fig. 1) in such a way as to give a fair image of the overburden applied to the formation to be perforated, as well as of the cemented casing, the following are found. 1. There is no cratering worthy of mention, even with bullets having 10 times higher impact energy per unit projected area than the steel balls mentioned in the article. This has been confirmed with sandstone as well as with other rocks (granite, limestone and chalk). See Figs. 2 and 3. 2. Penetrations vary closely as the logarithm of the impact velocity. On this matter I have established the relation

By R. W. Raymond

I DESIRE to call the attention of the Institute briefly, and by no means in the way of an exhaustive description, to the interesting developments recently made on the east bank of the Hudson River, in the mining of spathic iron ores. The mines to which I refer are those of the Hudson River Spathic Iron Ore Company, situated at Oakhill on Hudson, Columbia County, N. Y., five or six miles from the city of Hudson, and opposite the town of Catskill. The ore occurs in beds, constituting apparently members of the stratified series of rocks on that side of the river, coursing nearly north and south, parallel with the river, and dipping east. The principal outcrops are presented in a range of low hills, about one mile from the river, along the crest, on the western face of which the stratum of spathic ore is more or less exposed. The length of the line in this range, along which, at various openings the ore has been discovered in profitable quantity, is about two miles. To the northward, the hills are somewhat higher, and the stratification may possibly be disturbed, though the rapid examination of the locality which I made in November last did not, include any determination of this

By R. W. Raymond

I DESIRE to call the attention of the Institute briefly, and by no means in the way of an exhaustive description, to the interesting developments recently made on the east bank of the Hudson River, in the mining of spathic iron ores. The mines to which I refer are those of the Hudson River Spathic Iron Ore Company, situated at Oakhill on Hudson, Columbia County, N. Y., five or six miles from the city of Hudson, and opposite the town of Catskill. The ore occurs in beds, constituting apparently members of the stratified series of rocks on that side of the river, coursing nearly north and south, parallel with the river, and dipping east. The principal out- crops are presented in a range of low hills, about one mile from the river, along the crest, on the western face of which the stratum of spathic ore is more or less exposed. The length of the line in this range, along which, at various openings the ore has been discovered in profitable quantity, is about two miles. To the northward, the hills are somewhat higher, and the stratification may possibly be disturbed, though the rapid examination of the locality which I made in November last did not, include any determination of this

Jan 1, 1876

By Bai Shiwie, Li. Guangyu

This paper presents the study in situ on stress field of rock mass in a large dam site. By means of two different measure instruments and the method of stress relief, a lot of measure in situ has been done, including stress measurement of three dimensions at ten points and two deep-hole stress measurements in the perpendicular boreholes which are 59.4m and 53m deep seperately, and the basic accordant results corresponding two methods have been got. In the process of the deep-borehole stress measurement we got the stress value in critical state in which cylindrical core would become core-disking in the high stress area, which was first got in the world. The maximum principal stress was up to 650 kg/cm2. The stress value obtained by test and the thickness of rock disks all basically accord to the analysis by mechanical mechanism of core-disking The plane linear elastic finite element analysis has been completed. Results of inverse calculation all ac- cord to the measurement results in four different positions. The whole outline of the stress field of dam site was delineated clearly.

Jan 1, 1982

By Rush Sill

THE processes of superficial alteration depend on physical conditions, environment, geologic history and chemical and mineralogical composition. Superficial alteration is confined particularly to the zone of shallow circulation, as this is the zone of solution; its rocks are open and the circulation within it is compara-tively rapid. The enrichment of ore deposits in this zone, therefore, is of special interest. The depth of the vadose, or zone of shallow circula-tion, is variable, because its lower limit depends on the variable level of ground water. In moist, hilly countries its depth varies from a few feet to several hundred feet. In arid regions where the rainfall is low and evaporation great, this zone may extend to much greater depths. Permeability of the deposits . is essential to the downward migration of metals. In rocks, that have been fractured since the primary ore was deposited, there is generally more extensive and deeper enrichment than in ore deposits that have been but slightly fractured. A warm climate increases chemical action and abundant rain fall is favorable to enrichment. Low relief and slow erosion give long periods of weathering and thorough leaching.

Jan 9, 1922

By Edgar Stansfield

WHEN plants decay in a peat bog the woody parts form a brown pasty mass, or peat muck, largely soluble in. alkalis. This brown matter has been termed "ulmin." The same material, but commonly black in color, is found in coal, and there is evidence of the similarity between the material forming the main bulk of the coal and the bulk of the more recently decayed material in peat bogs. The. more recent or low-rank coals, such as lignite, little removed from the peat stage, contain notable percentages of alkali-soluble ulmins, but the percentage decreases with increased, degree of coalification and is negligible in bituminous or higher rank coals. The determination of the alkali-soluble ulmins in any coal gives, therefore, an indication, of its degree of coalification or rank. Coals which contain few or no ulmins soluble in alkalis do contain ulmins which can be rendered soluble by oxidation. The higher the rank of the coal, the more difficult it is to oxidize the insoluble ulmins and make them soluble. High-rank coals can be differentiated by oxidation tests on the, insoluble ulmins; but low-rank coals can be characterized by both their soluble and insoluble ulmins. This paper deals with the determination and significance of the alkali-soluble ulmins, present, as such in- the coal. The chemical nature and composition of ulmins are not discussed.

Jan 1, 1932

By W. N. Logan

THE petroleum industry in Indiana made no extraordinary progress during the year 1924. The surplus stock of crude, brought about by the production of 732,407,000 bbl. in the United States in 1923, as against a production of 557,531,000 bbl. in 1922, had its effect on prices though there were slight advances. These advances were more than offset by the continued high prices of labor and materials. TRENTON OIL DEVELOPMENT The principal development of the year occurred in the Hotmire pool of the Ridgeville district in northeastern Indiana. This pool lies partly in the southern part of Jay County and partly in the northern part of Randolph County. The oil is obtained from the upper horizon of the Trenton. During the past year, about 30 wells were drilled, 21 of which were productive. An attempt to extend the Hotmire pool to the northeast resulted in the discovery of a gas-producing area near the center of Pike township in Jay County; 10 wells have been drilled 4 of which produced oil. The Harvey Orr No. 1 produced 900,000 cu. ft. of gas per day.

Jan 3, 1925