Search Documents

By Ben Mirabile, Alan Campoli, Rodney Poland

"The majority of U.S. underground coal mines use some form of cable bolt as supplemental support to a primary roof bolting system. Many coal operators employ the high load capacity of non-tensioned cable bolts, cable roof trusses, or solid bar trusses in an attempt to suspend the primary bolted horizon to overlying strata. However, in cases where many discontinuities exist in the roof strata or where pre-existing fractures are present, these passive supplemental support systems often cannot adequately control roof deflection. This paper examines the application of tensioned cable systems to minimize roof deflection in very laminated and fractured strata. Three underground case studies are presented to demonstrate the application of tensioned cable bolts. The first case study involves the rehabilitation of a longwall head gate in the Eagle Seam with highly laminated and fractured sandstone. The second case study examines the recovery of a longwall face in the Alma Seam. The final case study addresses rehabilitation of a longwall head gate in the Pittsburgh No. 8 Seam that was developed in a sandstone channel margin area and subjected to horizontal stress concentration.INTRODUCTIONDuring the previous decade, Jennmar Corporation has recognized coal operators' increasing interest in tensioned cable bolts. The majority of these tensioned cable bolt systems have been applied in adverse roof conditions including broken ground, high horizontal stress areas, and highly laminated roof strata. In most cases, qualitative data on roof conditions after application of tensioned cable bolt support indicate successful implementation of these systems. The qualitative evidence suggests that the combination of high load' capacity and applied tension provides superior supplemental roof support in adverse roof conditions. This research aims to quantify the effects of applied tension to cable bolts. This paper will review the types and installation of tensioned cable bolt systems, present initial laboratory test data, discuss successful case studies, and propose an instrumentation system for quantification of tensioned cable bolt performance."

Jan 1, 2010

By Jacques B. Wertz

Detailed structural studies in southeast Arizona have successively revealed (1) the local attitudes of individual fractures (with lateral and/or vertical displacements), (2) the patterns exhibited by groups of fractures, and (3) the trends and directions shown by fracture groups or zones on a regional scale. The results of the studies have been twofold: First, domes were locally determined from these fracture arrangements, even where other criteria failed; and, second, fundamental breaks brought out the breadth of the Texas lineament in southeast Arizona as well as major northwest- and northeast-trending fracture zones. Coincidence of one or several domes with the major intersections of fundamental breaks can be centers of important mineralization, as in the instances of Bisbee, Ajo and Morenci. THE OVER-ALL STRUCTURE OF ARIZONA A northwest-southeast trending anticlinorium has been suggested as the structural setting of Arizona. Starting in Triassic and culminating in late Cretaceous times, this deformation resulted from stresses of considerable magnitude with varying ratios of com pres sional and uplifting forces. However, the series of parallel flexures could just as well have been caused by isostatic movements involving dilation under tension with only incidental compression, as later emphasized by dike filling and block faulting (Fig. 1). The anticlinorial deformation, which is also suggested by the fact that the Pre-cambrian rocks to the southwest are all concealed by sediments, could be somewhat reminiscent of the conditions that affected the classical swarm of parallel dikes of wager.' ANALYSlS OF DATA As a first step in this analysis, all structural information obtained on such features as fractures and their relative displacements, faults, dikes, anticlines, synclines, and Precambrian and Laramide-Tertiary intrusives were plotted on maps along with structural trends inferred from aerial photographic mosaics. Next, the faults in southwest Arizona were classified according to time of occurrence and relative importance. The fault assemblages were then examined as to geometric or spatial arrangement and correlated with the occurrences of domes and existing Finally, the conjunction of fracture intersections and domes was analyzed and compared with locations of known ore deposits. Differentiation of Faults According to Time and Relative Importance: The faults encountered were grouped as follows: (1) Basin and Range faults, latest in time; (2) secondary faults; (3) primary faults; and (4) lineaments, earliest in time by inference. BASIN AND RANGE FAULTS- Generally concealed by alluvium, the Basin and Range faults are normal

Jan 1, 1969

By D. H. Desy

This research was undertaken to establish the lncendivity of aluminum alloys against rusty steel under frictional impact conditions at typical coal mine fan speeds, to determine any differences in incendivity among various aluminum alloys, and to Investigate less incendive materials as substitutes for aluminum alloys. With a specially designed apparatus, three aluminum casting alloys and three constructional steels were tested for incendivity in frictional impact against rusted steel in flammable methane-air mixtures. Although varying in degree, all aluminum alloys investigated exhibited a high ignition probability under the test conditions; none of the steel specimens tested caused any ignitions under the same conditions.

Jan 1, 1973

By Frederick K. A1lgaier

The Bureau of Mines' Denver Research Center initiated a subsidence research program in 1978. The short ten goals of the program were to determine practical methods and equipment for measuring subsidence and demonstrate these methods by monitoring subsidence at several mines having mining, geologic and topographic variables typical of those encountered in the western United States. Data from the monitoring program would be supplied to cooperating mining companies and used by the Bureau to accomplish the long term objective of developing and validating subsidence prediction techniques applicable to mines in the West. Subsidence monitoring is being conducted at five mines in Colorado and Utah with substantially different mine plans, mining methods, depths of cover, and topography. The monitoring procedures used at each site are similar and include designing the monitoring network layout, installing the subsidence monuments, initial and periodic surveying of the monuments, and processing the survey data. The network layout, surveying methods, and types of monuments vary according to the conditions at the individual sites and the type of data being collected.

Jan 1, 1982

By T&apos Ke, ing-sui

Accoriding to the classical theory of elasticity, the elastic portion of the stress-strain curve is represented by a straight line. such a representation implies that there is a linear relationship between strain and stress and also that strain is a single-valued function of stress and vice versa. Actually, such a one-to-one correspondence between strain and stress does not exist in real metals. A well-known example is the elastic after-effect on unloading. Another familiar example is damping or internal friction, that is, the dissipation of energy attending vibration. In an extensive review of such phenomena, zener1,2 has proposed the term "anelasticity" to denote that property of a solid in virtue of which strain is not a unique function of stress in the non-plastic region. The phenomena arising from anelasticity are called anelastic effects. The measurements on anelastic effects are important in many fields of metals technology. The, in precise instruments such as watch springs, difficulties often arise from the slight dimensional changes after fabrication. The internal friction or damping capacity of metals is often an important factor in deciding whether they are appropriate for instruments in which there are accompanying vibrations.3 However, for metal scientists, the study of anelastic effects furnishes a powerful tool for understanding many properties Of meta1s in terms of their microstructures or atomic interactions. In order to utilize the anelastic measurements to their fullest extent for acquiring such information, the experimental studies Of anelasticity must be interpreted by appropriate mathematical analysis. For a great many problems, however, the necessary information often Can be Obtained by general qualitative arguments. From the definition of anelasticity, any physical changes occurring in a specimen as a result Of the applied stress will cause anelastic effects if such physical changes are accompanied by a delayed change of elastic strain. Under these circumstances, we have the condition that strain lags behind the stress. We may mention the stress-induced transportation phenomena as examples. These include the stress-induced thermal diffusion,4-7 the stress-induced diffusion of particles,8-l2 and the stress-induced viscous slip along the microelements in metals.12-15 The differential equations describing the microscopic mechanism in these phenomena lead to relations in which stress is linear with respect to strain (and/or their derivatives). Thus if we Can demonstrate that the superposition principle is valid under the circumstances in which the anelastic effects are observed, we would expect in the macroscopic relation a linear relationship between stress and strain and their derivatives. This report is to describe a number of anelastic effects observed in alpha-iron, and an attempt is made to derive valuable information from a critical study of these

Jan 1, 1949

By T&apos Ke, ing-sui

Accoriding to the classical theory of elasticity, the elastic portion of the stress-strain curve is represented by a straight line. such a representation implies that there is a linear relationship between strain and stress and also that strain is a single-valued function of stress and vice versa. Actually, such a one-to-one correspondence between strain and stress does not exist in real metals. A well-known example is the elastic after-effect on unloading. Another familiar example is damping or internal friction, that is, the dissipation of energy attending vibration. In an extensive review of such phenomena, zener1,2 has proposed the term "anelasticity" to denote that property of a solid in virtue of which strain is not a unique function of stress in the non-plastic region. The phenomena arising from anelasticity are called anelastic effects. The measurements on anelastic effects are important in many fields of metals technology. The, in precise instruments such as watch springs, difficulties often arise from the slight dimensional changes after fabrication. The internal friction or damping capacity of metals is often an important factor in deciding whether they are appropriate for instruments in which there are accompanying vibrations.3 However, for metal scientists, the study of anelastic effects furnishes a powerful tool for understanding many properties Of meta1s in terms of their microstructures or atomic interactions. In order to utilize the anelastic measurements to their fullest extent for acquiring such information, the experimental studies Of anelasticity must be interpreted by appropriate mathematical analysis. For a great many problems, however, the necessary information often Can be Obtained by general qualitative arguments. From the definition of anelasticity, any physical changes occurring in a specimen as a result Of the applied stress will cause anelastic effects if such physical changes are accompanied by a delayed change of elastic strain. Under these circumstances, we have the condition that strain lags behind the stress. We may mention the stress-induced transportation phenomena as examples. These include the stress-induced thermal diffusion,4-7 the stress-induced diffusion of particles,8-l2 and the stress-induced viscous slip along the microelements in metals.12-15 The differential equations describing the microscopic mechanism in these phenomena lead to relations in which stress is linear with respect to strain (and/or their derivatives). Thus if we Can demonstrate that the superposition principle is valid under the circumstances in which the anelastic effects are observed, we would expect in the macroscopic relation a linear relationship between stress and strain and their derivatives. This report is to describe a number of anelastic effects observed in alpha-iron, and an attempt is made to derive valuable information from a critical study of these

Jan 1, 1949

By Robert D. Schmidt

The Bureau of Mines is conducting an investigation to develop remediation techniques for residential water wells whose yield has been affected in the long term, by underground mining. Initial work relating to this project was conducted in 1984-1987 at a room and pillar mine in Indiana County, Pennsylvania. Piezometer nest data from the room and pillar mine reveals that a downward gradient in piezometric head exists in shallow strata as a result of drainage into the underlying mine void. The vertical gradient in head in turn results in well bore leakage in open-hole water wells. The relative yield of valley wells is only slightly affected however because the high surficial recharge rate through fractures more than compensates for fracture leakage into the underlying mine. The relative affect of well bore leakage on well yield is greater in certain hillside and hilltop wells that have comparatively low inflow rates at shallow depths. The static water level of such wells is determined to a much greater extent by the chance interception of deep outflow fractures, than is the case for wells drilled in a more intensively fractured valley bottom. The lower static water level of wells that intercept deep fractures does not necessarily reflect the water table conditions outside of a small radius around the affected well. The results suggest that permanently isolating well bore outflow fractures may remediate certain open-hole residential wells that have been affected by high extraction underground mining.

Jan 1, 1986

By Takahiko Okura, Chiharu Tokoro, Shunta Shibuya

Copper concentrates bearing arsenic as enargite (Cu3AsS4) or tennantite (Cu12As4S13) have disadvantage on copper smelting environmentally and economically, so those concentrates should be treated decently. In this paper, some experiments of arsenic removal from several kinds of copper concentrates by heat treatment in an inert atmosphere were discussed. In this study, several samples in which arsenic contents varied 0.18 to 8.3 wt % were heated to the temperature range of 400 °C to 700 °C under argon gas flow during 1 hour. The heat residues and volatilized materials (V.M.) were analyzed by XRD, XRF, ICP-AES, XAFS and MLA to analyze residual concentration of arsenic and residual mineral composition. Experimental results showed that arsenic removal from copper concentrates advanced in 2 steps; at the temperature range of 500 ° C to 550 °C and of 550 °C to 650 °C, respectively. MLA analysis showed that a few of arsenic in enargite was removed by 550 °C heating and a majority of it was still combined with copper and sulfur as tennantite. On the other hand, arsenic in tennantite was removed almost completely by 650 °C heating. Furthermore, a particular type of arsenic mineral, such as Cobaltite (CoAsS) still remained after heating at 700 °C.

Jan 1, 2014

By Gareth Mainwaring

The Cross Harbor Freight Movement Project is currently in the Environmental Impact Statement phase. The scheme is addressing alternative solutions to transport freight across the Upper Bay of New York Harbor, from New Jersey through to Brooklyn, Queens and Long Island. Amongst the alternatives being assessed are two tunnel options; from the north shore of Staten Island through to Brooklyn, and from Jersey City to Brooklyn. These tunnels are approximately 30,000 feet in length, and with up to17,000 feet under the Harbor, would make it one of the longest undersea crossings in the world.. The paper addresses the development of the project, from the Major Investment Study through to the current EIS, and describes the tunnel schemes that are being taken forward. The geological conditions that will be encountered, proposed construction methods, and the ventilation issues associated with such major undersea tunnels will all be described.

Jan 1, 2003

By H. Westengen

The AE alloy family exhibits remarkable combinations of properties when utilized as high pressure die castings. This performance relies on the fact that the rapid cooling rate resulting from the direct contact between the molten alloy and the steel die walls effectively refines the structure through rapid solidification. Furthermore, the rare earth additions modify the solidification pattern, dramatically reducing the solidification interval. A solid shell forms at temperatures exceeding 500C, reducing the tendency for die sticking and inverse segregation. As a result, the die castability is excellent, giving parts with a smooth and shiny surface. Unlike other magnesium die casting alloys developed to improve elevated temperature creep properties, AE alloys do not suffer from the commonly observed tendency to introduce brittleness. This feature is attributed to the fact that the massive magnesium- aluminium intermetallic phase is substituted by a finely dispersed lamellar structure of Al-RE intermetallics. The resulting combination of excellent elevated temperature properties and good ductility, as well as excellent corrosion resistance, means superiority of these alloys for demanding automotive engine and chassis applications.

Jan 1, 2006

By R Bradford, W Gift-Agbey, T Vorster, P Morgan, E Grobler

The Asanko Gold Mine in Ghana started processing ore from the Nkran pit in January 2016 at a production nameplate of 3 Mt/a. The flowsheet is a conventional SAG, ball mill and pebble crusher (SABC) with gravity-gold and carbon-in-leach (CIL) recovery. The nameplate production was comfortably achieved within 3 months, so much so, that it was clear the SABC circuit was capable of processing more than the downstream section of the plant. Consequently, a program of de-bottlenecking was initiated to rectify volumetric capacity constraints. This program was later referred to as ‘Project 5 Million’ (t/a) or P5M. Having completed the de-bottlenecking exercise, it became evident that the SABC circuit could not reach 5 Mt/a solely on hard rock from Nkran. The new challenge was therefore to increase the capacity of the milling circuit through a focused comminution initiative that would address the following: geometallurgical treatment plan; upfront fragmentation requirements; installation of feed and mill monitoring equipment; and integration of a knowledge-based control strategy. This paper takes the reader through the various measures implemented to increase the milling rates and to create a stable/ sustainable control philosophy. As a result of the implementation of advanced mill performance monitoring technology (MillSlicer) and the collaboration between a team of experts in comminution, control and operations, the Asanko Gold Mine process plant feed tonnage has successfully increased from 3 Mt/a to 5 Mt/a.CITATION:Bradford, R, Gift-Agbey, W, Grobler, E, Morgan, P and Vorster, T, 2018. Optimisation of Asanko’s Obotan SABC circuit to achieve ‘Project 5 Million’, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 477–484 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By W. G. Davenport

Methods of extracting copper are evaluated in terms of innovations during the 1970's, and predictions to the end of this century are made. It is concluded that between one and two new smelters and refineries will be needed per year until the turn of the century, and that most of these smelters will be of the oxygen or oxygen-enriched flash furnace type. For converting, the Peirce-Smith converter will still predominate, but the Hoboken converter will play an increasingly important role. Five Japanese pollution control systems are described and it is suggested that much of this technology will be included in future smelting installations. Further growth of hydrometallurgy is predicted, especially for oxide ores, based on improved product metal quality and low plant cost. A n increased level of scrap resmelting is also expected.

Jan 1, 1980

By Lorne Roberts

"This paper describes: how Falconbridge's fire protection system meets the needs of the Lockerby Mine; why the system was chosen over other alternatives; how it is unique, but can be applied to any underground situation; details of the system; how it was installed; the role of a fire protection company; and general considerations when choosing afire-suppresant system.IntroductionIn May 1981, after about three years of searching for the best fire protection system for the re-opened Lockerby nickel mine at Whitefish, near Sudbury, Ontario, Falconbridge Nickel Mines Ltd. installed an AFFF type of fire suppression system. It was designed and supplied by the Fire Protection Systems Division of Levitt -Safety Ltd.The system protects against loss of life, equipment and/or production, and it complies with legislation should fire occur in a fuel storage area and/or scooptram garage and service bay at any or all of the three levels near Shaft No.2.About 18 months after Levitt-Safety began working with Falconbridge, the system was designed and installed at a cost considerably less than that which would be incurred if fire damage caused the loss of two days of production.The fire protection system, which overcomes a limited water supply, is a self-contained balanced pressure proportioning system. It senses the flow and automatically determines the correct concentration of foam to water. It is triggered by a release mechanism which operates a bank of nitrogen cylinders, which in turn pressurize a pressure vessel to expel the foam concentrate and water from the tanks. This solution is piped to sprinkler heads in the specific area."

Jan 1, 1982

By Gordon L. Draeseke

"Before getting into more specific aspects of my talk today I should put in one disclaimer - one week in Mainland China and one day with Premier Kosygin does not make me an expert on Sino-Soviet affairs nor on Canadian-Chinese relations. Perhaps though there is a message in the fact that one meeting took place in relative openness in China and the other was at least partly in a bullet-proof limousine in Canada. I thought it might be interesting and appropriate to explain something of the forest industry to you who are engaged in the mining industry. Our industry, like yours, is based on a natural resource and the basic activity that we engage in is the extraction and conversion of that resource into saleable materials. However, the fundamental difference between our industries is that our resource is on top of the ground - easily visible and easily measurable, whereas yours is under the ground - difficult to find and, having been found, expensive to measure. A second difference is that ours is renewable while yours is extractive, and you must keep finding more to keep up reserves."

Jan 1, 1971

By Isaak I. Maksimov, Tatyana E. Koltunova, Mikhail F. Yemelyanov, Liudmila A. Otrozhdyonnova

"INTRODUCTIONMetals losses amount up to 50% in coarse fractions in (>100 µm) and composite particles, and to 20- 25% in fine fractions (<10 µm) at non-ferrous floatation concentrating plants of the CIS. Therefore, reduction of metals losses in difficult fractions is of high significance.IMPROVEMENT OF FLOATABILITY OF COARSE AND COMPOSITE PARTICLESReagent regimes with application of strong collectors – xanthates ?5-?8, combination of butyl xanthates and aerofloats ?10-?12, butyl xanthates with hydrocarbons are proposed for this purpose. Application of such reagent regimes for copper and copper-molybdenum ores permitted to increase copper and molybdenum recovery by 0.5-3.9%.Studies, performed by means of specially designed non-frothing flotation machine with independently controlled agitation intensity and narrow size-ranges of air bubbles, established that the best results are achieved with employment of bubbles of 0.5-0.8 mm size regarding particles of any size, with small amounts of up to 2 mm size “transport” bubbles to be expediently used for floatation of coarse particles.Energy dissipation in the main volume of floatation cells must be lower than 0.2-0.25 m2/s3.Performed experiments permitted to formulate requirements to development of machine for floatation of coarse and composite particles. Such floatation machine with volume of 8.5 m3 provided for weak agitation in the main volume of floatation cell and uniform distribution of coarse particles throughout the depth owing to establishing of pulp circulation with upward flows. In addition, in the upper part of floatation cell where agitation is considerably weaker, favorable conditions are created for attachment of particles to bubbles. Testing of this floatation machine demonstrated a 7.5% increase in recovery of +0.2 mm particles in pyrite floatation and a 12-14% increase in recovery of +0.2 mm particles in apatite floatation as compared with a reference floatation machine."

Jan 1, 2003

NEW MEMBERS The following list comprises the names of those persons who became members during the period Jan. 10, 1919, to Feb. 10, 1919. ADAMS, FRANCIS SPEARMAN, Supt., Power Dept., Anaconda Copper Min. Co.; Anaconda Mont. ALDERSON, G. E., Min. & Met. Engr 1317 Sloane Ave., Lakewood, Ohio. BENJOVSKY, T. D., Min. Engr., Cons. & Constr 2045 Vine St., Denver, Colo. BROPHY, OSCAR, Met 1523 S. Broad St., Philadelphia, Pa. BUTTRAM, FRANK, Chief Geol., Fortuna Oil Co., 424 Liberty National Bank Bldg., Oklahoma City, Okla. COCHRAN, R. B., Mine Supt., The Teziutlan Copper Co., Aire Libre Puebla., Mexico. CONNAR, T. C., Civ. & Min. Engr. & Geol.; Chief Engr., Zanesville Coal Co., Zanesville, Ohio. DAVE, E. O Capt., Co. A, 212th Engineers, Camp Devens, Mass. FOLEY, CHARLES B., Electro-Met., Martin Rockwell Corpn., 347 Madison Ave., New York,. N. Y. HOSFORD, WILLIAM F., Asst. Tech. Supt., Western Electric Co., Inc., Hawthorne Station, Chicago, Ill. HOSTER, M. T., Supt., French Creek Mines, E. & G. Brooke Iron Co., St. Peters, Pa. KAWASAKI, SHIGETARO, Chief Geol., Geological Survey of Chosen, Government General of Chosen, Keijo. Korea.

Jan 3, 1919

By P. Otto, G. Borm, Th. Dickmann, F. Amberg, R. Giese

Based on many years experience, the well approved Tunnel Seismic Prediction System (TSP) has been substantially enhanced for online geological prognosis in underground construction. The method provides high resolution seismic images of the rock mass ahead of a tunnel face via an array of standard anchor rods. These contain3D-geophones and can routinely be installed during the excavation process. A further outstanding feature of the system is the newly developed high frequency repetitive seismic source which can easily be fixed at a tunnel boring machine. A user-friendly software package enables online data acquisition, processing, 3D-visualization, and interpretation.

Jan 1, 2001

By Aziza A. Yousef, Suzan S. Ibrahim, Mahmoud A. Arafa, Mohamed A. Abdel Khalek

Due to the shortage of fresh water in the Middle East, seawater has been used as an alternative in flotation beneficiation. The flotation process requires about 7 m3 of water/mt ore. This article aims to study the effect of seawater cations and anions on the flotation. Natural pure francolite, calcite, dolomite and quartz were characterized by chemical, thermal and x-ray diffraction analyses, surface area, solubility and zeta potential. Synthetic seawater was prepared with the major chemical composition similar to natural seawater as follow; 2.45% NaCl, 0.52% MgCl2, 0.41% Na2SO4, 0.116% CaCl2 and 0.07% KCl. Also, natural seawater was used in application. The point zero of charge was estimated at pH 6.5, 7.8, 9.2 and 2.2 for francolite, calcite, dolomite and quartz, respectively. Calcium ions were released from the three minerals with Mg2+ and P2O5 3– released from dolomite and phosphate, respectively. The adsorption of collector, zeta-potential and floatability of pure minerals were studied. The effect of individual cations and anions predominant in seawater are studied on individual mineral or group. The troublesome Ca2+ and Mg2+ ions should be controlled by soda ash addition. Sodium silicate improved the selectivity of mineral mixtures and natural ore. At optimum conditions the calcareous phosphate ore yielded a concentrate of 34% P2O5, at 83% recovery with 0.61% MgO, from an ore assaying 25.3% P2O5 and 9.4% MgO. To minimize the Clcontent, fresh water of about 0.5 m3 /t was used and the Cl- decreased to about 0.09 %

Jan 1, 2003

By R. V. Vines, E. M. Wise

It is known qualitatively that the recrystallization behavior of platinum is dependent upon the amount and particularly the nature of impurities present, the amount of prior cold-work and the annealing time and temperature, but published data are limited. A study of the effects of cold-work and annealing temperature on the hardness of a sample of very pure platinum was undertaken to supply part of this information. Conclusions 1. The platinum used in the experiments had a probable platinum content of 99.99+ per cent, and had the following mechanical properties in the completely softened condition: Vickers hardness number, 39.4; ultimate tensile strength, 19,340 lb. per sq. in.; proportioilal limit, very low; elongation, 37.5 per cent in 2 inclles. 2. The effect of cold-rolling on the hardness is shown in Fig. 1. The hardness increases rapidly up to 10 to 15 per cent reduction and more slowly up to about 75 per cent reduction, beyond which it increases more rapidly. 3. The recrystallization temperatures for a 15-min. anneal, after cold-rolling 19, 39.5, 50.8, 66, 80.5 and 89.5 per cent reduction in thickness, are approximately 765°, 700°, 635°, 600°, 545&apos; and 425°C., respectively. 4. The recrystallized grain size of this platinum is a function of the percentage of cold reduction, being larger the lower the percentage of cold-work. 5. Little or 110 grain grourtll resulted from subjecting recrystallized samples to higher temperatures or annealing for longer times. Prior Work As already mentioned, data on the recrystallization of platinum are scarce. Gmelin&apos;sl handbook, which summarizes data published earlier than August 1938, lists values ranging from 400&apos; to 810°C. for the minimum temperature of recrystallization of samples with rather indefinite

Jan 1, 1940

By E. M. Wise, R. V. Vines

It is known qualitatively that the recrystallization behavior of platinum is dependent upon the amount and particularly the nature of impurities present, the amount of prior cold-work and the annealing time and temperature, but published data are limited. A study of the effects of cold-work and annealing temperature on the hardness of a sample of very pure platinum was undertaken to supply part of this information. Conclusions 1. The platinum used in the experiments had a probable platinum content of 99.99+ per cent, and had the following mechanical properties in the completely softened condition: Vickers hardness number, 39.4; ultimate tensile strength, 19,340 lb. per sq. in.; proportioilal limit, very low; elongation, 37.5 per cent in 2 inclles. 2. The effect of cold-rolling on the hardness is shown in Fig. 1. The hardness increases rapidly up to 10 to 15 per cent reduction and more slowly up to about 75 per cent reduction, beyond which it increases more rapidly. 3. The recrystallization temperatures for a 15-min. anneal, after cold-rolling 19, 39.5, 50.8, 66, 80.5 and 89.5 per cent reduction in thickness, are approximately 765°, 700°, 635°, 600°, 545&apos; and 425°C., respectively. 4. The recrystallized grain size of this platinum is a function of the percentage of cold reduction, being larger the lower the percentage of cold-work. 5. Little or 110 grain grourtll resulted from subjecting recrystallized samples to higher temperatures or annealing for longer times. Prior Work As already mentioned, data on the recrystallization of platinum are scarce. Gmelin&apos;sl handbook, which summarizes data published earlier than August 1938, lists values ranging from 400&apos; to 810°C. for the minimum temperature of recrystallization of samples with rather indefinite

Jan 1, 1940