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Jan 1, 1935

By R. M. Brick, Arthur Phillips, A. J. Smith

A PREVIOUS publication1§ has described the effect of quenching stresses on the lattice parameter values of high-purity aluminum-copper alloys particularly with reference to the solution and precipitation of CuA12. A similar study has been made of the aluminum-rich aluminum-magnesium alloys. Attention has been directed in the present investigation. to the magnitude of the quenching stresses as affected by the specimen size and shape, the number of solute atoms and the quenching rate. The effect of cooling stresses in causing plastic deformation or cracking has been considered in relation to the physical properties of the alloy. On reheating alloys in the two-phase field, the time required for precipitation to occur has been observed in connection with the degree of supersaturation, the rate of diffusion of the solute atoms as a function of the comparative atomic radii, degree of strain, temperature of reheating and grain size. A few qualitative comparisons on the relative effect of these factors have been drawn between the aluminum-copper alloys and the aluminum-magnesium alloys. STRAIN IN SOLID-SOLUTION ALLOYS A 10 per cent magnesium alloy in the form of chill-cast bars was furnished by the Aluminum Company of America through the courtesy of L. W. Kempf. Additional alloys were prepared using aluminum (99.95 per cent Al) and high-grade magnesium. The alloys listed in Table 1 were melted in an Acheson graphite crucible under a flux of fused MgCl2, CaC12, NaCl. Chill-cast rods were sealed under vacuum

Jan 1, 1935

By E. S. Rowland, Clair Upthegrove

The widespread interest in the alloys of beryllium with copper is due principally to the fact that certain compositions show very favorable precipitation-hardening characteristics and are, in fact, the stronges nonferrous alloys known at the present time. Investigations have been conducted by Masing and Dahl and others on the physical characteristics of ternary beryllium alloys, in an attempt to produce precipitation hardening effects with a smaller amount of beryllium than that required in the binary copper-beryllium alloys (2.0 to 2.5 per cent Be). The results of these investigations show that ternary alloys of beryllium with Cu-Sn, Cu-A1 and Cu-Zn, among others, exhibit promising improrcmc~nts in physical properties after precipitation-hardening treatment and, while the increases in properties obtained are not as high as those reahzed from the binary copper-beryllium alloys, excellent properties arc obtaincd with beryllium contents averagirlg about one-half the amount reqnired in the binary alloys. This paper presents the results of an investigation of the equilibriun relations of certain alloys containing copper, tin and beryllium. The alpha-phase boundary of the ternary system is given for alloys containing from 0 to 1 per cent beryllium. The equilibrium conditions beyond the alpha-phase boundary are presented for alloys containing up to 32 per cent tin and 1 per cent beryllium. The data were collected by means of quenching experiments, microscopic examination and thermal analysis The results of some powder-method X-ray determiniations on the alloys, conducted by Mr. William Mikulas and Prof. Lars Thomassen at the University of Michigan, are used as evidence in this paper. The con

Jan 1, 1935

By Russell W. Dayton

The metallurgical polarization microscope has been utilized in several researches in the last few years, thus attaining a fair degree of prominence, but little has been written in a manner suitable to a metallurgist concerning the theory of this instrument. In this investigation the theory was carefully studied, and the results are presented here in a detailed manner, yet as simply as possible. The theory is discussed with particular reference to the three chief functions of the instrument: (1) determination of anisotropy; (2) effect of strain; and (3) identification of inclusions. Each of these is investigated experimentally, with especial attention to the mechanism of producing any effect. Where possible, the discussion is supplemented by photomicrographs. The instrument used had numerous defects as a polarization microscope; these and their remedies are discussed. In the microscopic study of transparent mineral sections (chalcography) the use of polarized light has aided tremendously in the identification of a mineral. The determination of strain in transparent substances (photoelasticity) by the use of polarized light has lately become a commercial process, used in testing finished glass articles. The success of the use of polarized light with opaque materials has not been so great. The magnitude of the effects obtained is much less than that of the corresponding effects with transparent materials, and the mechanical difficulties are much greater. Königsberger,"' i in 1909, was the first to apply polarized light to the microscopic study of opaque substances; Endell and Hanemann(2) were the next, in 1913. In 1919 and 1920, Wright(3,4) prepared two papers on the subject. In the first he developed the detailed mathematical theory from the viewpoint of the electromagnetic theory of light, and in the second described the various methods in use, giving improvements of his own. Schwarz(5)

Jan 1, 1935

By Kirkhouse C. B

Soon after the Broken Hill Limited started operations at their Iron and Steel Works at Newcastle, NSW, it was found necessary to install a mill for rolling small merchant bars, rounds, etc.An arrangement of the first mill laid down is shown on Plate 1., Fig. 1. This mill commenced operations on the 18th July, 1917.The feed for this mill was rolled in the existing 18-in. mill and sheared to the lengths required before being delivered to the billet storage yard. The billet storage yard is 90 ft. span, and is served by one 10-ton electric overhead travelling crane. Billets were placed on the billet bed preparatory to being charged into the heating furnace.The heating furnace was of the continuous recuperative with end discharge and had a hearth 40 ft. long by 10 ft. wide. The billets were pushed through the furnace by means of two hydraulic rams, which could either act together and push one row of billets, or act singly and push two rows of billets. This furnace was fired by producer gas from the producers shown on Plate I., Fig. l.The gas was conveyed to the furnace by means of a brick underground flue.

Jan 1, 1935

By Theron Wasson

Discoveries in Michigan, which at the beginning of the year 1934 indicated possible new areas, did not develop into fields of market-breaking proportions. Hart, Oceana County, developed small production from the Traverse lime. Edmore, Montcalm County, proved a small area for oil from the Traverse. West Branch, Ogemaw County, previously reported as Ogemaw, had quite a drilling campaign but was somewhat disappointing because wells were small and erratic. During the year, 30 wells were completed at West Branch, and at the end of the year 15 others in and around this field were under way. At West Branch the Traverse lime, found at 1800 ft., has thin porous streaks near the top, which make small wells; the Dundee lime at 2800 ft. produces from a porous zone of varying thickness. Over the entire field the Dundee wells average 10 to 20 bbl. per day. Acid treatment has materially increased production from some Dundee wells in this field. About 3000 acres have been proved productive from the Traverse and Dundee. At the close of the year the well in Beaverton township, Gladwin County, is probably the most discussed of any in Michigan and may be opening a new field of some proportions. It had an initial production of 70 bbl. daily from the Dundee lime at 3830, which has decreased to 25 bbl. per day. Deeper drilling into the lime may increase production. During 1935 the area around this test will probably be the most active in the state. Structural conditions in Gladwin County, as in other parts of Central Michigan, are obscured by a thick mantle of glacial drift and it will take considerable drilling to outline subsurface conditions accurately. The most important new shallow gas area of the year is around Edmore in Mecosta and Montcalm counties. Eight wells have been drilled to the Michigan stray and the upper Marshall sand, having a combined initial production of 30 million cubic feet. These gas wells are scattered over so wide an area that an estimate of proven territory cannot be made until more drilling is done. At the present time no gas is being sold from Edmore.

Jan 1, 1935

By Walter Kauenhowen

The production of crude oil in Germany during 1934 totaled about 2,200,408 bbl., a 33 per cent increase over the 1,670,109 bbl. produced in 1933. This is an extension of a yearly increase which has continued uninterruptedly since 1928. Producing Fields The 1934 increase in production is due chiefly to developments in the north district of the Nienhagen field, where the production in 1934

Jan 1, 1935

Jan 1, 1935

By John R. Freeman

THIS paper relates entirely to the casting of brass under fluid pressure in steel dies Die castings of metals and alloys of low melting point have been available for many years but the development of brass die castings has been relatively recent, occurring within the past five years The successful development of brass die castings has resulted from the availability of alloy steels that would give satisfactory life as dies and the development of suitable die-casting machines The melting point of copper is 1084° C (1983° F ) and of a high brass about 900° C (1652° F ), as compared to 327 5° C (6215 °F) for lead, 419 4° C (786 7° F) for zinc and 658 7° C (1217 7° F) for aluminum, temperatures that ale indicative of the casting temperatures required for the various types of alloys, of which the melting points are somewhat lower than those of the pure metals TYPE OF DIE-CASTING MACHINE In the well-known plunger and gooseneck types of die-casting machines used for casting the alloys of relatively lower melting point, much of the working mechanism is immersed in the molten alloy For alloys having the relatively high melting point of brass, this obviously is impossible Machines with a separate melting chamber are essential Two rather distinct types are in extensive use at the present time, the Pack and Polak machines, the former designed by Charles Pack and developed at the American Brass Co , the latter developed by Zoseph Polak, of Prague, Czechoslovakia The principles of operation of these machines have been described in articles by Pack1,2,3 and by Sieg 4

Jan 1, 1935

By Ott F. Heizer

The mines and the mill of the Nevada-Massachusetts Co. are on the east slope of the Eugene Mountains, in Pershing County, Nevada, 8 miles northwest of Mill City, a station on the Southern Pacific R.R. and on the Victory Highway. Fig. 1. Supplies and, concentrate are transported by truck over an automobile road of easy grade. The property is at an average elevation of 5500 ft. and climatic conditions are generally favorable for continuous operation throughout the year. The ore treated is supplied by two adjoining mines, the Stank and the Humboldt. Physical and mineral characteristics of the ores produced by these two mines are substantially similar, although variations occur in hardness and mineral distribution.' The economic mineral is scheelite (CaWO4), composed, when pure, of 80.6 per cent tungstic trioxide (WO3) and 19.4 per cent lime (CaO).

Jan 1, 1935

By Heber Cole

THE gypsum industry of Canada, like all others connected with the construction business, has felt the full effect of the depression during the past few years, and sales of its products have been greatly curtailed. The year 1934, however, saw a decided turn for the better and a gradual but steady improvement is noticeable in all its branches. In many ways the depression has been a blessing in disguise to the gypsum industry; during the years from 1926 to 1930, demand increased so rapidly that companies were forced to expand and often new apparatus and machinery were placed in operation regardless of expense, or plants already existing were taxed to their limit and forced to keep running with the minimum amount of repairs. The depression, therefore, has really given the industry what might be called a breathing spell, in which it has had time to take stock of its position, to reduce its costs of production, to devote more serious attention to the quality of its products, and to con-solidate its operations into a smooth working whole, which as conditions improve will enable it to meet the demands of the trade with more varied products of a quality hitherto unattained. Progress in the gypsum industry, however, has not been confined to the years of the depression, for some of the greatest advances occurred under the spur of increased demand for its products by the building trade. The purpose of this paper is to review briefly some of the out-standing trends in the development of the gypsum industry in Canada during the past 10 or 12 years.

Jan 1, 1935

By Mark Malamphy

DURING the latter part of the year 1932, the Servico Geologico e Mineralogico do Brasil ordered four magnetic field balances with tem-perature-compensated magnetic systems and a photographic recording apparatus for the registration of the diurnal variation. These instru-ments were delivered during the early part of the year 1933 and a short time later were taken to Santa Catherina for use in the field. Before the field work was begun, a series of experiments was carried out to determine the behavior of these new instruments under existing field conditions. The recording instruments were mounted in an under-ground chamber and their sensitivities checked by means of a Helmholtz coil. The field instruments were then mounted at fixed stations and readings were taken to determine the diurnal variation and compare it with the photographic records. The data obtained with the horizontal field balances were concordant but that obtained with the vertical component instruments showed a considerable divergence. This divergence was of such a magnitude that it was necessary to spend considerable time in determining its cause and finding a means of improving the functioning of the instruments. This paper presents the results of our observations on these systems and the conclusions at which we arrived; also the means we took to partly elimi-nate the difficulty until new systems could be ordered from Germany.

Jan 1, 1935

All the TECHNICAL PUBLICATIONS and CONTRIBUTIONS published in 1934 are available at Institute headquarters, unless otherwise noted They are also on file in many public, university and technical libraries and, when so indicated in the list, may be found in the TRANSACTIONS Copies of the TECHNICAL PUBLICATIONS have been mailed to those members of the Institute who are registered in the different classes A-Metal Mining, B-Milling and Concentration; C-Iron and Steel Division; D-Nonferrous Metallurgy; E-Insti¬tute of Metals Division; F-Coal Division; G-Petroleum Division; H-Nonmetallic Minerals; I-Mining Geology; J-Mineral Industry Education Division; K-Mining Administration; L-Geophysical Prospecting Other members may obtain copies by writing to the Secretary Copies of CONTRIBUTIONS may also be obtained from the Secretary's office Additional copies are sold at the rate of 1 cent per page, minimum charge, 25 cents Nonmembers may purchase the papers at the prices mentioned

Jan 1, 1935

By Russell Dayton

THE metallurgical polarization microscope has been utilized in several researches in the last few years, thus attaining a fair degree of prominence, but little has been written in a manner suitable to a metallurgist concern-ing the theory of this instrument. In this investigation the theory was carefully studied, and the results are presented here in a detailed manner, yet as simply as possible. The theory is discussed with particular reference to the three chief functions of the instrument: (1) determination of anisotropy; (2) effect of strain; and (3) identification of inclusions. Each of these is investigated experimentally, with especial attention to the mechanism of producing any effect. Where possible, the discussion is supplemented by photomicrographs. The instrument used had numerous defects as a polarization microscope; these and their remedies are discussed. In the microscopic study of transparent mineral sections (chal-cography) the use of polarized light has aided tremendously in the identification of a mineral. The determination of strain in transparent substances (photoelasticity) by the use of polarized light has lately become a commercial process, used in testing finished glass articles. The success of the use of polarized light with opaque materials has not been so great. The magnitude of the effects obtained is much less than that of the corresponding effects with transparent materials, and the mechanical difficulties are much greater. Konigsberger,(1)? in 1909, was the first to apply polarized light to the microscopic study of

Jan 1, 1935

Jan 1, 1935

By Anthony Anable, J. V. N. Dorr

When separate treatment of sand and slime by cyanidation was the rule rather than the exception, as now, and when gravity concentration, rather than flotation, was the accepted method of dressing copper, lead, zinc and other base ores, classification was a separate step in ore treatment. Today, however, the picture is much different. The trend toward all-slime treatment in cyanidation and flotation has made fine closed-circuit grinding essential, and the mechanical classifier is of equal importance with the mill in the preparation of an ore for its treatment. Actually, a mill and classifier are a unit, a variation in either affecting the desired results. In developing this thesis—the mutual interdependence of the rotary mill and the classifier in modern fine-grinding practice—it would be well to consider first the different types of classifiers and mills in use today, their scope and limitations and the factors governing their selection. From such a basis as this a logical approach may be made to modern closed-circuit fine grinding, the evolution of multiple-stage grinding practice, the relation of the classifier to the mill and, finally, the trend to higher and higher circulating sand loads in the mill-classifier circuit. Such data as are germane to the subject will be given to support the thesis advanced. Mechanical Classifiers Theory.—Stokes' law, applicable to the uniform slow motion of a rigid sphere in a viscous fluid of infinite extent, states that the velocity of a particle settling under the influence of gravity is a function of the square of its radius: _ 2 g(ds - de)?2 v =9 S Where V = velocity of particle in cm. per see. g8, acceleration due to gravity d8, density of particle de, density of fluid ? = radius of particle S = viscosity of fluid

Jan 1, 1935

By Ravitz, S. F

76-B Unpublished manuscript. Not available in printed form. An experimental and Theoretical investigation of Quantitative Microscopic Mineralogical Analysis. By S.F.Ravitz and H.A.Steane. Manuscript in Engineering Societies Library.

Jan 1, 1935

An Outline Classification of Mining Systems for Ore and Coal. See COAL Progress at the Homestake Mine. By Guy N. BJORGE. (Min. & Met., June, 247. 4400 words.) Homestake's mining methods today are controlled to a con¬siderable extent by that which has been done in the past. The two main operating shafts were begun m 1878 and 1896 respectively, so that the location of shafts, loca¬tions of all the drifts on the upper levels, and a great deal of stoping was done before any of those now connected with the mine had anything to do with it In this paper is described the general plan of development. A table shows percentage of total production mined by the different methods in recent years. Average daily produc¬tion for several years now has been about 3850 tons milled. With the present schedule of 6-day operation of the mine, that means about 4450 tons a day mined This ore is treated at three plants, with respective capacities of 2000, 1200 and 600 tons The principal novelty in milling is at the largest mill where the stamps are used as crushers only, and where in the last two years a notable increase has occurred in the size of screens used A unit has been added to cyanide plant No 3 The construc¬tion of a new shaft is described, as is also the hoist building The company operates its own lumber and timber department It has a well equipped hospital Housing at Lead is an individual matter. Rejuvenating the Golden Chariot Property in Idaho. By R. S. MCCLELLAN (Min. & Met, November, 443. 2300 words) An effort to rejuvenate the Golden Chariot group of properties near Silver City is now being carried on by the John Hays

Jan 1, 1935

By R. K. Hopkins

Fox a great many years fusion welding has been used in and around petroleum refineries, but it is only within six or seven years that the more important pressure vessels have been constructed by this process, because before that time the properties of fusion welds would not withstand such rigorous service. Since the adoption of fusion welding for the construction of this equipment, the refiner has required pressure vessels suitable for operation over a very wide range of conditions. On the one hand, vessels must operate at extremely high temperatures, in the range of 950° to 1000° F., and on the other vessels must be suitable for operation at sub-zero temperatures down as low as -75° F. Also, vessels are required suitable for operation at pressures upwards of 1000 lb. per sq. in., and as low as a 29-in. vacuum. In addition, vessels are required to withstand the attack of very corrosive mediums. It has been a rather difficult task for the fabricator to meet all of these requirements, but as a result of the extensive research carried on by steel manufacturers and several fabricators of class I vessels, practically all of these demands have been met. In order to meet the refiners' requirements for this wide range of conditions, the fabricator has worked closely with the metallurgist. This has enabled him to choose the proper base metal for each service condition, but it has been the fabricator's problem to develop a welding rod and welding technique, as well as a heat-treatment, that would produce in the welded vessel characteristics in and around the weld comparable to those in the base metal. Where corrosion is not a serious problem, and where the operating temperatures are not too high, ordinary carbon steel has served very well. But when corrosion is serious, and/or when the temperatures are either very high or very low, it is necessary to use some form of alloy steel to give satisfactory service.

Jan 1, 1935

By A. L. Field

This general subject has been so thoroughly discussed by Dr. Herty and his associates, especially with regard to the degree of oxidation of the metal at the time that the silicon pig or spiegel is added, that I am not going to spend much time on that today. I should like to propound a question, which is based on my own observations made some years ago while with a large alloy-steel company which had two open-hearth furnace plants. It is true that one of these plants was not engaged particularly in making alloy steels, but there were certain relations between slag and metal composition which appeared to me to be entirely different in the two plants. I have an explanation for it that is more or less incomplete, but possibly Dr. Herty or Mr. Reinartz or some of the others may be able to complete it. Suppose we take our three layers; the metal on the bottom, on top of that the slag, and on top of the slag, the gas. We cannot overlook the gaseous phase. Regardless of the effect of the iron oxide in the slag on the rate of carbon elimination—and that, of course, is rather important in alloy practice since it is not desirable to have the carbon dropping too rapidly at the time the deoxidizing is had in the furnace—it will probably be admitted that it depends on the iron oxide in the metal for a given carbon oxide. I have seen cases where with approximately identical metal and slag compositions one furnace would work twice as rapidly as another in removing carbon. Of course, there is some explanation of this in what others have already said, that the question of the exact lime and silica content of the slag determines the activity and viscosity of the slag; but I am convinced, without having reviewed the actual records since I was asked to make this talk, because they were not available at the time, that the slags in these two furnaces were not materially different. Putting it another way, one furnace would have

Jan 1, 1935