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By R. G. O’Meara, M. M. Fine

ONE of the principal activities of the Bureau of Mines connected with the recent war was to help to increase the supply of strategic and critical minerals. Fluorite was one of the most critical of the nonmetallic minerals because of the increased demand for it as a flux in basic open-hearth and electric steel furnaces and as a raw material for the production of artificial cryolite used in the aluminum industry. Wartime developments in the technology of hydrofluoric acid, such as the use of the anhydrous acid as a catalyst in production of high-octane gasoline and the use of organic fluorides as carriers for insecticides, also increased the demand for acid-grade fluorite.[t] In 1943 the consumption of acid-grade fluorite was advancing at a more rapid rate than production, and was only slightly less than production during the latter half of the year.1 The outlook for the postwar market for fluorite is encouraging. Steel production is expected to remain high until the domestic demand for commodities not manufactured during the war is satisfied. The uses for hydrofluoric acid are expected to increase under the impetus of war-initiated research. In consideration of these and other factors some authorities predict a postwar demand for fluorite equal to about 60 to 75 per cent of the wartime production.1,2 Others believe that the postwar fluorite industry will be permanently expanded over its prewar status.3 ACKNOWLEDGMENT This paper is one of many reporting on various aspects of the Bureau of Mines program directed toward the more effective utilization of our mineral resources. The program has been under the general supervision of R. S. Dean, Assistant Director, since July 1942. The scope of the paper falls in the province of the Metallurgical Branch, whose activities embrace the separation of difficultly beneficiated ores, the production of pure metals from domestic deposits, the exploitation of marginal ore reserves, the recovery of secondary metals, and the improvement of present industrial metallurgical practice. The investigation was initiated at the request of Mr. J. H. Steinmesch, vice-president and general manager, Minerva Oil Co., Eldorado, Ill. His hearty cooperation and helpful suggestions, and those of Mr. O. E. Anderson, mill superintendent,

Jan 1, 1946

By S. A. Rholl

This paper describes the Bureau of Mines experimental test program which evaluated the effectiveness of using high explosives to enhance orebody permeability. To determine the effect of stress on the fracture network generated by blasting, fifteen single-hole laboratory tests in granite blocks up to .067 m3 (2.4 ft3) in size were blasted using .12 to .20m (4.8 to 8.0 in) of 1.6xl0-3-, 3.2xl0-3-, or 6.5xl0-3-kg (25-, 50-, or 100-grain) detonating cord. In situ stresses were simulated using polyaxial load cells to apply uniform stresses of 1.72xl06 to 1.76xl07 Pa (250 to 2550 psi). All of the blocks were sawed to expose the blast-induced fracture patterns for analysis.

Jan 1, 1991

By R Neivandt, Kane, M O&apos, D Browne

Newmont Australia is the operator of the Mt Leyshon mine near Charters Towers, Queensland. Mt Leyshon is an open cut gold mine, which processed on average 5.0 Mt of ore and produced up to 250 000 ounces of gold per year. Mining was completed in early-2001, followed by treatment of low-grade ore stockpiles for a further 12 months. Approximately 250 ha of waste rock dumps have been rehabilitated. Rehabilitation of two of the three tailings storage facilities (TSF) has been completed and the third is in progress. A field performance monitoring system that includes an automated meteorological station, large-scale lysimeters (measurement of net percolation), and in situ moisture content sensors (measurement of moisture storage changes in the cover material) were installed to monitoring performance of the cover systems placed on the waste storage facilities. This paper focuses on the installation and calibration of the in situ moisture monitoring system. The moisture monitoring system provides automated detailed in situ volumetric water content data above and within the large-scale lysimeters. A portable unit that provides spatial in situ moisture content measurements at additional locations on the cover system is also utilised. The paper will focus on installation and calibration of the in situ water content monitoring instrument in the waste rock, coarse cover material, and fine textured cover materials of the tailings facility and waste rock dump cover systems.

Jan 1, 2003

By R. R. Klimpel

The process of flotation is an extremely important solids separation technique employed in a wide variety of industrial process applications. Froth flotation is practiced in the coal industry to recover fines produced during the mining and cleaning of coal. A recent review article by Aplan (1) covers the processing variables encountered in the flotation of coal and the variety of chemicals and operating conditions which affect recovery. Numerous engineering and scientific studies have been performed with the goal of providing semifundamental laws of flotation behavior for improved screening of flotation chemicals, better equipment scale-up factors, etc. Often the results of such work are expressed in the form of mathematical models (e.g. 2, 3, 4, 5, 6) which are potentially useful for evaluating (simulating) on paper such alternatives as possibles process operating or configuration changes, the effects of ore and reagent changes, etc. It appears to be commonly accepted that a complete scientific/engineering characterization of flotation is immensely complicated and not sufficiently developed at the present to accurately predict (or understand) many important industrial facets of flotation. Thus, one is often reduced to detailed experimental characterization in both the laboratory and plant in order to fully evaluate flotation changes or alternatives. It is the purpose of this paper to describe a method of batch laboratory data characterization that is useful in evaluating flotation chemical reagents including froth flotation of coal. The approach consists of running a series of time-recovery curves in a batch float cell followed by the computer curve fitting of this data to a series of mathematical models based on semi-physical reasoning. The unknowns or parameters of these models are then optimally chosen so as to best fit the experimental data. It has been found in both coal and mineral systems that changes in reagent type, concentration, system pH, grind, etc. cause very consistent and logical changes to

Jan 1, 1979

By Richard A. Mullins, James J. Merle

Systematic sampling and analysis in coal-washing plants results in product control and economical operation. A well-organized laboratory system reduces operating costs and increases sales if the operating and sales companies make full use of information it supplies. The operating cost of a control laboratory is less than 1 pct per ton of coal produced.

Jan 5, 1950

By D W. Airey

Frictional rock bolts are widely used because of their low cost. However, they have a thin wall section that makes them prone to corrosion, and they cannot be relied on to provide long-term ground support. It is difficult to assess the capacity after the bolts have been installed as they can only be pulled out if this has been allowed for during insertion. The questions of how long can the rock bolts function effectively and the effectiveness of various surface coatings, which can have significant cost implications are, investigated in this study.A series of accelerated corrosion tests have been performed on frictional rock bolts. The rock bolts, typically 900 mm long, have been inserted into concrete cylinders produced using a styrofoam insert to create the hole for the bolt insertion. Strata rock bolts with four surface coatings have been tested: uncoated black steel, galvanised, enduro (plastic coated) and coated with a proprietary aluminium/zinc alloy. Tests have been performed on two diameters of bolts. Following insertion of the bolts, the concrete cylinders were placed in a large drum filled with saltwater and current was applied to accelerate the corrosion process. The rock bolts were then extracted at various times after the commencement of corrosion. Comparison of the insertion and extraction resistances shows that corrosion initially increases the bolt resistance and that substantial section loss is required for the bolt resistance to drop significantly.CITATION:Airey, D W, 2014. Laboratory corrosion tests of frictional rock bolts, in Proceedings AusRock 2014: Third Australasian Ground Control in Mining Conference , pp 257–262 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Nov 5, 2014

By W. L. Freyberger

In many papers concerned with fundamentals of the froth flotation process, authors have considered the contents of a flotation cell to be comprised of two immiscible phases, the froth and the pulp. I (Of course, each of these phases is in turn made up of several solid phases plus air and water.) This generalized concept of the flotation system can be extended by considering the cell contents to include two phases: an extracting phase, the air bubbles plus the collector, which removes a selected mineral component from the second phase, the ore pulp. Thus, there is an analogy between a flotation system on the one hand, and chemical extracting systems, such a solvent extraction system or a leaching system, on the other hand. Such extracting systems may be operated in cocurrent or countercurrent fashion. This paper includes first a brief discussion on the general nature of cocurrent and countercurrent operation as applied to froth flotation, and then presents the experimental results of flotation of a specular hematite ore by each method, using a tall oil fatty acid as collector. Cocurrent Flotation A conventional flotation circuit involving roughing, scavenging, and cleaning flotation is illustrated schematically in Figure 1. In such a circuit the col¬lector, or extractant, and new feed ore enter together at the head of the rougher circuit, and flow cocurrently to the scavenger circuit where more collector is added. According to this practice, sufficient collector is added to the head of the rougher (and scavenger) so that the final tailings are of low enough grade to be discarded. Since the flow of collector and ore is cocurrent, the process consists of single stage contact between the extracting phase and the ore pulp. If the scavenger concentrate is recycled to the head of rougher, the overall circuit has some of the characteristics of countercurrent flow. In such a case part of the extractant (collector) is added at the discharge end of the circuit, and may

Jan 1, 1971

By Z. Henderson, J. Saylor, L. R. Mendoza

"Diesel particulate Matter (DPM) is a byproduct of fuel combustion in diesel engines. It is classified as a carcinogen, with associated respiratory and cardiovascular health effects. The composition, size, and concentration of DPM is dependent on factors such as engine type, loading and fuel composition. Though a number of DPM abatement and control strategies currently exist, particularly in underground mining environments, occupational exposures remain a serious health concern. As a novel abatement approach, DPM scavenging by fine water or “fog” droplets has been proposed and a laboratory set-up has been built to test the efficacy on engine exhaust. Here, we describe a series of tests that varied engine load, system flow rate and fog drop number density. While none of these factors had overwhelming effects on the results within the ranges tested, the improvement in DPM mass removal attributed to the fog treatment was about 45% on average in comparison to no treatment. INTRODUCTION Diesel engines have seen widespread use for well over a century due to their relatively high thermal efficiency and fuel economy1. More recently, however, adverse health risks of diesel exhaust have become increasingly clear. Many of these risks are associated with the physical and chemical properties of exhaust components1–3. The term diesel particulate matter (DPM) is used to refer to the solid components of diesel exhaust, which are a mixture of elemental and organic carbon (EC and OC) and minor constituents including sulfates and metal ash3. The OC fraction of DPM results from unburned fuel and lube oil, whereas EC or soot is formed during the combustion of locally rich regions within the fuel. DPM is classified as a carcinogen6,7 and epidemiological studies have demonstrated a positive correlation between long-term exposure to DPM and other combustion-related fine particulate and increased cardiovascular and pulmonary diseases8,9. Diesel engines operate in relative fuel rich/oxygen lean conditions and are characterized by relatively high emissions of particulate as compared to spark-ignition engines2,3,10. Typically, these emissions range from 107 – 109 particles/cc and cover two primary size ranges: the nuclei mode where particles have diameters less than about <50 nm, and the accumulation mode where diameters are from about 50-10,000 nm. Most OC resides in the nuclei mode as semi-volatile compounds, while most EC is in the accumulation mode3. The physical and chemical properties of DPM vary with the type of engine, fuel (e.g., petro- vs. bio-diesel) and operating conditions such as loading (i.e., a function of torque and rotational speed)2,3,9,11,12. Loading is a particularly important factor with respect to DPM toxicity9,13,14, and on the effectiveness of after-treatment technologies2,3,15. Engine load alone can affect the EC/OC ratio, and the size distribution and number density of DPM. For diesel engines, the load is roughly proportional to the equivalence ratio3, defined as the actual fuel/air ratio over the stoichiometric fuel/air ratio for complete combustion. Light loads generally favor the formation of OC and small particles. As load is increased the volatiles are oxidized leading to larger soot particles (i.e., EC), but lower total number density of DPM. With further loading, the formation of soot offsets the decrease in volatiles, resulting in increased DPM mean size and number density3."

Jan 1, 2017

By Z. Henderson, J. R. Saylor, L. Rojas-Mendoza

"Diesel particulate matter (DPM) is a major occupational health hazard in underground mine environments, even with available abatement technologies. Prior work has demonstrated that micrometer-scale water droplets, or “fog,” may be effective in removing significant number fractions of DPM from a conditioned exhaust stream. Here, a series of laboratory experiments are described which demonstrate that such a treatment can remove significant DPM mass from an unconditioned stream. The removal mechanism involved coagulation of the DPM and drops. The fog treatment removed about 45 percent more DPM mass on average than no treatment. Varying engine load, flow rate and fog droplet number density did not significantly affect the results under the range of conditions tested. IntroductionDiesel engines have seen widespread use for well over a century due to their relatively high thermal efficiency and fuel economy (Heywood, 1988). Recently, however, the adverse health risks of diesel exhaust have become increasingly clear. The term diesel particulate matter (DPM) is used to refer to the solid components of diesel exhaust, which are an ultrafine mixture of elemental and organic carbon (EC and OC) and minor constituents including sulfates and metal ash (Kittelson, 1997). DPM is generally considered to occur almost entirely in the submicrometer range. It is classified as a carcinogen (Occupational Safety and Health Administration, 2013), and epidemiological studies have demonstrated a positive correlation between long-term exposure to DPM and other combustionrelated fine particulates and increased cardiovascular and pulmonary diseases (Pope et al., 2002; McDonald et al., 2011). Many of the risks of diesel exhaust are associated with the physical and chemical properties of exhaust components (Heywood, 1988; El-Shobokshy, 1994; Kittelson, 1997). Exposures are generally measured and regulated on the basis of mass concentration. However, DPM number density and particle size are increasingly recognized as critical factors in terms of health outcomes (Bugarski et al., 2012; Kittelson, 1997; Occupational Safety and Health Administration, 2013; Pope et al., 2002)."

Jan 11, 2017

By Fookes R. A, Gardner K. J, Gravitis V. L, Watt J. S, Steffner E. J

Two radioisotope techniques suitable for the rapid laboratory determination of the ash content of coal have been tested ou unwashed coal samples from four Australian coal seams. In one techniqne, measurements of backscattered 238Pu L X-rays and iron K X-rays from finely ground coal samples have been combined to determine ash content in uuwashed coals to &#177;0.5 weight per ce111 ash (ls) for three seams and 0.9 weight per cent ash for the fourth.The second technique, which involves measurements of the transmission by the coal of narrow beams of 241Am 60 keV and 123Ba 356 keV ? rays, requires less sample preparat ion. The ash was determined to within the range of 0.8 to 2.6 weight per cent for the four seams (unwashed coal). For washed coals, errors are expected to be &lt; &#177;0.5 weight per cent ash.

Jan 1, 1982

By Myles P. Reilly, Randall A. Snowdon, John Temporal, O&apos

The paper describes studies made at the Transport and Road Research Laboratory, UK, of the mechanical cutting characteristics using disc cutters, of rocks with compressive strengths up to 340 MPa. These studies have been performed in both the single pass mode, where interactive breakout occurs between adjacent grooves on every pass of the tool, and the multiple pass mode, where several passes may be required to cause breakout. In addition, experiments to determine the effect on cutting performance of the hydraulic stiffness of tunnelling machines are described. The results of these tests are analysed and discussed in the context of the design of full-face tunnelling machines.

Jan 1, 1983

Laboratory electrical resistivity measurements of rocks are reviewed. Inductive and galvanic methods are discussed together with the ten important experimental factors which should be considered in an investigation.These experimental factors are electrodes, sample preparation, measurement errors, temporal current variations, current density, frequency, electrolyte composition, electrolyte saturation, pressure, and temperature.

Jan 1, 1969

By Satya Harpalani

The four most important parameters controlling the flow of gas in coal are the gas content, permeability, diffusion coefficient and cleat characteristics. Estimates of these and, more importantly, a knowledge about the variation in their values over time are required for simulation of long-term gas production. This paper describes experimental techniques to determine each of these, along with their time dependency, under simulated in situ conditions. It is shown that the permeability, diffusion coefficient and the cleat aperture values are not constant as usually assumed to be. There is a significant variation in their values as a result of changes in the microstructure of coal associated with release and flow of gas.

Jan 1, 1995

By S. Ouyang

The four most important parameters controlling the flow of as in coal are the gas content, permeability, diffusion coefficient and clear characteristics. Estimates of these and, more importantly, a good knowledge about the variations in their values over time are important for proper simulation of long-term gas production. This paper describes experimental techniques for the estimation of diffusion-coefficient and permeability values, along with their time dependency under simulated in situ conditions. It is shown that the permeability and diffusion-coefficient values are not constant, as they are usually assumed to be. There is a significant variation in their values, probably as a result of changes in the microstructures of coal associated with release and flow of gas. Finally, a technique to estimate clear parameter is presented.

Jan 1, 1997

Gravity concentration of tin at Renison Limited uses tables and spirals to treat the various coarser fractions produced from sulphide flotation tailing. An acceptable final tailing cannot be made from one pass over the tables and spirals and therefore the tailing from these separators is reground and combined with the sulphide flotation tailing as the feed to the classification section. The gravity section became increasingly overloaded in the years preceding 1976 due to efforts to maximize tin recovery to the gravity concentrate. In April, 1976, two 2DSV Reichert cone concentrators in series were installed to treat the table and spiral tail- ing stream, prior to regrind, to scavenge a small tonnage of hard, coarse low tin grade material for rejection to final tailing. Gravity section loadings were decreased markedly, allowing operator attention to be directed more to table performance than to spillage collection. An increase in mill throughput of approximately 15% was possible following the commissioning of the Reichert cones. The cones are currently operated to make the minimum tonnage of tailing consistent with reasonable- gravity section loadings.

Jan 1, 1978

By J. A. Organiscak

In the United States, respirable coal mine dust exposures are limited to a 2 mg/m3 time weighted average for a working shift. If the silica content of the sample exceeds 5 percent, the 2 mg/m3 standard is reduced according to 10- (% silica) to limit silica dust exposures to 100 µg/m3. Examinations of dust sampling data collected by the federal coal mine inspectorate showed that roof bolter occupations continue to be at risk for overexposure to respirable silica dust. Testing at the Pittsburgh Research Laboratory of the National Institute for Occupational Safety and Health assessed the effectiveness of a canopy air curtain for controlling occupational exposures to respirable silica and coal dusts. Initial testing found that zones of higher velocity airflow shrank as distance beneath the canopy increased. This suggested that protection from occupational dust exposures would likely decrease as distance beneath the canopy increased. Further testing revealed that coal dust reduction efficiencies were most affected by changes in interference air velocity and, to a lesser extent, changes in canopy air quantity. However, respirable silica dust percentages under the canopy were not affected by such changes and, in fact, were not significantly different from silica percentages measured outside the canopy. This implied that the air curtain was equally effective on both respirable coal and respirable silica dust particles.

By Nicola Baldo, Marco Pasetto

"The paper discusses the results of a laboratory study, aimed to evaluate the suitability of the bottom ash from Municipal Solid Waste Incineration (MSWI), obtained from different Italian plants, to be recycled in the lithic skeleton of bituminous mixtures, for base layers of road and airport pavements. The research involved a preliminary study of the physical and geotechnical properties of the bottom ash by itself; it was followed by a mechanical characterization of the bituminous concretes. The traditional Marshall methodology was used to identify the optimum bitumen content; the mixtures were also mechanically checked by means of the stiffness modulus test, repeated load axial test and fatigue test. Because the requisites for acceptance in the Italian Specifications and Standards have been satisfied and given the positive mechanical performances, it has been verified that the MSWI bottom ash can be used as substitution of the lithic materials in the road bases, also with very high contents (up to 81% on the weight of the aggregate). Introduction The incineration of Municipal Solid Wastes (MSWs) provides for by-products which can be mainly classified as bottom ash and fly ash. The first one, corresponding to the 25% on the weight of the wastes to be incinerated, so resulting the principal product of the process, is mainly composed by Silica (Si), Iron (Fe), Calcium (Ca), Aluminium (Al), Sodium (Na) and Potassium (K) oxides, so presenting a composition similar to that of different natural materials. Its metallic fraction can be recovered; the remaining part is usually stocked in dumping or, less frequently, recycled. Bottom ash can be re-utilised in the construction of new infrastructures, especially in bitumen bounded mixtures, because of the inert properties of the binder which covers the grains with a subtle film, that prevents the release of heavy metals. The paper describes a study aimed to design new bituminous mixes for flexible road and airport pavements, realised with the highest content of 4 types of bottom ashes, deriving from different MSWI plants of the Northern Italy. The ashes will be named as BA1, BA2, BA3, BA4 respectively (the origin cannot be specified)."

Jan 1, 2008

By J. M. Goris

"Researchers at the U.S. Bureau of Mines are conducting research on cable-type ground supports to assess their material and support properties and to provide design criteria for implementing cable supports as a workable roof control system under various underground mining conditions. Much of this work involves laboratory assessment of the material and support properties of cable supports using both conventional and birdcage steel cables. Included in this assessment are single and double cables, effects of changes in embedment length on support strengths, water-cement ratios, use of breather tubes, and pumpability and water-bleeding properties of grouts.IntroductionSince cable supports were introduced in the early 1970s, considerable research has been conducted in laboratories and at mine sites to understand their behaviour. The U.S. Bureau of Mines began a laboratory evaluation project in 1985 at the Spokane Research Center (SRC) to study the behaviour of cables supports under uniaxial loads so that the effects of various cable support components, such as grout and breather tubes, could be identified. Other objectives were to compare the behaviour of various types of cables and grouts and to collect meaningful data for numerical analyses. Pull tests were conducted to determine how cables supports reacted under uniaxial loads and how they failed when ultimate loads were exceeded. Such data are essential for the development of numerical models for analyzing rock mass behaviour when the rock is supported with cables.Test ProgramBecause each cable support can be composed of either single or double cables as well as a breather tube, pull tests were designed to include a variety of samples containing these components. A series of samples containing a single conventional cable, a neat cement grout having a water-cement ratio of 0.45, and no chemical additives was selected as a standard (Table I). Then one component in the system, such as the presence of a breather tube, was changed, and results of tests compared to results obtained for the standard samples to determine what influence that component might have on the behaviour of the support system. If significant changes in test data occurred, they could be attributed to that one component. To control the quality of the samples, the physical condition of the cables and tubes were monitored closely, and compressive and tensile strengths as well as flow properties were determined for the grout used in each test series."

Jan 1, 1991

By H. H. Murray

Clay minerals are one of the more important industrial minerals. They are used in many products and because of different specifications may require special processing which can be either wet or dry. The clays discussed are bentonites, kaolins including ball clays, and palygorskite (attapulgite). In order to design a process flow sheet for these clay minerals, the physical, chemical, mineralogical, and optical properties need to be evaluated. Each species of clay minerals require a group of special tests which are described in this paper.

Jan 1, 2009

By I. Demers

The abandoned Manitou mine site covers an area of approximately 190 ha near Val d?Or, Quebec. This old site has been generating acid mine drainage for several decades. In 2006, a partnership was established between the Quebec Ministry of Ressources Naturelles (MRN) and Agnico-Eagle Mines to reclaim the Manitou site using tailings from the nearby Goldex mine. These neutral tailings were to be deposited on top of the Manitou site. An extensive study was performed to evaluate specific reclamation scenarios to control acid mine drainage using Goldex tailings as cover material. The article first describes the global approach used for this evaluation, which includes in-situ hydrogeological monitoring, tailings characterization, laboratory column tests, and numerical modelling. Of the thirteen column tests, three were conducted to evaluate the parameters affecting the performance of covers made of Goldex tailings placed over the spillage area of the Manitou site. Geochemical and hydrogeological parameters were assessed during the leaching column tests for almost two years. The tests aimed at evaluating the effect of water table level and monolayer cover thickness on the overall performance. The testing procedure involved monthly leaching and measurement of geochemical parameters. Results indicate that water table position is the most important factor affecting the monolayer cover performance to control AMD. Based on these results, it was established that the water table must be located near the interface between the Goldex and Manitou tailings to effectively reduce AMD generation. Cover thickness also has an impact on cover performance, which is however less significant than the water table position. The testing scenario with a water table located at the interface with a one-meter Goldex tailings cover showed progressive improvement in effluent quality.

Aug 1, 2013