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By A. E. Raddatz

The Federal Bureau of Mines, as part of its goal to minimize undesirable environmental impacts associated with mineral processing, has investigated a soda-smelting technique for processing ilmenite into pig iron and a titanium slag that is suitable for a feed to a sulfate-process titania pigment plant. By this procedure, the generation of ferrous sulfate waste and its associated disposal problem is obviated. Molten titania slag was quenched, water leached, and filtered to yield a sodium titanate intermediate product containing about 70 wt-pct Ti02, 1 wt-pct Fe, and 20 wt-pct Na20. This intermediate product, high-soda titanate (HST), was mixed with H2S04, calcined, quenched, and water leached to produce a low-soda titanate (LST) product that contained only 2 wt-pct Na20. Both the HST and LST were evaluated as feed materials for preparing titania by the sulfate process. About 95 pct of the Ti02 was extracted from HST and LST by digestion in concentrated or 50-wt-pct-H2S204 solutions. About 95 pct of the solubilized Ti02 was subsequently recovered from the titanyl sulfate solutions by hydrolysis. Barren solutions from hydrolysis, containing about 26-wt-pct H2S04, were upgraded by vacuum-thermal evaporation or electrodialysis. The regenerated acid solutions were used to digest additional HST and LST.

Jan 1, 1979

By Christopher Mark

Roof bolt system design means the selection of the type, length, capacity, and pattern of bolts for a particular application. Despite research efforts dating back 50 years, no design methodology has found wide acceptance. This paper begins by identifying four mechanisms that roof bolts use to reinforce the ground. It argues that the reinforcement mechanism is determined by the roof geology and stress level, not by the type of bolt. Next, the attributes of roof bolts are discussed in the light of recent research, including anchorage mechanism, installed tension, length, capacity, timing of installation, and installation quality. Several significant areas of controversy are identified. Design methods from around the world are discussed, including those based on empirical research, numerical modeling, and roof monitoring. Finally, some simple guidelines for preliminary design of roof bolt systems are proposed based on statistical analysis of roof support performance at 37 U.S. mines.

Jan 10, 2000

By Errol D. Sehnke

This U.S. Bureau of Mines report provides detailed information on worldwide bauxite production capacity by mine and country, including bauxite substitute materials in countries of the former Soviet Union, The information was compiled from a variety of domestic and international sources and was based on information available to the Bureau through December 31, 1994. Capacity data represent announced installed and planned capacities and do not necessarily reflect a U.S. Bureau of Mines judgment of actual mine operating levels or timing of planned expansions. The year-end capacity is the ?in place? capacity or estimated production capacity, whichever is larger.

Jan 1, 1994

By W. K. Kleysteuber

This report covers the design and testing of a novel bulk materials conveying device by the Bureau of Mines. The transport concept of the device is to create a traveling wave with a steep front so that the bulk material slides and cascades down the front of the wave with some horizontal motion. Ideally, the front should act like a continuous chute. The concept of moving bulk materials along a belt without any forward movement of the belt itself was demonstrated. The conclusions reached were that the mechanism as designed could not overcome the inherent major disadvantages that would make the undulatory conveyor suitable for practical applications.

Jan 1, 1974

By Ann G. Kim

Hydrocarbon gases, primarily methane but also the C2 through C5 paraffins, the C2 and C3 olefins and possibly the C4 and C5 olefins, are byproducts of coal formation. Although it is generally believed that coal formation occurred at temperatures below 200° C, most experimental work on gas formation from coal has been performed at temperatures between 200° and 1,000°C. The objective of this Bureau of Mines experiment was to determine if observable changes in the gases from coal could be produced at temperatures below 200° C in relatively short periods of time. The experiment involved heating coal samples from six coalbeds at constant temperatures and analyzing evolved gases. The composition of the gases at three temperatures was compared. At 35° C, over 99 pct of the gas is methane; at 125° and 150°, methane constitutes approximately half of the hydrocarbon gas. Isobutane and pentane are the predominant higher hydrocarbons at temperatures between 100° and 150° C.

Jan 1, 1974

By Frank J. Wiebelt, Spangler Hicker

The Iron Mountain investigations were part of a comprehensive program for making a national inventory of raw materials used in the production of steel. A tentative program of core drilling by the Bureau of Mines was set up for exploration of more promising iron deposits. Iron Mountain was selected as worthy of investigation because it could serve as a potential source of ore for the war-created steel plant at Fontana, Calif. The deposits were reported on by an engineer in October 1943. The purpose of the project was to determine the lateral and vertical extent of ore bodies and to obtain accurate material data on them.

Apr 1, 1948

By R. O. Dannenberg

The Bureau of Mines investigations described in this report were undertaken to devise a process to economically recover precious metals and copper from low-grade, complex electronic scrap generated in large quantities by military and civilian electronic operations. Leaching with various media is applicable to certain selected items of electronic scrap but cannot be practically applied to complex mixtures of scrap. A process comprising incineration, caustic leaching to remove aluminum, smelting with a siliceous slag, and electrolysis recovered 99.9-percent-pure copper metal and anode slimes assaying more than 7,000 ounces per ton of combined precious metals. Silver, gold, and copper recoveries were 93, 95, and 87 percent, respectively. Cost analysis indicated that an alternative process using direct smelting of the scrap to make assayable products for sale to a custom smelter would provide better overall financial returns.

Jan 1, 1972

By W. H. Blackburn

This paper describing the milling practice at the Tybo concentrator is one of a series of similar papers being prepared by the United States Bureau of Mines on milling methods and costs at the various mills in the United States. ACKNOWLEDGMENT A large part of this paper way prepared by H. M. Lewers, mill superintendent of the Tybo plant of the Treadwell Yukon Co., Ltd.

Jan 1, 1931

By H. Dale Nichols

[The growing importance of the Sundance (Jurassic) formation as a source of oil in the Rocky Mountain area has prompted the making off a series of porosity determinations of core samples collected from the reservoir sands of the Lance Creek oil field, Niobrara County, Wyo. These analyses are preliminary to a study of fluid and energy relations in the Basal Sundance reservoir of that field, and the determinations of porosity will be used in subsequent studies requiring calculations of the volumetric capacity of the reservoir and estimation of the reserves of oil and gas.]

Jan 1, 1938

By Frank D. Lamb, Lloyg H. Baning

"The crushed-stone industry has long been troubled with the problem of producing a more or less cubical product for use as concrete aggregate. Its seriousness varies widely for each producer, depending upon the character of the rock employed for raw material and the ultimate use of the crushed stone. For many construction uses, such as the macadam or bituminous-concrete- type road, flat pieces are not objectionable and may even be preferable to more cubical rock. However, most specifications for concrete require that the stone must be reasonably free from flat and elongated pieces.The rigid specifications set by many contractors have resulted in the rejection of coarse aggregate that, except for the presence of an excessive amount of flat and elongated pieces, would be entirely acceptable. In many instances, if an efficient, economical method of removing flat and elongated pieces were available, local producers could meet the requirements of the contractor and thus eliminate the necessity for importing more cubical material.A brief investigation of the problem of removal of flat and elongated pieces from crushed aggregate, carried out at the Eastern Experiment Station of the Bureau of Mines, indicated that it is mechanically possible to remove flat pieces from crushed rock.TEST EQUIPMENTA number of mechanical devices are used by the coal industry for separating slate from coal; these depend upon the difference in shape of the crushed slate as compared with the coal. Such devices as shutter screens, spiral separators, and the Norman picker would be suitable for removing flat pieces from crushed rock in the same manner as they are used by the coal industry. None of these devices was immediately available for testing purposes, so an attempt was made to construct a simple device that could be used in commercial operations."

Sep 1, 1944

By Donald P. Mickelsen

The raining and quarrying trends data shown in this report were reported to the U.S. Bureau of Mines (USBM) by mining and quarrying companies on the Mine Information Supplement survey, as well as by mineral producers on 58 annual USBM production and consumption surveys covering 59 nonfuel mineral commodities. The 1993 data presented in the tables of this chapter, were processed for the first time using the USBM Automated Mineral Information System. Domestic mining of nonfuel mineral materials totaled 3.7 billion metric tons in 1993, including 2.2 billion tons of crude ore nun& or quarried and 1.5 billion tons of mine waste and ore from development. This \vas an overall increase of 11% over that of 1992. These data do not include construction sand and gravel which until 1993 has been surveyed biennially. Starting in 1994, construction sand and gravel and the stones, which were also surveyed biennially, will be surveyed annually.

Jan 1, 1993

By Thomas J. Peters

The Snowbank study area, which had been proposed as Wilderness, lies about 5 air mi southwest of Cascade, Idaho, and about 60 air mi north of Boise. The eastern boundary of the north-south-elongate study area lies 1-to 2-mi east of Cascade Reservoir; the western boundary is contiguous, in part, with the western boundary of Valley county. The 8,200-acre study area is underlain by Cretaceous granitoid rocks of the Idaho batholith. Three prospects were found in or near the study area during a library and field search. Gold occurs at one 30-ft adit, but the gold-bearing structure appeared too narrow to contain resources. Two other prospects appeared essentially unmineralized. No evidence of geothermal activity was observed. Rock in the area is not potentially useful as dimension stone because it does not split into flat slabs. To be used as aggregate, the rock would require crushing and hauling to distant markets. One of 18 alluvium concentrate (placer) samples contained free gold, worth $1.07 per cubic yard of gravel (at a $350 per oz gold price). No alluvial bars were seen; deposits were too small to contain gold resources or be considered gravel resources.

Jan 1, 1993

By Oliver C. Ralston

The growing popularity of perlite (sometimes spelled pearlite) as a raw material for thermal expansion into pumicelike products in the Western States has prompted a preliminary investigation of the properties of such material and the problems that want solution to put a perlite industry on a firm foundation. The Bureau of Mines is undertaking the gathering of data and the solution of these problems, and the following paper records some of the available information. and the promise of the material, with some comparisons of advantages of the various competing lightweight aggregates that can be made from siliceous volcanic glasses and rocks containing entrapped or dissolved water that causes their expansion on' quick heating to their softening points. This new industrial rock has caught the fancy of the mineral industry in the western States because it has Fume advantages over natural pumice. Chemically, it is typified as rhyolitic in composition, and one may find obsidian, rhyolite, pumice, pumicite, and perlite from the same vant and contemporaneous in origin. The material need not be rhyolite but should be a siliceous or acid lava and contain 2 to 5 percent water still in "solution" in the rock. On quick heating to the softening temperature the material puffs, due to conversion of the contained eater into bubbles of steam. Slow heating causes gradual release of the imprisoned water by decrepitation and. cracking and-results in, very little puffing. Perlite is often in the form of ovoid volcanic bombs formed by explosive eruption of large masses of lava into the air, where they, quickly cool, with escape of little of the contained water, exceptt perhaps for a hollow interior. Since they cool in layers they have an onion-type structure and a pearly luster from interference of light between the. layers, which is' the origin of the name "perlite." Perlite may occur in intruded flows that have been quickly cooled and partly expanded but retained most of their magmatic water content. Obsidian may be the same lava cooled quickly under conditions that prevented crystallization of feldspars and other minerals, leaving the volcanic glass that may or may not retain all of the original contained water.

Jan 1, 1946

By H. Kenworthy

Laboratory experiments were conducted on several materials to determine their suitability for the production of mineral wool. By blending raw charges in the proper proportions and in some instances by adding lime, acceptable wools were made from samples originating in Alaska, Florida, Texas, and Virginia. It was shown that satisfactory wools can be produced from many kinds of raw materials if the ratios of acidic and basic constituents are properly maintained. INTRODUCTION The Federal Bureau of Mines has facilities at the Mississippi Valley Experiment Station, Rolla, Mo., for examining and testing mineral-wool raw materials. Samples are evaluated through small-scale wool-blowing experiments, aided by petrographic, chemical, and physical analyses of the raw materials and finished wools. When enough experimental data have been accumulated they are made public through Government reports and periodicals. This report of investigations follows that published in 19513/ and presents test data on samples received and examined since 1951.

Jan 1, 1956

By Willard L. Hunter

A series of steel heats, one low-alloy and nine carbon, was made by the Bureau of Mines in a 1-ton arc furnace from ferrous scrap from incinerated refuse, steel cans, and detinned steel cans, both alone and blended with heavy-melting scrap. Two additional control heats, one of carbon steel and one of low-alloy steel, were made from electric furnace heavy-melting scrap to pro-vide comparative data. The steel products were cast into two 4-by 4-inch nominal 50-pound ingots; in most heats, an 8-by 8-inch nominal 7S0-pound ingot was also obtained. Tests of these ingots indicated that reinforcing bars of acceptable quality can be made from urban refuse components such as steel cans.

Jan 1, 1976

By T. A. Henrie

The Federal Bureau of Mines has investigated methods of sodium reduction of titanium chlorides to produce high purity titanium metal (14).4/ This investigation was made to obtain a better understanding of the reactions involved in sodium reduction of titanium chlorides and was part of the Bureau's activities toward improving the technology of titanium. Theoretical and experimental evidence show that sodium reduction of titanium tetrachloride occurs by stepwise reactions. The first stage reduction between sodium vapor and vapors of titanium chlorides produces titanium di-and trichlorides which subsequently condense with sodium chloride to form a salt mixture. The second stage reduction takes place in the condensed salt mixture between sodium and titanium subchlorides. Final reduction is a heterogeneous reaction between two separate phases, the a phase which consisted of sodium dissolved in sodium chloride and the ß phase titanium subchlorides dissolved in sodium chloride. The mechanism of the heterogeneous reaction between these phases is electrochemical in nature. The model proposed is a galvanic reaction at the interfacial region.

Jan 1, 1960

By George F. Dana

Oil yields, lithology, and stratigraphy have been evaluated for 15 cored wells and two sampled wells representing 10 square miles of the Tipton Member of the Green River Formation near Green River, Wyo. The area evaluated is being used by the Bureau of Mines for experimental production of oil from the oil shales in place. Lithology and oil yields were correlated to produce a stratigraphy diagram for the in situ study area, permitting precise designation of comparable sections. Because of lateral uniformity of oil shale, oil yields from eight cores and two sets of drill-cutting samples within a quarter section show the range of variation in average oil yield arising from experimental error. Variation in average oil yields from the seven cores representing the 10-square-mile study area lies within the expected experimental error. No difference in oil-shale richness across the study area is indicated. Average oil yields for three Tipton sections in the study area were deter-mined as follows: (1) The entire Tipton Member oil shale (about 145 feet thick), 13.3 gallons per ton; (2) the 40-foot upper rich zone, 21.0 gallons per ton; and (3) the 21-foot zone in which the Laramie Energy Research Center is conducting in situ experiments, 22.4 gallons per ton. One acre of the 21-foot experimental section represents 34,300 barrels of oil in place, and 1 acre of the Tipton's 40-foot rich upper layer represents 62,000 barrels.

Jan 1, 1972

By A. E. Back

A method has been developed in the laboratory for successfully treating titaniferous magnetite ore from the deposit at Iron Mountain, Wyo. The ore is roasted with 15 percent sodium carbonate to convert the vanadium to a water-soluble form and fix the soda for the subsequent electric-smelting step. Approximately 90 percent of the vanadium is recoverable in a product assaying 80 percent V2O5. The leached calcine is briquetted and smelted in a graphite-lined electric-arc furnace. Substantially all of the titanium is recovered in a soda slag, assaying 60 percent TiO2 and 2 percent Fe, which can be upgraded to 75 to 80 percent TiO2 by leaching with dilute sulfuric acid. The upgraded slag could be utilized for the production of titanium dioxide pigments or titanium tetrachloride. About 90 percent of the iron is recovered as pig iron, containing only minor amounts of vanadium, titanium, and sulfur. The high TiO2 slag compares favorably with slag containing about 70 percent TiO2 being produced by the Quebec Iron & Titanium Corp. at Sorel, Quebec. The data obtained from this investigation indicate that a feasible process has been developed for treating Iron Mountain ore, and larger-scale testing is warranted to develop engineering data for the ultimate utilization of this deposit as a source of titanium, iron, and vanadium. There are adequate supplies of basic raw materials, electric power, water, sodium carbonate, coal, and petroleum products within fairly short distances of Cheyenne and Laramie, Wyo., the nearest cities and probable plant- and labor-supply points.

Jan 1, 1952

By Joseph J. Wallace

1. The investigation shows that there are two coal beds of major importance in Perry County from the standpoint of present production -Flag and Fire Clay -and two beds of minor importance -Haddix and Hindman. The Flag and Fire Clay beds contain the largest remaining known reserves. 2. Known measured and indicated reserves in all beds, based on a minimum thickness of 14 inches and 1,800 tons per acre-foot of coal in place, are estimated at 840 million short tons as of January 1, 1954. Of this total, 720 million short tons is in beds 28 inches and more thick. Areas in each bed were omitted from the estimate because available data relative to the bed characteristics are too meager for making an estimate that conforms with the definitions of measured and indicated coal adopted for this study. Should future drilling or development prove reserves in these areas, these should be added to the total estimated reserves.

Jan 1, 1954

By Ernest Ph. Hérivel

The mine and treatment plant of the Teziutlan, unit of the Mexican Corporation, S. A., are located at Aire Libre, in the District of Teziutlan, near the northwest edge of the State of Pueblo, Republic of Mexico. The property is leased from the Teziutlan Copper Co. The town of Teziutlan is the terminus of a branch railroad starting from Oriental Junction or the Mexico-Jalapa-Veracruz narrow-gage system of the National Railways of Mexico. A branch line 18 km in length from Teziutlan to Aire Libre belongs to the Teziutlan Copper Co. and is leased and operated in conjunction with the mine.

Jan 1, 1933