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By A. Viksne

A series of tests were conducted by the Bureau of Mines to determine the best means of reducing noise generated by the detonating cord that is utilized for trunklines in quarry blasting. Ten different types of detonating cord were tested and evaluated for their acoustic qualities. The results of the investigation showed that noise levels produced by "low-core-load-per-foot" detonating cord "not covered" were lower than those produced by "high-core-load-per-foot" detonating cord covered with 6 inches of unconsolidated material.

Jan 1, 1972

By Christopher Van Dyke, Knox Van Dyke, Lixin Wu, Jaime Gutierrez

"I. INTRODUCTION(SILICA, THE LUNG, INFLAMMATION, AND FIBROSIS)Inhalation of respirable-size silica (0. I to 5 µm in diameter) deposits the particles in the deep spaces of the Jung where oxygen is exchanged. The resulting pattern of inflammation is substantially different compared to that observed from other inhaled substances such as carbon, polystyrene titanium dioxide etc. 1 Following the inflammatory reaction the body attempts to isolate the damage by walling off the area via fibrosis. 2 The unique nature of the inflammatory response to silica makes it logical to infer that fibrosis is a later-stage manifestation of the initial inflammatory damage. In addition to the inflammation extensive lysis and cellular death particularly to macrophages and neutrophils, can occur, depending on the dose of silica.' The ingestion of significant amounts of silica by macrophages and neutrophils produces an inflammatory sequence which activates the lipoxygenase pathway of arachidonic acid metabolism and produces platelet activating factor (PAF) and leukotrienes (LT).4·5II. CALCIUM IONOPHORE MIMICS SILICA TOXICITY IN VITROPhagocytic cells exposed to silica in vitro produce PAF and LT. This response is reminiscent of phagocytic cells exposed to the calcium ionophore (A23 l 87) in the presence of ionic calcium.6-8 A23 l 87 forms a complex with free ionic calcium which passes through cellular membranes, thus transporting calcium inside the cell. The increased intracellular calcium concentration triggers the production of small amounts of prostaglandins large amounts of LT. PAF and. depending on dose cellular death (see Figure 1 ). Could silica cause LT production and cellular death by a similar mechanism? How could silica - an inert solid - act in a similar fashion as a soluble stimulant? Clearly the negative SiO2 and OH- surface of silica can bind calcium ions9 and therefore could theoretically act as a solid-state ionophore releasing bound calcium inside of cells following phagocytosis."

Jan 1, 1998

By Jun Yi

In this paper, single-component gas sorption and transient diffusion processes are described within coal matrix exhibiting bimodal pore structure. The coal matrix is treated as a poroelastic medium manifesting swelling and shrinkage effects due to the sorption of gas under effective overburden stress. Gas transport is considered Fickian with molecular (bulk) and surface diffusion processes simultaneously taking place in the macro-and micropores of coal, respectively. The numerical formulation is intended to be explicit in nature to investigate the influences of sorption phenomena on the macropore volumes and on the overall gas transport for the cases of gas uptake by and release from coal. Results of the study show the presence of hysteresis during a sorption?desorption cycle of the gas. It is also found that the overall gas transport takes place at a rate significantly less than that in the macropores only. Thus the existence of a retardation effect in the overall gas transport is concluded. This retardation effect is primarily due to the micropore resistances, in particular gas adsorption, and is independent of the changes in the macropore volumes. It is shown that macroporosity of the coal matrix may change during gas transport due to combined effects of pressure and sorption-induced swelling or shrinkage of the coal. It is estimated that the macroporosity variation is non-uniform in space and time, as it is expected in reality, and typically taking values less than ±10 percent of the initial porosity.

Jan 1, 2009

By M. D. Carver

This investigation was undertaken by the Bureau of Nines to determine the effects of impurity levels on the mechanical properties of columbium at low temperatures. High-purity, electron-bombardment-melted columbium was purchased and used as a basis material. Variations in impurity levels were obtained by arc-melting charges containing definite amounts of added impurities. Tensile tests were conducted at low temperatures. Results showed the almost pure basis metal to be ductile at minus 194° C., the lower limit of the range used, Ductility of less pure columbium appeared to depend on interstitial element content. The ductile-to-brittle transition temperature appeared to be raised by increasing carbon content in the range of 50 to 730 parts per million, nitrogen content in the range of 50 to 200 parts per million, or total interstitial element content in the range of 240 to 1,380 parts per million. Some evidence was obtained indicating that decreasing cold work also raised the transition temperature, but recrystallization appeared to have no effect on it. Variations in interstitial element levels appeared to have little or no effect on ultimate strength of columbim in the range of room temperature to minus 194° C, Physical metallurgy studies of massive arc-melted and electron-bombardment- melted columbium were included in the columbium-tantalum research work assigned to the Albany Metallurgy Research Center in fiscal year 1959.

Jan 1, 1961

By B. J. Dalton

Several relationships between coexisting phases for analytical binary solutions near the critical point are given. These relationships were developed from a consideration of a (G u, P) surface at constant temperature and a (G u, T) surface at constant pressure, where G is the molal Gibbs free energy, u is the concentration of component 1 expressed as a mole fraction, G is the pressure, and T is the temperature. These formulas should facilitate the calculation of some of the quantities useful in making thermodynamic consistency checks on phase equilibria data about the critical point.

Jan 1, 1970

By T. A. Hendrickson

The Bohemia district, situated about 30 miles southeast of Cottage Grove, Oreg., in the Calapooia Range, has been the major producer of lead and zinc in Oregon. Sporadic production has been Maintained from the district since its early discovery about 1858. In 1942, a selective-flotation mill was built at the Champien mine, which operated for only a short time and was forced to close because of the war and lack of labor. The Champion mill reportedly has been operated as a custom mill for the treatment of ore from the Musick and Helena mines, located in the district sometime in the past. This report summarizes the results of laboratory ore-dressing studies made on ore samples from the Musick and Helena Mines.

Jan 1, 1951

By M. S. Seehra, V. S. Babu, L. Farinash

"The diesel particulate matter (DPM), a constituent of the diesel engine exhausts, is known to be a potential carcinogen. 1- 3 Consequently, suitable methods to control/eliminate DPM have ·been under investigation in recent years. The DPM can be controlled by using fibrous ceramic traps. However, clogging of traps by DPM requires the impractical periodic trap replacement. Following the recent work by Garner and Dent,4,5 we are investigating the in situ use of microwaves to regenerate the ceramic traps, thereby eliminating the trap replacement step in this process. The use of microwaves instead of conventional heating for trap regeneration has the advantage of selective heating of the DPM instead of the trap, if the trap absorbs insignificant microwave power relative to the DPM. Also, the oxidation characteristics of the DPM are needed to understand fully this regeneration process.The rate of energy absorption P per unit volume of a sample is given byP = wE"" |Eo|2 • (1 )where w is the angular frequency, |E0|2 is the intensity of the microwave radiation, and E” is the imaginary part of the dielectric constant (E = E’ + iE”) . Thus measurements of E11 for DPM and ceramic trap material are needed to determine their capacities for microwave absorption. In this paper, we report these measurements carried out at · a frequency of 8.7 GHz. Following microwave absorption, the DPM is expected to oxidize. The oxidation characteristics of the DPM have been investigated using Fourier transform infrared (FTIR) spectroscopy of the evolved gases CO2 and CO and using thermogravimetric analysis (TGA). Finally, some information on the structure of carbon in DPM has emerged from the analysis of its x-ray diffraction spectra. Results of these experiments are reported in the following pages."

Dec 1, 1996

By R. C. Buehl

An experimental iron blast furnace of 3-foot-diameter hearth, producing about 12 tons of metal per day, was operated for 2 weeks with various proportions of anthracite replacing a corresponding amount of coke. The furnace operated well with anthracite in amounts up to 40 percent of the total fuel and produced metal of uniformly low sulfur and normal silicon contents. An increase to 50 percent anthracite during two attempts resulted in poor operation and the charge hung in the s haft of the furnace. INTRODUCTION Anthracite production in Pennsylvania decreased from 84,400,000 net tons in 1926 to 40,600,000 net tons in 1952, and there was a further decline in 1953 to 30,900,000 net tons. Employment in the anthracite industry dropped from 165,000 men working an average of 244 days per year in 1926 to 57,900 working an average of 163 days per year in 1953,3/ which has naturally resulted in considerable unemployment in the region. The industry is actively engaged in promoting new uses for anthracite to increase the demand and thus improve economic conditions in the region. One possibility is the use of anthracite to replace part of the coke for smelting iron ore in blast furnaces. The tests in this report were made to determine whether this use of anthracite would be feasible.

Jan 1, 1955

By G. R. Hopkins

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Jan 1, 1927

By Wm. W. Odell

For a number of years there has been a very appreciable annual,, increase in the production and recovery of natural gas and natural-gas gasoline2 in the United States the latter product being used largely for blending with gasoline from petroleum in the production of motor fuel. On account of the increased amount of oil cracking in the production of gasoline and the accompanying increased percentage of low-boiling constituents in the resulting product, the specifications for the natural gasoline suitable for blending have been altered, that is, the amounts of propane and butane which it can contain have been limited. The result has been that large quantities of the latter materials are wasted because there has been no ready market for thorn in large quantities. Because of this wasteage and because it is probable that large quantities of there and similar materials will be produced in the near future us a result of the more general use of oil cracking processes, a study was made by the Bureau of Mines, under a cooperative agreement with the assistance of the Phillips Petroleum Company, of the suitability of these materials alone or in mixtures for use as gas enricher in the carburetion of water gas for city distribution. This investigation included: (a) A study of the properties of the low boiling members of the paraffin series including pentane with particular reference to their utilization as gases.

Jan 1, 1927

By E. J. Schneider

In view of the current interest in the constituents of low-temperature tar, the Synthesis of three known xylenols and their hydroxyacetic acid derivatives has been undertaken by the U. S. Bureau of Mines. One of these xylenols, the 1,3,2 derivative first reported by Steinkopf and Höpner,4 has been described by Brown and Branting.5 The other two derivatives, the 1,3,5 first reported by Schütz6 and the 1,2,3 reported by Steinkopf and Höpner, have now been studied in greater detail. In the present work the synthesis of 1,2,3-xylenol and 1,3,5-xylenol was repeated, with some improvements in the former. The hydroxyacetic acid derivatives were also prepared, and it was found that while the melting point of the 1,2,3 derivative agreed with that of Steinkopf and Höpner. that of the 1,3,5 derivative was found to be 111° instead of 85 to 86° as reported by Schütz, by Steinkopf, and later by Bruckner. The discrepancy between the melting-point figures is doubtless due to differences in the purity of the xylenols used in the synthesis of the acids. Schütz obtained his 1,3,5 acid by recrystallizing an impure sample obtained from a mixture of xylenols. The difficulty of obtaining a pure acid by starting with a mixture is demonstrated by Bruckner, who despite painstaking efforts was unable to obtain the pure 162.5° melting 1,2,4 isomer from a mixture that persistently melted at 138° C. Steinkopf did not repeat Schütz's work but merely used the latter's figures in compiling a table. Bruckner, on the other hand. apparently also made the acid (by an improved method), and it is difficult to explain his checking Schütz's figure, unless it is that he, too used a symmetrical xylenol obtained from a tar and not prepared synthetically, as was the one reported in this paper.

Jan 1, 1929

By Joan T. May

The Federal Bureau of Mines investigated the potential for recovering aluminum from copper-dump leach liquors by use of single-contact ion-exchange technology. A strongly acidic ion-exchange resin was used to extract aluminum from a typical dump leach liquor and from synthetic leach liquors. Aluminum was stripped from resin with a HS04 or NaCl solution. Bench-scale experiments indicate that a single-contact ion exchange is technically feasible, but that the process is limited by the relatively low loading capacity of the resin and the excessive amount of stripping agent required. A further limitation is that significant amounts of magnesium and iron are loaded and stripped along with the aluminum.

Jan 1, 1976

By R. S. Dean

The principle of explosive crushing depends upon the fact that an expandable substance contained within the pores of a solid body will disrupt such a body upon expansion. Such expansion may be obtained by the detonation of an explosive or by the sudden release of pressure of a superheated liquid. That this principle of disruption may be applied to minerals rests on the fact that cracks, cleavage planes, and pores exist in all mineral to an extent hardly conceived possible heretofore. Crushing by this method takes advantage of force applied from within the mineral rather than from forces applied from without. The application of a force from within would appear to be more effective. A consideration of the possibilities of such a method for crushing led to some experimental work of a preliminary nature, the results of which are embodied in this paper. No systematic program was followed in the work and the results are, therefore, not final and far from complete. The success attained so far, with the mediocre apparatus available seems to warrant a preliminary report, with the expressed hope that the work may be carried on as well-outline program covering such phases as have been impossible to investigate at this time.

Jan 1, 1931

By W. L. Parker, W. A. Selvig

"Introduction.Powdered or pulverized coal is extensively used as a fuel, the total annual consumption*** in the United States being about 12.000,000 tons, and growing steadily. As the coal is usually pulverized so that 70 per cent or more parses through a 200-mesh sieve, it presents difficulties in sieving, because such finely divided material tends to clog the meshes. A fineness test is desirable in order to judge the efficiency of the pulverizing apparatus, and as an indication of the particle size of the coal being burned.Committee D-5 on Coal and Coke, American Society for Testing Materials, has recognized the desirability' of a standard method for determination of fineness of powdered coal. The Bureau of Mines, in co-operation with this Committee, conducted sieving tests on two standard samples of powdered coal, which are described in this paper. As a result of this work a method for making fineness tests, by band sieving, is recommended as a standard method, while a rapid method, by machine sieving, is given for routine tests.Outline of Investigation.Preliminary trial tests were made by the bureau and tentative methods were formulated for making the sieving tests both by band and by machine.Each of two samples of powdered coal was carefully mixed, and portions were sent to the twelve laboratories mentioned later. These were requested to make duplicate sieving tests on the two standard samples, by the hand-sieving and machine-sieving methods, and to follow the tentative procedure exactly as outlined. All of the laboratories made sieving tests by hand shaking and eight of them made tests by machine shaking."

Nov 1, 1923

By Wm. F. Netzeband

The purpose of this paper is to present to the operators, in other districts a detailed description of the ruining method used and the results obtained to exploiting one of the zinc-lead deposits of the Kansas-Oklahoma-Missouri district. No. 1. mine is located in the heart of the town of Picher in the extreme northeast corner of Oklahoma. HISTORY The first prospect drilling was done at No. 1 mine late in-1914, and shaft sinking was started early in 1915. Sufficient ore was developed to start construction of the mill in April, 1016, Production begin in August, 1916, and the mine s been producing, except for short periods, to the present time. The property was originally a 40-acre tract, but additional properties have been consolidated with the original one until the mine now covers 200 acres.

Jan 1, 1929

By George H. Holmes

This report describes the results of a reconnaissance survey of areas in California and Nevada considered favorable to beryllium mineralization. Pegmatite dikes, veins, intrusive sills, contact metamorphic, and disseminated deposits as well as tactite deposits in the former major tungsten-producing districts were investigated. A general geographic pattern of beryllium mineralization was found to be concentrated along a wide belt in eastern Nevada extending from the Ruby Mountains, Elko County, south through the Fish Creek Range, Eureka County, the Snake Range, White Pine County to the Virgin Mountains in Clark County, Nev., and Mohave County, Ariz. Sporadic occurrences of beryllium are in central and southern Nevada, and in the pegmatite dikes of San Bernardino, Riverside, and San Diego Counties, Calif., and the granite masses of the southern Inyo Mountains, Inyo County, Calif. Principal company activities are centered in the Snake Range, Fish Creek Range, and the Virgin Mountains, Nev., and the Inyo Mountains, Calif. Other areas in California and Nevada have been superficially explored with results indicating either limited or widespread, but submarginal, mineralization. Although beryllium was found to occur, to some extent, in many of the deposits, mining has been hindered by the lack of a market for beryllium ores and concentrates other than standard-grade beryl and also by the erratic pattern of mineralization and the high exploration and beneficiation costs required to produce a marketable product.

Jan 1, 1963

By George H. Holmes

This report describes the results of a reconnaissance survey of areas in California and Nevada considered favorable to beryllium mineralization. Pegmatite dikes, veins, intrusive sills, contact. metamorphic, and disseminated deposits as well as tactite deposits in the former major tungsten-producing districts were investigated. A general geographic pattern of beryllium mineralization was found to be concentrated along a wide belt in eastern Nevada extending from the Ruby Mountains, Elko County, south through the Fish Creek Range, Eureka County, the Snake Range, White Pine County to the Virgin Mountains in Clark County, Nev., and Mohave County, Ariz. Sporadic occurrences of beryllium are in central and southern Nevada, and in the pegmatite dikes of San Bernardino, Riverside, and San Diego Counties, Calif., and the granite masses of the southern Inyo Mountains, Inyo County, Calif. Principal company activities are centered in the Snake Range, Fish Creek Range, and the Virgin Mountains, Nev., and the Inyo Mountains, Calif. Other areas in California and Nevada have been superficially explored with results indicating either limited or widespread, but submarginal, mineralization. Although beryllium was found to occur, to some extent, in many of the deposits, mining has been hindered by the lack of a market for beryllium ores and concentrates other than standard-grade beryl and also by the erratic pattern of mineralization and the high exploration and beneficiation costs required to produce a marketable product.

Jan 1, 1963

By S. P. Kinney

Economy in blast-furnace practice depends largely upon efficient gas-solid contact in the shaft of the furnace. If efficient work is not done in the shaft the hearth and bosh will not function properly. A condition may be readily imagined where the particles of ore in the shaft are so large that the time entailed in the descent of these materials into the bosh is not sufficient to permit proper reduction and preparation prior to the time the ore enters the bosh of the furnace. Another condition may be pictured where the density of the stock column and the flow of stock is such that the ore will take one course and the gas another. Both of these examples will result in insufficient contact between the gas and the ore. Unreduced ore will reach the hearth, and gas which has not been efficiently oxidized will reach the stock line. The result is the use of an excess of carbon in the smelting process. An example of the result of inefficient gas-solid contact in the shaft of a blast furnace is shown by the curves in Figure 1.

Jan 1, 1930

By Chas. G. Maier

The bright annealing of copper is an industrial practice of considerable importance. In connection with this process, equilibrium concentrations of carbon monoxide and dioxide, which may exist in contact with copper and cuprous oxide at elevated temperatures, are of interest. Data obtained at the Pacific Experiment Station of the U. S. Bureau of Mines enable estimates of these equilibrium concentrations to be made in two independent ways. Although the publication of final data on one method can not take place until certain further experimental work is accomplished, repeated requests which the Bureau of Minus has had for data relative to the annealing and deoxidation of copper justify the present preliminary report. This paper deals with the calculation of gas concentrations in the reduction of cuprous oxide, using more scientific data which will be published later, and refers especially to those conditions of temperature and concentration of practical implication, and from which critical limits ensue.

Jan 1, 1929

By Len Blackman

The Absaroka-Beartooth Study Area is a tract of approximately 1.4 million acres of National forest land in southern Montana, part of the Greater Yellowstone Area. This study evaluated the mineral potential of four mineral terranes containing undiscovered resources in the area. The geological data is probabilistic, with estimates of the possible number: of deposits and their grades and tonnages. Possible future development scenarios range from no development to many mines, including some very large. As two thirds of the study area is within the Absaroka-Beartooth Wilderness, the future development scenarios reflect the area's mineral potential, not what we expect to see in the foreseeable future. Based on the analysis performed on these four terranes, the most likely future scenario for the study area would include the potential for two medium sized, (predominately) gold, mines, each employing a few hundred workers. There is a small chance, less than 5%, that a large Porphyry Copper or Superior Iron deposit would be discovered and be economically feasible to develop.

Jan 1, 1994