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By Laurance L. Oden

The Bureau of Mines is developing melting data for binary combinations of the alkaline earth fluorides and yttria to facilitate the formulation of slag compositions. The present report deals with the SrF2-Y2O3 system for which liquidus and solidus temperatures and solid solubilities were determined. The information is presented as the phase diagram. The phase diagram was constructed from information obtained by ceramogra¬phy, X-ray diffraction, thermal analysis, and electron probe microanalysis of small specimens encapsulated in platinum-20 percent rhodium or molybdenum ampoules. The data indicate a simple eutectic system with limited terminal solid solubilities. The eutectic temperature is 1,457°±5° C, and the eutectic composition is 4±1 mole-pct Y203. Strontium fluoride containing up to 2 wt-pct 0 2 was studied to determine the effects of oxygen contamination. Oxygen levels in excess of 0.2 wt-pct resulted in eutectic formation between SrF2 and SrO. The eutectic composition is between 0.2 and 0.7 wt-pct 02, and the eutectic temperature is 1,447°±5° C. No intermediate oxyfluoride phases were detected.

Jan 1, 1974

By Cleo Griffith Rall

The method for determining the effective porosity, of oil- and gas- bearing sand described in this report is a development of an earlier method devised by Bureau of Mines. The apparatus has been improved and made more convenient to use, but the procedure has been in use for many years without essential changes. A tabulation at the end of the report gives the results of more than 2,000 porosity determinations for oil sands in the fields of 13 states. A selected bibliography of articles containing descriptions and evaluations of various methods of determining porosity Is a. part of this report. The method was devised and developed at the Petroleum Experiment Station at Bartlesville, Okla., as part of the Bureau's research on fluid-energy relationships and ,on methods of improving the recovery of crude oil from underground reservoirs.

Jan 1, 1949

By G. Asai

The purpose of this Bureau of Mines investigation was to determine the properties of arc-melted iron-chromium alloys ranging in chromium content from 12 to 50 wt.-pct. Alloys were prepared by consumable-electrode arc melting of electrodes composed of high-purity chromium and high-purity iron. Alloys were fabricated to rod and sheet, and the following data were obtained: Electrical resistivity, hardness, tensile strength, and impact strength at room temperature; and creep-rupture life at 650° C. (1,200° F.). As the chromium content of the annealed alloys varied from 12 to 50 pct., the properties varied as follows: The electrical resistivity increased proportionally from 41 to 53 microhm-cm,; the Rockwell hardness varied from A 38 to A 58; the tensile strength ranged from 52,000 to 96,000 p.s.i.; the impact strength of V-notched charpy specimens varied from 140 to 405 ft.-lb., and the 100-hour creep rupture life at 1,200° F. varied from 5,000 to 16,000 p.s.i.

Jan 1, 1962

By H. S. Caldwell

The objective of this investigation by the Bureau of Mines was to develop and test for laboratory use a retort embodying many features required for practical commercial-scale applications of vacuum distillation of metals. A gas-fired vacuum retort was developed comprising a hollow, cylindrical graphite liner encased in a thin shell of stainless steel. The liner prevents the shell from collapsing under vacuum and protects it from corrosion by metal vapors and the molten metal charge. The vacuum-tight shell protects the liner from oxidation and flame erosion. The retort was used to distill zinc from dross and die-casting scrap. More than 99 percent of the zinc was recovered as a condensate containing 99.8 to 99.9 percent zinc. (Atmospheric distillation recovers 95 to 98 percent at a purity of 99.5 percent zinc.) Distillation rates of 50 pounds of zinc per hour were attained at a temperature of 65° C. with pressures ranging between 50 and 100 microns. Distillation at this low temperature is not practicable at atmospheric pressure. Also, the retort is suitable for distilling other volatile metals such as cadmium and magnesium.

Jan 1, 1961

By Albert W. Cox

This paper, one of a series prepared for the United States Bureau of Mines discussing the methods used in mining, crushing, and grinding materials for cement manufacture, deals particularly with the methods used at the Security plant of the North American Cement Corporation. These papers are designed to disseminate technical information regarding the methods used. The cost tabulations represent local operating expenditures only and not total production costs. It is recognized that publication of, total production costs might in many instances cause embarrassment to individual producers as well as to the industry as a whole. On the other hand, operating costs are essential to the technical discussion and study of methods employed. The attention of the reader is specifically called to this differentiation in order that no misunderstanding of the scone of the cost tabulations shall ensue.

Jan 1, 1932

By T. E. Ackman

Scale inhibitors and slow-release polymers were tested by the Bureau of Mines at mine drainage treatment facilities. The scale inhibitors were investigated to determine their effectiveness in controlling gypsum (CaSO4) scale; the polymers were investigated to determine their effectiveness for increasing settling rates of suspended iron hydroxide. Two types of scale inhibitors were tested at a site having a severe CaSO4 scaling problem. Both proved to be effective in controlling scale formation; in addition, one caused the dissolution of CaSO4 deposits. Slow-release polymers were tested at three mine drainage treatment facilities. These gelatinous polymeric flocculants were found to be convenient and easy to use, but only effective when pH could be controlled.

Jan 1, 1984

By H. G. Skavlem

This paper is prepared the United States Bureau of Mines and is descriptive of methods, practice, and costs at the McIntyre Porcupine Mines, Ltd., Schumacher, Ontario. The property is located in the Pearl Lake section of the Porcupine mining district. It is reached by a branch line of the Temiskaming & Northern Ontario Railway from Porquois Junction. There is also a good motor road into the district. The Hollinger Consolidated Gold Mines and the Coniaurum Mines, Ltd., are adjacent properties. Power for both the mining and the pulp and paper industries in the district is supplied by an extensive development of the water-power resources. Weather conditions are favorable for mining operations.

Jan 1, 1933

By Robert N. Roby

Deposits of iron ore in Judith Basin County, Mont., generally referred to as the Running Wolf deposits, were examined by an engineer of the Bureau of Mines in August 1942. During the Summer of 1943 the Federal Geological Survey made a reconnaissance survey of, the Running Wolf Iron district and also made a detailed study and a topographic and geological map of the eastern end of the district. Two deposits of iron ore at the eastern end of the district were trenched and drilled by the Bureau of Mines during the fall and winter of 1943-44, This report presents the factual data obtained from the trenching and drilling' operations. The iron deposits of thy Running Wolf district are accessible from Stanford, Mont., by 14 to 16 miles of county highway and 2 to 3 miles of rough mountain road or trails (see fig. 1). No shipments of ore have been made from of these deposits. The ore is a replacement of Madison limestone at the contact with syenite porphyry. The contact can be traced for about 6 miles in a general northwest direction. 'At least five. deposits occur along this contact.

Jan 1, 1949

By Benjamin W. Haynes

This Bureau of Mines publication comprises a compilation of the state of the science in Pacific Ocean manganese nodule mineralogy and elermental composition. The report is divided into three sections: morphology, mineralogy and elemental composition. The nodule morphology section defines what is considered a nodule for the study, and details the external characteristics and internal structure. Nodule mineralogy is discussed in three sections: manganese minerals, iron oxide minerals, and accessory minerals. The major manganese minerals discussed are todorokite, birnessite, and vernadite. The iron oxide minerals are less well known and include feroxyhyte, goethite, and lepidocrocite. Accessory minerals present include quartz, clays, and other silicates and nonsilicates. A discussion on moisture content is also included. The elemental composition section presents data on 74 elements occurring as cations or anions. Summary data, histograms, and interelement correlation coefficients are presented. The elements are grouped as follows: major and minor elements of potential economic interest (8), other major and minor elements (9), elements of environmental interest (8), rare-earth elements (15), precious-metal-group elements (6), radioactive elements (3), other trace elements (17), and anion-forming elements (8). Cross sectional determinations of Ni, Cu, Zn, Co, Pb, Fe, Ce, and Ba are given for a single nodule to show the general tendency of different growth patterns within a nodule because of different element associations and composition.

Jan 1, 1982

By J. L. Kohler

Component failures in the electrical control circuits of mining machines account for a large percentage of the total downtime of the machine, Once a failure has occurred it is always a tedious and usually a time-consuming task to locate the failed component. Moreover, the pressure to quickly locate the cause of a delay can lead to compromises in safety. Thus an onboard diagnostic system, essential for an automated machine, would be a very useful addition to existing machines. This report details U.S. Bureau of Mines development of a generic procedure for synthesizing diagnostic systems for electrical-control-circuit failures in mining machinery. A continuous mining machine is used as the testbed to illustrate the application of the developed methodology. Substantive differences among mining machine control circuits made it impossible to achieve a generic diagnostic system, but a generic approach for the synthesis of the diagnostic system was possible. As the research progressed, it became apparent that an algorithmic approach was better than an expert-system-based implementation. A prototype system was constructed and used to evaluate the diagnostic system. Prototype implementation issues are also examined.

Jan 1, 2010

By R. E. Morgan

[IN COMPILING the table of analyses of this bulletin every available source of information was studied. These sources, as listed at the end of the table, were many and varied, and it believed that the tabulation gives the best general information obtainable. However, its known accuracy and completeness of coverage necessarily fall far short of published data on coals of the United States. A table of world production of coal and lignite, as and published by the Bureau of Mine, of world resources of coals, brown coal, and lignite, as published in the Yearbook of the World Power Conference, 1948, are included for convenience of the reader. The six continental maps at the end of the bulletin show the general location of the principal coal fields.]

Jan 1, 1952

By J. E. Chilton

The U.S. Bureau of Mines has developed an intrinsically safe carbon monoxide (CO) monitoring system for mines by coupling a fiber-optic data telemetry (FODT) system with a prototype electro-chemical CO monitor. The CO monitoring system can be used in a coal mine as one component of an early fire warning system. This system may be used in belt haulage entries when the entries are used for supplying ventilation air to working places. The FODT accepts a 0.1-to 1.1-V analog signal from the monitor and converts it to pulses (0 to 5 V) at frequencies from 1.1 to 11 kHz that drive a light-emitting diode (LED). An electrically nonconducting fiber-optic cable carries the LED signal to a remote receiver. The receiver analyzes the incoming light signal and displays the measured CO concentration in parts per million. This report discusses the performance of the FODT system and characteristics of the CO monitor such as response times, linearity, and temperature and pressure effects.

Jan 1, 2010

By Fun-Den Wang

This report presents the results of two large scale field coal pillar strength tests (80 ft by 80 ft), the results of a series of laboratory small core sample tests, and the correlation between those field and laboratory tests. The concept of applying laboratory coal sample strength data to predict the in situ coal pillar strength appears to be feasible. The deformation property of large pillars can be obtained successfully by testing the coal sample in the laboratory within acceptable accuracy. There are prevailing directional strength and deformation properties in coal pillars along the butt and face cleat system.

Jan 1, 1976

By E. Morrice

The Bureau of Mines investigated methods for beneficiating platinum-palladium ores from the Stillwater Complex, Montana. Results of bench-scale and pilot-scale studies employing froth flotation to recover sulfide concentrates containing platinum-palladium values from a serpentinized ore are presented. Best results in the pilot mill were obtained with a sodium isobutyl xanthate-normal dodecyl mercaptan col-lector combination at a natural pH of 8.2. A rougher concentrate con-taining 1.7 oz/ton Pt and 4.7 oz/ton Pd was prepared. Recoveries of platinum and palladium were 96 pet and 86 pet, respectively. Batch cleaner flotation of rougher concentrates yielded concentrates contain-ing 3.7 oz/ton Pt and 9.8 oz/ton Pd.

Jan 1, 1984

By E. Morrice

The Bureau of Mines investigated methods for beneficiating platinumgroup metal ores from the Stillwater Complex , Montana , as part of its program to increase the supply of critical and strategic minerals and metals from domestic resources . This report presents results of a 5- day continuous campaign employing a pilot flotation mill to recover sulfide concentrate containing platinum- palladium values from anorthositic ore . A mercaptobenzothiazole - sulfuric acid reagent suite was used . The pilot flotation mill was operated at an average feed rate of 106 lb/ hr of ore . A rougher concentrate containing 8.5 pct of the feed was prepared ; it assayed 1.1 oz /ton Pt and 3.5 oz / ton Pd . Recovery of platinum and palladium were 91 and 87 pct , respectively .

Jan 1, 1965

By Fay B. Dillard

This Bureau of Mines report reviews the disposition of natural gas as delivered to industrial consumers via main line sales. Salient information on main line, or direct, natural gas sales to industrial users is presented by State) standard industrial classification code (SIC) revenue, and type of sales for the years 1968 through 1973.

Jan 1, 1975

By C. W. Davis

This is the first of a series of papers being; prepared as the work progresses in a study of the hydrometallurgy of manganese. The investigation is being made in an endeavor to make possible the utilization of lour-grade domestic manganese ores. The value of a hydrometallurgical process for manganese depends on the present and future uses for manganese products.

Jan 1, 1930

By O. C. Blade

This report on the properties of motor fuels sold through service stations in the United States was made in accordance with a cooperative agreement between the American Petroleum Institute and the Bureau of Mines of the United States Department of the Interior. By agreement with the American Petroleum Institute, identification of the items is confidential. It presents analytical data for 4,421 samples, representing the products of 131 companies. The samples were collected during June, July, and August, 1953. As in previous surveys, the gasolines covered by this survey include those from both large and small suppliers. The data were obtained by laboratories of various refiners, motor manufacturers, and chemical companies and submitted to the Bureau of Mines for compilation. A list of the National Motor-Gasoline Survey reports published during the past 10 years is given on page 5.

Jan 1, 1954

By A. C. Fieldner, G. W. Jones

Tests were made at the Government Fuel Yard , operated at Washington , D. C. by the Bureau of Mines , Department of the Interior , in order to determine and improve the adjustment of the carburetors on the trucks used for transporting coal from the Fuel Yard to the different Government buildings in Washington . The tests were made possible through the hearty cooperation of G , S. Pope , engineer in charge of the Fuel Yard . Joseph Burrows and A. E. Foote of the garage department assisted during all the tests and supplied information on the mileage obtained by the trucks for the months preceding and succeding the time the tests were made . The Mack trucks used range in capacity from 2-1/2 to 7-1/2 ttoonnss .. The majority of the carburetors were Stromberg G- 3 type , as shown in Table 2. During the winter months , when the demand for coal is heavy , from 30 to 35 trucks are used . At the time the tests were made , only about ten of the trucks were in daily use , owing to the small demand for coal during the summer months , and scarcity due to labor conditions . Samples of the exhaust gas were taken on the trucks kept in service for summer hauling in order to determine the carburetor adjustment as used . Changes were then made to a more economical adjustment wherever possible , without sacrificing flexibility of operation and power . In every case the adjustments were maintained for maximum power , but were adjusted to the leanest position to give that power . In all but one case the carburetors were found to be adjusted too rich for maximum power and economy . These results are considered in detail in a later part of this report .

Jun 1, 1923

By Walter E. Lewis

Ventilation-air-heating plants are in use at several iron mines on the Menominee Iron Range, Iron River, Mich. Many of the mines are exceptionally wet; during winter months, when fresh air is forced down the wet air shafts into the mine, it is usually necessary to heat the fresh air to above freezing so that the openings will not be closed by ice. The problem of ice closing air shafts has been solved by the practice of reversing the air current before the openings have become completely closed. This procedure involves drawing warm air from the mine up the usual down-draft air shaft. The M. A. Hanna Co. has found, at some of their mines on the Menominee Range, that it is more convenient to heat the below-freezing air rather than reverse the air current. Intermittent freezing and thawing of ice that has formed in the air shaft tends to loosen the wall rock, requiring major shaft repairs. The openings are kept free of ice the year around by heating the fresh air during periods of below-freezing weather. Table 1 shows the monthly minimum moan, maximum mean, and mean temperatures for the Iron River area. Under normal conditions of temperature, the furnaces are fired in November and usually are not allowed to go out until April of the following year.

Jan 1, 1951