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By Božidar Šarler, Umut Hanoglu

A rolling simulation system has been developed to calculate the macroscopic rate of deformation, stress, strain, and temperature fields by using a novel meshless method. The model is based on two-dimensional traveling slice assumption. The slices are aligned towards the rolling direction. The initial size of the billet, bloom or slab and the geometry of the grooves at each rolling stand, the distances between the rolling stands, and continuous or reverse rolling can be arbitrarily considered. The purpose of this paper is to complement these development by predicting and visualizing also the grain size of steel over the strand cross-section for each position in the rolling mill. The grain size models have been in one-way coupled to the macroscopic calculations. First the critical strain for dynamic recrystallization is being checked. If the calculated strain is higher than that, considering also the time for meta-dynamic recrystallization, dynamic or meta-dynamic grain size calculations are carried out. If the strain is too low then only the static recrystallization is considered together with its required time. Finally, austenite grain size and ferrite grain size are calculated respectively as the steel cools down. The listed physical models are based on collection of empirical relations found in literature. The user of the system is free to choose or create the model he wants with his own parameters. The simulation system has been coded as a user friendly computer application for an industrial use based on C# and .NET framework and runs on regular PCs. The computational time for a rolling simulation is usually less than one hour and can thus be straightforwardly used for optimization of the rolling mill design in a reasonable time.

Oct 1, 2019

By Cristiano José Scheuer

The effect of low-temperature plasma carburizing treatment on the micro-abrasive wear resistance of AISI 420 steel was investigated by mean of a CSM Calowear ball-cratering equipment. Carburized samples were treated at temperatures of 350, 400, 450 and 500°C for a fixed time of 12 h, using a gas mixture containing 99.5% (80% H2+20% Ar)+0.5% CH4. Micro-scale abrasive wear tests were conducted with a 25.4 mm AISI 420 steel sphere, using an abrasive suspension of alumina (Al2O3) with particle size of 1 ?m (abrasive concentration of 0.11 g/cm³). The contact normal force, abrasive flow and ball rotation speed were fixed at: 0.5 N, 0,2 drop/s, and 120 rpm. The wear craters were analyzed using a confocal laser microscope, Olympus OLS 3000. The wear analyses were performed for test times of: 30, 60, 90, 120, 180, 360, 540, 720 and 900 s (equivalent sliding distance: 0.84, 1.68, 2.52, 3.36, 5.04, 10.09, 15.14, 20.19 and 25.23 m, respectively). The results indicate that the wear coefficient in the outer layer and in the diffusion layer are different, being lower in the latter. It was also verified that the wear coefficient on the outer layer region decreases with increasing treatment temperature in the range of 350 to 450 °C, and increase again for 500ºC. The diffusion layer wear coefficient is similar for all the carburized samples. Finally, for all studied conditions, the analysis of the wear craters surface indicates the occurrence of grooving and micro-rolling abrasion wear modes.

Aug 8, 2018

By Alessandro Martinis

The performance requirements for modern steelmaking facilities are ever more stringent, as customers and markets are continuously pushing for technologies which allow having high quality steel produced in an economic and sustainable way. In the details, this paper has the aim to present the excellent results obtained by integrated steel plant where an EAF is fed with high quality hot ENERGIRON DRI. The recent technology developments, combined with the affirmed basic process design, contributed to further maximize the energy of the DRI, reaching the EAF at temperatures above 600°C with a carbon content up to 3.5%, as confirmed by plant data. These improved input material characteristics resulted in reduced electrical energy consumption and increased liquid steel production.

Aug 16, 2017

By Flávia Tereza dos Santos Fernandes Tolomelli

Este trabalho teve como objetivo estimar as temperaturas de transformação de fases por meio de termodinâmica computacional (A1 e A3), dilatometria (Ac1 e Ac3) e monitoramento do resfriamento ao ar após passes de laminação a quente em escala piloto (Ar3 e Ar1). Objetiva ainda descrever a evolução microestrutural da austenita em um aço baixo C microligado ao Nb onde se almeja a produção de um aço ferrítico-bainítico, coletando-se amostras após cada passe de laminação através do congelamento da microestrutura por intermédio de resfriamento em salmoura com o objetivo adicional de verificar a ocorrência de recristalização entre passes.

Jul 30, 2018

By Xiaowei Du, Xitao Wang, Xuekun Shang

The deformation behaviors under both tensile and compressive forces and microstructure evolutions of cast SA508-4N steel were investigated at elevated temperatures. True stress-strain data were obtained from hot deformation experiments performed on a Gleeble-3500 thermal-simulator under different temperatures (750-1200C) and strain rates (0.001-10 s-1). The reduction of area decreases as a function of temperature from 750C to 900C and then increases. At 1200C, the reduction of area reaches more than 99% with the strain rates of 0.5 s-1 and 1.0 s-1. The dynamic recrystallization under compressive stress occurs at 800C under low strain rate and a complete dynamic recrystallization can be observed when the temperature reaches above 1100C. A “two-stage” flow stress constitutive model concerned with dynamic recovery and dynamic recrystallization was established based on the true stress-strain data. This model shows good agreement with experiment results. Moreover, we developed a dynamic recrystallized grain size model to describe the average grain size after complete dynamic recrystallization.

Oct 1, 2019

By Janaina Goncalves Maria Da Silva Machado, Francisco Carlos Gomes da Silva Junior, Stephany Aparecida Santos da Mata, Walney Silva Araújo, Matheus Souza Rodrigues

O aço inoxidável duplex (AID) ASTM 890 de grau 3A tem grande utilização na indústria de tubulações de petróleo no Brasil e no mundo. O estudo da variação do tempo necessário para solubilizar um material é importante, pois, diminuindo esse tempo, pode ser reduzido gastos com forno. O objetivo desse trabalho é comparar diferentes resultados para três tempos distintos de solubilização do aço inoxidável duplex fundido ASTM 890 de grau 3A. A literatura indica que a solubilização desse aço deve ocorrer na temperatura de 1120°C, no período de 4 horas. Entretanto, não existem trabalhos que mostrem a influência da diminuição do tempo do tratamento térmico na resistência á corrosão desse material. A fim de analisar isso, foram feitos trés tratamentos térmicos a 1120°C, em tempos 30 minutos, 2 horas e 4 horas. O grau 3A tem como característica, por exemplo, não conter cobre em sua composição, ter 1%p Mn e ter também 25%p Cr. Para tal estudo foi feito uma análise microestrutural em microscópio ótico para observar diferenças nas fases do material. Em seguida, foi usado ensaios eletroquímicos de monitoramento de potencial de circuito aberto, espectroscopia de impedância e polarização pontenciodinâmica anódica, utilizando um eletrólito de NaCl 1M, para ver o desempenho contra a corrosão nessa liga. Também foi feita uma avaliação mecânica do aço sendo exposto a testes de microdureza. Por fim, foi obtido, com esses resultados, pouca mudança significativa no comportamento do material após diferentes tempos.

Mar 1, 2019

By Eleir Mundim Bortoleto

A finite element modeling approach was developed to study adhesion phenomena during the unidirectional contact between a two-dimensional plane-strain square and a flat slab. Surfaces were metallic or ceramic, different pairs of materials were analyzed and their adhesion was considered by means of a FORTRAN subroutine (DLOAD), which was connected with commercial finite element code Abaqus and provided surface attractive forces based on the Lennard-Jones interatomic potential. Adhesive loads were considered both during approximation and separation of the surfaces. During the separation step, material transfer between surfaces, due to adhesion, was modeled by means of damage initiation and propagation at the flat slab. The parameters considered in the simulations were normal load, chemical affinity and system size and the different conditions were analyzed by comparison of the interaction forces during approach and withdrawal. This work also presents detailed descriptions of: (i) the evolution of energy dissipation due to adhesion hysteresis, (ii) the formation-growth-breakage of adhesive junctions and (iii) the evolution of stress distribution during the process. Results have indicated that chemical affinity between the bodies in contact is more relevant for adhesion than the applied load. Besides, smaller asperities are less prone to promote adhesive wear, but they may be subjected to high stress concentration effects.

Jul 31, 2018

By Luiz Gabriel da Silva Nascimento

Um material que vem sendo muito estudado quando imerso na matriz de outros materiais, são os nanotubos de carbono, uma forma alotrópica do carbono, que são milhares de vezes mais finos que um fio de cabelo, mas que apesar disso, possuem uma extraordinária resistência mecânica. O alumínio por apresentar um baixo peso específico e ter a facilidade de se unir a outros materiais pode nos fornecer excelentes propriedades e muitas aplicações tecnológicas. Através de ensaios metalográficos e mecânico, esse trabalho avaliou o comportamento microestrutural e de microdureza do alumínio depois da adição nanotubo de carbono e nanotubo mais níquel em sua estrutura. Foi usado um processo de fabricação por fusão com agitação mecânica por um pequeno motor elétrico e resfriamento brusco por água. Depois das análises nesses diversos materiais, com composição diferenciada, o que melhor apresentou propriedade mecânica foi o Al-3%Ni+nanotubo de carbono.

Aug 7, 2018

By Sebastien Flament

More and more Hot Strip Mills are facing defects on their products that lead to a rejection of complete product batches by their customers. Several of those defects are induced by excessive work roll degradation. This paper is focussed on the understanding of work roll corrosion and oxidation mechanisms in a hot strip mill. Several laboratory trials (Hot rolling simulator, cyclic oxidation) have highlighted important factors influencing corrosion of work rolls as well as helping the understandings of oxidation of a work roll in the roll bite and along the roll circumference in a stand. The attention is focussed on several elements present in water used in HSM for direct roll cooling (e.g. chloride, bactericides, sulphates, phosphates) and their effect on roll surface degradation. The second part of this paper is focused on the understanding of work roll oxidation along the roll circumference. The effects of roll composition, roll temperature, water composition and water temperature have been studied in order to understand the oxidation/corrosion mechanisms in a HSM.

Aug 16, 2017

By Marjorie Benegra

This study aims to compare the wear resistance assessed in rubber wheel abrasion test of nickel aluminide coatings deposited by for Plasma Transferred Arc (PTA) and High Velocity Oxigen Fuel (HVOF) manufacturing, using the same raw material. A nickel aluminide powder was atomized and deposited on 316L steel plate substrate. After deposition, some specimens were submitted to a heat treating (1200 °C for 24 h followed by 760°C for 24 h). The coatings deposited using PTA developed different microstructures due to the incorporation of substrate elements, its performance was better than the HVOF coatings, although their Vickers hardness was similar. After heat treating, a significant variation in hardness and wear resistance was observed. For PTA specimens, there were decrease in hardness of 35%, while for HVOF ones this drop was approximately 20%. Nonetheless, the effect of thermal exposure in wear resistance was quite different: an increase of 21% was observed for HVOF coatings, while a reduction of 20% occurred in PTA ones. Microstructures modifications in PTA coatings were significant for their wear resistance. On the other hand, the reduction of porosity and sintering were responsible for a better performance of heat-treated HVOF coatings.

Jul 31, 2018

By Marcos Felipe Macêdo Cardoso

Com o aumento dos investimentos energéticos na região amazônica, surge a necessidade de recapacitação das linhas de transmissão existentes, a fim de mitigar as interrupções de fornecimento de energia para os grandes centros urbanos. Dentro deste contexto, as ligas termorresistentes possuem alta capacidade de transmissão de eletricidade, propondo-se avaliar a influência do tratamento térmico sobre as propriedades da liga Al-0,05%Cu-[0,35-0,45]%Fe modificada pelo teor de 0,15%Zr. Os lingotes foram obtidos por fundição direta em coquilha metálica, usinados e envelhecidos artificialmente por 04 (quatro) horas a 150ºC e comparado seus resultados para a mesma liga sem tratamento. A influência do tratamento térmico foi avaliada através da caracterização macroestrutural, elétrica (ensaio de resistividade) e mecânica (ensaio de tração). Foi selecionado o diâmetro que apresentou os melhores resultados nos ensaios, para realização dos testes de termorresistividade, segundo o Protocolo COPEL e a Norma ASTM B941-10. O tratamento térmico provocou ligeiro aumento nos valores de condutividade elétrica e limite de resistência à tração (LRT), sem alteração da macroestrutura. Como destaque, o diâmetro 3,0 mm apresentou os melhores resultados de LRT e condutividade, cujos fios foram caracterizados como termorresistentes com e sem tratamento térmico segundo o Protocolo Copel, e somente os fios com tratamento térmico segundo a norma ASTM B941-10.

Oct 30, 2017

By Tiago Silva Costa

Os tratamentos térmicos são um conjunto de operações que têm por objetivo modificar as propriedades dos aços e de outros materiais através de um conjunto de operações que incluem o aquecimento e o resfriamento em condições controladas. Os aços SAE J403 1045, SAE J403 1075 e DIN 100CrV2 são aplicados em diferentes setores industriais graças às diferentes propriedades que podem ser alcançadas através de tratamentos térmicos. Este trabalho visou caracterizar e descrever as fases formadas nos aços SAE J403 1045, SAE J403 1075 e DIN 100CrV2 após tratamentos térmicos de têmpera, normalização e recozimento pleno.

Aug 16, 2017

By Dr. Steven G. Jansto

The market demand for reduced fuel consumption and CO2 emissions in the automotive, energy and construction sectors have further increased the demand for new and advanced higher quality microalloyed grades produced via TMCP. The technological integration of the process and physical metallurgical advancements of value-added niobium (Nb) microalloyed thermo-mechanical controlled process (TMCP) steels continue to be developed and is an important element for these more demanding end user requirements and cost-effective steel production. The reheat furnace process step has a profound effect on the TMCP performance, final hot rolled steel quality and mechanical property consistency during the production of hot rolled steels. The uniformity of heating applied across the entire width, thickness and length of the slab or billet is essential in the successful achievement of consistent customer properties regardless of the chemistry. The resultant ferrite grain size in the final hot rolled product is significantly governed by the initial prior austenite grain size. However, the transition from laboratory melted and TMCP hot rolled heats to the production scale is often quite challenging. Aberrations in the reheating process step at the industrial furnace are often the root cause of mechanical property quality issues. These combustion process metallurgy parameters connect directly to the resultant TMCP product quality and is defined as Combustion Metallurgy

Oct 1, 2019

By Giuseppe Pintaude

This study aims to evaluate the effect of specimen preparation on the dry sliding wear behavior of CA-6 NM stainless steel. Two different surface finishing manufacturing processes were applied: lapping and metallographic polishing. The wear tests were conducted in reciprocating ball-on-flat system, performed for two loads: 5 or 8 N. For all test conditions, hardmetal ball was employed as counterbody. The surfaces were evaluated using 3D interferometry technique to determine their surface roughness, including texture analysis regarding isotropy. Surface characterization results indicated the presence of texturing and preferential orientation, since the parameter Str was smaller than 0.5 for samples of both the studied conditions. Two distinct levels of isotropy evaluated through Str parameter were achieved: 0.13 for lapping and 0.3 for metallographic polishing process. It is clear from wear tests that the variation of average surface roughness is the key point for tribological behavior of CA-6 NM stainless steel.

Jul 31, 2018

By Ariella Vianna Fontes

Os dutos de plástico reforçados com fibra de vidro, devido a sua boa relação entre resistência mecânica, peso e resistência à corrosão, são amplamente utilizados, por exemplo, na indústria petrolífera. Todavia as conexões de vários trechos desses dutos, realizadas por juntas adesivas, podem apresentar defeitos como a falta de adesão e a falta de adesivo, tornando-se pontos propícios ao colapso. Até o momento ainda não há uma metodologia de ensaio não destrutivo consolidada, capaz de avaliar a integridade das juntas adesivas. A técnica mais utilizada é o ensaio de ultrassom, porém com fortes limitações. Dentro desse contexto, o presente trabalho apresenta a caracterização dos defeitos utilizando a técnica de microtomografia 3D, visto que esta permite examinar a estrutura interna do material. Foram confeccionados e avaliados corpos de provas contendo os defeitos típicos encontrados em campo. Os resultados mostraram que a técnica utilizada é adequada para caracterização qualitativa e quantitativa dos defeitos típicos em juntas adesivas encontrados em campo.

Aug 16, 2017

By Anderson Esteves Bragança

Foi identificado na área da unidade técnica da laminação de tiras a quente uma necessidade de cruzamento de dados de diversos sistemas de nível 1 (Instrumentação), nível 2 (Automação) e nível 3 (TI), para análise do processo. Todo esse processo de extração e formatação dos dados levava dias, com necessidade de suporte da equipe de TI, ou às vezes nem era possível devido à complexidade de cruzamento de informações. A ideia era prover uma ferramenta capaz de acessar diferentes bases de dados permitindo a integração dessas informações de forma simplificada e ágil. Após avaliação de ferramentas disponíveis no mercado (Ferramentas de Analytics e BI) a opção foi por uma que trouxe: a integração dessas bases, redução do tempo gasto na preparação de indicadores e um maior tempo disponível para investigação e solução de problemas por parte dos especialistas. A conclusão do projeto foi uma unidade técnica mais produtiva e autônoma, com uma menor dependência da equipe de informática e automação.

Oct 30, 2017

By Raúl Daniel López

Un objetivo de seguridad y calidad en los moldes de la colada continua de Siderar fue la de tener un menisco estable y controlado. A lo largo de los distintos periodos de inversiones y mejoras, el control de nivel de Siderar logro como objetivo contener su variación de nivel de acero en el molde en un rango de variación menor a +/-2 mm y con una velocidad de cambio inferior a 1,5 m/segundos. Esta etapa trajo una relativa mejora en los aspectos mencionados (calidad y continuidad operativa) pero el hecho de tener como sistema de medición de nivel un sistema radiactivo (fuente Co60 y contador de centelleo) mantenía serias limitaciones en ambos rubros dado que este sistema no diferencia la interface escoria /polvo colador con el menisco de acero. Este trabajo tratará de mostrar y contar las tareas de desarrollo y aplicación de esta nueva tecnología, hoy vigente en la nueva Colada Continua N° 2 (CCD2) y en etapa de puesta en marcha de la CCD1.

Aug 15, 2017

By Heidy de Oliveira Simões

Visando entender os impactos causados pela formação de trincas e deformação das pelotas na qualidade física do material, foi desenvolvido um algoritmo que, através de análise automática de imagens, é capaz de medir o tamanho da trinca, sua largura e comprimento, bem como efetuar as medições de tamanho e morfologia da pelota queimada. Foram analisadas pelotas produzidas com minério hidratado (elevado teor de goethita) com 2 perfis térmicos distintos. Os dados obtidos na análise de imagem foram correlacionados com a resistência à compressão das pelotas e evidenciaram o tamanho das trincas denota notória correlação com a sua resistência física. A medição das trincas formadas pela deformação da pelota no leito (denominadas resiliência) permite evidenciar o quanto a pressão no leito de pelotas impacta na qualidade após a queima, bem como indica o ponto ótimo para que não acarretem em perda da resistência. A medição do tamanho das trincas térmicas mostra-se essencial, pois mesmo em perfis mais suaves de queima pode haver a formação de tais trincas, sendo que o tamanho e a abertura da trinca é que definem a melhor ou pior resistência. O conhecimento, e possível aplicação prática, da avaliação das trincas poderá auxiliar na otimização de perfis térmicos de fornos de pelotização.

Aug 16, 2017

By Luis Armando Espitia

AISI 410 martensitic stainless steel specimens were low temperature plasma nitrided at 400°C in a mixture of 75%N2:25%H2, during 20 h. Active screen technic was used to avoid any edge effect The nitrided case is composed of expanded martensite (a’N) and e-Fe3N iron nitride, whilst chromium nitride precipitation was avoided. Surface hardness reached 1275 HV0.01. The transverse microhardness profile shows a gentle hardness gradient with a NHT nitrided case depth of 28 µm. Nanoindentation tests were carried out in order to assess the hardness (H), the Young modulus (E), the H/E and H3/E2 ratios and the elastic recovery (We) of both nitrided and non-nitrided specimens. The cavitation erosion mass losses were measured as a function of exposure time. The results showed a decrease of 27 times of the mass loss compared to the non-nitride specimens. Wear rate decreased from 2.56 mg/h for the non-nitrided condition to 0.085 mg/h after nitriding. The increment in the elastic recovery and the higher hardness values are responsible for the greater cavitation erosion resistance exhibited by the expanded martensite. Such results showed that low temperature plasma nitriding and the formation of expanded martensite are effective to increase cavitation erosion resistance of AISI 410 stainless steel.

Jul 31, 2018

By J. Bas A. F. Smeulders

Traditional laboratory lubrication tests, including those for cold rolling lubricants often involve measurement of neat oils. To achieve increased levels of test severity, such tests are often carried out at high temperatures and prolonged durations. However, we found that the levels of lubricant degradation and wear in these tests can be much higher than in the field. Moreover, steel rolling is not done with neat oils, but with emulsions, where the presence of water influences film formation, surface chemistry and oil composition in the roll bite. To better approach the situation in the field, and thus to be able to develop rolling oils with improved lubrication performance, several lubrication tests were developed for emulsions: direct measurement of film formation and measurement of Stribeck curves, in which the emulsions can be assessed in terms of their boundary lubrication and elastohydrodynamic behaviour. The key innovation is that also another test method was developed, which focuses on boundary lubrication and wear, and the role of extreme pressure and anti-wear additives. Realistic levels of test severity are achieved in the tribometer by mimicking frictional power intensities and flash temperatures for typical cold rolling or tinplate mills. Test conditions can be adapted according to the mill stand or pass number and other cold rolling process parameters. The emulsions are kept at normal operational temperature. Clear differences could be observed between emulsions of various concentration and composition. The viability of the method is illustrated by a number of field cases, in which a good correlation is demonstrated between the laboratory tests and the performance in a pilot or production mill.

Jul 30, 2018