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By André Carlos Silva

Dewatering stage is among the most important industrial unit operations, and is wide adopted in many different industries, due the fact that a large portion of industrial products is produced using suspensions of solids in liquids. Nowadays the mineral processing tailings disposal is a big problem due the environmental degradation produced. The phosphate rock processing in Anglo American Phosphate Brazil, situated in Catalão/Go/Brazil, generates around 180 t/h of tailings for a plant feed of 480 t/h (approximately 37,5% of the processing plant feed), with 5 to 10% of solids and approximately 14% of P2O5. Nowadays the tailings are sent direct to the tailings dam. The present work proposes the paste production using with the tailings from phosphate rock processing plant divide in two different stages. The first one composed by the free settling of the material in presence of industrial flocculants in a graduated cylinder with 2.0 L of internal volume for one hour, in the same way it must occur in conventional thickeners. After that time, the clarified liquid was drained and the remaining pulp was sent to the second stage consisting in the tailings vacuum filtration. Ten different flocculants and nine different filter media were tested. The found results were satisfactory for paste tailings production with solids percentage around 65%.

Aug 8, 2018

By Enrique Francisco Somolinos Garcia-Morales

In this paper we will discuss the benefits of a very innovative way of introducing MgO in the blast furnace operation through the sinter, using mini lumps of dunite. By changing the traditional way of using an MgO bearing material in fines form (particle smaller than 5 mm), most of the MgO inserted material behaves as inert during the sintering process, with the effect of having the following parameters (among others) improved: productivity at the sintering bed, permeability inside the blast furnace, energy consumption, stability of the operation.

Aug 1, 2018

By Evan Thomas

It has been shown before that liquids can slip at a solid boundary, which prompted the idea that parallel-surface bearings can be obtained by the use of alternating slip and non-slip regions in the direction of fluid flow. The amount of slip at the wall depends upon the surface tension at the liquid - solid interface, which in turn depends on the chemical composition of the surface and its roughness. In the present study a heterogeneous surface was created by coating half of a circular glass disc with a coating repellent to glycerol. A rotating glass disc was placed at a known distance above the coated stationary surface and the gap was filled with glycerol. With the top surface moving in the direction of slip to non-slip region, a pressure build up can be theoretically predicted. The pressure gradient in the two regions is constant, similar to that in a Rayleigh step bearing, with the maximum pressure at the boundary. In order to accurately measure the force generated by the pressure increase, a load cell was attached to the heterogeneous disc. Experiments were conducted by varying both sliding speed and distance, and the resultant load carrying capacity was measured and compared with theoretical calculations. This allowed the slip coefficient of the coated surface to be evaluated.

Jul 31, 2018

By Mery-Cecilia Gómez-Marroquín

O presente trabalho trata da formação da ferrita de zinco a partir da mistura e posterior reação solido-solido entre o óxido de zinco e óxido de ferro - Fe2O3 puros em proporções equimolares. A faixa de temperatura onde teve lugar a formação foi entre 1073 e 1373 K. Testes de redução da ferrita da zinco sintética-ZF e pós de aciaria elétrica–EAFD foram realizadas usando misturas de CO e CO2 que variaram entre 50 e 100% CO. Ambos os testes (formação e redução de ZF e EAFD) foram suportados usando técnicas de caracterização física, química, estrutural e microscópica. No caso da redução, foi observado que tanto a temperatura como a percentagem de CO, foram os fatores que, mais afetarem a redução de ferrita de zinco contida no EAFD. A máxima percentagem de redução da ZF foi 85%, para 100% CO, 1373K e 105 min, e 52%, para 50% CO, 1373K e 105 min. Por outro lado, atingiu o 100% para 100% CO, 1273K, em 80.75 min, 60%, para 50% CO a 1373K durante 105 min. no caso da redução do EAFD

Aug 17, 2017

By Osvaldo Guilherme Comineli

While the hot cracking of Cu-containing steels is a serious and widely known problem for the industry, the literature reports that copper only slightly impairs the hot-ductility measured in laboratory. A distinction is drawn between hot ductility and hot shortness and the respective cracking operating mechanism involved at the respective range of temperature. The representability of the laboratory assessment of hot cracking of Cu-containing steels by hot tensile tests compared with actual results in industrial practice is discussed. The effectiveness of the variable affecting in each cracking mechanism and respective temperature range, focused in improving the hot cracking assessment of Cu-steels and the relative importance of oxidation will also be discussed. It is concluded that the hot tensile test in argon might be a good simulation if properly interpreted and that the role of oxidation is secondary in causing hot shortness. A schematic diagram for the hot tensile test is proposed.

Oct 30, 2017

By John Anthony Vasquez

During the last years Riva Acciaio Verona has taken the decision to invest in the route of a fully automated meltshop. The aim is to reduce at the minimum the operator's intervention from the bucket preparation till the ladle transfer to the continuous casting bay. The foundation for achieving the goal is the introduction of innovative technological solutions (fully automated cranes for bucket charge in the EAF, robots for sampling, etc. The paper underlines how the different solutions are based on the best practices to improve operator's safety and describes the different steps of the project, the different solutions adopted and the results in terms of production, energy savings, cost reduction and improved safety. Details are presented for: scrap yard management and bucket preparation, EAFs centralized controls and related robots for auxiliary operations (sampling, EBT cleaning, scraper for slag door automation, complete mass & energy balance based on process control), LFs centralized controls and process integration.

Aug 16, 2017

By William Sergio Flores Roman

Los aceros para armaduras de hormigón tienen que exhibir una buena relación entre resistencia y tenacidad que se ve reflejado en la performance del producto en servicio al ser aplicado a esfuerzos exigidos. Acerbrag es una empresa que produce aceros para la industria de la construcción teniendo en su gama los aceros de medio carbono para la fabricación de barras conformadas de dureza natural para armaduras en estructuras de hormigón. El objetivo de este trabajo es encontrar criterios de ventanas de trabajos operacionales y de control para la manufactura de aceros con buenas propiedades mecánicas en términos de resistencia y tenacidad. Este paper muestra los resultados de los trabajos realizados en las diferentes áreas productivas para conseguir un producto final con mayor resistencia a altas exigencias en servicio, además, reporta diferentes aspectos del proceso de manufactura del producto que van desde el ajuste de la composición química del acero, incluyendo criterios de propiedades mecánicas objetivos, criterios de calidad interna mostrando la microestructura de la barra antes y después de los cambios y finalmente la calidad dimensional y superficial de la barra nervurada, este último potenciando la falla prematura del material. Todos estos cambios, se ven reflejados finalmente en la performance de la barra, sometida a los nuevos criterios de exigencia en los ensayos mecánicos.

Oct 30, 2017

By Jean-Philippe Houde

The Blast Furnace Campaign lifetime is highly depending on the wear progress of the hearth lining. This progress is monitored in general through single and double thermocouples at the cold side of the lining. This type of monitoring becomes ineffective as soon as heat resistance will be formed in the refractory lining. Paul Wurth’s monitoring system, consisting of MTP-Sensor and Heat Flux Probes, is able to identify such heat resistances to give a true hearth lining wear. Since last year Paul Wurth is also able to install safely those MTP-Sensor and Heat Flux Probes on running blast furnace without salamander tapping, thanks to a newly developed cooled core drilling device. Blast Furnaces that are equipped with Paul Wurth’s monitoring system have optimized their campaign lifetime as they received right information upon the true wear lining such as detection of heat flux transfer failure, detection and monitoring of brittle layer or detection of hot spot.

Aug 16, 2017

By Rogério Felício dos Santos

Nitriding of metallic materials using electric discharges generated during electric discharge machining (EDM) is a recently developed technique. The aim of this paper was to correlate mechanical properties of a nitrided layer produced in AISI 4140 steel by EDM nitriding with the type and amount of nitrides. A conventional die-sinking EDM equipment and electrolytic copper electrodes were used to generate the electric discharges. The electrolyte was a solution of urea in deionized water. Knoop microhardness profiles assessed the variation of hardness along the nitrided layer, whereas the elastic modulus of this layer was measured using nanoindentation tests. Optical microscopy and X-ray diffraction (XRD) were used to characterize the nitrided surface. The results showed the formation of a nitrided layer containing iron nitrides with average thickness of around 25 µm. The amount of nitrides reduced from the surface towards the centre and these results correlated well with microhardness profiles obtained.

Jul 31, 2018

By Francisco Morganti

This report gives in the first part the metallurgical basics for the production of AHSS grades in integrated steel plants starting at the melt shop and ending at the annealing lines of the cold mill. The corresponding process and plant technologies in each production step with its specifics and rules are explained. In the second part by way of example the practical requirements for TRIP 780 steel grade are highlighted like a recipe for process control in the steel plant, hot and cold rolling mill, annealing line and finally skin pass mill. Measuring of mechanical technological properties on samples shows that the specifications according to DIN EN 10268 are fulfilled.

Oct 30, 2017

By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Douglas Glenn Stalheim

The uniformity of the final cross sectional microstructure and subsequent final mechanical properties and shape of structural steels is dependent on the type or types of recrystallization behaviors that are created. There are three main recrystallization behaviors that are the foundation of the metallurgy created during production. Alloy design and subsequent processing design strategy drive how much of each recrystallization behavior is created through the cross section of the product. Carbon manganese steels create only one basic behavior while the addition of microalloys, in particular niobium, can add two additional behaviors. The behaviors are intertwined with each other and build upon each other. The three behaviors are Type I, static recrystallization, Type II, no-recrystallization, and Type III, metadynamic/dynamic recrystallization. How much of each behavior is generated through the cross section through the production influences the final transformed microstructure and corresponding mechanical properties and shape performance. This paper will discuss the three behaviors, how they are generated, how to identify which behavior is occurring through modeling or actual mill data. Actual examples from production will be discussed.

Aug 16, 2017

By Valeria Romina Stricker

Acerbrag es una empresa Argentina siderúrgica de 50 años de trayectoria, desde el año 2007 pertenece al grupo Votorantim de origen Brasilero. Se dedica a la elaboración de aceros largos para la construcción. La planta industrial cuenta con un proceso de acería integrado, horno eléctrico, horno cuchara y máquina de colada continua. La materia prima es 100% chatarra, característica que la diferencia del resto de las acerías del país. Debido a esto el enfoque principal de este proyecto es reducir el costo de fabricación mediante un “empobrecimiento” de la carga metálica a partir de la flexibilización de los límites de especificación. Esto implica un mayor control del desempeño de los procesos a fin de detectar posibles desvíos, para ello fue necesario implementar la utilización de herramientas estadísticas y gráficas para su monitoreo. La modificación en el mix de fabricación no muestra una alteración significativa en la composición química y propiedades mecánicas de los productos terminados, situación favorable para la continuidad del proyecto. Se observa además, de la reducción de costo esperada, una ventaja en la operación del patio de chatarra y el proceso de acería y en la utilización de chatarras con altos niveles de residuales tales como Cr – Ni.

Aug 16, 2017

By Gilmar Zacca Batista

The present work is a part of a comprehensive program that aims to evaluate the girth welding procedures for heavy wall API 5L X65 pipes produced for sour service applications. This article describes the results of toughness, strength and sour resistance of girth welds produced with different welding consumables. The methodology applied included girth welds production with GTAW process for root pass using ER70S-6 consumable and FCAW process for filling passes using E71T- 1CJ and E91T1-GM-H4 consumables. Mechanical tests of Charpy, CTOD, tensile, hardness and stress corrosion cracking were also performed. The E71T-1CJ resulted in a girth weld with tensile and yield strength around 7% lower than the pipe. However, according to the papers analyzed at this study, a value up to 10% of undermatching could be acceptable. The CTOD and Charpy tests showed good toughness and weld metal embrittlement was not observed. The hardness and the stress corrosion cracking tests demonstrated that the consumable ER70S-6 is suitable for sour service. All properties evaluated met the requirements specified by the onshore pipeline standards, showing that the consumables ER70S-6, E71T-1CJ and E91T1-GM-H4 are suitable for the welding of heavy wall X65 pipe with sour service and toughness requirements. If an overmatching is required, the E91T1-GMH4 shall be used to assure a strength overmatching and prevent plastic strain concentration at the weld metal. The results provided by this paper can be used for consumable selection and for welding procedure qualification of pipelines construction when heavy wall API 5L X65 are used for sour gas transportation.

Aug 16, 2017

By Edmar de Souza Silva, Antonio Augusto Gorni, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Controlled rolling followed by accelerated cooling, known worldwide as TMCP, aims to increase mechanical properties without toughness deterioration. The process principle is to promote the plate cooling with water jets along the range of the austenite transformation temperatures. The accelerated cooling process is only fully effective when controlled in an integrated manner, as it alone cannot ensure significant improvements in the final properties of steels. Plate surface quality depends on some parameters that must be controlled before the start of the plate accelerated cooling. Good flatness is essential to avoid irregular water accumulations during cooling. After the reheating process, the slab should have uniform temperature, uniform austenitic grain size and easily removable scale. The slab thermal and microstructural heterogeneities are inherited by the rolled plate and tend to increase further during the accelerated cooling. This results in flatness problems, high level of internal stresses and mechanical property variations. The descaling strategy is an extremely important factor and must be determined with great caution. It is important that scale thickness and distribution is uniform to ensure homogeneous cooling over the entire plate surface. Otherwise, there will be an uneven temperature distribution, which can cause serious problems of flatness, surface quality and mechanical properties.

Oct 1, 2019

By Dyego Monteiro de Souza

This study compares the wear resistance of specimens lubricated with biofluids or mineral oil. Tribological studies were performed by ball-cratering test. In these tests were used as lubricants epoxidized soybean oil, castor oil and mineral oil. The specimens used were untreated and nitrided AISI 4140, while a steel ball AISI 52100 was used as a counterbody. In order to analyze the results obtained, the worn volume was calculated and the characterization of the crater, after the test, was made using optical microscopy and SEM. Wettability was also measured for the different surface condition and lubricants. As expected both specimens showed a smaller volume worn when lubricated with mineral oil due to inherent properties of this type of lubricant. Among the vegetable oils studied, the castor oil showed a better performance in the lubrication of the specimens untreated while on the nitrided specimen have shown less wear when lubricated with epoxidized soybean oil, indicating a difference in the efficiency of oils, as lubricants, depending on the surface conditions of the mechanical components.

Jul 31, 2018

By Fernando Ruiz Díaz

En aplicaciones a elevadas temperaturas como por ejemplo en cámaras de combustión y toberas de vehículos aeroespaciales se requiere el uso de aleaciones que permitan una elevada extracción de calor y buenas propiedades mecánicas. En este trabajo se realiza un análisis comparativo de las aleaciones Cu-Cr-Zr y Cu-Ag-Zr. Las mismas fueron sometidas a ensayos de resistividad eléctrica entre 25ºC y 700ºC y de tracción a 150ºC, 450ºC y 700ºC. Los resultados de los ensayos de resistividad eléctrica fueron convertidos a conductividad térmica mediante la relación de Wiedemann- Franz. A través de este análisis se observa que la aleación con mejor conductividad térmica es la de Cu-Ag-Zr presentando además un cambio de fase que no es observado en la aleación Cu-Cr-Zr. Respecto al ensayo de tracción la aleación Cu-Cr-Zr presenta mayores valores de resistencia a la tracción y tensión de fluencia a las temperaturas estudiadas.

Aug 16, 2017

By Túlio Magno Fuzessy de Melo, Luciano Santos Marques, Vicente Tadeu Lopes Buono

The influence of the coiling temperature after hot strip rolling on the microstructure and on the tensile and hole expansion properties of a 800 MPa multiphase steel was investigated. For the temperatures between 150°C and 600°C the microstructure consisted of a ferritic matrix with a dispersion of fine martensite-austenite (MA) and regions of degenerated upper bainite. In all cases the ferrite presented a heterogeneous mixture of polygonal, quasi-polygonal and acicular grains. The yield and tensile strengths showed a tendency of decreasing with the increasing coiling temperature, probably because of the larger fraction of MA particles at lower temperatures and higher fraction of quasi-polygonal ferrite at higher temperatures. The elongation was not significantly affected by the variation of coiling temperature. The average hole expansion ratio showed a maximum of 80% for the material coiled at 400°C and fell below 50% only for the coiling temperature of 150°C, probably due to the larger hardness difference between the ferrite matrix and the MA particles.

Oct 1, 2019

By Satish V. Kailas

For product sustainability “closing the cycle” is the first requirement. If the materials used in making the product is not replenished at the rate at which it is being extracted, the cycle is open and the product would not be sustainable. This includes the materials used in generating the energy used to make the product, the transportation, use and disposal. If the materials used in a product, that includes lubricants, is one that cannot be replenished, it has to be recycled for the product to be sustainable. The other basic condition for sustainability is the eco-friendliness of the product. It is argued that the present lubricants do not fall in this category. Using the example of cutting oil emulsions we have shown that it is possible to meet the conditions of sustainability in terms of both the material extraction-replenishment cycle and eco-toxicity. Cutting oil emulsions made from coconut oil and natural additives are shown to have superior cutting properties and are completely eco-friendly. It is concluded that products made using these conditions are possible and is a necessity for man to lead a sustainable life. Closing the cycle, with respect to the energy used in the cycle will make the product completely eco-friendly.

Jul 31, 2018

By Gabriel Oliveira Glória

Due to growing concern about the ambient impacts, lignocellulosic fibers are been investigated to replace the synthetic ones in polymer composites The giant bamboo fiber, a relatively unknown lignocellulosic fiber with potential for composite reinforcement, still needs to characterize for possible engineer applications. However the giant bamboo fiber has low adhesion with the polymeric matrix. In order to understand the interaction that occurs between the bamboo fiber and the polymer matrix is necessary to evaluate its physical and chemical characteristics. Therefore, the present work analyzed the giant bamboo fiber by means of Fourier Transform Infrared (FTIR) spectroscopy. The spectrum revealed main absorption bands typical of giant bamboo fiber specific molecular interactions.

Aug 16, 2017