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By C. S. Barrett, D. F. Clifton

THE transformation that occurs in lithium and its solid solutions containing magnesium1,2 is similar in many respects to other diffusionless transformations of the martensitic type. This general similarity makes it desirable to investigate the transformation curves in detail. The current interest in the phenomenon of stabilization in martensitic transformations has created a need for a careful appraisal of possible stabilization effects in both cooling and heating transformations in lithium alloys. The effect of prior heat treatment on the temperature at which transformation begins and the effect of various temperature cycles in partially transformed alloys also merit attention. Limited data on some of these features were presented previously,' but the present studies have been made with improved apparatus, in which erratic fluctuations were smaller than in the earlier work, and include many independent determinations of certain critical observations. Material and Methods Geiger counter X-ray spectrometers were used: a Norelco instrument, original model, and a General Electric XRD-3. The low-temperature specimen holder has been described elsewhere." Specimens 10 mm in diam and 1.5 mm thick were held in firm contact with a copper block which was attached to the lower end of a stainless steel tube that extended up to a reservoir of liquid nitrogen. A heating coil on the tube permitted a controlled temperature gradient along the tube, so that desired temperatures and rates of heating and cooling could be obtained by controlling the heating current. The specimen was surrounded by an atmosphere of evaporated nitrogen in an insulated chamber having double cellophane windows. The temperature of the specimen was read by a thermocouple imbedded in it close to the irradiated area; the specimen could be held at constant temperature within 1°C for long periods. The body-centered cubic 200 reflection near 8 = 26" was used as the index of the amount of b.c.c. material present; occasional checks were made using the most suitable line of the low-temperature phase, the close-packed hexagonal 110 line near 8 = 29". Copper radiation was used throughout. A continuous record was made of the reflected intensities on a strip chart recorder, both when the peak intensity of a line was being followed and when the lines were being scanned at constant temperature. On the continuous recordings of peak intensity, periodic checks were made on the background intensity between the lines, and on the setting of the spectrometer for maximum intensity. The lithium-base solid solution containing 12.4 atomic pct Mg (33.3 wt pct) that had been used previously' was chosen, as it had a transformation range at relatively high temperatures, so as to permit wide temperature cycling within the range. Just prior to use a pellet was cut from the ingot,

Jan 1, 1951

By J. E. Breen, J. Weertman

The creep rate of polycrystalline tin was studied as a function of temperature and stress in constant stress experiments. The temperature was varied from room temperature to almost the melting point of tin. Activation energies were calculated from tests run at the same stress. It was found that on a log creep rate vs inverse temperature plot the experimental points did not fall on one straight line but on a line which changed its slope in the 90° to 160°C region. Two activation energies for the creep of tin can be calculated from the data: a value around 26,000 cal per mol at high temperatures and a value around 11,000 cal per mot at low temperatures. It is suggested that the discrepancies between the creep activation energies and those of self-diffusion can be accounted for if self-diffusion takes place predominately by Zener's ring mechanism rather than through vacancy or interstitial movement. SHERBY, Orr, and Dorn' and Dorn' have recently reviewed some of the data on high temperature creep of metals. -The data show that the activation energy of high temperature creep is approximately equal to the activation energy of self-diffusion. This same correlation has also been successfully made between the activation energy of grain boundary relaxation and that of self-diffusion.3,4 The metal tin does not fit into this simple picture. Its activation energies of self-diffusion differ appreciably from that of grain boundary relaxation and of creep. Fensham,5 from a precisely performed experiment, has determined that the activation energies of self-diffusion of tin are 10,500 and 5,900 cal per mol along the C and A axes, respectively. There are two energies because of the anisotropic nature of tin. Rotherham, Smith, and Greenough6 have shown that the grain boundary relaxation activation energy is 19,000 cal per mol (measurements made from room temperature to 100°C). Puttick and King7 found the same activation energy for grain boundary slip in bicrystals of tin (180° to 225°C region). Until recently, there was no high temperature large strain creep data on tin suitable for activation energy calculations. At rather small strains (up to 0.01), Tyte8 had made a series of measurements on tin from which activation energies can be calculated. In Fig. 1 are plotted some of his data on a log creep rate vs inverse temperature graph. It can be seen that Tyte's work indicates that at a relatively low temperature the activation energy is around 7,400 cal per mol but at higher temperatures the activation energy increases. Since Tyte measured the creep only for small strains, it is doubtful if a

Jan 1, 1956

By A Wanninayake, E Novello, I Gillani

A residue storage facility (RSF) was designed to cater for Davidson Creek Area and Robertson Range Area operations under the FerrAus Pilbara iron ore development project in the Pilbara Region, Western Australia. Annual ore production was about 15 million tonnes over a period of up to 15 years. The RSF was designed to handle a tailings production rate of 2.2 Mt/a over the project life with ability to be expanded at a later date. The composition of tailings was predominantly -45 ¦ material with some spiral reject material. The fraction of solids was expected to be between 40 per cent and 50 per cent solids by weight.The RSF was designed as an above ground storage facility, integrating with a mine waste dump planned close to the selected RSF site. This integration helped to increase the stability of the RSF embankment and to reduce the construction cost. The main source of construction material for the remaining part of the RSF embankment was selected to be mine waste. The RSF was designed to be constructed in stages by considering the availability of mine waste according to the mining schedule. The use of mine waste for construction of RSF embankments has several benefits over use of borrowed material. These include less construction costs and less disturbances to the environment, by minimising borrowed areas and waste dump footprints.CITATION:Wanninayake, A, Novello, E and Gillani, I, 2013. Effective use of mine waste in the design of a residue storage facility, Pilbara region, Western Australia, in Proceedings Iron Ore 2013 , pp 39-44 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 12, 2013

The paper highlights the conceptual developments in rock mechanics applied to quantify the effect of bolts in the stabilization of joints and yielding soft rocks. NOTATION Aa = stress change after excavation Eä EE, Eä = moduli of intact rock, single joint and jointed rock Eb = elastic modulus of the bolt k, = normal stiffness of joint Ab = cross section area of the bolt A, = area of influence per bolt ab = axial bolt stress e, = axial strain of the bolt eä e,, ej, = strains of intact rock, joint and jointed rock Ai = area of the joint ,r+ = shearing resistance of the bolt (at the joint) a = normal stress at the joint plane aäa3 = major and minor principal stresses c;, 4i; = cohesion and friction angle of the joint 0 = angle between the bolt and the joint a = inclination of the joint to the vertical axis P = bolt density parameter u, = convergence of unsupported tunnel section u, = convergence of bolted tunnel

Jan 1, 1992

By Donald R. Williamson

Statistical studies at Cyprus Pima Mine indicate that samples from 22 blastholes are necessary for determining average copper grades, within a desired range of precision, for mine-model blocks by arithmetic averaging. The average number of holes in such blocks is 14. Many considerations show that more holes will not be drilled for sampling. A way to determine block grades more reliably than by" arithmetic averaging was sought. Thus far arithmetic averaging has proven to be the best procedure for the particular operation characteristics despite the small number of samples. It naturally follows that expenditure of great effort in sampling blasthole cuttings is unwise.

Jan 1, 1977

By Harry C. Gatos, Frank J. Bachner, Mario D. Banus

The portion of the Nb-Sn phase diagram between 75 and 79 at. pct Nb at temperatures near the liquidus has been investigated by melting alloys of known composition and examining the microstmc-tzlres resulting when these melts were quenched. The Nb-Sn samples were contained in magnesia sleeves, and were mounted in a high-pressure apparatus. It was shown that Nb3Sn me1ts by a peri-tectic decomposition and that the composition of the compound Nb3Sn at the peritectic horizontal lies between 77 and 78 at. pct Nb. Analysis of the phases present in the samples was accomplished by anodic staining techniques and an electron-microbeam analyzer. DURING the past several years a great deal of work has been devoted to the Nb-Sn system, and the bulk of this work has been primarily concerned with the intermetallic phase Nb3Sn. However, the melting characteristics of Nb3Sn have not been investigated because of the difficulty in maintaining known compositions due to tin losses by vaporization, and the added difficulty of containing Nb-Sn alloys without sample-container reaction at the high temperatures involved. This paper reports on the development of a technique for containing Nb-Sn alloys under pressure high enough to prevent tin losses at temperatures in excess of the liquidus. Using this technique, melts of known composition were made and a phase diagram near the liquidus is proposed based on the microstructures resulting when these melts were quenched. EXPERIMENTAL The Nb-Sn alloys weighing 0.7 g each were prepared in the form of cylinders. Niobium powder, -200, +325 mesh, and tin shavings with a minute amount of tin powder for a binder were mixed in the desired proportions and cold-pressed at 50,000 psi in a 0.150-in. die. This cylinder was then enclosed as shown in Fig. 1, and the entire arrangement mounted in a 2.6-in. pyrophyllite tetrahedron.' The desired temperatures (-2500°C) presented several problems in high-pressure container materials. Boron nitride, the usual sample holder, was found to react with niobium to form the nitride. However, MgO cans and plugs machined from refractory rods did not melt nor react with the sample. Thick tantalum contact disks were used to carry the large currents (~450 amps) to the graphite heater, since tantalum did not melt and had enough strength to prevent extrusion of the sample. It was further observed that the graphite heater and tantalum disks could not be in direct contact with the pyrophyllite because it melts and decomposes at these temperatures to kyanite and coesite (SiO2),2 the former reacting with graphite and the latter with tantalum to form the silicide. The use of a MgO outer sleeve

Jan 1, 1965

By Tamal K. Ghosh

In this study, the QEMSCAN technology is used to acquire quantitative modal, textural, mineral association and liberation data on different products generated from with or without washing, fractionation by size and density using screens and heavy liquids/panning, which has provided significant information on the quality and beneficiability of four categories of low Grade iron ores from Jharkhand-Orissa region. The deposit of low Grade iron ore has been categorized into four categories viz. Grade-I with <45% Fe(t) a) containing shale rich type and b) BHJ rich type; Grade-II with 45-55% Fe(t) and Grade-III with >55% Fe(t) containing conventional flaky, hard, kanga, lateritic, shale and BHJ litho/ore types in varied proportions. Mineralogy is similar across all samples being hematite, martite, goethite, kaolinite and gibbsite. Banded Hematite Jasper has difficult liberation characteristics due to highly compact banded mode of silica mineral occurrence with hematite. In all categories, the grade dilution is by the presence of 1) ?Discrete gangue rich litho types? at lump size and 2) ?Within ore types?. The second type of grade dilution contains coating of gangue phases around the iron ore minerals and different degree of locking of gangue phases within iron ore minerals. Further characterization and beneficiation assessment details are discussed in this paper.

Sep 1, 2012

INTRODUCTION The International Finance Corporation (IFC) is affiliated with the International Bank for Reconstruction and Development (World Bank) but operates with a separate staff and funding. It supplements the activities of the Bank by providing, to private business, equity and loans without government guarantees in whatever form and combination most suited to the project. IFC frequently complements the Bank&apos;s activities by utilizing, for example, the Bank&apos;s public sector infrastructure activities to support IFC&apos;s private sector projects. In the case of local financial institutions especially, IFC collaborates with the Bank by providing technical and financial assistance. IFC is the world&apos;s largest multilateral organization which finances private sector business in developing countries. IFC&apos;s fundamental purpose is to promote the economic development of its developing member countries through the support of the private sector. Of the 124 member countries of IFC, more than 100 are developing countries. Since it began operations in 1956, IFC has been associated with more than 2,000 companies and financial institutions in supporting over 700 business ventures in more than 80 countries. The total capital costs of these projects exceeds $26,000 million. In the 1984 fiscal year, IFC approved 62 projects in 37 countries with a total project cost of $2,473 million. IFC will make investments only if sufficient capital cannot be obtained on reasonable terms from other sources. IFC often serves as the catalyst for a project by encouraging other investors--from inside and outside the host country--to make their own equity investments along with the local sponsor for a particular project. IFC&apos;S SPECIAL ROLE The significance of IFC&apos;s role extends beyond just its financing and technical assistance: IFC&apos;s capability to raise investor confidence in a project and to help all the participants to arrive at mutually satisfactory investment arrangements is its distinctive character. Direct Investments IFC invests in all types of projects both large and small. Heavy industrial ventures not only supply essential materials and equipment for other domestic enterprises, but also earn foreign exchange through exports. In recent years, increased emphasis has been placed on agriculture and agribusiness products, aquaculture, food and food processing, and other renewable and nonrenewable resources such as metals and energy. [ ] An overall objective of IFC is to assist entrepreneurs and others in the private sector raise the needed capital for business ventures. IFC does not compete with, nor seek to replace private initiative and capital. Rather, IFC helps to raise funds in order to undertake projects that would otherwise be held back by the lack of adequate funding. IFC can do this in several ways: IFC can invest in equity and make loans for its own account. But beyond that, IFC can reach out into the international capital markets in search of additional capital. Because of IFC&apos;s 25 years experience and record, outside investors who might otherwise be

Jan 1, 1985

By H. Herbert Hughes

Soapstone commonly is associated with talc , and reports on either commodity usually contain a discussion of the other . From a geological or mineralogical standpoint the combination is justifiable , for soapstone essentially is impure talc . Commercially , however , the relation between them is remote . About 95 per cent of all talc sold in the United States is in ground form, whereas practically all soapstone is sold as furnace blocks or as fabricated structural slabs for many and diverse applications .

Feb 1, 1932

By Giulia M. B., Ferruccio Cribari, Alessandro Bertero, Eliano Romani, Roberto Sorge, Francesca Casini

"The use of Artificial Ground Freezing (AGF) to form earth support and seepage control barrier systems has had applications worldwide. These cover a variety of construction problems, including the formation of frozen earth walls to support deep excavations, structural underpinning for foundation improvement, and temporary control of ground water in construction processes. An application of AGF during construction of Line C of Rome underground is described in detail.The new line “C” of San Giovanni metro station was constructed adjacent to the existing line “A” of San Giovanni station; the new metro line “C” is deeper than line “A” and runs below the existing station. The underpass project envisages an Artificial Ground Freezing in order to create a structural and waterproof temporary cut-off suitable to the two new tunnels excavation, while keeping trains running in the safest possible condition. The excavation of tunnels under the water table, with a hydraulic head of over 10 m in not homogeneous soils having different mechanical properties and permeability and below existing sensitive structures, involves special ground freezing sequences and methods, as well as peculiar drilling systems and operations, such as TDDT (Trevi Directional Drilling Technology).Artifical Ground Freezing IntroductionNatural freezing occurs seasonally in many areas of the globe and can affect negatively the engineering performance of geotechnical structures; on the other hand, man-made freezing is a controllable process that can be used by civil engineers to stabilise temporarily the ground in order to support and/or exclude groundwater from an excavation until the final retaining and lining structures are constructed. Freezing and thawing of the pore fluid within soils involve complex thermal, hydraulic and mechanical processes that have significant mutual interactions. For example, phase changes of the pore fluid caused by temperature variations can modify the pore water pressure in the soil, which, in turn, can induce mechanical deformation. At the same time, any changes in the hydraulic and mechanical conditions affect the thermal processes by advection and changes of ice and water contents.An application of AGF which will be presented in the paper, refers to the construction works of Line C of Rome underground. In this case AGF was carried out to provide temporary support during excavation of the two Line C running tunnels directly underneath the existing S. Giovanni station of Line A, in the safest possible condition. In order to keep the trains of Line A operational during excavation, a temporary structure was installed and a real-time monitoring system was conceived in order to control the temperatures of the soil during freezing and the response of the structures of the existing station."

Jan 1, 2016

By L. S. Zhou

HermesTM metal magnetic liner (MML) has been invented and manufactured by China Metallurgy and Mining General Co. (CMMC). This paper describes its mechanism, structure, magnetic field distribution, application, economic benefit and safety performance. The 10 years? service life in Benxi Steel?s Waitoushan Mine, along with 6 years? technological analysis on its application in 5500mm×8800mm (diameter × length) ball mill in Anshan Steel?s Diaojuntai mineral processing plant, has proved its advantages such as super reliability, long service life, light weight, thin thickness, low noise and short payback period. It has also demonstrated its positive effects on the grinding process such as high productivity, energy-effective performance and low consumption of grinding media. It reduces labour intensity and improves working conditions, due to its easy installation, free maintenance and the fact that it doesn?t require fastening bolts or cause slurry leakage. It is de-signed scientifically in accordance with the varieties of processing lines, mill specification, ore type and grinding media, and has been applied in different grinding processes for magnetite, hematite, gold ores, nonferrous ores and other materials. HermesTM MML has three types of products: General, Composite and Heavy-duty. They are designed to meet the requirements from customers in China and abroad. So far, more than 400 sets of MML have been applied in ball mills with diameter rang-ing from 1500mm to 5500mm. It has become highly popular in American market recently due to its safe and effective performance.

Jan 1, 2014

By Elaine T. Cullen

Underground mining, like many high-risk industries, is facing a crisis in the near future. This industry has traditionally relied on a master-apprentice relationship to train new workers, but experienced miners are retiring in large numbers, leaving few "masters" to properly train their replacements. With a recent resurgence in mining, many new miners are entering the workforce each day. The rise in the number of inexperienced workers has implications for worker safety in an industry in which one mistake can blow up the entire workplace. The explosion in the Darby Mine in May 2006 that killed five miners illustrates what can happen in hazardous environments such as underground mines. The Health Communications Team at the National Institute for Occupational Safety and Health Spokane Research Laboratory was asked to address this problem by developing new training and safety awareness materials to promote safe flame cutting and welding practices. This article describes how occupational ethnographic techniques provided insights needed for "new product development." The result of this work was a national initiative to raise awareness and to protect underground coal miners from the dangers of flame cutting and welding in an environment filled with solid fuel and methane (natural gas). Although this project was initially designed for the mining industry, the approach and lessons learned are applicable to any high-risk industry and should be of interest to other social marketing or occupational safety and health professionals.

Jan 1, 2009

By Dale C. Matthews

Pressure oxidation of refractory gold ores is becoming more popular in our environmentally sensitive society. This paper will discuss some specific process problems and solutions involved with starting up and operating an autoclave circuit.

Jan 1, 1991

By Priscila Alves da Silva Machado

A busca por pesquisas que provem soluções e inovações que utilizam parte de tais resíduos vem ganhando grande destaque. O poli (tereftalato de etileno) é um polímero termoplástico, e é o material base para produção de embalagens plásticas que são comercializadas mundialmente. Sabe-se que é de grande volume os resíduos sólidos provenientes de tais embalagens plásticas. Com o objetivo de solucionar um problema ambiental e verificar a viabilidade técnica, foram fabricados em proporções de 0%, 5%, 10% e 15% m/m, materiais compósitos de base cimentícias reforçados com fibras de poli (tereftalato de etileno) provenientes de resíduos de garrafas plásticas (PET), posteriormente amostras passaram por caracterizações mecânicas. Destacou-se um aumento das resistências a compressão axial e diametral do material produzido com fabricação de adição de poli(tereftalato de etileno). Tais resultados referente a resistência foram positivos, propondo assim a utilização do polímero na composição de novos compósitos.

Oct 30, 2017

By Johannes Labenski, Christian Moormann, Johannes Aschrafi

"Open steel pipe piles are used for various applications in costal engineering, port structures and increasingly important for offshore structures. During the installation of open steel pipe piles the formation of a plug has an influence on the installation process of the pile and also on the final bearing capacity. The formation of the plug depends on different factors, e.g. the pile diameter and the installation method. This paper starts with a structured overview about analytical methods (API, EAP-EAU, UWA-05, HKU-12, Modified API) to calculate the axial bearing capacity of open steel pipe piles. The numerical simulation of the installation process of open steel pipe piles has to fulfill high demands, i.e. to accurately represent the penetration of the pile inside the soil, the formation of the plug and also the stresses and strains during the installation. A numerical back analysis of a comprehensive field test, using the Coupled Eulerian-Lagrangian (CEL) method and a hypoplastic constitutive model for sand, reveals the stresses and displacements of the soil and of the piles. The analysis provides a comprehensive understanding of soilpile interaction.INTRODRUCTIONThe particular difficulty in the numerical simulation of plug formation, is that the effect of plugging inside open ended steel pipe piles has not been fully investigated. In scientific papers different approaches are documented to explain this phenomenon. Some are based on in-situ tests and others are based on numerical simulations. One of the challenges is to determine the end bearing capacity and shaft friction of the steel pipe pile. Different approaches have been developed over the years to determine them e.g. from Randolph et. al. (1991, 1994) and Paik et. al. (2003). Recent approaches are the ICP-05 Method (Jardine 2005), the UWA-05 Method (Lehane 2005) and the HKU-12 Method (Yu & Yang 2012a). A comparison of some methods can be found in Schneider et al. (2010). A plug inside an open steel pipe pile can be visualized as a spatial bracing of soil between the inner surfaces of the pile, cf. Lüking (2010).. However according to Lüking & Kempfert (2012) this bracing only exists for the height in the end of the pile equal to twice its diameter.To identify a plug inside a pile, there are different measurable parameters. One parameter is the development of stresses around the pile during and after its installation. Henke (2013) measured the inand outside horizontal stresses at the pile tip during the installation. The results showed higher stresses on the inside compared to the outside. To validate his measurements he performed a numerical back-analysis of the measured installation process and got matching results."

Jan 1, 2017

By Paulo Ricardo Bastos de Queiroz

Após estudo realizado, verificou-se que a CSP - Companhia Siderúrgica do Pecém, possuía alta vulnerabilidade às oscilações de frequência, sejam elas oriundas de falhas nas unidades geradoras ou problemas nas linhas de transmissão que compõem o SIN (Sistema Interligado Nacional), onde tais perturbações poderiam provocar desde a parada total da planta a danos irreversíveis em equipamentos como motores síncronos. Com base nesse estudo, foi implantado um sistema automatizado e de rápida resposta capaz de diminuir ou eliminar todos os efeitos provocados por tais distúrbios, atuando de forma dinâmica e coordenada com o cenário energético ao qual a planta siderúrgica encontra-se no momento do evento. Dentre os ganhos apontados em estudo, destaca-se a confiabilidade de se ter um sistema de distribuição de energia em uma usina siderúrgica capaz de assegurar a continuidade do processo ou em piores casos proporcionar uma parada emergencial com total segurança.

Oct 30, 2017

By Luciana Vilarinho Ramos de Carvalho

O objetivo deste estudo foi desenvolver um modelo matemático capaz de prever as propriedades mecânicas de uma barra redonda laminada a quente em aço ao carbono, em termos de limite de escoamento e limite de resistência, considerando equações consagradas na literatura e dados industriais de processo. Foram utilizados os parâmetros de processo da laminação, tais como temperatura, deformação, taxa de deformação e tempo entre passes, e a composição química do aço SAE 1020. Os resultados calculados pelo modelo apresentaram boa concordância com os resultados medidos nas amostras, com diferença percentual de 3,34% para limite de escoamento e 2,14% para limite de resistência, além de mostrar-se adequado para previsão da evolução microestrutural, considerando as equações de recristalização estática e dinâmica. A utilização deste modelo pode levar à redução de custos com ensaios de tração e atender à demanda crescente dos clientes por estas informações nos certificados de qualidade.

Oct 30, 2017

Abrahamson. Guy C., (S&apos;43) Univ. of California, Berkeley. Calif. &apos; Abrego, Alfredo, (S&apos;43) Texas College of Mines Metallurgy, El Paso, Texas. Adamec, Lew, (S&apos;42) c/o Braden Copper Co., Ran¬cagua, Chile. Adams, Charles E., (S&apos;42) Box 1527, Stockton, Calif. Adams, John W? (S&apos;42) Asst. Petr. Engr., Vander¬ bilt Dist., Magnolia Pets. Co., Edna. Texas. Adams, Karl S., (S&apos;43) Univ. of New Ha mpshire, Durham; N. H. Adamson, Charles R., (S&apos;41) Univ. of Utah, Salt Lake City, Utah. Aguilar, Ruperto G., (S&apos;43) Texas College of Mines, El Paso,. Texas. Almone, Francis M., (S&apos;41) Univ. of Toronto, Toronto, Ont., Canada. Ainge, Ronald Farra, (S&apos;43) Otago University, Dunedin, New Zealand. Akarun, Cevdet A., (S&apos;44) Pennsylvania State College, State College. Pa.

Jan 1, 1944

By Fabiano Rodrigues Soares

O Mandril é um dos mais importantes componentes da laminação de tiras, pois trabalha diretamente na qualidade do produto, tanto para o cliente interno quanto para o cliente externo. Para atender a demanda do mercado de Siderurgia e Alumínio para a área de laminação a quente, a frio e linhas de processo, temos a necessidade de entender os conceitos existentes e desenvolver novas formas para aumentar a performance do equipamento, resultando em menores gastos com manutenção e um menor número de tempo parado da linha, culminando em lucro para a empresa. Será apresentado neste trabalho tecnologia em reengenharia e projeto de Mandris, aplicando know how adquirido dentro de vários anos de experiência e ainda contando com o apoio tecnológico de nossos colegas da Alemanha com soluções de excelente qualidade para o cliente. Estas soluções podem ser através de novos materiais, novos revestimentos e novos conceitos de trabalho do equipamento.

Oct 30, 2017

By H. C. E. Regidor, M. G. Mena, H. D. Mendoza

Cyanidation leaching has always been the most widely used method of extraction of gold in the world. Its low cost and high selectivity has made it the prevalent choice for mining companies, and even for the small scale miners. The use of cyanidation in small scale mining has been an issue for the longest time, mainly due to the operation’s lack of safety measures, health care or environmental protection regulations. In pursuit of more environmentally friendly methods of extraction of gold, several alternative extraction processes have been explored, one of which is chlorination. The chlorination process is advantageous when recovering refractory gold locked in sulfides, as it simultaneously oxidizes the surrounding sulfides as well as dissolve any gold exposed to the lixiviant. This research was conducted to study and develop a safer alternative way of extraction of gold from small scale mining operations, without compromising the recovery of gold. In this study, a variation of the chlorination process has been employed for a refractory flotation concentrate wherein the majority of the gold is locked in sulfides. Hypochlorite-bearing reagents were used as the leaching reagents, and the method developed was a 2-stage leaching process in differing pH conditions. The solution pH and Eh was monitored all throughout the runs, and aliquot samples were taken at time intervals for analysis. SEM-EDS imaging was used to determine the mode of oxidation of the chlorination process, and the image obtained showed that the oxidized layer followed the shape of the particle, suggesting a diffusion controlled process. XRD analysis of the sample before and halfway through leaching further confirmed the oxidation of the sulfides. The amount of gold dissolved in the aqueous solution and in the solid residue were used as the basis for the determination of the recovery of gold. An average gold recovery of up to 84.38% was obtained using the developed method in just 7 hours of leaching. This method was then employed for a pilot-plant scale test and a gold recovery of 79.2% was obtained.

Jan 1, 2018