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By P. A. Beck, A. H. Lutts

IN the classical picture of recrystallization the growth of strain-free grains at the expense of a strained and work hardened matrix is responsible for the softening of cold worked metals on annealing. It has been commonly assumed that the release of the stored energy of cold work, softening, and re-orientation take place simultaneously, as the high angle boundaries of the new recrystallized grains sweep over the cold worked matrix. However, recent evidence indicates',' that, at least in some cases, considerable or even complete soften- ing may take place essentially without reorientation (i.e., without the migration of ordinary high angle grain boundaries, or "recrystallization'') and the release of most of the stored energy of cold work may precede softening. These cases suggest that the property changes, taking place during the annealing of cold worked metals, may be associated with various distinct processes. The study of such situations is of considerable interest, since quantitative data are still scarce. In the present work, isothermal softening curves were determined for a heavily rolled aluminum single crystal, under such conditions that no "recrystallization" occurred until after complete softening. The hardness data were correlated with X-ray diffraction pinhole patterns in order to detect any reorientation that may occur and with measure-

Jan 1, 1955

By Stuart McHugh, Douglas Keough

INTRODUCTION AND BACKGROUND Because of the potential for large reserves from increased production in the eastern Devonian shales, the Department of Energy (DOE), Morgantown Energy Technology Center (METC) selected these materials for the application and evaluation of existing and novel well stimulation techniques. One technique selected for further study was pulse tailoring, or tailored pulse loading, i.e., shaping the input borehole pressure history to produce a specific fracture pattern and to increase communication with the reservoir. The complexity and expense of in-situ mineback experiments prohibits direct evaluation of pulse tailoring in various geologic formations. An alternative approach used by SRI International consisted of evaluating fracture enhancement by computational simulations with supporting laboratory experiments and using data from field tests by other agencies to validate the computational model (McHugh and Keough, 1980). Laboratory experiments were conducted on core samples to determine fracture phenomenology and parameters and to verify material properties. The fracture parameters were obtained from posttest measurements of fracture distributions and correlation with stresses calculated by a wave propagation code. Model development was guided by these experiments and similar experiments in various materials performed by other agencies. The validity of the modeling, parameters, and scaling was evaluated by comparing fracture patterns from field tests with calculational simulations.

Jan 1, 1982

By Harvey S. Chase

During the recent great depression in iron, little has been done in the magnetic separation of iron-ores; and previous to the present decade the art was in its infancy, so that there were few, if any, successful separators on the market, and but scanty practical data could be obtained as to the industry itself. Moreover, the recent development of the great Mesabi Bessemer beds, coincident with the intense depression in business, has discouraged active attempts to solve the problems presented in the crushing and separation of the refractory magnetites of the South. Experiments have been carried on, however, upon a practical scale in separating these ores magnetically, at the well-known Cranberry mines, in Mitchell county, N. C., with results which are encouraging. The magnetites of the Blue Ridge, in the South, have been known, and the soft ores of the region have been used in Catalan forges, since very early times. The original settlements in East Tennessee were made along the Watauga river by Daniel Boone, William Bean, John Sevier, and other stalwart pioneers; and this valley lies parallel with the " Cranberry " lead, which is undoubtedly the most celebrated and the most extensive deposit of workable magnetic ore in the Southern States. This lead I have personally traced along the outcrop, be-

Jan 1, 1896

By I. Iwasaki

The steel industry is facing an unprecedented challenge. I would like to point out the role that flotation technology could play in meeting this challenge by providing high quality raw materials to the steel industry. Of all the technology available to a blast furnace operator, raw material preparation is by far the most important. Raw material preparation has been a key to the success of the Japanese steel industry. The foremost proponent of better raw material preparation was Professor Joseph at Minnesota. He gave a Howe memorial lecture to the AIME audience in the early 1950s, prepared from the lecture notes that he gave in his classes. At about that time he was invited to Japan. It is ironic that the Japanese steel industry listened and made it a success. In order for our steel industry to be competitive, first we must supply high quality and uniform quality raw materials to improve the efficiencies of our blast furnaces. Where does flotation fit in to the iron ore industry then? First, as a primary means for concentrating for oxidized iron ores. Second, to touch up magnetite concentrates for the removal of the last few percent of silica. And third, in the preparation of super-concentrates for direct reduction.

Jan 1, 1984

Assaying, mineralogy, and geology appear in ancient records as early as mathematics, physics, and chemistry. Agricola was the first author to unify the earth sciences, the mineral extractive industries and the mineral processing industries. His text, De Re Metallica, published in Latin in 1556, is recognized as the first technical literature. In 1702 mining instruction was started at Freiberg, Germany. The purpose of this school was to train skilled workers, a program corresponding to present-day, on-job, vocational-technical, upgrading extension training. Formal instruction in mining engineering began at Schemnitz, Hungary, in 1763, at Freiberg, Germany, in 1766, and at St. Petersburg, Russia, in 1773. It is interesting to note that these three schools initiated instruction in mining engineering before formal instruction in civil engineering began at Paris, France, in 1775. Early mining engineering, 1763-1900, was expected to cover all eventualities in the mineral industries. Optional curricula were offered early in the 20th Century but did not reach into all branches until after World War I. Specialization crystallized during World War II under three organic units: (1) Earth Sciences; (2) Mineral Engineering; (3) Mineral Technology, the three together constituting the mineral arts and sciences of the modern world (Fig. 10).

Jan 1, 1950

Abel, Charles Edwin, Student, Univ. of California Los Angeles, Cal. '31 Adams, Horace M.5148 Benton Ave., Downers Grove, Ill. '31 Ahlskog, Harold A., Student, Washington State College Pullman, Wash. '30 Aldridge, John, Student, New Mexico School of Mines Sbcorro,, N. M. '30 Allen, Hugo K., The Univ. of Texas 104 W. 33rd St., Austin, Tex. '31 Ames, Marshall B., Student, Washington State College Pullman, Wash. '31 Ancell, Virgil F., Student,. Missouri School of Mines Rolla, Mo. '30 Anderson, Norman John, Student, South Dakota School of Mines Rapid City, S. D. '32 Annett, Norman T., Student, Mackay School of Mines, Univ. of Nevad Reno, Nev. '32 Apablasa, Salvador C., Student, Univ. of California Los Angeles, Cal. '31 Armstrong, James Arthur, Jr., Student, Michigan College of Min. & Tech., Houghton, Mich. '31 Armstrong, John R. Box 274, Neosho, Mo. '31 Armstrong, Robert H., Student, Lafayette College Easton, Pa. '31 Armstrong, Thomas E., Student, Univ. of California Los Angeles, Cal. '31 Arnot,. Paul H 2617 Haste St., Berkeley, Cal. '31 Ashby: Harve I., Willow Creek Mines Wasilla, Alaska. '31 Aud, Robert A., Student, Lafayette College Easton, Pa. '30 Augenthaler, Robert L., Student, New Mexico School of Mines Socorro, N. M. '32 Augustine, Grant, Jr., Instrument man, Min. Dept., Fairbanks Exploration Co., Fairbanks, Alaska. '31

Jan 1, 1932

By Frederick Forscher

Frederick Forscher (Nuclear Materials and Equipment Gorp.)—It is gratifying to see another series of experimental results that essentially reconfirms our reported observations of "Strain-Induced Hydrogen Embrittlement in Zirconium" (F. Forscher: AIME Trans., 1956, vol. 206, p. 536, noted as Ref. 3 of paper). However, several important considerations may have been overlooked, or—at least—have not been specifically pointed out. It is the purpose of this discussion to present some of these considerations. The statement is made that "the equilibrium concentration of hydrogen in solution at 20°C in zirconium is approximately 10 ppm; i.e., no zirconium hydride precipitates are formed at or below this hydrogen content." This is perhaps the case in the unstressed condition. In the presence of triaxial (plastic) strain however, even as little as 1.4 ppm H2 (Forscher's Figs. 6 and 11) will cause porosity near fracture in 20°C tests. The necked-down region that develops during a tensile test provides the triaxiality necessary for these pores to open. Both Beevers' and Forscher's micrographs show that porosity is concentrated in the necked region. So-called "pure zirconium" containing about 10 ppm H2 also shows pronounced porosity near fracture (Beevers' Fig. 3). Since it is generally agreed that such porosity is

Jan 1, 1965

By Louis D. Huntoon

The Hammond Mining and Metallurgical Laboratory is the gift of Prof. John Hays Hammond to the Sheffield Scientific School of Yale University. Professor Hammond was graduated from this school in the class of 1876, and has always shown great Merest in its welfare and progress. In 1903, he offered to build and equip for it a mining and metallurgical laboratory. This offer was gratefully accepted by the trustees; and in October of the same year the architect, W. Gedney Beatty, and I were employed to draw up plans for the building, which is the largest of its kind in this country. The Treasurer's report shows the total gift of Professor Hammond, including land, building, and equipment, to have been $128,741.53. This does not include $5,000 given by Professor Hammond to defray incidental expenses. The detailed cost of the machinery and installation, included in the above sum, is as follows: Macbinery,.......$9,846.00 Pipe and fittings,......925.05 Hangers, shafting, pulleys, belts, etc.,.. Steel-work, tanks, launders, etc.,...272.19 Screens for sizing ore,.....411.37 Lumber,.......1,896.36 General Supplies : Hardware,......$135.96 Tools,.......263.66 Paints,.......204.63 Electric and incidental,.... 439.57 ----------1,043.82 Machine-shop material, . 259.44 Labor,.. 722.29 ----------981.73

Jan 1, 1910

One-half fare return rate again available to members of the Institute and dependent members of their families. DON'T FORGET YOUR RAILROAD CERTIFICATE Over 300 members of the A. I. M. E. and dependent mem-bers of their families attending the last annual meeting se-cured return railroad tickets at half price by means of the railroad certificate, thereby saving several thousand dollars. DIRECTIONS 1. Be sure to obtain your railroad certificate when pur-chasing your railroad tickets for the meeting or you will lose money. 2. Purchase your tickets at regular one-way adult tariff fare between the dates specified for your territory in the accom-panying table. 3. Present your certificate for valida-tion at Institute headquarters in New York immediately after registration. Certificates will be validated on Feb. 21 and 22 between 9 a. m. and 5.30 p. in. 4. You must use your return half-rate tickets not later than Feb. 27. 5. Use the same route for both going and return trip. PLEASE REMEMBER THIS 1. Unless-250 certificates are validated at headquarters it will be impossible for anyone to secure the reduced rate. 2. Unless you secure a certificate you cannot take advantage. of the half-rate return fare, even if the necessary 250 certificates are validated.

Jan 2, 1928

On Feb. 16, 1948, the Board of Directors of AIME authorized the publishing of "Technical Notes" in METALS TECHNOLOGY. The purpose is to provide prompt publication of very shod items of the following general types: I. Results of short investigations which do not warrant a paper. 2. The conclusions of extensive investigations of insufficient general interest to justify a regular paper. 3. Conclusions arising in the course of an investigation, which, because of interest to others in the field, the author wishes to present prior to completion of the investigation. 4. Pertinent factual comment (not mere argument) on the subject matter of previous ''Notes." Such Notes will be subject to the approval of the Auxiliary and AIME Publications Committees, but can be handled more promptly than regular papers because they need not be referred to readers. 'The recommended maximum length is 500 words; notes in excess of 1,000 words will not be considered for this type of publication. A graph or photograph may be included as part of the note when particularly illustrative. As with regular papers, contributions to the new section should be submitted to the Secretary of the AIME. Please furnish two copies each complete with illustrations.

Jan 1, 1948

By Frederick J. Rich

INTRODUCTION Coal characterization involves a variety of analyses which are designed to yield as much information as possible about the properties of coal. The types of analyses which are now regarded as necessary for any truly quantitative assessment of coal include the following: 1. proximate analysis 2. ultimate analysis 3. petrographic analysis The two traditional forms of analyses are the proximate and ultimate types. A proximate determination reveals the amount of moisture, volatile matter, fixed carbon, and ash which are present in the coal. Nowadays, a sulfur determination is usually included in the proximate analysis. The ultimate analysis, in contrast, includes a major alkaline oxide determination, which tells how much sodium, calcium, and potassium are found in a sample. Sulfur forms, i.e. sulfide and sulfate vs organic sulfur, are also identified as well as carbon, hydrogen, oxygen, nitrogen, and trace element concentrations. Proximate and ultimate analyses have been used for many years. The petrographic analysis, one which identifies and quantifies organic microcomponents of coal, is a comparatively new technique of coal characterization. Petrography adds great detail to a coal analysis and, to be sure, is a necessary component of any complete analysis. Coal is not at all uniform in its composition. Material from different mines within one coal-producing region will display varia-

Jan 1, 1983

By P. Martignan

UNTIL quite recently, Alsace was the only district in France where petroleum could be found in somewhat industrial quantities. The Pechelbronn fields produce, however, only about 80,000 tons a year, which represent approximately one-eighth of the domestic consumption. Much research work has been done in Alsace to find the prolongation of the Pechelbronn fields, but instead of oil the drillings revealed the existence of large deposits of potash. This can, be easily explained when one remembers that the Pechelbronn oil is of the Oligocene period, and, that in the Alsatian stratification the Oligocene lies immediately on the Keuper, i. e., on the strata that originate from a period during which the largest salt and potash deposits were constituted. Before the war, and mostly at the end of the last century, some wells were drilled in various districts of France where some analogies could be found with the Alsatian geology, the borings being mainly made in the Triassic and Tertiary beds. They led to negative results. After the war, the growing importance of oil urged the necessity of resuming the explorations. But it is our belief. that this was greatly facilitated by the enacting of new legislation, which is embodied in the Mine Act of May 16, 1922.

Jan 3, 1925

By F. R. Hensel

ACCORDING to statements by Guertler,1 Smith and Hamilton were the first to study the copper-titanium alloys, but owing to the presence of large amounts of impurities their data are inconclusive. M. A. Hunter and I. W. Bacon later investigated the electrical conductivity and the temperature coefficients at room temperature. The present writers reported their results2 in November, 1930. Recently Droll published data on copper-titanium alloys3 which agree closely with those obtained by the authors. MATERIAL TESTED The titanium used was in the form of square sintered rods, the analysis of which runs as follows: titanium, 95.4 per cent; silicon, 0.7; iron,1.8; aluminum, 1.4; copper, 0.1; manganese, 0.05. . The ingots were prepared in a high-frequency induction furnace in air atmosphere. Their analyses are given in Table 1. Up to 5 percent titanium the alloys could be forged. Above that amount they were red short and broke up easily. Owing to their rapid absorption of nitrogen and oxygen from the air, the alloys with the higher amounts of titanium tend to form surface films which greatly increase the casting difficulties, especially when small masses of metal are handled. It was, however, possible to prepare sound ingots up to 25 per cent titanium.

Jan 1, 1931

By R. W. Rausch

BELT-CONVEYOR 'history in this country dates back to the end of the eighteenth century. Up to 1896 they were crude in design and application. The second era, dating from 1896 to about 1920, saw special study given to belt construction and idler design. The latter part of this era saw the beginning of the present-day antifriction idler. The third era followed World War I, when industry began to expand rapidly. Mines and quarries, steel mills, and power-generating plants became larger and greater quantities of ore, stone, and coal were being handled. It became vital that belts handle larger capacities, that they be longer, and that they be dependable for 24 hours per day. In this third era a radical change in belt conveyor design and application occurred. The design has became more scientific. Studies have been made to find out what factors influenced the power required for a belt conveyor and it was found that the sag of the belt between idlers and the flattening of the load between idlers had considerable effect on power requirements. So definite initial tension was put into the belt at the loading end and idler spacing was reduced at the foot end to limit this sag. Belt manufacturers made tougher and stronger belts.

Jan 1, 1947

By G. F. Tagg

EARTH-REISTIVITY measurements are often of service in obtaining information regarding geological formations, particularly when applied to structural problems. In such problems the masses of the various bodies are large, and have a corresponding effect on the average resistivity of the soil. Much work has been done using such measurements, but in general the method of interpretation employed is empirical. Since certain simple cases can be investigated mathematically, it appears to be quite sound to endeavor to apply the mathematical solutions to the practical results, in order to deduce from the latter such unknown quantities as depth. This paper deals with such a method of interpretation for the simple case of a single horizontal stratum. SURFACE Of EARTH In the method described by FIG. 1.-WENNER'S METHOD OT MEASURING Wenner1 for measuring earth resis- EARTH RESISTIVITY. tivity, four stake electrodes are driven into the earth in a straight line as shown in Fig. 1. A current I amperes is passed between the two outer stakes and the potential difference . V volts between the two inner stakes is measured. Then if a is the electrode separation, the specific resistance of the soil, which is assumed to be homogeneous, is given by the formula

Jan 1, 1932

I. PRESIDING OFFICERS. At all Business meetings of the Institute the President, or, in his absence, the Vice-President, or, in the absence of both of them, any other member of the Board of Directors to be chosen by the meeting, shall preside. At all other meetings of the Institute the President of the Council or, in his absence, one of the Vice-Presidents, if present, shall preside II. ORDER OF BUSINESS. At each Business meeting of the Institute the order of business shall be as follows 1. Reading of minutes of preceding meeting. 2 Report of the President. 3. Report of the Treasurer. 4. Report of the Secretary. 5. Election of Directors. 6. Reports of Standing Committees. 7. Reports of Special Committees. 8. Special Orders 9. Miscellaneous business. This order of business may be changed by a vote of a majority of the Members and Associates present in person or by proxy. The usual parliamentary rules shall govern all meetings of the Institute except in cases otherwise provided by the Constitution or the By-Laws. At all sessions of the Institute other than business meetings, the order of proceedings and the time of adjournment, shall rest in the discretion of the presiding officer

Jan 1, 1923

I. PRESIDING OFFICERS. At all Business meetings of the Institute the President, or, in his absence, the Vice-President, or, in the absence of both of them, any other member of the Board of Directors to be chosen by the meeting, shall preside. At all other meetings of the Institute the President of the Council or, in his absence, one of the Vice-Presidents, if present, shall preside II. ORDER OF BUSINESS. At each Business meeting of the Institute the order of business shall be as follows 1. Reading of minutes of preceding meeting. 2 Report of the President. 3. Report of the Treasurer. 4. Report of the Secretary. 5. Election of Directors. 6. Election of Members of the Council. 7. Reports of Standing Committees. 8. Reports of Special Committees. 9. Special Orders 10. Miscellaneous business. This order of business may be changed by a vote of a majority of the Members and Associates present in person or by proxy. The usual parliamentary rules shall govern all meetings of the Institute except in cases otherwise provided by the Constitution or the By-Laws. At all sessions of the Institute other than business meetings, the order of proceedings and the time of adjournment, shall rest in the discretion of the presiding officer

Jan 1, 1917

By D. M. Jamieson, M. P. Pearse, E. R. A. Plumstead

In 1948 the shaft sinking record in the Republic of South Africa was held by the Van Dyk Consolidated Mines Ltd. for a ventilation shaft with a footage of 461 ft sunk during the month of August 1941. This record remained for some ten years; but in the ensuing nine years it was broken no less than 13 times. Table I gives shaft sinking records throughout the world for the 21 years, 1940 to 1960. History shows that the wide, deep, timbered rectangular shaft had passed its peak of popularity by 1948, although it still had a great deal to commend it, both from the sinking and operational points of view. In sinking, it is easy to clean manually, and water can be handled by bailing when wet ground has to be negotiated; its shape also lends itself to equipping concurrently with sinking. In operation it provides the most convenient "in line" hoisting arrangement, and if the ventilation requirements so demand, it offers the simplest solution in that it can be divided into upcast and downcast sections. Furthermore, in the case of a multi-level mine, the shaft compartments can be reduced conveniently if the full area of the shaft is not required to serve all levels.

Jan 4, 1963

By W. Evans, C. E. Ells

The agglomeration of hydrogen in pure aluminum and A1-Mg alloys has been studied through use of hydrogen introduced into the metal by cyclotron proton irradiation. Both the growth and dispersal of the agglomerates have been followed by metal-lographic techniques. During the cyclotron irradiation, agglomeration occurs at temperatures i 100°C for hydrogen concentrations as low as 1 ppm. On heating at elevated temperatures, 300°C to 600°C, intragranular agglomerates first coarsen and then disperse. The agglomerates formed at grain boundaries are much larger than the intragranular agglomerates; with hydrogen concentra- tions > 10 PPm, heating for 1 hr at 500°C results in extensive grain-boundary cracking. The hydrogen agglomerates have been shown to inhibit grain growth, but no inhibition of recrystallization has been observed. The ability of hydrogen to enter aluminum at a free surface, combined with its high-diffusion rate at elevated temperatures, accounts both for growth and dispersal of the agglomerates. Irradiations at elevated temperatures give results consistent with the explanation proposed for agglomerate behavior on post-irradiation heating. 1 HE formation of hydrogen-filled bubbles, or blisters. in aluminum and its alloys has been studied for over' thirty years. The work up to 1952 has been reviewed by Kostron' and since then Ransley and

Jan 1, 1963

Meeting of Nov. 21, 1913.-The President reported the appointment of the officers and members of the Committee on Non-Metallic Minerals, published elsewhere in this Bulletin. The President appointed the Executive Committee of the New York Section as a local .committee to have charge of the Annual Meeting of the Institute in February, 1914, with power to add to their numbers. It was voted that the Chairman of each Technical Committee, be made ex officio a member of the Committee on Papers and Publications. At the request of the Secretary, Burr A. Robinson was appointed Assistant Secretary of the Institute. E. Gybbon Spilsbury was nominated as representative of the Institute on the John Fritz Medal Board of Award. It was voted that the next summer meeting of the Institute be held in Salt Lake City in August, 1914, with power to the Executive Committee to fix the exact date. Substantial reduction was made in the price of the back Transactions of the Institute in accordance with the notice published on p. i of this Bulletin.. The By-Laws of the Montana Local Section were approved. The printing contract for the year 1914 was made with the Maple Press. Thirty-eight Members, one Associate and three Junior Members were elected.

Jan 12, 1913