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By Christiano Gianesi Bastos Andrade

Clays with high content of smectite are denominated bentonites, and are widely used in industry as, for example, agents for bleaching of vegetable oils, animals and minerals. For this use, the smectite clays are treated with inorganic acid of high concentration at temperatures under boiling point, which provide the bentonite´s bleaching power. In the present study, a sample of smectite from Cubati, Paraiba, Brazil, was submitted to treatment under moderate conditions (90°C, reaction times of 1, 6, 12, 18 and 24hours in close reactor, concentration of the aqueous solution of hydrochloric acid 1.5 M, acid solution/clay ratio of 1g/10mL), aiming to reduce impurities, responsible for the color of the clay, without causing significant changes in their structure. Thus, clay can be used in the cosmetics industry and other products with high added value. The treated clay was characterized by scanning electron microscopy (SEM), stereomicroscopy, energy dispersive X-ray detector (EDS) and X-ray diffraction (XRD). It was observed a bleaching in samples with time of 12h to 18h. With the DRX was possible to monitor the peak intensity of the clay structure and the sample with 12 hours of treatment was not significantly altered its crystalline structure, maintaining the peak clay at d001. The most pronounced changes in the bleaching occurred within the first 12 hours of acid treatment.

Aug 8, 2018

By Werner Klein

The Production Management solution (Level 3) covers TYASA’s existing steel making plant, billet caster and new Castrip based coil production line in Ixtaczoquitlan, Mexico. It steers the order based production utilizing product routing information and corresponding process instructions for the individual processing units. A seamless material tracking along the entire production route from heat creation in the electric arc furnace down to the final coil product provides TYASA with the genealogy information customers require for flat products. At each important process step the Level 3 compares actual quality related production results with order requirements. In case of deviations from ordered quality the plant staff is guided by rule based dispositions. The highly configurable solution supports customer to operate its production plant as a smart factory in the sense of industry 4.0.

Oct 30, 2017

By Aloizio Cesar Gonzaga, Leandro de Paula, Ismael de Souza Dias, Gladston Santos

Looking for greater competitiveness, Gerdau started in 2013 the operation of its hot strip mill in Ouro Branco, being a milestone in Gerdau's history, where it definitely entered the flat products business. This mill consists of the reheating furnace, primary scaler, a Duo-reversible Quadrupole Steckel mill, accelerated cooling and final coiling. The Steckel mill works with two backup rolls and two working rolls, the backup rolls being responsible for supporting the rolling forces and the working rolls for shaping and surface quality to the strips, having as main requirement quality of surface finish. These rolls suffer high wear due to the lamination process and are exchanged with high frequency to ensure the quality of the laminated strips, after the exchange are sent to the Work Roll Shop for grinding and are positioned Grinded work rolls for the next planned change. This movement is accomplished through the crane and an exchange device that attaches to the cylinders to be transported from the Rolling Mill to the Work Roll Shop. The target in this article is focused on an improvement in this Device to increase operational safety and reduce stoppage losses downtime at the mill, improving the cost / benefit ratio and increase production.

Oct 1, 2019

By Waleska Campos Guaglianoni

With the growth of nanoscience and nanotechnology, the synthesis of nanostructured oxides has received a special attention. Metal oxides are widely used in the manufacture of microelectronic circuits, piezoelectric devices, fuel cells, catalysts, filters and bactericides systems. These metal oxides represent a large class of semiconductor materials suitable for photocatalytic processes. In recent years, new materials of this class such as TiO2 and ZnO have been developed due to their photo-catalytic abilities to degrade various environmental pollutants. This work aimed to evaluate the photocatalytic activity of zinc oxide previously synthesized by combustion synthesis in solution using citric acid as fuel and different reasons fuel/oxidant. After synthesis, the powders were subjected to heat treatments at different temperatures and photo-catalysis. The photocatalytic activity was evaluated by the degradation of a solution of methyl orange in a photochemical reactor of UV illumination, after which the transmittance of the samples measured with the assistance of a spectrophotometer. To analyze the results, a commercial zinc oxide was used as standard. The products of combustion synthesis in solution showed that photocatalytic activity varied according to the ratio fuel/oxidant and as a function of heat treatment. The results showed a higher photocatalytic activity for the products obtained with disabilities fuel in the reaction and heat treated.

Aug 8, 2018

By Walter Hartig

Rogesa is operating two medium sized Blast Furnaces, No. 4 and No. 5 at Dillinger integrated steel works plant. The history of the results of the cooling concepts of the intersection between tuyère belt and bosh shows failures at both furnaces. At the 3rd reline of No. 5 Blast Furnace in 2010 changes were made to improve the cooling efficiency of the mentioned area. Two rows of copper cooling plates were installed. After commissioning and a short operating time hot spots occurred in the area of the cooling plates. The decision was taken to develop a new cooling concept together with Paul Wurth Umwelttechnik GmbH, Essen-Germany by replacing the cooling plates by one row of a short copper stave. The duration of the shutdown to perform the work was only 17 days including salamander casting. The operational results after the commissioning are very satisfying with outstanding performance of the new bosh cooling system.

Aug 1, 2018

By Mark Gilliam

Control of true steel level in the tundish during casting is desired in order to maintain the correct pressure head and thus provide a stable flow to the mold. Also the control of tundish draining prevents slag carryover and can increase yield at each end of cast sequence. At Steel of West Virginia (part of the SDI Group), it was understood that to be able to measure the true steel running level and control the drain level at the end of casting would be a great benefit during production at their three strand billet caster. This paper sets out to show how an evaluation process was started to find the best method to determine steel level in the tundish and to prevent the steel level dropping low enough to allow slag to enter the mold. Also how the decision was taken and a real time molten steel measurement system was installed and by utilizing the resulting data in the process, how slag in the mold was removed as an issue, how lost production was reduced and how consistent steel level has provided constant casting speeds and improved stream integrity, all leading to realized quality improvements. Other areas discussed within the paper will be the training of operational staff, the difficulties to be overcome when first installing new equipment and how these teething problems were cured by close co-operation between the steel plant and the equipment suppliers. In conclusion the paper will discuss the production improvements achieved, production cost savings at the plant and how the generated data was integrated into the plants process control system.

Aug 16, 2017

By Michael Brandner

In the past the research and development of new materials for hot mill rolls was mostly done by trials. Such trials are expensive and difficult to transform from small size to the big size of a solid roll. Computation is the cheaper way to get ideas processed and can be varied in different directions. The main part before simulation is the generation of the needed basic data of the specific materials. Some data is already well known and can be bought from databases; others have to be done specifically for our materials. The evaluation of such results has to be done still with solid trials, but the number of trials can be reduced. The advanced techniques of finite element calculation offer a wide range of possibilities to get answers about alloys, solidification, casting parameters and their influence. The possibility to calculate a heat treatment cycle and to get an answer about the internal stress modification during the cycle is a great help to understand the principle of transformation. Examples of different calculations in various fields will be given. The close cooperation with universities and other research institutes as well as the in-house possibilities will be presented.

Jul 30, 2018

By Martin Dirks

Nowadays the sinter cooler often becomes the bottleneck of the sinter production, with outdated equipment leading to low productivity and high operation and maintenance costs. Furthermore valuable energy is simply destroyed in the cooler, which is not compatible anymore with a cost efficient and environmentally friendly sinter production. Paul Wurth has developed and improved two types of coolers, the annular cooler and the shaft cooler which offer flexible solutions to the specific situation of each client. The classic design of the annular cooler was completely revised and is now composed of a rigid ringframe construction as opposed to the traditional design with individual sintering cars, avoiding the typical problems of centering. Additional features of the PW annular cooler are the low air leakage rate and the increased effective cooling surface due to the removal of dead areas. This leads, in addition to the lower weight, to lower operating costs and a smaller space requirement. The shaft cooler stands out with an even smaller space requirement and a lower sinter outlet temperature because of a very long residence time of the sinter inside the shaft. Its development into a pure counter flow cooler aims at maximizing its energy efficiency, as it is designed as a system with a very low demand for cooling air, high air discharge temperatures and highly reduced dust emissions. For both cooler types flexible heat recovery solutions can be offered. These solutions include the supply of hot combustion air to the ignition hood burners and the sinter strand, the production of steam for the clients steam grid or the production of electric energy.

Aug 16, 2017

By Kengo Usui

The energy consumption of Iron-making, especially Blast Furnace (BF), is very large. In order to maximize the utilization of limited resource, it is essential to reduce energy consumption and recovering waste energy in BF. This paper introduces energy saving equipment based on NSENGI’s over 80 BF construction experiences since 1963. The first is the technology for the Top Charging System for low fuel-rate operation. One of the important factors to achieve such operation, the burden should be charged uniformly. Since 1974, NSENGI have developed and delivered over 80 Top Charging equipments for such purpose and nowadays, developed new type Top Charging equipment with improvement of charging precision. The second is the technology for Solely BFG Operation in Hot Stove, which means no use of other fuel gas such as LDG, COG. It is realized by high combustibility of NSENGI’s Top-Combustion Hot Stove with Metallic Burners, and large amount of heat recovery of Waste gas Heat Recovery system with heat medium. The third is the technology for effective energy recovery in TRT. With NSENGI’s latest Gas Cleaning System “Multi-Vessel Electrostatic Precipitator" (MVEP), TRT will be able to generate higher electrical energy by approx. 30% than that of wet-type. In comparison with dry bag-type, MVEP allows temperature fluctuation which lead to generate higher electrical energy by approx. 10% NSENGI therefore, will be able to accept and meet your request widely.

Aug 1, 2018

By Raíza da Silva Juvenal, Suelen Silva Rocha, Artur Ângelo Alcântara de Assis, Jorge Luiz Valença Mariz

Um estudo de viabilidade econômica deve considerar parâmetros e incertezas inerentes a um projeto para produzir resultados econômicos consistentes, fornecendo ao investidor uma ferramenta de tomada de decisão. O presente estudo objetivou efetuar inicialmente a avaliação econômica convencional do cenário realista de uma mineração de agregados em fase de implantação localizada em Pernambuco, cujo Valor Presente Líquido (VPL) obtido foi R$ 24.006.309,20, o que representa um resultado positivo. Através da metodologia de Monte Carlo foi efetuada uma análise de risco considerando incertezas em 100.000 cenários, nos quais nove variáveis assumiram valores estocásticos dentro dos domínios definidos, produzindo assim uma distribuição estatística do VPL ao invés de um único número, sendo ainda efetuada uma análise de sensibilidade para identificar e quantificar as variáveis que mais impactam no resultado da avaliação. Por fim, os dois fatores mais influentes identificados na análise de sensibilidade inicial foram isolados e submetidos a uma nova análise de risco em outros 100.000 cenários. Foi concluído que o projeto é economicamente viável e que a probabilidade de gerar lucro aos investidores é de 99,77%, embora a probabilidade do VPL ser igual ou maior que o previsto pelo método convencional seja de 49,98%.

Oct 3, 2019

By José Adilson de Castro

In the integrated steel industries the sintering process plays an important role furnishing raw material to the blast furnace. In this work, a computational simulation of the sinter process is developed that is able to predict the most important phenomena within the sintering bed. The model is based on the multi phase concept with multiple components described by conservation equations of each component coupled with the momentum, chemical reactions and heat transfer. The model validation was carried out comparing the model predictions with averaged industrial data and local temperature measurements within the sinter strand. The model predictions presented good agreement with the averaged values measured on the industrial sinter process.

Aug 2, 2018

By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Ramon Augusto Moretti, Henrique da Rocha Severino, Renato Nascimento de Castro, Fernando Cesar Sousa

Rolling stand 12 (LTx) of long steel, installed in the company A, Piracicaba - SP unit, had presented high levels of vibration, which affected its internal components, such as: shaft, gears and bearings, generating downtime. To evaluate this equipment a study was proposed by the following engineering techniques: Conventional Vibration Analysis, Operational Deflection Shape (ODS) and numerical simulation by the Finite Element Method (FEM). In the Conventional Vibration Analysis, high levels of vibration were observed during manufacturing process, especially when the material reaches the equipment. Impacts generate high values in acceleration, on average 80 m/s² peak to peak. In the moment of impact, misalignment of internal components was observed by ODS. Field results were correlated to those obtained by the Finite Element Method, which allowed to calibrate FEM model. Thus, the most effective structural modification already numerically evaluated was implemented in the system. Afterwards, new measurements by vibration and ODS techniques were performed, and attenuation of vibrational levels and operational mode, which overloaded the internal components rolling stand, were verified.

Oct 1, 2019

By Samuel Filgueiras Rodrigues, Clodualdo Aranas Jr., Gedeon Silva Reis, Eden Santos Silva, Fulvio Siciliano

When austenite is deformed above the Ae3 temperature, partial amount of it transforms dynamically into ferrite by a displacive mechanism. After unloading, it retransforms back into the stable austenite by a diffusional process. This influences the rolling load which decreases under isothermal condition or does not increase with decreasing temperature as rapidly as expected under cooling. Plate rolling simulations under isothermal and continuous cooling conditions were carried out on a 0.09 wt.% Nb X-70 steel. Pass strains of 0.2 were employed together with interpass times of 10 s, and 30 s for the cooling conditions and 0.3 with interval of 10 s at 900 °C for the isothermal experiments; strain rate of 1 s-1 was used during the simulations. The mean-flow-stress (MFS`s) behavior of both conditions indicates that dynamic transformation and dynamic recrystallization were taking place during straining. The critical strains for the initiation of dynamic transformation fell around 0.06 while the critical strain for DRX was 0.12. It has been shown that ferrite is formed due to the applied deformation of roughing passes and increases its volume fraction throughout the finishing rolling stage. Under cooling conditions, the ferrite formation is also favored as the temperature approaches the Ae3 line. Such ferrite forms when the driving force for dynamic transformation is higher than the total free energy barrier preventing its formation. This obstacle consists of the free energy difference between austenite and ferrite as well as the lattice dilatation work and shear accommodation work. The addition of Nb retards the retransformation of the ferrite into austenite. Moreover, holding times after rolling increases the amount of austenite available for microstructure control on subsequent stages. The dynamic transformation (DT) mechanism can be used to design improved rolling schedules

Oct 1, 2019

By Diego Pacheco Wermuth

Micrometric surgical components typically have high geometric complexity and stringent regulatory specifications. These components need to have excellent mechanical properties and a high demand of products. Besides these factors, it is necessary to maintain a low manufacturing cost, performing essential research on new manufacturing technologies. Metal Injection Molding (MIM) is a process that has been explored , providing an interesting alternative for making medical devices. The research in the production of microcomponents obtained for MIM is gaining momentum and prominence, due to low cost and high productivity of this process. This paper is a study and development of feedstocks with AISI 316L alloy , which is known for its biocompatibility. Four feedstocks with 61%vol. of metal powder were analyzed by capillary rheometry and DSC/TGA.

Aug 16, 2017

By Lucia Vieira

Kelvin probe force microscopy (KPFM) can be used to monitor electrostatic charges on the surfaces of materials. In this paper, we describe the use of KPFM to evaluate the electrostatic effect induced by silver nanoparticles incorporated as clusters in diamond-like carbon (DLC) films, before and after scratching. The results are compared to those obtained for DLC films without silver nanoparticles. Raman spectroscopy was used to identify the DLC signature, and energy dispersive X-ray spectroscopy (EDX) was used to confirm the presence of silver in the film. The morphology of the DLC film containing silver was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings suggest that the incorporation of silver nanoparticles in amorphous materials could offer new options for electrostatic energy storage on the surfaces of these materials.

Jul 31, 2018

By Samuel F. Rodrigues, Clodualdo Aranas Jr., Fulvio Siciliano

The application of thermo-mechanical control processing (TMCP) in hot rolling of steels has become a common routine since the last 60 years. The understanding of the physical metallurgy behind TMCP played a major role in the early developments. Physical and numerical simulation works are performed firstly to derive the fundamental metallurgical knowledge and secondly to conceive existing TMCP practices. In this paper, a summary TMCP techniques is presented. The occurrence of dynamic transformation of ferrite in the austenite region is shown by means of synchrotron light diffraction methods. This phase transformation mechanism is taken into consideration and its effects on TMCP are proposed in an exploratory way.

Oct 1, 2019

By Jorge Madias

Neste trabalho se leva a cabo uma revisão da literatura sobre defeitos em beam blanks. O foco é no mecanismo de formação e as soluções propostas para diminuir sua ocorrência. Os defeitos superficiais incluidos são as trincas longitudinais e transversais, bleeding, pinholes e escória. Os defeitos internos levados em conta são os blowholes, as trincas centrais e as trincas nas pontas das abas. A revisão incluie as técnicas utilizadas para pesquisar os defeitos: caracterização metalográfica, CFD, modelagem termodinâmica e termomecânica, etc. As medidas adotadas estãorelacionadas a mudanças no sistema de lingotamento (por exemplo o design da vâlvula submersa), design do molde, mudanças e regulação do resfriamento secundário, suporte dos veios.

Oct 30, 2017

By Jari Larkiola, Aarne Pohjonen, Juha Jokisaari, Oskari Seppälä, Joonas Ilmola

Finite element method (FEM) is widely used to model the hot strip rolling process. Flatness defects e.g. front-end bending in multipass hot strip rolling is studied by authors using a finite element (FE) model with interactively operating automated controlling logic (ACL) [1]. However, industrial corresponding grade of accuracy in strip thickness subsequent to the rolling pass is not easily accessible in FE-model without separate calculation of significant rolling parameters and integrated roll gap control. In order to study flatness defects and optimize pass schedules the controlling and physics of the FE-model must correspond to the industrial process. For this need the automated controlling logic is upgraded by setup calculations to predicting roll force and work roll flattening. These predictions are utilized in setup positioning of a work rolls. Reliable setup calculation enables smooth multi stand rolling process without significant additional adjustment of roll gap clearance. State of art rolling technology requires above-mentioned setup controlling for the FE simulations to simulate different pass schedules without time consuming preparations. Operational setup calculations together with automated controlling logic of hot strip rolling enable simulation of new pass schedules and efficient problem solving.

Oct 1, 2019

By Danilo Gonçalves de Oliveira, Rogério Martins Pereira

Chatter is a widely studied vibration phenomenon that affects most cold mills around the world and its impact on these lines are tremendous: from productivity and quality losses to mechanical equipment damage. The investigation of its origins and how to minimize the occurrences and their impact on the equipment require special instrumentation and algorithms in order to have a detection of the vibrations as soon as they start. This paper presents three methods of identification of chatter on a Tandem Cold Mill and the actions to leave the vibration frequency range before its amplitude achieve catastrophic values.

Oct 1, 2019