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By Rodrigo Vitorino da Silva

Ligas a base de zircônio são utilizadas na indústria nuclear devido à suas boas propriedades mecânicas, baixa absorção de nêutrons e boa resistência à corrosão. No entanto, durante a operação do reator, o hidrogênio é absorvido pela liga, resultando na formação de hidretos. Para aumentar o tempo de operação desses componentes é necessário o desenvolvimento de novas ligas que retardem ou diminuam esse efeito. Este trabalho tem como objetivo avaliar a influência dos tratamentos termomecânicos no zircônio puro, através de testes que avaliem a corrosão, absorção e dessorção de hidrogênio nas condições laminada a frio e tratada termicamente. Análises de difração de raios-X indicam a existência de uma matriz Zr-a para as condições analisadas. Após a hidrogenação são formados ZrH e ZrH2. O zircônio puro encruado absorveu 1,23%p H. O zircônio puro laminado e tratado termicamente absorveu 0,85%p H. O resultado de DSC mostra que a decomposição dos hidretos ocorre em faixas de temperatura entre 318 e 368°C para a condição tratada termicamente. Para condição laminada, o resultado mostra uma transformação de fase entre 565 e 650°C. O conjunto de resultados permite concluir que a amostra tratada termicamente absorve menos hidrogênio, porém o início do processo é menor. A amostra tratada termicamente é menos resistente a corrosão e a velocidade da corrosão é menor.

Aug 16, 2017

By Staff

In 2012, the estimated value of mineral production increased in the United States for the third consecutive year. Production and prices increased for most industrial mineral commodities mined in the United States. While production for most metals remained relatively unchanged, with the notable exception of gold, the prices for most metals declined. Minerals remained fundamental to the U.S. economy, contributing to the real gross domestic product (GDP) at several levels, including mining, processing and manufacturing finished products. Minerals? contribution to the GDP increased for the second consecutive year. Trends in other sectors of the domestic economy were similar to those in mineral production and consumption rates (Table 1). After continued decline following the 2008-2009 recession, the construction industry began to show signs of improvement late in 2011 and throughout 2012, with increased production and consumption of cement, construction sand and gravel, crushed stone and gypsum, mineral commodities that are used almost exclusively in construction.

May 1, 2013

By James P. Bennett

To identify construction materials for emerging technology in chemical and metallurgical processes, the Bureau of Mines investigated the acid resistance of ceramic materials. Eight commercial ceramic materials comprising two red shale, two fire clay, a silica, a five-claybonded silicon carbide, a carbon, and a high-alumina brick were evaluated. Samples were exposed for 110 days to 20 wt pct HCl at 50°, 70°, and 90° C and to 30 wt pct HCl at 70° C. Statistically significant changes in cold crushing strength, volume, and weight were generally small or not detected. The leach rates of Al, Ca, Fe, K, Mg, Na, Si, and Ti ions were monitored. The carbon brick sample had the best acid resistant properties with a maximum total leached ion weight loss of 0.004 wt pct. The silicon carbide, the silica, and one of the fire clay bricks also had excellent acid-resistant properties.

Jan 1, 1983

By Ben Habermann

"The object of the work described in this paper was to increase the understanding of the relation that capillary pressure of a rock, hydro-dynamics, and accumulation of oil in stratigraphie traps have to one an-other. The hydrodynamic oil-water tilt equation is derived by considering the two vector gradients involved: (1) buoyancy of oil in water and (2) hydraulic gradient.Recent theories show the necessity for oil to have a continuons phase in the reservoir rock in order to mi-grate; this fact applies to hydro-static as well as to hydrodynamic conditions. Hydrostatically, the displacement pressure of the rock deter-mines the amount of oil that can be trapped behind a permeability barrier. If the buoyancy of oil in water exceeds the displacement pressure, oil will migrate up-dip; an oil trap will be formed where displacement pressure is greater.In stratigraphie traps the pressure drop caused by moving water is positive when its direction is down-dip, helping accumulation; and it is negative when its direction is up-dip, forcing the oil into the tighter section of the reservoir. Theoretically, pro-vided we have data such as: (1) the displacement pressure of an up-dip permeability pinchout, (2) density difference between the oil and water in place, and (3) the direction and magnitude of the hydrodynamic gradient (if any), the possible extent of a stratigraphie oil accumulation down-dip can be predicted.To test the above theory sample cores from three wells in the Denver Basin were analyzed and the oil column that could be held under hydro-static conditions was calculated. After the hydrodynamic influence was considered, the results were compared with actual field data.The significant fact shown by this investigation is that the calculated oil column in one reservoir very closely approximates the actual extent of the oil column in a well. Also in accordance with the theory, the capillary pressure caused by the buoyancy of the oil column exceeded the measured displacement pressure on core samples from another productive field. For very tight shaly sand and questionable oil shows, the interpretation of data is very critical, as shown by experiments on core samples from a third field."

Jan 1, 1960

This summary of State laws or explosives was compiled primarily to ascertain what subjects relating to their control have been acted upon by each State legislature and, in general, how they have been treated. It does not include any legislation passed after 1942, or any proclamations, regulations, or administrative orders. It does not purport or attempt to be authoritative. If any problem arises involving interpretation of the statutes of any particular State, the original source must be consulted for the exact words used by the legislature. This summary, however, will be useful In determining whether relevant statutes exist, and In locating them quickly,-with a minimum of effort. It will be of value also in comparing statutes in one State with similar statutes in other States to determine what construction has been placed upon them by the courts of those jurisdictions or to contrast the varying provisions of many States upon a similar subject. To make these comparisons easier, the statutory provisions for each State have been grouped under several major topics in outline form. Although this sometimes has resulted in disruption of the continuity of individual acts, the increased general clarity and availability of comparable sections have more than justified the procedure followed.

Jan 1, 1943

By Wenjun Ju, Xiaodong Sun, Jianwei Zheng, Bingding Yi, Zhaorui Ma, Pengfei Jiang, Lingfu Zhu, Yangfa Zheng

The presence of hard roof poses a significant threat to the safety of underground coal mining. In this study, a mechanical model is established for underground stopes to analyze the overburden structure with the advancing of the mining face. It is indicated that the load-bearing arch structure (LBAS) is formed above the stope for roofs with regular hardness, whereas the reversed-basin bearing structure (RBBS) is formed for hard roofs. Compared with the LBAS, the RBBS can induce an additional pressure at the foot of the bearing structure, and this effect becomes less as the distance between the hard roof and stope increases. The ultra-deep borehole hydro-fracturing technique (UHT) is proposed to weaken the hard roof for pressure release, and the associated equipment and procedures are also presented. The UHT is based on horizontal drilling along the axial direction of the roadway in the roof, and then the receding segmented hydraulic fracturing technique is used to achieve the purpose of fracturing (weakening) of the surrounding rocks. Field tests are carried out in 3022 roadway of Daliangwan coal mine in Yulin to assess the developed technique, equipment, and fracturing procedures. To evaluate the fracturing effect, deep borehole stress-meters are installed at different depths of the fractured and un-fractured zones of the roadway, along with hydraulic support pressure sensors placed at the mining face. The results show that compared with the un-fractured zone, the pressure on the wall and pillar sides is lower than that in the fractured zone, and the associated weighting duration and weighting area ratio of the fractured are reduced by 53.23% and 33.59%, respectively. This indicates that the presented UHT can provide a new solution for the prevention and control of mining disasters induced by hard roof failures in underground coal mining.

Nov 2, 2020

By R. J. O'Dea

"The United States hat large reserves of titaniferous iron ores that are a potential future source of both iron and titanium. Although it is not now economically feasible to recover iron and titanium metals from these ores, they may become important in times of stress and, in some instances, already have served as a source of pigment-quality titania.The iron- and titanium-bearing constituents of the ores considered in this report are not completely separable from each other by ore-dressing methods, and chemical (or smelting) procedures must be employed. It is im¬portant, therefore, that information be available concerting their reactivities. The most important titanium-bearing constituent is ilmenite (FeTiO3), the thermodynamic properties of which were discussed in a previous publication.3/ The results of thermodynamic studies showed that both hydrogen and carbon monoxide are relatively ineffective reducing agents for the iron in limonite. On the other hand, carbon theoretically is effective at tempera¬tures above 8510C., at which. point the combined equilibrium pressures of CO and CO2 from the reactionsFeTiO3 + C = Fe+ TiO + COand200 = C+ CO2reach 1 atmosphere.This report gives results of small-scale tests of selective reduction by carbon of the iron in titaniferous iron ores, both with and without addition of sodium carbonate. It is shown that the bulk of the iron may be reduced and separated without serious reduction or loss of titanium. Three Wyoming ores, Iron Mountain, Shanton, and Taylor, wore studied. The principal factors investigated were temperature, time, carbon:ore ratio, particle size, and sodium carbon ore ratio.Two methods of investigation were employed. In the first, intimate mixtures of ore and carbon were roasted and the reduced iron and titanium evaluated by leaching with dilute sulfuric acid and analyzing the leach solution (and, in some instances, the dried residues).Twenty grams of ore were mixed thoroughly with carbon and tamped into an alundum thimble having a loosely fitting cover. The thimble and contents were placed in a test-tube end porcelain tube and heated to the desired temperature in a Globar tube furnace. The open end of the porcelain tube was connected to a bubbler containing sulfuric acid, in a manner that permitted complete shut-off of the tube when desired. This allowed removal of the tube from the furnace at the end of the roast period without exposure of the contents to the atmosphere."

Jun 1, 1946

By R. J. Evans

The generation and disposal of solid waste from electric utility plants using a lime or limestone wet-scrubbing system and the potential effects on the environment were estimated for 1975 and 1980. The study indicated that in 1975 approximately 5.8 million tons of desulfurization solid waste (50 percent solids) will be generated. In 1980, when it is estimated that desulfurization will become commercially accepted, approximately 71.4 million tons of this material will be generated for disposal and/or utilization. The desulfurization waste material when combined with lime, fly ash, and water may have potential for use as a roadbase material, landfill reclamation, and synthetic aggregate.

Jan 1, 1974

By Fabiano Della Libera da Silva

Este artigo propõe uma metodologia para a construção de um Referencial Estatístico para a Utilização Física de equipamentos de mina. Para tanto, calcula-se um valor mensal (RE) apoiando-se em conceitos importantes para a operação de mina e que estão e inter-relacionados, como o comportamento sazonal da precipitação pluviométrica, o Teorema do Limite Central e a Gestão da Lacuna de Resultado. A metodologia proposta foi aplicada em uma mina de ferro a céu aberto e às frotas de transporte de um complexo minerador no Norte do Pará.

Aug 17, 2017

By Charles A. R. Lambly

This paper, which describes the mining practices of the Pend Oreille Mines & Metals Co. at Metaline Falls, Wash., is one of a series being prepared by the Bureau of Mines on mining practices, methods, and costs in various mining districts of the United States. ACKNOWLEDGMENTS Acknowledgment is made to L. P. Larson, president, and Jens Jensen, secretary, of the Pend Oreille Mines & Metals Co. for permission to publish this paper. information was supplied by E. Berglund, mine superintendent; Earl Miller, chief engineer; Lynn Kinney, John Currie, and Wally Frick, engineers; Arthur Newman, chief clerk; and Jack Crampton, assayer.

Jan 1, 1941

By Alexander E. Morrow

Oxygen breathing apparatus for use in mines was introduced to the United States in 1907. Despite their intended purpose of safeguarding lives, the apparatus led to the deaths of many men because of inherent or developed defects in the equipment, lack of training,, physical shortcomings of wearers, and improper procedures. The Bureau of Mines pioneered in research and training to curb logs of life among users of such apparatus and promoted development of safer equipment and procedures. As a consequence, deaths have been far less frequent. In 1944 the Bureau issued Information Circular 7279, Loss of Life Among Wearers of Oxygen Breathing Apparatus. That publication listed the case histories of 26 deaths that had occurred since the introduction of such equipment to American mining. The author, the late G. W. Grove,3/ asserted that further loss of life could be avoided if good equipment were used, teams were properly trained, and the basic principles of safe procedure were followed. This publication is a sequel to I.C. 7279 and contains information on eight deaths among wearers of oxygen breathing apparatus that were overlooked in the original compilation. It also describes the single death that occurred since I.C. 7279 was published.

Jan 1, 1959

By Jr. Gabler

World resources of cobalt appear ample for the foreseeable future; however, political and economic events have caused concern over the availability and reliability of an uninterrupted supply. Because of this concern, the U.S. Congress requested that the U.S. Bureau of Mines initiate a study of the flow of cobalt in the economy that would delineate and quantify the production areas where metal values are lost. As a result, the Bureau has developed a computerized commodity flow model. A major attribute of this model is that it is amenable to updating as supply, demand, and/or production data change. This report follows the flow of cobalt through its metallurgical and chemical applications and highlights areas where significant losses occur due to downgrading, export, or disposal. The study indicates that about 4,300,000 lb of cobalt-bearing materials are lost each year, representing 24 pct of U.S. domestic demand.

Jan 1, 1990

By S. Potgieter-Vermaak, T. T. Chiweshe, W. Purcell

The advantage of using ammonium phosphate salt as flux is the selective precipitation of chromium(III) compounds, which are considered nontoxic and environmentally friendly. The technique in this paper is determined to have potential to be applied in the metallurgical industry, where it can be used in the beneficiation of chromite mineral ores. The higher chromium contents of chromite ores often require furnaces to run at higher temperatures of above 1,300 °C, which can cause shutdown of the ore processing plant and accumulation of the sticky chrome compounds — including toxic chromium(VI) waste — which are generated as byproducts. The other advantage of this technique is its low to moderate energy consumption compared to existing techniques.

By Carlos Eduardo dos Santos, Geraldo Lúcio de Faria, Sidney Nicodemos da Silva, Rogério Felício dos Santos, Darlan Vale Bayão, Emiliana Cristina Marques Arthuso, Ivete Peixoto Pinheiro

Os aços inoxidáveis duplex (AIDs) são ligas metálicas que possuem uma microestrutura bifásica constituída por frações volumétricas aproximadas de ferrita () e austenita (). Esta microestrutura proporciona ao material uma combinação atrativa de propriedades mecânicas e de resistência à corrosão. O desbalanço das frações volumétricas destas fases pode ocorrer quando os AIDs são expostos a temperaturas elevadas, seja durante os processos de produção, soldagem ou até mesmo em condições de serviço e podem provocar alterações indesejadas nas propriedades da liga. Nesse contexto, a utilização de metodologias eficientes que permitam avaliar quantitativamente as frações dessas fases em AIDs é de grande relevância. Diante disso, o objetivo deste trabalho foi avaliar e comparar os resultados da aplicação das técnicas de estereologia quantitativa e ferritoscopia para quantificar as frações de  em amostras de um aço duplex UNS S31803 (2205) submetidas a um tratamento térmico de solubilização a 1050°C e diferentes intervalos de tempo de envelhecimento a 850°C. Concluiu-se que o ferritoscópio subestima os valores da fração de , quando comparado com a estereologia quantitativa. Parâmetros como textura, distorções na rede cristalina, geometria da amostra e padrões de calibração exercem influência em sua medição. Sendo assim, a estereologia quantitativa mostrou-se como a técnica mais adequada para a quantificação de fases nos AIDs.

Oct 15, 2019

By Pedro Jorge Walburga Keglevich de Buzin

O cloro no processo de aciaria elétrica tem sua principal fonte nas contaminações de origem orgânica existentes nas matérias-primas usualmente empregadas, principalmente na sucata. Apesar dos atuais níveis de cloro não perturbarem a fabricação do aço nas mini-mills, a presença deste elemento e dos compostos por ele gerados tem influência deletéria nos aspectos laborais, ambientais, de manutenção das instalações e na reciclagem das poeiras de aciaria. Neste trabalho, com base na integração de dados da literatura, da indústria e de propriedades físicas, químicas e termodinâmicas das substâncias envolvidas é feita uma avaliação qualitativa da passagem do cloro na aciaria elétrica e sua distribuição nas diversas correntes de massa de saída do processo. Foi concluído que a maior parte do cloro que entra no FEA deixa o sistema concentrando-se nas emissões do processo, principalmente nas poeiras de aciaria, sob a forma de cloretos alcalinos.

Oct 30, 2017

This investigation addressed two products from Samarco?s desliming circuit, namely underflow of cleaning cyclones and underflow of desliming cyclones. The roughing cyclones receive the product of the grinding circuit. The underflow of the roughing cyclones feeds the cleaning cyclones and the overflow feeds the desliming cyclones. The underflows of cleaning and roughing cyclones are combined to constitute the feed of the flotation circuit. These fractions were characterized and a new process route was proposed. The size distributions of the two fractions are quite different. The desliming cyclones underflow presents higher amount of material passing 37 µm and of ultrafines as compared with the cleaning cyclones underflow. Laboratory scale flotation tests were performed in a mechanical machine aiming at comparing the performances of these products in the presence of the reagents employed in the concentrator. Pi-lot scale column flotation yielded enhanced iron recoveries for both products in comparison with those achieved in laboratory mechanical cells, without impairing the concentrate quality. The in-crease in recovery was more significant in the case of the cleaning cyclones underflow. These results suggest the use of columns in the flotation of this product aiming at increasing the overall iron recovery. Nevertheless the results also showed that the use of columns to float the cleaning cyclones underflow should also be taken into consideration. Despite the fact that this product requires a longer residence time in order that the required silica content in the concentrate is achieved, the indication is that higher levels of iron recoveries might be reached. The conclusion is that, due to the different behaviors of the two products, they should be processed in distinct circuits to maximize the iron recovery.

Jan 1, 2014

By Steve Kral

"Liebherr, as most anyone involved with the global mining industry knows, is one of the world’s largest makers of mining and construction heavy equipment. The familyowned company has been around since the 1940s and, according to Stefan Heissler, by the end of next year, will employ about 44,500 people worldwide. Heissler is a member of the board of directors of Liebherr International AG.It all started for the Switzerland-based company when Hans Liebherr first recognized a need for heavy equipment in the construction industry, Heissler said. His first product, introduced in 1949, was the TK10, a mobile crane that, at the time, was a groundbreaking innovation to the heavy construction industry. From there, the company began its growth into a world-leading heavy equipment manufacturer that always relied on innovation.In October, Liebherr gathered a group of mining and construction magazine editors in Leoben, Austria to take a look at the company’s latest addition to the global mining and construction markets. On the mining side, Liebherr provided a demonstration of its T-236 100-t (110-st) haul truck and the PR- 766 50-st (55-st) crawler tractor. The one-day demonstration took place at the Erzberg iron mine near Leoben, where both machines are being proven.The Erzberg Mine, operated by VA Ersberg, has been in operation for about 1,300 years and is said to be Europe’s largest surface mine. It employs about 230 people and mines about 12 Mt/a (13,200 million stpy) of ore, producing about 3 Mt/a (3.3 million stpy) of fine-grained iron ore.T-236 rigid-frame truckThe new T-236 rigid-frame dump truck, with a diesel electric drive system, is Liebherr’s entry into the 100-t (110-st) class and is the first in this class with a four-corner, oilimmersed braking system. The haul truck was first introduced during the 2016 MinExpo in Las Vegas, NV. The unit has since successfully completed its testing phase and is currently in its first field operation trials at the Erzberg iron mine in Austria."

Jan 12, 2017

By A. Chattopadhyay

Porphyry copper deposits are the most important source of copper and also gold within the orogenic belts. These deposits are characterized by low grade copper ore (0.2% to 1% copper) and host precious metals like gold, silver and platinum. A characterization tool has been developed for complex porphyry type copper-gold deposits with an aim to quantify copper and precious metal deportment. This quantification is a challenging task due to low grades and also due to the presence of both visible and invisible precious metal content in different sulphide and non-sulphide phases. Studies were initiated on various complex, ore deposits and also on samples representing various processing streams such as flotation and leach products. This paper presents the development of a systematic approach to diagnostic metallurgy using state-of-the-art optical and automated mineralogy, micro-probe, dynamic SIMS and TOF-SIMS analysis for quantification of invisible and visible precious metals content in various species. The relevance of this characterization to metallurgy will also be briefly discussed in this paper.

Sep 1, 2012

By Frank E. Cash

The data in this circular were compiled so that individual phosphate companies might have the benefit of the experience of other phosphate companies, and that industries in general might compare experiences (taking into consideration relative hazards), thereby promoting accident preven¬tion. ACKNOWLEDGMENTS The descriptive matter is taken in part from a. paper by Cash and von Bernewitz.4/ Production figures ore from Mineral Resources of the United States;5/ accident data were furnished by each of the operating companies in the pebble-phosphate district, and their assistance in making this report possible is gratefully acknowledged.

Jan 1, 1936

By Bengt H. Fellenius

The design of pile foundations is much more commonly verified by means of a full-scale test, than is the design of other foundation units. The reason is not that our knowledge of pile behavior is more uncertain than our knowledge of other foundation types making the verification necessary, but more that the loads in a structure are more concentrated to single foundations in a structure founded on piles as opposed to structures on footings or mats. Therefore, should a pile cap fail or move, the adverse consequence of this is often drastic, as the piled structure has little freedom to transfer its need for support to other foundation units. Consequently, it becomes important to assure the design of piled foundations. In many, maybe in most instances, the static pile loading test is routine and geared toward determining an at least capacity, only. However, in these times there is an ever increasing liability of the professional, demands for increased economy of the foundation, and frequent lack of the involvement in the test of the experienced old-timer exercising good judgment. Furthermore, modern pile design is leaving the single, simple concept of capacity and requires more information from the test to assist in determining aspects of long-term behavior and settlement. Therefore, even the straight forward, routine static loading test requires improved planning, execution, and analysis.

Jan 1, 1990