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By H. B. Carroll

The Bureau of Mines has designed and built a controlled-environment test chamber specifically for instrument evaluation in simulated work atmospheres. The atmosphere inside the 300-liter stainless steel chamber can be controlled at any selected temperature and relative humidity in the range of 2° to 93° C and 20 to 95 percent, respectively. Instruments placed inside the test chamber are subjected to an atmosphere at a preset temperature and humidity containing various concentrations of toxic gases such as CO, C02, NO, NO2, S02, and H2S. Toxic gas losses resulting from wall reactions, monitoring instruments, and instruments under evaluation are compensated by the use of a dynamic gas blending system.

Jan 1, 1973

By Ted C. Briggs

A removable-jacket distortion apparatus was constructed and used to measure distortion coefficients for two high-pressure vessels. The measured distortion coefficients were used to compute distortion coefficients for volumes VI and (V1+V2) of a 1,000-atmosphere Burnett compressibility apparatus for the temperature range 0° to 75° C. Young?s modulus for Armco 17-4 PH stainless steel, heat treated to condition H1150-M, was computed from experimentally determined distortion coefficients. A 10-to 14-percent correction to the values obtained for Young's modulus may be required because pressure vessel end effects were neglected. The distortion coefficients of the compressibility apparatus are believed to be accurate to about 1 percent.

Jan 1, 1970

By Alan H. Goode

As part of the Bureau of Mines program to broaden utilization of abundant low-quality mineral materials, the Tuscaloosa Metallurgy Research Laboratory conducted beneficiation studies on two Alabama clays. The main purpose of these studies was to develop improved plasticity and green strength in both clays and compare these improved properties with those of a typical ball clay. Whiteness of the clays was also considered. The results indicated that by adjusting the pH of the kaolin to approximately 9, a substitute for ball clay could be obtained. The investigation also showed that by a combination of attrition grinding and sodium dithionite leaching to remove iron, the underclay could be upgraded to a ball clay material.

Jan 1, 1975

By J. A. Eisele

The Bureau of Hines conducted a bench-scale investigation of a concentrated H2S04 reaction for recovering and separating rare-earth elements, barium, and strontium from a bastnasite ore and byproduct. Barium and strontium were dissolved in the concentrated acid and precipitated as a mixed product by water dilution. Separation of strontium from barium was effected by reaction with Na2C03 solution, followed by a dilute acid leach of the SrC03 formed. After removing the barium and strontium from bastnäsite are, the rare-earth elements were roasted to water-soluble sulfates. The rare-earth sulfate solution was subsequently processed by solvent extraction to produce rare-earth oxides low in lead and magnesium.

Jan 1, 1974

By R. R. Sayers

The terms "sanitation and }\Vgienen are often used interchangeably, but it is more "' usual to apply ttsani tat ion'' to th environment or surroundings, and nr.ygieneto the iiiividual, The subject,. h9wever, is so broad that only a few of the phases of sanitation will be di.acusae in ·this paper, vmile the various Fsea of hyg:tene will be deferred for later consideration. One of the bes.t .iaf ini tions of sanitation that I have hearci was given by ur. L. L • Lumsden, of the U, S. Public Heal th Service, who state.d that "'sanitation is t-he c.oir .. 'Don-sens$ application of the principles of cleanliness,

Aug 1, 1922

By Elaine T. Cullen

Safety training materials appropriate for specific underground noncoal operations in the United States are often outdated or nonexistent. The Spokane Research Laboratory (SRL) of the National Institute for Occupational Safety and H ealth has developed several new training tools, including three videos on common underground activities, software that will allow trainers to create a virtual training mine using their own mine map, and toolbox training materials. SRL is working closely with industry in the development of these tools. Teams of safety professionals are involved in the early stages, and actual mines and miners are involved throughout the production phase. This presentation describes the development process and results of SRL’s safety training projects.

By Ludwig Schmidt

The policy of buying crude oil on a gravity basis , recently instituted by the major crude oil purchasing agencies in the Mid- Continent field , has caused a new and vital interest to be taken in the work of the U. S. Bureau of Mines for preventing evaporation of crude . From the early years of the industry oil men have recognized that the gravity of crude oil is usually an index of the gasoline content , but it has not been so generally known that the gravity of the crude oil decreases if evaporation is permitted . In 1919 the Bureau of Mines began a survey to determine the evaporation losses of crude petroleum in its various stages of handling from the well to the refinery , The results of this study are presented in Bulletin 200 ( Wiggins , J.H. , Evaporation losses of petroleum in the Mid- Continent Field , Bulletin 200 , U. s . Bureau of Mines , 1922. ) and Bulletin 225 ( Wiggins , J.H. , Methods of decreasing evaporation losses of petroleum , Bulletin 225 , U. S. Bureau of Mines , ( In press ) The findings of this survey were so startling that soon after the preliminary report had been published , several tank companies began manufacturing vapor- tight tanks for the purpose of reducing these important losses . Since that time the development of this type of apparatus has been so rapid that today , every oil trade journal carries numerous advertisements of vapor- tight tanks and equipment as well as technical articles dealing with various problems in connection with the elimination of evaporation losses , whereas three or four years ago the subject was scarcely even thought of. The present report has been prepared in response to numerous requests for information on the apparatus actually being used to prevent evaporation losses . At this time oil operators are also extremely interested in holding the lighter fractions in the crude oil in order to prevent a lowering in gravity . The practice of removing the vapors from crude- oil tanks by means of a slight vacuum and extracting the gasoline from them is not discussed here .

Feb 1, 1923

By H. H. Schrenk

There are several well-recognized procedures for controlling exposure to hazardous atmospheres in industry. They include (a) substitution of less toxic material, (b) enclosure of processes, (c) wet methods, (d) local exhaust, (e) general ventilation, and (f) use of respiratory protective devices. In addition to their employment as a control measure in occupational exposures, respiratory protective devices also are essential in emergencies that may arise from failure or improper use of other control equipment. Respiratory protective devices usually are employed to supplement other methods of control, as temporary expedients, or when other methods are not readily applicable or practicable. It seems reasonable to assume, however, that where respirators are used consideration has been given to the factors involved and that the devices can provide satisfactory protection if used properly. Their use should not be arrived at simply by a process of elimination of other methods that are more difficult to apply.

Jan 1, 1943

By Richard J. Kline

The underground mining industry is presently using the fluid network analyzer and digital computer to analyze ventilation systems. The availability of the digital computer and ventilation programs to mining companies has escalated its use, permitting the design and modification of new or existing mine ventilation systems to be projected completely and thoroughly with consistent precision. Because the analog computer has been analyzing ventilation systems accurately for many years, a comparison of the analog and digital methods was warranted. This report summarizes a detailed comparison for one mine, based on parallel analyses by the two computer systems.

Jan 1, 1972

By J. M. Stuve

Heat of solution measurements of high-purity neodymium metal and neodymium trichloride (NdCls) in 4.360 molal hydrochloric acid (HCI) were used to determine the standard heat of formation (6EPr) of NdCls? From solution data obtained, the heat of formation of NdCls (c) was computed as -248,970 ±260 cal/mole at 298.150 K.

Jan 1, 1965

By J. V. Scalera

Because of U.S. dependency on imported critical metals, the Bureau of Mines has conducted research to evaluate the possible substitution of nitrided low-alloy steels for higher chromium-containing alloys. The corrosion data for nitrided steels are limited primarily to the Soviet literature. The objective of this study was to determine the corrosion properties of six commercially nitrided low-alloy steels in a 5-wt % NaCl solution at pH 4. Weight-loss tests indicated that, in deaerated test solutions, most of the nitrided steels were less corrosion resist-ant than nontreated steels. However, electrochemical tests indicated that under more oxidizing conditions, nitrided materials are converted to a passive state with a significantly reduced corrosion rate. Elec-trochemical tests performed in an aerated environment confirmed the passivity of the samples in an oxidizing environment.

Jan 1, 1984

By George H. Schnakenberg

Automation of coal mining activities at the face offers improvements in worker safety, health, and productivity. Introduction of integrated computer-sensor systems to current mining machines will enable these machines to perform some of the most hazardous tasks through supervised teleoperation. The U.S. Bureau of Mines is pursuing the development of the enabling technology necessary to achieve this goal. The research program consists of both basic and applied research, each focused on the fundamental issues of computer and sensor technologies. Short-term research is directed to providing computer-assisted, remote supervisory operation of present underground equipment; the long-term goal is the development of progressively more intelligent mining systems. The research program includes a review of robotic machine and autonomous vehicle technologies and of current mining technology, which provides a base for developing innovative mining methods; research in navigation and guidance technology, emphasizing control of a continuous mining machine; research on coal-rock interface sensing technology for horizon control, and rib thickness control in highwall mining; the development of computer systems and hierarchical architectures for real-time control; and development of expert systems for machine system fault diagnostics and predictive maintenance. This report presents a brief background and the current status for each of these research areas.

Jan 1, 1989

By L. B. Berger

"INTRODUCTION Accurate determination of carbon monoxide in concentrations ranging from 0.2 to about 0.5 percent by volume is troublesome, because such concentrations are too high for some analytical methods and too low for others. Methods that are sensitive to concentrations of carbon monoxide considerably less than 0.2 percent are approaching their upper limit of usefulness when applied to the analysis of samples containing 0.2 percent or more of carbon monoxide, and it may be necessary to resort to dilution of the sample with a known proportion of air, or otherwise modifying the analytical technique, to obtain satisfactory results. Such methods include the determination of carbon monoxide by reduction of heated iodine pentoxide 3/4/5/ by the ""Pyrotannic acid"" method 6/ and by the so-called ""phosphomolybdic acid"" method. 7/ The use of conventional gas-analysis equipment, such as the Orsat type, in the determination of carbon monoxide in concentrations ranging from 0.2 to 0.5 percent is not desirable, as possible analytical errors may be of about the same magnitude, thus producing results of little quantitative value.For several years prior to this publication, the Gas Analysis Laboratory of the Health Division of the Bureau of Mines has used a modification of the Haldane type 8/9/10/ gas-analysis apparatus for the determination, by absorption in a chemical reagent, of carbon monoxide in low concentrations that are not readily determined by other methods. The method is applicable also to the determination of higher concentrations. As the procedure has proved successful and has been adopted by others, this report was prepared to describe the method and to present results of analyses obtained with it."

Nov 1, 1947

By John J. McClelland

The U.S. Bureau of Mines formed a team in 1991 to begin developing a long-range research plan for computer-assisted mining that would benefit the metal-nonmetal mining industry. This report details the team's accomplishments, specifically, the development of a model that identifies metal-nonmetal mining research needs that could be addressed by the application of automation technology. The report also provides a summary of automation needs and applications based on visits with mining company representatives. The status and future direction of this work is also presented.

Jan 1, 1994

By Jan M. Mutmansky

"When, in 1973, a limit was placed on the amount of dust in the coal mine atmosphere, restricting the average exposure of a coal miner to 2 milligrams of dust per cubic meter of air (mg/m'), skeptics in the United States and abroad Said the standard could never be achieved. They cited much more lenient standards already established in other countries and refused to believe that the United States could meet the world's most stringent requirements in mines where dust had never before been regulated. Yet 10 years later the goal had largely been achieved and miners were working underground in a cleaner atmosphere than ever before. It was a major achievement and a big stride in what had become a war on coal workers' pneumoconiosis (CWP), the black lung disease prevalent among miners in underground coal mines.Although the health hazards caused by working in a dust-filled mine atmosphere have long been recognized, the problem became particularly acute in this century with the mechanization and increased productivity of underground coal mining. The United States was much slower than some other countries to address the problem of respirable diseases among miners. While dust levels in South African gold mines were first regulated in 1912, in the United States it was only when 476 workers died of silicosis while blasting a tunnel through a mountain near Gauley Bridge, West Virginia in the 1930s that widespread public attention became focused on the plight of workers in dust-filled environments. Another 30 years passed before regulation of dust finally became law in the Coal Mine Health and Safety Act of 1969.With a stringent new standard imposed in all underground coal mines, the industry was faced With the daunting problem of reducing levels of airborne dust from perhaps 6.5 mg/m' to 2 mg/m', in an inherently dusty operation carried out in the close confines of underground passageways. Most of the coal dust is made by the cutting operation in which the continuous miner or longwall machine can produce several thousand milligrams of respirable dust for each ton of coal mined. Other dusty operations such as drilling holes for roofbolts, loading and unloading coal on shuttle cars, and the operation of conveyor belts contribute to the overall problem.Since the institution of the new dust control standards, a number of strategies have been adopted for reducing the coal dust in the mine atmosphere. These strategies involve engineering and design improvements that help lo prevent the generation of particles, keep particles of dust from becoming airborne, carry dust away from the working area, and isolate the dust from the workers in the mining operation. These procedures have been pursued vigorously by the Bureau of Mines, and many successful methods have been developed to reduce the mass concentration to which the workers are subjected. The mining companies were reluctant at first to confront the problems but after a period of trials and gradual improvement, they joined with others in the fight to reduce the dust concentrations in the working place."

Jan 1, 1990

By E. M. SEELEY, F. S. LOTT

Expansion in total capacity of the natural-gasoline industry.to produce light products continued in 1944 and 1945. The average rate of gain, however, was reduced to about 6 percent annually from over 9 percent in the preceding 4-year period. New facilities at cycle plants again accounted for most of the increase in productive capacity. Between January 1, 1944, and January 1, 1946, the number of cycle plants increased from 32 to 37 and their total capacity from 3,278 thousand gallons daily to 4,848 thousand (48 percent). Capacity of all other plants in the industry increased in the same period from 12,735 thousand gallons daily to 13,080 thousand, or only 3 percent. The capacity of the average plant increased to 28,600 gallons a day from 24,400 gallons on January 1, 1944, continuing the established trend. The average capacity of cycle plants increased to 131,000 gallons a day from 102,400 gallons, and the average capacity of all other natural-gasoline plants increased to 22,200 gallons a day from 20,400 gallons. Although the number of plants increased in only three States in the 2-year period (Texas, Okla- homa, and Arkansas), the total capacity of plants increased in eight States. A further decline of 29 reduced the total number of plants to 626 on January 1, 1946. Compared with 10 years earlier, gasoline plants were more numerous in only 4 States: Texas (48 more), New Mexico (7 more), Arkansas (2 more), and Louisiana (1 more). The largest declines, in order, were in Oklahoma, Illinois, Pennsylvania, West Virginia, and California. The number of plants with fractionating equipment for separating the liquefied gases from heavier fractions was 202 on January 1, 1946 and 182 2 years earlier. The principal changes in number and capacity of shut-down plants were an increase in Texas and a decrease in California. Shut-down natural-gaso- line plants are usually among the smallest units in their vicinity.

Apr 1, 1947

BIBLIOGRAPHY Allen, C.A, Analyses of Utah Coals, United States Bureau of Mines Technical Paper 345, 1925, pp. 90. Allen, J.E. and E.M. Baldwin, Geology and Coal Resources of the Coos Bay Quadrangle, Oregon, Oregon Department of Geology and Mineral Industries Bulletin 27, 1944, pp. 160. "Aluminum Boom Raises Productivity", Coal Age, Vol. 82, No.6, June, 1977, pp. 103.

Jan 1, 1978

By A. W. Deurbrouck

This Bureau of Mines report describes the preparation characteristics of the significant coalbeds from which samples could be obtained in Upshur County, W. Va. One of the 14 samples collected was of metallurgical quality as received, 6 could be sufficiently upgraded to provide acceptable products, and 7 could not be upgraded to metallurgical quality because of their high sulfur contents.

Jan 1, 1967

By W. M. Myers

"The continued expansion of modern industry broadens the markets for minerals and their product. With these increasing demands new uses are being found for minerals that heretofore were considered as possessing no commercial possibilities. This tendency is reflected in the nonmetallic field in a constantly increasing demand for minerals formerly considered to be of scientific interest only, Furthermore, nonmetallic minerals of established commercial importance are used in new ways in various products, and this tends to expand the markets for these minerals. Some recent outstanding developments in applications of minerals are given in the following pages.The Andalusite GroupAmong the minerals that until recently were considered of scientific interest only, may be listed those of the andalusite group. This group is composed of the three minerals, andalusite, cyanite (or kyunite), and sillmanite, which are all forms of the compound Al2SiO5 (A1203, S1O2), and are therefore identical in chemical composition, but differ in physical properties,"

Mar 1, 1924

By R. E. Morgan, J. F. Barkley

"INTRODUCTION In city smoke-abatement work it is customary to require approval of the sizing of fuel-burning equipment. This is to insure that, with reasonable attention, the equipment can be operated essentially smokelessly, having such features as ample furnace volume and air supply. To answer the many inquiries that come to the Bureau of Mines as to what dimensions are acceptable and standard, the requirements of a number of smoke-abatement ordinances have been tabulated.CONCLUSIONSStudy of these tabulations shows that even after many years of fuel-burning practice and experience there is no common standard. Variations in the requirements for the same type of equipment under the same conditions of operation are great. This causes considerable difference in installation costs. Over-all costs being affected, the competitive positions of different types of fuel-burning equipment are also affected. It is apparent that there is a lack of information as to proper dimensions that is commonly accepted as authoritative.DISCUSSIONTable 1 gives the minimum furnace-setting heights required by various cities for mechanical underfeed stokers installed under H.R.T. boilers. Figure 1 shows a typical installation. The dimension given for each case is the distance from the dead plate of the stoker to bottom of boiler shell, unless otherwise noted. As shown in the table, different cities use different size-classification systems; it is not possible to make complete, exact, direct comparisons. Table la gives a comparison for various cities, showing the approximate percentage difference in H.R.T. furnace-setting heights required from those recommended by the Stoker Manufacturers' Association arbitrarily chosen to serve as a basis of comparison. The percentages are approxi¬mate because they were calculated as if all heights as given were measured from the dead plate of the stoker. In two cases a lower height is permitted, in a number of cases the height may be the same, and in a number of cases the height must be greater. The percentage increase goes to 100 in one case. Lack of uniformity is quite evident."

Mar 1, 1950