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By Olexandr Gydin

The evolution of grain and dislocation structures during cold deformation of the new steel LH800 of Salzgitter AG is investigated in the frame of this work. The main feature of this material is its ability to air-harden by carbon content of about 0.1%. The initial ferrite structure of the metal provides high plasticity at cold deformation and subsequent heat treatment increases tensile strength approximately two times. Described are results of in-situ tensile tests in the SEM. SEM and TEM analysis of grain and dislocation structures evolution in samples, which have been uniaxially deformed to certain strains, are carried out. After statistical evaluation of results the grain elongation against strain is determined. A microstructure of a deep drawn cup is analyzed by means of SEM. A quantitative evaluation of grain elongation on the different cup zones and comparison of these data with prediction results based on tensile tests are carried out.

Jan 1, 2009

By K. Dzieciol

The paper presents a study about three image correlation methods ?common cross-correlation, mutual information and phase-correlation ? applied to characterize microstructures reconstructed with X-ray tomography. It is shown that phase correlation is not only the fastest, but also the most sensitive method for detection of similar microstructure features, cavities in the present case. A new image correlation indicator is proposed, which takes into account both the phase shift and the amplitude of similar features in compared images. Some preprocessing aspects related to the tomographic reconstruction and filtering out of characteristic noise are also discussed.

Jan 1, 2009

By E. Salinas R.

This work is related with a whole characterization of cantera stone, to establish its characteristics that can give it an additional value for the reuse and reutilization of dust, slurries and small pieces of stone which can be treated as wastes. The obtained results reflects that the residues studied can be used as substitutes of feldspars in the production of pieces of ceramic, and also in the elaboration of paints for the same pieces according to the mixes that can be made with the variation of Na2O, CaO and K2O. According to the humidity proofs and specific gravity done, this material can be proposed as a soil improver into hydroponics systems, leading so an important alternative for food production in zones leaking of water. In the same way, it was found the possibility of use this material as a seal 3A in processes of asphalting of roads, highways and streets.

Jan 1, 2009

By C. M. F. Vieira

The main characteristics and physical and mechanical properties of clays from the county of Campos dos Goytacazes, located at the northern part of the State of Rio de Janeiro, Brazil, are presented. The characterization included mineralogical composition, chemical composition and particle size distribution. The properties related to water absorption, linear shrinkage and flexural rupture strength were obtained in samples that were prepared by 20 MPa uniaxial pressing and fired at 950 and 1100oC. The results showed that the clays are predominantly kaolinitic with high percentage of clay minerals. The kaolinitic structure associated with a small amount of fluxes confers a refractory behavior which makes difficult the sinterization and impairs the ceramic consolidation.

Jan 1, 2009

By David Cocke

Study of surface and subsurface interfacial chemistry of metallic and similar systems has its enormous technological importance. Copper, for example, is a common component of many alloys and bulk amorphous systems. It is being increasingly studied today because of its use for electronic interconnect systems where processing is done below 200 ºC. Since several types of copper oxides exist, and the degree of their formation is dependent on temperature, perhaps characterization by EDS-SEM depth profiling and EIS might delineate one type of oxide from another. In this paper, we described our work on transformation of copper oxides with temperature ranging from 70 to 350 °C and their characterization by SEM, EDS, and XRD. We also showed the use of the phase angle portion of the impedance as a means to identify the predominant structure and the transition through Cu3O2 between the predominant stable CuO and Cu2O.

Jan 1, 2009

By Sumantra Mandal

The hot deformed microstructure of the 15Cr-15Ni-2.2Mo-Ti modified austenitic stainless steel (commonly known as alloy D9) was investigated employing electron backscatter diffraction (EBSD). Hot compression tests were conducted in a Gleeble thermo-mechanical simulator at temperatures of 1173K-1373K (in steps of 100K) with a strain rate of 10 and 100 s-1 to different strains. Various kinds of deformation patterns were observed inside the deformed grains. These were inferred as the development of geometrically necessary boundaries or formation of parallel set of micro-bands. Recrystallized grains were partitioned from the deformed grains employing grain orientation spread approach. Extent of dynamic recrystallization (DRX) was found to be minimal at 1173K. DRX was predominantly found to happen at and above 1273K which increases with increase in strain. DRX nucleation and development mechanisms were discussed with respect to bulging of the parent grains and sub-grain rotation. Special emphasize is given on the role of annealing twins on DRX nucleation and subsequent expansion.

Jan 1, 2009

By Sergio N. Monteiro

From the leaves of the sisal plant (Agave sisilana) a relatively strong fiber can be extracted and is nowadays being investigated as a possible reinforcement for polymeric matrix composites. For this purpose, it is important to determine the critical length of the fiber with respect to the matrix to be reinforced. This has never been properly done for sisal fibers in polyester matrix. Therefore, this work characterized the critical length of sisal fibers, with different sizes, embedded in polyester capsules by means of pullout tests. The critical length obtained allowed the sisal fiber/polyester matrix interface shear stress to be calculated. The relevance of these values for polyester composites reinforcement with sisal fibers is discussed.

Jan 1, 2009

By Sergio N. Monteiro

Fibers extracted from the ramie plant have been traditionally used in textile and are now being considered as polymeric composite reinforcement owing to their superior strength. Recently the mechanical behavior of ramie fiber reinforced polyester composites was investigated but no significant improvement was found. Therefore, the objective of this work was to carry out a similar investigation by changing the type of polymeric matrix. Specimens with up to 30% in volume of ramie fibers incorporated into epoxy were bend-tested until fracture. The results showed a moderate improvement with a tendency of decreasing stress for higher amounts of ramie fibers due to the weak interface developed with the epoxy matrix.

Jan 1, 2009

By Denise Cristina de O. Nascimento

Natural lignocellulosic fibers are increasingly being used as polymeric matrix composite reinforcement owing to economical and environmental advantages as renewable and biodegradable materials. Among these, the piassava fiber extracted from a palm tree native of South America stands as one of the most rigid with a potential to be used as composite reinforcement. Therefore, the present work investigates the notch toughness behavior, by Izod impact tests, of epoxy composites reinforced with up to 40 % in volume of continuous and aligned piassava fibers. It was found that the incorporation of piassava fibers results in significant increase in the impact energy of the composite. Scanning electron microscopy analysis showed that the nature of the piassava fiber interface with the epoxy matrix is the major responsible for the superior toughness of the composite.

Jan 1, 2009

By S. Y. Tan

As CMOS devices are scaled down into nano-region, SiO2 dielectric is approaching its physical and electrical limits. High-k material has been investigated widely in recent years, and gate oxide take place growth oxide with Hf-based below 45nm gate length technology node has been shown. The phenomenon of interfacial property between bulk silicon and gate dielectric materials (HfO2 and HfSiO) was focused. A comparison of capacitance-voltage (C-V) characteristic of gate insulator was presented. Furthermore, the electrical property and thermal stability of high-k dielectric materials at various post deposit anneal (PDA) temperatures were established. The X-Ray diffraction technique was (XRD) utilized to analyze crystallization of the thin films, and the X-ray photoelectron spectroscopy (XPS) was applied for surface chemical bounding energy to identify the silicon and dielectric layers. Results show that HfSiO films have exhibited a superior performance on both thermal stability and electrical performance.

Jan 1, 2009

By Sugui Tian

By means of the T6 treatment, the measurement of creep curves and microstructure observation, the influence of T6 heat treatment on the microstructure and creep properties of Ti-6Al-4V alloy is investigated. Results show that the microstructure of the forged alloy consists of the banded-like a phase and networks b phase. After sub-temperture T6 treated, the microstructure of alloy consist of the block a phase and ?networks basket? structure. Under the conditions of the applied stress of 575 MPa at 4000C, the forged alloy displays a lower creep lifetimes, after T6 treated the creep lifetimes of the alloy is enhanced to 548 h from 66 h, which is attributed to the formation of the network basket structure in which the needle-like phase are dispersedly distributed. As creep goes on, the denser dislocations in the a phase are concentrated to occur the dynamic recrystallization for refining grain. which is a main reason of the alloy displaying a better creep lifetimes and plasticity. Thereinto, the creep mechanism of the forged alloy is thought to be the slip of the straight <a> and <a+c> dislocation are activated on the prismatic planes and pyramidal planes, while the creep mechanism of T6 treated alloy is that wave-like <a+c> dislocations are activated on the pyramidal planes.

Jan 1, 2009

By Sergio N. Monteiro

Polymer matrix composites have been applied in components such as helmets and shielding for which toughness is a major requirement. Natural fiber presents interfacial characteristics with polymeric matrices that favor a high impact energy absorption by the composite structure. The objective of this work was then to assess the Izod impact resistance of polymeric composites reinforced with different amounts, up to 30% in volume, of a promising high strength natural fiber from the Amazon region known as curaua. The results showed a remarkable increase in the notch toughness with the amount of incorporated curaua fibers. This can be attributed to a preferential debonding of the fiber/matrix interface, which contributes to an elevated absorbed energy.

Jan 1, 2009

By Sne?ana Devi

Mineralogy is a significant scientific discipline, essential in establishing the nature and the character of raw materials, regardless of whether they are monomineral or polymineral. Mineralogical characterization is very important, because its results give valuable information on features and nature of examined materials. Information&apos;s on mineralogical nature of mineral raw materials influence directly the quality assessment of a raw material, and thus the possibility of its use. The possibility of use of mineralogy in different industrial branches confirms constant activity of this scientific discipline. By use of methods within mineralogical analysis (optical microscopy, x-ray diffraction and others) data on mineral raw materials can be obtained as support in mineral raw materials quality assessment. Short description of results of mineralogical analysis of some mineral materials (granodiorite, dolomites, clay, refractory materials, slags and casting powders) in this paper shows the importance of its support to quality assessment and determine the possibilities of their use.

Jan 1, 2009

By F. Freme

Coal production in the United States in 2008 reached a record level of 1.06 Gt (1,171.5 million st), according to preliminary data from the U.S. Energy Information Administration (EIA) (Table 1). This is an increase of 2.2 percent, or 22.5 Mt (24.8 million st) above the 2007 level and 7.9 Mt (8.7 million st) above the prior record level set in 2006. Although coal production was higher in 2008, U.S. total coal consumption decreased in all sectors for the year. Coal consumption in the electric power sector in 2008 was lower by 0.3 percent, while coking coal consumption decreased by 2.8 percent and the other industrial sector declined by 3.7 percent. The commercial and institutional sector, that had been called the ?residential and commercial? sector prior to 2008, declined by 0.6 percent in 2008. It is the smallest of all the coal-consuming sectors. (Note: All percent-age change calculations are done at the short-tons level.) U.S. coal exports were significantly higher in 2008, while coal imports decreased during the year. Total coal stocks increased in 2008, as some consumers added to their stockpiles. The coal synfuel industry, which grew throughout most of this decade, disappeared from the scene due to the expiration of the available federal tax credits at the end of 2007. The decline in coal consumption during the year was the consequence of slowing domestic economic growth, particularly in the latter half of the year, combined with the weather conditions in 2008, resulting in lower demand for electricity. Preliminary data show that total generation in the electric power sector (electric utilities and independent power producers, including useful thermal output) in the U.S. decreased in 2008. Coal-based generation also decreased, resulting in a 3.2-Mt (3.5-mil-lion st) drop in coal consumed in the electric power sec-tor. Coal use in the non-electricity sector decreased by 3.3 percent to a level of 72.6 Mt (80.1 million st). The international coal markets in 2008 were the driv-

Jan 1, 2009

By Adam K. Smith

Over-exposure to noise remains a widespread, serious health hazard in the U.S. mining industry despite 25 years of regulation. Most other categories of illnesses and injuries associated with mining have improved, with the exception of hearing loss. In order to reduce cases of Noise Induced Hearing Loss (NIHL) in the mining industry, retrofit acoustic treatments and controls are being developed to subdue noise at the source. The Mine Safety and Health Administration (MSHA) coal noise sample data collected from 2000 to 2005 has determined that continuous mining machines rank first among all mining equipment whose operators exceed 100% noise dosage. The continuous mining machine conveyor, used to move coal from the cutting face to the rear of the machine, has been identified as a dominant noise source. A dual sprocket conveyor chain was tested as a potential solution. Sound power level measurements conducted at the Pittsburgh Research Laboratory (PRL) accredited reverberation chamber showed a 3 dB reduction in the A-weighted sound power level when the dual sprocket chain was implemented. Underground results show an 8-hour Time Weighted Average (TWA8 hrs) reduction a 3 dB for continuous mining machine operators. Utilizing this newly developed noise control, along with previously proven controls, provides continuous mining machine operators an opportunity to be within the MSHA-Permissible Exposure Limit (MSHA-PEL).

Jan 1, 2009

By Sergio N. Monteiro

Jute fabric obtained from discarded sackcloth is a promising low cost and post-used material being considered as reinforcement of polymeric matrix composites. In particular, the combination of this fabric with a recycled plastic constitutes an environmentally correct composite with both economical and environmental advantages. The present work investigates the toughness of recycled polyethylene composites reinforced with up to 40 wt% of post-used jute fabric extracted from discarded sackcloth. Standard Izod notched specimens were impact tested and the results showed an increase in toughness with the amount of jute fabric. Observation of the composite fracture by SEM revealed that the fabric weave, in spite of damages caused by the previous use of the sackcloth, act as an effective obstacle to crack propagation.

Jan 1, 2009

By Jewel Gomes

Produced water (PW) is salty water trapped in the reservoir rock and brought up along with oil or gas during production. It subsists under high pressures and temperatures, and usually contains hydrocarbons and metals. Therefore, it must be treated before being discharged to surface water. Different techniques are being used to treat PW through phase separations, system control and design, and chemical treatments. In this paper, we discuss our experimental results on treating PW through electrocoagulation (EC). The performance of EC was investigated for the reduction of chemical oxygen demand (COD) and metal ions. Effects of different electrodes, residence time, current density, and pH were also studied to optimize the treatment conditions. Different kinds of cleansing agents, such as lime and borax were used to break the buffering effect encountered during treatment. FTIR, SEM/EDS, and XRD were used to characterize the EC-floc and thus to elucidate removal mechanisms.

Jan 1, 2009

By Peter Zhang

The immediate roof at the test site consisted of laminated clay shale that is likely to be susceptible to weathering. With seasonal dry-wet cycles in the mine ventilation air, the roof in the intake air would deteriorate and lose integrity over time. In many instances, the weathering-prone roof would gradually scale off piece by piece between bolts and over the entry corners. In some long-term entries, roof weathering could develop up to 2-3 ft deep with columns of bolted roof hanging under the upper intact roof. If wire mesh is used, the roof bags down and reduces the entry height, and the weight of the bagged roof tends to pull the bolts out and poses a safety hazard. An effective measure is always sought to support this type of weak roof that is sensitive to moisture degradation. One solution is to seal the roof shortly after entry development to prevent moisture penetration so that roof integrity can be maintained for the long term. In this application, a polymer-based sealing material was tested in the Rockspring mine for weathering protection and reinforcement. The material is a one-component polymer powder for spray application onto the roof and rib. The sealant material is mixed with water in the spraying nozzle to apply to the roof and rib as a paste. The product sets within 5-10 minutes and forms a membrane as thin as about 1/8-in. The membrane will quickly develop tensile and bonding strength within minutes and completely cure within a few days. Through sealing, bonding and lateral reinforcement, the integrity of the weak roof can be maintained. The material has been tried in a long-term evaluation over several months in a set of main entries in the Rockspring mine owned and operated by Rockspring Development, Inc., affiliate of Foundation Coal. Preliminary evaluation has shown that the material is an effective and economical solution to ensuring the long-term stability of weathering-prone roof.

Jan 1, 2009

By John Ellenberger

The National Institute for Occupational Safety and Health (NIOSH) has collected pillar and span data at 34 stone mines in 10 states to develop pillar and roof span design guidelines for underground stone mines. Pillar, floor and roof conditions each contribute significantly to the overall mine stability. The roof may be stable for a century, or it may appear to be stable but fail with little warning. Clearly, an assessment of the mine roof is critical to the safety of these operations. However, up until now, the assessment of the mine roof came primarily from exposures in roof falls or portal areas. This provides only limited information, and a more proactive approach is needed to assess changing mine conditions. A separate effort was undertaken to examine the roof structure with the use of a borescope. Numerous physical and geologic roof structures were observed with a stratascope/borehole video camera. The objective of this work was to develop a technique of assigning numerical values to features seen within the mine roof and apply those values to formulate a roof stability evaluation. Such features as changes in color, grain size, and general lithologies are readily observed. Minor structures in the rock, fossils and fractures are also readily identified. Each feature may have a variable and site-specific impact on roof quality. A number of mines were visited and a series of holes were borescoped in each mine. The features identified in the roof were classified and potential for roof damage related to each feature was assessed. A process is presented that relates the structures and their locations to provide a numerical value, or roof quality index that can be used to assess roof stability.

Jan 1, 2009

By Slawomir Bock

One of the fundamental issues having a great influence on the safety of operations performed in underground mines is the support of workings which should assure their stability in a given geological setting and mining-technical conditions during the life of their use. The process of designing and planning support for roadways may use analytical and empirical, as well as numerical methods. In view of the rapid increase in the data processing capacity of computers and the development of more and more enhanced software for numerical modeling, it seems to be advantageous to use numerical methods in searching for design solutions ? especially in the case of non-typical mining and geological conditions and in cases that need to take into consideration a great number of factors. The assessment of rock mass quality is of basic significance in designing mine supports. Fractures, dividing the rock mass into blocks, have an essential influence on the stability of the rock mass and underground construction. This paper presents examples of the fundamental underground investigations on the rock mass conducted by the Department of Extraction Technologies and Mining Supports of the Central Mining Institute in Poland, such as: penetrometric tests, introscopic examination, laboratory testing of rock samples and ground penetrating radar. Moreover, this contribution also presents examples of applications of three-dimensional numerical modeling for the purposes of stress-strain analysis of the rock mass around mine workings and computer-aided support design by means of FLAC3D (developed by Itasca) and Cosmos/M (developed by Structural Research and Analysis Corporation).

Jan 1, 2009