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By Ryoma Fujiyoshi

In this article, the technologies of highly durable MgO-C bricks for the scrap impact zone and bottom blowing tuyere of converters are demonstrated. On the bases of our recent investigations, wear of scrap impact zone and bottom tuyere are explainable in terms of crack initiation and propagation. Theoretically, crack propagation in brittle material is regarded as generation of new crack surface area. It occurs when the elastic strain energy stored in the material exceeds the energy required to generate a new crack surface area. Since the overall energy consumed for crack propagation until fracture is evaluated by fracture energy, materials exhibiting high fracture energy can be regarded as materials with high fracture resistance. Therefore, two fracture energy-improving technologies for MgO-C bricks were developed. One is matrix reinforcement and the other is carbon bond enhancement. These technologies were applied to bricks for the scrap impact zone and bottom tuyere. As a result of commercial applications, notable decreases in wear rates were recognized for high fracture energy materials for the scrap impact zone and bottom blowing tuyere of converters.

Oct 30, 2017

By Ernesto Gustavo Maffia

En la actualidad, el moldeo por inyección es una tecnología muy utilizada en el procesamiento del plástico pues permite fabricar formas geométricas complejas. Para fabricar los moldes se utiliza ampliamente la aleación C17200 (Cu-2%Be), pero están en desarrollo algunas alternativas con aleaciones base cobre libres de berilio, que tienen valores de dureza por encima de los 30 Rockwell C y buena conductividad. Las aleaciones base de cobre, tipo CuNiSiCr son las más adecuadas como reemplazo. El siguiente trabajo trata del estudio y desarrollo del proceso de fabricación, por fusión, colado y conformado, de una aleación tipo CuNiSiCr de alta dureza y buena conductividad para ser utilizada en la fabricación de moldes de inyección para la industria del plástico. Los resultados preliminares de esta investigación demuestran que a través del aumento sistemático en el contenido de níquel y silicio se consigue un aumento de la dureza (>32 Rockwell C) y una aceptable conductividad eléctrica (˜25%IACS). El fenómeno segregación interfiere fuertemente en los tratamientos termomecánicos, pues se forma una segunda fase interdendrítica, de características frágiles, que genera fracturas en el conformado. Los resultados demuestran que la aplicación del recocido total y control de la temperatura durante la forja minimizan este problema.

Aug 7, 2018

By Haruki Inami, Takashi Ishida, Kazuhiro Ohara, Hiroyuki Imanari

The highly competitive business environment of the international metals industry is driving demand for more cost-effective operation of steel making facilities, rolling mills, and strip processing lines. Achieving stable operation is vital if the steel industry is to produce high-quality products constantly and productively. In recent years, advances in computer processing speeds, data acquisition rates, and data storage capacity have rapidly led to greater use of the new technologies of big data, analytics, the IoT, and AI by control system designers and process engineers, and the introduction of industrial applications. The “Smart Rolling Mill” solutions for hot strip mills have been developed by our group with the goal of achieving sophisticated, state of the art, and automated operation in steel rolling mills. The various solution engines improve process stability, increase the performance of mill equipment, and provide improved process control. These solution engines are based on extensive knowledge of the rolling process and the associated control systems. Two solution engines in particular are the diagnosis systems for rolling condition and for product quality that contribute to cost-effective operation and lower yield loss. This paper focuses on the diagnosis systems for rolling condition and for product quality in hot strip mills. Advanced information technologies using big data analytics and machine learning are applied to real-time data collected from the automation system that controls operation and the rolling process. We have developed diagnosis solutions for rolling condition and product quality utilizing predictive and clustering diagnosis. Predictive diagnosis prevents serious problems by detecting changes in the state of the plant or in the rolling condition. Clustering diagnosis classifies patterns of fluctuation in product quality trend charts, providing effective tuning guidance for improving product quality. This paper describes these applications with several examples.

Oct 1, 2019

By Zou Zhongpping

Under the new normal state, blast furnace outputneeds to be adapted to the market demand, however the limitation in blast furnace output has significant impact on blast furnace operation and is prone to cause inactive furnace hearth and higher fuel ratio. To address such problems, some practices to maintain stable and smooth operation of blast furnace in case of output limitation are proposed based on data analysis philosophy, which allows the blast flow and hence the top pressure to be determined based on the hot metal output, and adequate kinetic energy of blast supply can be assured by adjusting the tuyeres. Matching between the oxygen enrichment and the pulverized coal injection is also proposed based on theoretical flametemperature, and burden distribution cycle calculation method is proposed, whichoffersnew approach for analyzing the change in burden distribution pattern.

Oct 30, 2017

By Massimilinao Svetina

In 2010 Danieli & C. S.p.A. put into operation a new Pickling Tandem Mill in Cremona (Italy) at Acciaieria Arvedi, the last Pickling line coupled Tandem Cold Mill (PLTCM) in Europe. The plant was tailor-made to suit the specific requirements of this customer; a very broad range of sizes and grades (IF to AHSS as well as DP and TRIP1000) including ultra-thin hot band can be processed, achieving a total capacity of 1.6 Mt/y. The Danieli & C. S.p.A. Turboflo® process was selected because of its proven efficiency and ability to handle ultra-thin gauges at speeds exceeding 400 mpm in the pickling tanks. All the equipment, i.e. pickling section and rolling mills was provided with the last generation of Danieli market-oriented technologies. Danieli & C. S.p.A. - with the support of Arvedi and feedback from the field - is continuously improving its technical design solutions and optimizing plant operations.

Aug 16, 2017

By Paolo Demetlika

In this paper it is shown how the “Zero Operator” concept on the casting floor has been reached by adoption of a standard 6 axis industrial anthropomorphic robot coupled with the most innovative machine vision technology. This has been achieved by automating all the operations related to the ladle and tundish activities, including shroud manipulation, powder addition, ladle nozzle identification, nozzle opening by lancing, temperature measurement and chemical sampling. Q–Robot CAST family products are the result of the successful alliance between industrial robotics and the most advanced technology in process automation. This led, for each production area, to the introduction of flexible automation in dangerous places, even where some degree of human intervention is still necessary. By using anthropomorphic robots, human operators can be reassigned to safer environments. Furthermore, robots are suited to deal with repetitive and labor intensive tasks thus guaranteeing a high process quality.

Oct 30, 2017

By Breno Totti Maia

This work was a continuous and multidisciplinary development. Through studies of the blowing process and its parameters results, evolutions, improvements and adjustments were made on the lance’s hot face with Slagless® technology, as well in the process parameters and mitigating actions of the projection of materials out of the converter. The main results are the increase in the nozzle’s life with a “record mark” of 1785 heats, and water leakage occurrence in the cartridge decreased considerably reaching the mark of one year without any occurrence.

Oct 30, 2017

By Roberto Balarini Junior

Tribological behavior of Si3N4 balls sliding against Al2O3 discs in water was investigated by studying the influence of parameters such as initial surface roughness and circular axial run-out of the discs. The objective was to relate these parameters with the occurrence of the phenomenon known as ultra-low friction coefficient (ULFC), which is characterized by µ < 0.01, including the correlation with running-in duration. As a general trend, greater initial surface roughness and circular axial run-out resulted in greater running-in duration. In addition, it was verified that a mixed lubrication regime (hydrodynamic and boundary) is required to guarantee the occurrence of ULFC by comparing the calculated minimum film thickness with the composite roughness of the worn surfaces. Also, ICQ-OES analysis of the water after the tests indicated that a silicon concentration greater than 1.3 mg/l should be fundamental for the occurrence of µ < 0.01.

Jul 31, 2018

By Masakazu Iida

In this article, technologies of unburned Al2O3-MgO (UAM) refractories are demonstrated in terms of microstructure evolution. During operation, Mg2+ diffuses from MgO to Al2O3 through the liquid phase to form spinel (MgAl2O4) network. Molten slag tends to penetrate along the voids in the spinel network structure and spinel dissolves in the penetrated slag. Therefore, maintaining a high degree of spinel saturation in the penetrated molten slag is important. In order to achieve the condition described above, suppression of overall mass transfer through penetrated slag is effective. This is achievable by evolution of complicated spinel network structure with small pore diameter, which increases the flow resistance of molten slag. Thus, optimization of refractory composition and fabricating conditions, with the aim of creating on improved spinel network, is essential. The effectiveness of spinel network improvement was validated by commercial applications. According to the investigation of UAM brick after use, further densification due to heating under restrained conditions was recognized. Hence, it was concluded that the evolution of the spinel network structure in UAM refractories is essential technology needed to improve durability.

Oct 30, 2017

By Mario González Ramírez

The safe transport of sour gas requires steels with enhanced hydrogen induced cracking (HIC) resistance. Centerline segregation bands of high hardness microconstituents and non-metallic inclusions are the heterogeneities usually linked to HIC failures in pipeline steels. Full-scale production heats of a new low Mn, Nb microalloyed steel were produced by different steel mills aiming at the application in sour gas environments. The new alloy design provides both effective strengthening and control of sulphide inclusions. Coil microstructure consisted of fine grained ferrite with a small volume fraction of uniformly dispersed eutectoid aggregates. Most importantly the microstructure was uniform in both the longitudinal and transverse directions and exhibited exceptional consistency. Samples from this steel were submitted to HIC testing according to NACE standards TM0284-2003 without any sign of cracking. The results, so far, confirm that this new alloy design provides the unique opportunity to economically produce a high strength pipe steel grade with improved sour service resistance for the linepipe industry.

Aug 8, 2018

By Patrick E. Connell

During the ABM Conference of 2015 the latest design and process features of the new 3-roll RSB® generation were presented together with a unique Size Control System SCS® for a real time closed loop control to produce an extraordinary quality SBQ – day in, day out. In the past two years, Kocks has focused on improving the repeatability of the rolling process and developed technology to enhance the performance of its equipment. These developments include Fast Remote Control (FRC), Stands Adjustable Under Load (AUL) implementation of closed loop Size Control System (SCS), and finally a state of the art laser Gauge (4D Eagle) that pulls all of these developments into a complete package of quality. Gauges used in the past generally operated with the “shadow” measuring system. The latest gauge developments are based on the “light section” method. This method is more suitable to provide real time measurement parameters of the rolled bar. Placed close to the last rolling stand, the “light section” gauge is capable of measuring around the complete diameter with a clear definition of the bar stage in relation to the axes of the rolls. It is also capable of making these measurements using a very high measurement frequency. Following requirements of the market, requiring the highest gauge measuring frequencies which display the bar in the most accurate way even at the highest rolling speeds, the “4D Eagle” gauge was developed. This paper describes all the process features and parameters of this impressive and unique newly developed gauge as well as the other described technical improvements.

Oct 30, 2017

By Davidson Marcos de Oliveira, Antonio Adel dos Santos, Vicente Tadeu Buono

The benefits of using the controlled rolling process followed by accelerated cooling (TMCP), currently used in the main rolling mills in the world are already well known and metallurgically based. The need to obtain mechanical properties with a high degree of homogeneity means that in some situations the ends of the rolled material are discarded, negatively affecting the metallic yield of the process. Therefore, this work focused on the determination of the mechanical properties variation at the ends of thick plates processed by TMCP of steels for application in oil and gas pipelines, in order to map the extent of these differences and to correlate them with the microstructure obtained, the profiles of temperature and cooling rates in these regions. To perform the work, two slabs of the studied material were rolled, and the temperature profile was recorded along the plate in the controlled rolling and accelerated cooling processes. The ends of the material were sampled in sections at every 100 mm and subjected to tensile test, hardness and the Charpy V-notch impact test, as well as dilatometry and microstructure evaluations. For the used process conditions, the results indicated the formation of a banded microstructure, basically consisting of polygonal ferrite and bainite, occasionally containing small fractions of perlite. The mechanical properties in the top and the base were higher than the values found in the plate middle, justified by the microstructure found. The work allowed understanding the relationship between the mechanical properties, microstructures and process conditions at the ends, helping the team to improve the process in order to result in a high degree of homogeneity of the product and, thus, lead to optimization of the metallic yield.

Oct 1, 2019

By Jeremy Fletcher

In today’s world, the requirement of Steel Producers to revamp and modernize their blast furnaces on-time, safely and with the latest technology is paramount. In addition they must meet the detailed design, construction and safety legislation and regulations, which can be different for the various countries around the world. Siemens MT is renowned for its ability to perform Blast Furnace rebuilds, relines and modernisations within extremely tight time frames and in a safe manner. Modular Blast Furnace construction concepts have been perfected to minimise project duration and plant downtime for furnace rebuilds. Safety and certainty are the keys for success. Siemens MT are constantly introducing new technologies into the market place including cyclone gas cleaning and triple external cone gas scrubber, along with step changes in technology such as dry gas cleaning and dry slag granulation. The economic environment and the continuing requirement for improved environmental performance, drive many of these innovations. This paper describes some of the latest rebuild reference projects of Siemens MT, along with the latest technical innovations installed on these furnaces, and some of the construction methodology used for a safe and secure rebuild.

Aug 1, 2018

By Steven George Jansto

The hot ductility behavior of different microalloyed steel chemical compositions was examined simulating the thermal and strain conditions through the straightening or unbending section of the continuous casting machine. All samples were obtained from industrial slab casters ranging from 200 to 300 mm in slab thickness from steel mills throughout the world including China, Brazil, North America and Europe. The slabs were crack-free and hot rolled into prime quality products. No laboratory heats were tested. Although these microalloyed steels exhibit inherently lower hot ductility behavior, as measured by percent reduction in area at elevated temperature, these steels still exhibit sufficient ductility to satisfactorily meet the unbending stress and strain gradients existing in the straightening section of most casters. The majority of the published hot ductility data, as measured by % reduction in area (%RA), were based on laboratory heats and hence, are inaccurate in accessing the propensity for slab cracking on an industrial caster. This situation then results in invalid conclusions for different chemistries. This research has determined the minimum required %RA for crack-free casting is significantly lower than results based upon previously published laboratory generated data. For example, the literature quotes 40% RA minimum for Nb-bearing steels when in fact as low as 10% minimum RA is more than sufficient to assure crack-free casting based upon the extensive testing and analysis performed in this study. Instead of %RA, the measurement of strain energy has been introduced to evaluate hot ductility behavior. It is concluded that strain energy is a better measure of hot ductility behaviour than %RA. There is considerable value in the evaluation of the hot stress and strain curves, process metallurgy parameters and their relationship to slab quality instead of just basing hot ductility decisions on simple %RA measurements.

Aug 16, 2017

By Dagoberto Brandão Santos, Kairo de Barros Guimarães, Túlio Magno Füzessy de Melo

The effect of the cooling conditions on the microstructure and hardness of a Dual Phase hot-rolled steel 800 MPa strength was investigated. Simulations of the cooling conditions using a dilatometer were carried out from samples of a hot rolled coil with variations of the intermediary temperature from 620 to 740°C, isothermal holding time between 1 and 10 s and coiling temperature between 50 and 400°C. In addition, two CCT (Continuous Cooling Transformation) diagrams were developed to evaluate the effect of the isothermal holding time on the phase transformations of the remaining austenite. It was observed that the intermediary temperature has a strong influence on the kinetics of the phase transformation, as well as the isothermal holding time influences the amount of ferrite formed and, consequently, the final microstructure and hardness of the material. The coiling temperature did not cause significant changes in the amount and morphology of the ferrite, but a gradual replacement of martensite with bainite was observed, which, in addition to the self-tempering effect, contributed to the hardness reduction.

Oct 1, 2019

By Liao Jianfeng

The Baosteel Zhanjiang 5,050m3 blast furnaces have been built with highly independent integration and innovation technologies and represented the state of the art of the world’s huge BFs. The proper of BF1 and BF2 is designed with long-campaign technology; both BFs share the same set of stockhouse, water and PCI systems; the BCQS serial-hopper no-bell top, TRT and blower are all local equipment as applied; four top-combustion stoves systems are matched; the BFG is cleaned by fully dry process; and the automation control system for the main process is self integrated. The BFs have been started up and performing with sound indicators. Their smooth proceedings symbolize China’s huge blast furnace ironmaking technology ascending a new high.

Oct 30, 2017

By Fábio Dian Murari, Antônio Adel dos Santos

The effect of reheating temperature of slabs on the precipitates dissolution and mechanical properties of Ti-Nb microalloyed steel was investigated in pilot scale. It was verified, by means of transmission electron microscopy, a significant decrease in precipitates formed during the solidification of the steel as the reheating temperature increased from 1100°C to 1200°C. No significant changes in size and shape of the precipitates were observed with further temperature increase up to 1280°C. In line with the precipitates dissolution behavior, an increase in strength was observed with the elevation of the reheating temperature up to 1200°C, due in part to the reprecipitation of fine Nb-rich precipitates during the hot rolling. At 1200°C the presence of deformed ferrite on the microstructure contributed to the additional increase in strength. After reheating above 1200°C up to 1280°C, a decrease in strength of the rolled plates was noticed. This effect has been credited to the absence of deformed ferrite grains and also to a small increase in the low angle grain boundaries size. The results were in agreement with Thermo-Calc and Dictra simulations.

Oct 1, 2019

By Douglas Glenn Stalheim

The demands for improved mechanical properties in hot rolled long products are increasing as the expectations of global Standards and construction designer’s increase. Cost constraints limit the excessive use of expensive alloys to meet these expectations. In addition, depending on the mill, equipment can limit what can be realized to meet the increasing expectations. The most effective way to meet the increasing expectations for improved mechanical properties of optimum strength and ductility is through producing steel with as fine as possible uniform cross sectional grain size in the “as-rolled” condition. The best solution to the development of this fine and uniform cross sectional grain size is to develop a cost effective alloy design coupled with proper metallurgical process control implemented into an existing mill’s equipment capability and layout. In other words, properly bringing together alloy, metallurgy, process control and existing equipment capabilities to develop an optimum product that can meet the increasing demands of the construction designer. This paper is designed to give a solid understanding of the production and metallurgical requirements to achieve a grain size in “as-rolled” long products that is as fine as possible within the limitations of the process and production parameters of the individual plant.

Jul 30, 2018

By Milan Terčelj, Matej Drobne, Urška Klančnik, Peter Fajfar

The study of oxidation behavior of High Chromium Steel material used for surface layer of work rolls was carried out. Specimens taken directly from the roll were subjected to thermal fatigue in the temperature range between room temperature and 500 °C up to 700 °C by using thermo-mechanical simulator Gleeble 1500D. Our observation was focused on the impact of oxidation as a principal mechanism of degradation of the roll’s surface layer - mainly on the characteristics of oxidation propagation in relation to the test temperature and microstructure constituents characteristics of the material. Oxidation is considerably accelerated by certain characteristics of eutectic and primary carbides, i.e. their size (area), composition, morphology, orientation regarding to the water-cooled surface, etc. In the presented paper selected cases where emphasized oxidation takes place are investigated, analyzed and explained. Obtained results thus represent a contribution to explanation of conditions which lead to acceleration of oxidation behavior that in turn can lead to chipping or even early spalling of material from the roll surface layer.

Oct 1, 2019

By Ananda Moreira Vaz Ourique de Avila

High and intermediate temperature fuel cells (FC) are power generators characterized by high efficiency and their use in cogeneration systems. The single fuel cells are connected in series by the use of interconnects to form a fuel cell stack. Ferritic stainless steels have been used in the making of high and intermediate temperature operation solid oxide fuel cells interconnects. However, at high temperatures, on the order of 700-8500C, these steels can present significant oxidation and degradation processes, promoting increased electrical resistivity and corrosion losses that result in contamination of the electrodes and reducing the performance and the useful life of the FC. Intensive R&D activities have been made to minimize these problems and the use of composite coatings on metallic substrate has been considered. This paper evaluates the use of coatings of copper and nickel, with particles of La2O3, Y2O3, CeO2, LaCrO3 and doped chromites applied on ferritic stainless steels AISI 430, AISI 441 and Crofer22APU produced by electrodeposition. The produced samples were evaluated by microscopy techniques, gravimetric analysis and by electrothermal characterization. The most significant results were obtained with chromites coatings (LaCrO3 pure, mono- and multiple-doped) showing the combination of the best features of metal coatings, substrates and ceramic particles with semiconductor properties.

Aug 7, 2018