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By Welland L. Ott, Hans J. Rumland

The Falconbridge Dominicana laboratory receives samples from all parts of the operation. Ore, metal and oil samples are taken by operating departments, gas and water samples by the laboratory staff. Physical sample preparation is essentially standard and produces comminuted samples for wet-chemical analysis and X-ray fluorescence analysis (XRF). T he main operating sections of the laboratory are described indicating in each case the type of instrumentation and method used, sample types analysed and comments on problems experienced. Emphasis is given to the sample preparation and X-ray sections especially with regard to the difficulties caused by our heterogenous ore material, calibration of the instrument and operational malfunctions. General problems related to our remote location and the tropical climate are discussed. Limited statistics on instrument availability, and stability, accuracy, precision, etc., are given.

Jan 1, 1979

By J G. Dunn, S M. Thurgate, A C. Chamberlain, P Franzmann, M Jeffrey, L J. Warren, G E. Poinen, T Williams

Gold has always fascinated mankind. From Tutankhamen's mask to the huge nuggets that have been found in the Australian outback, gold has quickened the pulse and fevered the eye. But in recent years, governments around the western world have shown a singular lack of interest in research into gold processing, with many programs being cut. There are some notable exceptions, fortunately, and this paper summarizes a large research effort that is well supported by the Australian government and the Australian gold industry. The AJ Parker Cooperative Research Centre for Hydrometallurgy is an unincorporated joint venture between the CSIRO Division of Minerals, Murdoch University, Curtin University of Technology and the Western Australian Department of Minerals and Energy. The Australian Mineral Industry Research Association (AMIRA) is the Parker Centre's broker for generic R&D contracts with industry. Each of the partners makes available staff, students and equipment to further the work of the Parker Centre, and the Australian Government provides additional funding. The Parker Centre is nearly five years old and has grown spectacularly in that time. There are now about 30 full-time-equivalents of effort from 50 scientists and engineers, as well as about 40 postgraduate and honours students. The fundamentals of the key operations in hydrometallurgy are studied in three programs: leaching (which includes pretreatment by roasting etc), precipitation (or crystallisation), and surface processes (which includes solid/liquid separation, adsorption, solvent extraction, etc). A large part of the Parker Centre's R&D is directed towards gold processing technology. In Australia, a dramatic increase in gold production, from about 30 to nearly 300 tonnes per year (1977-1997), has been made possible largely as a result of a brilliant metallurgical innovation, the carbon-in-pulp process. However, falling head grades eg 2.56 to 1.84 g(Au)/t over the last 10 years, and environmental concerns, are squeezing profit margins. There is increasing pressure to reduce costs, and the Parker Centre program is focussed on providing the scientific understanding required to do this. A selection of research highlights will be given, to indicate the depth and breadth of the R&D at the Parker Centre.

Jan 1, 1997

By K. O. Johnson

Contaminant transport of mine and mill tailings is controlled by the hydrologic flow regime and the geochemical mobility of the contaminants. Contaminant' mobility is primarily determined by chemical reactions occurring within an interface zone between the tailings and soil The large geochemical differences between tailings and groundwater create a disequilibrium in the groundwater with respect to the soils when seepage from tailings enters the groundwater. Precipitation and dissolution reactions involving the major chemistry occur to return the perturbed system to chemical equilibrium between groundwater and minerals. Retardation of trace elements depends upon the chemical character of the groundwater and the adsorption substrates. In the case of uranium mill tailings, the mobility of contaminants is controlled primarily by precipitation/dissolution reactions which neutralize the pH, modify the Eh (redox potential), and produce highly adsorptive substrate for retardation of trace elements.

Jan 1, 1988

By James H. Nulty, Joseph S. Roti

Wetting agents used for heap leach gold applications would appear to have technical merit in aiding in recovering higher levels of precious metal. Many questions, however, remain as to whether they will function in practice, on what type of ore are they effective and if there are any negative affects associated with their use. A series of experiments are conducted at Bateman Labs, Sparks, Nevada, to determine under what conditions reagents of this type are useful. Carbon kinetics test work was also performed to determine if there are negative aspects associated with carbon loading with the use of these treatment chemicals. This paper outlines the results of these research evaluations, the general chemistry associated with action of wetting agents on leach ores and future work which is planned to further determine the viability of these products in the mining industry.

Jan 1, 1998

By P. M. May, J. S. Solis, G. T. Hefter

Chemical speciation plays a critical role in many areas of gold processing. These include the formation of HCN in plant liquors, interference by copper in the extraction efficiency of gold, the recovery of adsorbed gold, and the behaviour of plant effluents in the environment. Thermodynamic modelling provides a cost-efficient method of rationalizing and even predicting of chemical behaviour. Unfortunately, because thermodynamic data for cyanide complexes are of poor quality and few are known under hydrometallurgical conditions. Such models are currently of limited use. This paper describes recent work on the thermodynamics of cyanide complexes of a range of metal ions. Data will be presented on the stabilities and enthal­pies (heats) and entropies of formation of a variety of metal ion species determined by potentiometry and calorimetry. Particular emphasis will be placed on the Cu(I)/CN- system.

Jan 1, 1995

By Jeffery S. Thompson

In this report, the effect of catalytic amounts of activators on gold dissolution in clear solutions with gold disks and with slur­ries of gold ores is presented. Activators are nitrogen and sulfur aromatic heterocyclic compounds, which catalyze the gold dis­solution reaction in cyanide and other lixiviant solutions. Gold dissolu!ion studies in clear solutions indicate that the catalyst must bmd to the gold surface to catalyze the dissolution reac­tion. A concentration dependence for activation is observed· the optimum catalyst concentration depends on choice of activtor lixiviant concentration, and solution agitation. Nitrogen and sul fur aromatic heterocycles catalyze gold dissolution in slurries of gold ores with cyanide and other lixiviants. The typical proce­dures of agitated leach and rolling bottles were used to evaluate gold leaching rates. Activation has been demonstrated with a variety of ore types.

Jan 1, 1996

By Paul Hamilton, Brian Jones

Traditionally,relatively large gold mines in developing countries have relied on imported process plant engineering, design, pro­ject management and advisory skills. In 1995, there was a significant departure from this in Zimbabwe, when a locally based engineering company under­took and completed the construction of a one hundred and twen­ty thousand tonne per month capacity gold extraction plant for the treatment of sands/slimes residues integrated with run of mine ore. This paper describes the challenges of designing, construct­ing and commissioning a Carbon in Leach (CIL) gold extraction plant in a developing country, and discusses the various con­straints associated with it. In addition, the paper reviews the application of technology which is innovative to Zimbabwe, including the use of dewatering cyclone clusters, and two and a half tonne capacity elution/electrowinning convection units.

Jan 1, 1996

By David G. Abbott, Frank Coluccio

This paper will discuss the construction of nearly 165 m (540 ft) of 3.5. m (138 in) o.d. reinforced concrete pipe to replace an existing utilidor under the Duwamish River in Seattle, Wash. The project required that two 27.4 m (90 ft) deep shafts be installed for use as jacking and reception shafts during the tunneling operation, and permanent vaults once completed. Soil conditions to be excavated consisted of soft saturated sand and silt with a 21.3 m (70 ft) water head. This required the shafts to be constructed using ground freezing techniques and the tunnel installed by pipe jacking, using a Mechanical Earth Pressure Counter Balance (MEPCB) slurry shield. The original utilidor was constructed between 1924 and 1925, and has since been deliberately flooded because it is considered to be structurally unsound.

Jan 1, 1995

By Mary Korpi

So now you ask, Where are the transcripts? The well-organized co-chairs, Harry and Mary, did their job. Doug Halbe was active in the audience encouraging people to speak up and keeping everything moving along. So where are they? Were the comments so provocative that they could not be written? Was the profanity so bad (even for miners!) that it couldn't be repeated? It appears that at the first session of the Plant Operators' Symposium a glitch occurred with the recording equipment. Thanks go to everyone who did comment during the dis- cussion period. The People I session had a lot of lively conversation and we are sorry that it will not be printed. However, there is now another reason to hold the plant operators' sessions on a regular basis! Another People session can and will be held in the future.

Jan 1, 1998

Rinker Materials Corporation (Rinker) operates construction aggregate operations in 15 states across the US. Thirteen of those operations are located in Florida, where Rinker produced approximately 40 million tons of aggregates in 2002. Because the deposits being mined in Florida are shallow sedimentary deposits of limestone and natural sand, with the deepest being approximately 75 feet deep, abundant acreage is mined annually. Rinker mines about 300 acres/year in Florida alone, and because there are so many wetlands and complete avoidance is nearly impossible, there are also wetland impacts. Thus, there is ample need for reclamation and mitigation, which presents an opportunity to involve local school groups with the planting and monitoring of these various projects. Rinker has successfully worked with a half dozen or so schools on these projects, involving students from grade school through college, with surprising success and outstanding results.

Jan 1, 2004

By Patrick R. Taylor

The hydrometallurgical fundamentals review did not arrive in time for publication in the May issue. Papers presented at the SME Annual Meeting, in Phoenix, AZ were available as preprints. The EPD Congress 1992 from The Metallurgical Society had several papers related to hydrometallurgy. Minerals Engineering 1992 was published in Minerals Engineering and contains several papers related to hydrometallurgy. In addition, a conference was held to honor Ernie Peters. The proceedings contains a large number of hydrometallurgy papers. Precious metals Gold extraction in the potassium cyanide-primene JMT sulfate-Xylene system was studied by Caravaca and Alguacil (Hydrometallurgy). Adams, Friedl and Wagner presented results on the mechanism of gold cyanide adsorption onto activated carbon (Hydrometallurgy). Adams also studied the adsorption of silver cyanide and used an IR method to evaluate adsorbed aurocyanide species on activated carbon (Hydrometallurgy).

Jan 1, 1993

By Fathi Habashi

ION FLOTATION was introduced by F. Sebba in 1959. This technique permits the recovery of metal ions from solution through the introduction of an appropriate cationic or anionic surface-active agent into the solution. The surface-active agent, called a collector, is added in stoichiometric amounts in relation to the metal content of the solution. It reacts with the metal ion to form an insoluble soap, and is levitated to the surface by gentle bubbling of air to form a foam which collapses into an insoluble scum. The optimum conditions for the ion flotation with soaps of C10-16, fatty acids are shown in Table 15-1. Baarson and Ray (1965) found that once the metal was completely precipitated as the hydroxide, as little as one hundredth the stoichiometric amount of the collector was required to cause complete flotation of the [ ]

Jan 1, 1970

Continuous improvement has become the watchword of the 1990s for most iron-ore-processing operations. In many instances, this improvement has been achieved through stepwise application of advanced control techniques to optimize operations. The benefits of this stepwise application have been great. However, they have fallen short of the full potential offered by the prospect of overall plant optimization. The successful integration of computers, instrumentation and control software throughout a plant promises to deliver an additional 3% to 5% of productivity in even the best-run plants (Herbst and Bascur, 1984). LKAB is Europe's largest iron-ore producer and a leading implementer of advanced control technology. In the late 1980s, LKAB introduced advanced control in its concentrator at Kiruna, Sweden to improve plant performance through higher productivity, greater efficiency and lower costs at each processing step.

Jan 1, 1995

By L. Buckingham

Barrick Goldstrike Mines Inc. has embarked on a continuous improvement effort to ensure that Barrick Gold Corporation will retain its lead in the gold industry in years to come. The continuous improvement initiative is based on careful mapping of the key levers associated with each activity of business. The individual levers are then evaluated to determine their potential to affect the profitability and safety of the operation. The most promising are diagnosed for root causes. These root causes are then addressed to enhance benefits. Through a structured approach of mapping, brainstorming, evaluating and instigating change with follow up measurement and reporting; Barrick Goldstrike is anticipating an increase in throughput at the autoclave facility of 10% with little or no capital expenditure. The resultant approach to Continuous Improvement will be utilized throughout the Goldstrike facility and then throughout Barrick's world-wide operations.

Jan 1, 2002

By Pat Gochnour, Jim V. Rouse

Advances in the design and construction of heap­leach pads and process plants have greatly reduced. the potential for accidental releases of process olut1on. While workers in the field, and regulatory agencies such as the EPA have long recognized that the potential effects of any spills would be short term in nature due to cyanide attenuation and degradation (Engineering-Science, September, 1986, Pyrih, 1990, Rouse and Pyrih, 198, Rouse and Pyrih, 1991 ), unfortunately the general pubhc has held a perception that such a spill would be an environmental catastrophe. Few factual data on actual accidental releases have been available to dispel such a concept. Such data now exist and shoul? be disseminated to show that prompt response, using a combination of chemical oxidation, natural attenuation, and enhanced biodegradation of cyanide, can limit the effects of such rare releases, in both time and space.

Jan 1, 1992

By Deepak Malhotra, Sean Armstrong, Linda Baltich

The economic profitability of any mineral company is dependent upon maximizing mineral recoveries while minimizing costs. The effectiveness of any strategy to meet this objective is dependent upon firstly obtaining quantitative information concerning the steady-state metallurgical balance of the plant, and secondly, how efficiently this information is used to improve/optimize plant performance. This two-step approach can be designated as a "plant audit." Plant audits on a routine basis can be very expensive and time-consuming. Most plants have reduced staffs to cut costs. The remaining staff has to spend time to solve production/operation problems, thereby leaving limited resources (i.e., people, time, and money), for plant auditing. This paper briefly reviews plant auditing categories, and a systematic approach to auditing which has been successfully used at several operations. An example illustrating the use of this approach in gold operations is discussed in this paper.

Jan 1, 1992

By James Y. Oldshue, Paul M. Kubera

Most coillillercial processing applications employing mixers in various types of slurry systems are continuous flow. These applications may also be multiple stage, with the stage number varying anywhere from two or three to ten or more. Two questions that usually come up at the beginning of any proposed pilot plant study are (1) can the pilot plant unit be operated batch-wise, and the results extrapolated both on the basis of scale and fluid motion to the full-scale tank which will be continuous-flow (and probably multi-stage), or (2) does the pilot plant need to be operated in a continuous-flow fashion, and if so, does the exact number of tanks/stages that are proposed for the plant need to be used in the pilot plant? We will consider these possibilities in sequence and present the principles involved in running some of the various pilot-plant arrangements.

Jan 1, 1992

By Matthew J. Hrebar

A comparison of hydraulic shovels (HS) versus front-end loaders (FEL) is commonly made when an excavator with some degree of mobility and medium reach is required. These applications are often found in hard rock open pit and surface coal mining applications, among others. The purpose of this paper is to present a comparative economic study of the two excavators. Production data was collected from both HS and FEL manufacturers as well as operating mines. Availability, operating costs, and estimated operating life were gathered from operating mines, while capital costs were obtained from manufacturers. The data was limited to studies and operations which included both types of mid-size excavators. The economic study is followed by a discussion of other factors considered by mine operators in excavator selection. The study was originally made for a presentation at the 23rd Intermountain Minerals Conference at Vail, CO.

Jan 1, 1992

By A. N. Papadopoulos

The life cycle assessment and the performance of pine fence posts treated with water borne preservatives and oils after 18 years exposure in ground contact were examined in this study. Vacuum CCB treated fence posts were subsequently treated at their lowest part (ground contact) with creosote using the open hot and cold tank process and exposed under warm dry temperate climatic conditions in Greece. After 18 years exposure, samples were taken from the above ground contact, top, middle and ground contact and tested for toughness using a Denison single blow impact bending test machine. There was no significant reduction of toughness in any of these zones. Chemical analysis of the residual CCB of unexposed and exposed samples by ICP showed that copper and chromium losses were insignificant while boron losses were significant (more than 50% of the initial content). This was attributed to an effect of creosote treatment.

Jan 1, 2008

By D. R. East

Recent experiences within certain sectors of the international mining industry suggest an underestimation of the environmental risk associated with the design of mine waste management facilities. These experiences show that the technical and managerial challenge of responsible mine waste management is not always fully appreciated. Unfortunately, the image of the mining industry's environmental performance is negatively impacted by a relatively few number of failures. This negative view overrides the many positive contributions made by the majority of mining companies. The fact that these failures continue to occur to this day in both developed and developing countries is indeed remarkable, and indicates a degree of risk-taking approaching unacceptable levels. The design requirements for tailing storage facilities are, in many cases, more demanding than those of conventional water dams, because seepage of fluids which contain dissolved metals may pose a greater threat than the mere loss of water.

Jan 1, 1999