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By Bianca Harue Ueharar

Os métodos de pré-concentração, dentre os quais podemos destacar o gravimétrico, magnético, peneiramento e ore sorting, eliminam grande parte da massa a ser alimentada na usina, o que consequentemente impacta nas características do material que irá alimentar a moagem. Assim, este trabalho busca fazer uma comparação no desgaste de circuitos de moagem com e sem a pré-concentração em minérios de baixo teor. Através de ensaios laboratoriais de AI de Bond, foi obtido o valor da abrasividade e com isso é possível estimar o consumo de material de desgaste e revestimento dos circuitos. O estudo indica que o resultado é benéfico pois, eliminando-se mais da metade da massa, o desgaste dos equipamentos decai de forma proporcional, com um ganho maior no caso do ensaio em que a abrasividade do material pré-concentrado é menor. Portanto, do ponto de vista econômico, além da pré-concentração ter baixo custo operacional, a redução nos gastos com revestimento e bolas na moagem diminui de forma muito significativa.

Oct 30, 2017

By Miguel Barron

Recently, a new lance design for BOF steelmaking has been proposed in the literature. This lance, in addition to six peripheral inclined supersonic nozzles, contains a vertical centered nozzle whose oxygen flow is independent from the main oxygen supply. The above authors affirm that their lance maximizes the droplet generation without causing spitting. In this work, the performance of a lance with four peripheral nozzles and one vertical centered nozzle is numerically modeled by means of Computational Fluid Dynamics software. Transient two dimensional computer simulations were carried out considering two phases, namely molten steel and gaseous oxygen. Numerical results confirm that bath agitation and droplet generation are enhanced as a result of the vertical centered nozzle, however a proper performance of this lance, related to a conventional one, strongly depends on the Mach number of the oxygen jets and the lance height.

Jan 1, 2008

By P. L. Swanson

Over a recent 20-month observation period, the U.S. Bureau of Mines obtained seismogram records from a single vertical-component, short-period seismometer installed at the surface of a metal mine in northern Idaho. The seismic events were analyzed for local (Richter) magnitude (M), time of occurrence, location, and relation to rock bursting and production blasting. Approximately 150 seismic events with -0.5 = M = 2.9 were located within the mine, yielding a b value (slope of the logarithm of the number of events with magnitude greater than M versus M) of 0.5. Event locations were constrained using a dense underground array of high-frequency accelerometers. Twenty of the surface-recorded events, with 0.5 = M = 2.9, were associated with rock bursts that produced damage requiring at least 1/2 day of cleanup and/or repair. Other possibly hazardous rock bursts, with magnitudes as small as -1.1, were numerous but were not associated with significant structural damage. Approximately 60 pct of the seismic events with M > -0.5 and 75 pct of damaging rock bursts occurred within 45 min of blasting. Estimates of characteristic rupture dimensions for rock bursts with -1.1 = M = 2.9, based on a conventional dislocation shear-slip model of failure, range from 3 to 300 m.

Jan 1, 2010

By A. Ghadyani

This investigation was undertaken to assess the possibility of ash and sulfur removal by microbial action of high sulfur-content coal. Thiobacillus ferrooxidans and Thiobacillus thiooxidans have been used for biodesulfurization of coal. Feed samples were provided from Tabas coal mine located in Yazd province, Iran. The sample contained 28.80% ash and 2.30% sulfur. Flotation tests were implemented to optimize the effective parameters in these cells which were constant during bio-flotation tests. According to the results, obtained from various tests using Taguchi orthogonal array design (L27), the values of optimized parameters were pH at 7, 1000 g/t gas oil as a collector, 10% solid content, 15 min conditioning time, 100 g/t MIBC as a frother and 800 rev/min rotor speed. Bio-flotation tests are carried out by means of laboratory double discharge cell and mesophilic bacteria as depressant reagent using above mentioned optimized parameters. The bio-flotation experiments were conducted based on a Taguchi orthogonal array design (L9) with four variables (bacteria type, bacteria count, rotor speed of mixer and bio-conditioning time). The collected data was analyzed by using DX7.0, Minitab14.0 and WinRobust1.02 softwares for evaluation the effect of each parameter on the optimization criteria. Considering the highest combustible recovery and the lowest ash and sulfur content, the value of optimized bacteria type, bacteria count, rotor speed of mixer and bio-conditioning time were Thiobacillus ferrooxidans, 5×107 cells/g(coal), 100 rev/min and 20 min respectively. Under this condition, ash and sulfur content and combustible recovery were predicted 12.39%, 2.08% and 82.03% respectively.

Sep 1, 2012

By E. W. Dean

A previous report of the Bureau of Mines* has supplied data for the physical and chemical properties of samples of crude petroleum produced in the eastern fields of the United States. It was issued as a preliminary chapter of a bulletin which is to cover the results of a survey of the entire country. The present report is a second preliminary chapter including figures that are available for the producing fields of the Rocky Mountain district. Work is being continued. with a series of samples from the States of Kansas and Oklahoma which will be described in a third preliminary chapter, to appear at a subsequent date. Acknowledgments. The obtaining of samples was rendered possible through the courtesy of representatives of a number of producing and refining companies operating in the Rocky Mountain district. The Bureau hereby acknowledges its appreciation of the hearty spirit of cooperation that was universally encountered.

Jan 1, 1921

By T. N. Alexandrova

Results of mineralogical-technological research of carbonaceous rocks of Kimkansky precious metal occurrence are presented, on their basis new typemorphic natural and technological microelement associations were revealed using mathematical statistics methods. Keywords: carbonaceous rocks, processing, microelements, flotation, statistical criteria

Sep 1, 2012

By W. B. Braden

This paper presents a suitable method for predicting gas-free oil viscosities at temperatures up to 500F knowing only the API gravity of the oil at 60F and the viscosity of the oil measured at any relatively low temperature. The API pravity and the one viscosity value are used as parameters to determine the slope of a straight line on the ASTM slanaord viscosity-temperature chart. Then, knowing the slope of the line and one point on the line, the vrscosities at higher temperatures can be determined. The line slope correlations were developed at I00 and 210F since viscosity data are frequently measured at these temperatures. A procedure is given for predicting line slopes from measurements at other tetnperatures. A nomogram is furnished for solving the relationship. The correlation has been evaluated at temperatures up to 5OOF for oils varyzng in gravity from 10 to 33 " API. The correiution is applicable only to Newtonian fluids. Comparison at 500F of true viscosities and those predicted from values at 100F shows an average deviation of 3.0 per cent (maximum deviation of 6.0 per cent). Predictions from the values at 21 0F for the same oils how an average deviation of 1.5 per cent (maximum deviation of 3.4 per cent). INTRODUCTION Correlations have been developed by Beal' and by Chew and Connally' for predicting viscosities of gas-saturated oils at reservoir conditions. Each of these correlations requires a knowledge of the solution gas-oil ratio and the viscosity of the gas-free oil at the reservoir temperature. For temperatures below 350F, measurements of the gas-free oil viscosities can be made easily using commercially available equipment. In thermal recovery processes, however, reservoir temperatures well in excess of 350F are encountered. Viscosity measurements at such conditions are more difficult and time consuming and require modification of existing equipment or the construction of new equipment. Measurements are further complicated by the difficulty of handling highly viscous oils associated with thermal recovery processes. Therefore, it is desirable to have a correlation which allows accurate prediction of viscosities at high temperatures. A commonly used technique for predicting viscosities at high temperatures is to measure the viscosities at two lower temperatures, plot the values on ASTM standard viscosity-temperature charts and extrapolate to the temperatures desired. If either of the values is slightly in error, the extrapolated value can be significantly in error. To justify an extrapolation, three points are actually necessary. This procedure can consume much time, particularly with heavy oils. Considering the cost of viscosity measurements, it would be desirable to eliminate the need for direct measurements by having correlations which would allow viscosity predictions from other physical or chemical properties. Beal1 investigated the possibility of correlating viscosity with oil gravity at temperatures from 100 to 220F. While showing that a general relationship exists, he also found significant deviations. It is possible that correlations will be developed based on oil composition as more information becomes available. While not eliminating the need for viscosity rneasurements, the method presented herein requires that only one viscosity measurement be made. The API gravity must also be known. The theory is based on the fact that the viscosity of paraffins (high gravity) changes less with temperature than does the viscosity of naph-thenes or aromatics (low gravity). The gravity. therefore, is used as a parameter to determine the slope of a straight line on the ASTM standard viscosity-temperature charts. The correlation is applicable only to Newtonian oils, and deviations due to thermal decomposition and nonhomo-geneity cannot be predicted. Oils containing additives have not been evaluated. PROCEDURE Fifteen oils were used in developing the correlation; eight were crudes and seven were processed oils. Oil gravities varied from 9.9" API (naphthene base) to 32.7' API (paraffin base). The temperature range studied was 81 to 516F. Each oil used had a minimum of three viscosity measurements and each plotted essentially as a straight line on the ASTM charts. In all, 91 viscosity measurements were used in the correlation. Saybolt, rolling ball and capillary tube viscometers were used for the measurements. Viscosity data for Samples 1, 2, 4, 7, 10, 11 and 14 were obtained in Texaco, Inc. laboratories. The data for Samples 3, 5, 6, 8, 9, 12 and 15 were from Fortsch and Wilson,3 and data for Sample 13 were from Dean and Lane.' All data points used in the correlation are plotted in Fig. 1. It is seen that some of the viscosity values deviated slightly from the straight-line plots at the higher temperatures. Properties of the oils after exposure to the

Jan 1, 1967

By Angel Rafael Arce Chilque

Este trabalho tem por objetivo estudar a relação da escória (coproduto da siderurgia) com a lama (rejeito da mineração de ferro), visando a utilização da mistura destes como insumo na construção civil particularmente na confecção de tijolos, mitigando impactos ambientais gerados pela extração de argila. O estudo envolveu a realização de ensaios de caracterização química e granulométrica da escória, lama e argila, compactação e modelagem da mistura, queima, absorção de água, cálculo de porosidade aparente e características geométricas dos tijolos confeccionados e determinação de resistência à compressão dos mesmos. Os resultados mostraram que não existe uma relação simples entre a resistência a compressão e a porosidade, indicando com isto que outros fatores devem ser considerados no controle da resistência à compressão.

Aug 8, 2018

By I. H. Gundiler

Although cyanidation has been universally applied in the processing of gold and silver ores, the search for less toxic alternatives continues. Difficulties encountered in processing ores containing oxidized copper minerals and the inherently slow kinetics of cyanidation have generated a renewed interest in thiosulfate leaching. This process, as well as the catalytic effects of copper ion, were well recognized and widely applied towards the end of the past century. In this study, the effects of copper, ammonia, and thiosulfate concentrations on gold dissolution were investigated using the rotating disk technique. Extraction of gold and silver from an oxidized copper-bearing ore was also studied utilizing a statistical experimental design, and these results were displayed in the form of contour plots.

Jan 1, 1993

By Gautam Chandra Mondal

An attempt has been made to carry out qualitative assessment of mine water discharges from the different mines of West Bokaro Coalfields of Hazaribag district of Jharkhand, India. A total of 33 mine water samples were analyzed for pH, electrical conductivity (EC), major cations (Ca, Mg, Na, K), major anions (HCO3, SO4, Cl, NO3), and heavy metals (Fe, Mn, Cu, Zn, Pb, Cr, Ni, Co, As). The hydrochemical data has been evaluated in terms of major ion chemistry, solute acquisition processes and suitability of mine water for domestic, industrial and irrigation uses. The pH of the analyzed mine waters varies from 5.27?8.43 indicating acidic to alkaline nature of the water. The electrical conductivity (EC) values varied from 276 µScm-1 to 1598 µScm-1 for measured samples and spatial differences between the EC values reflects the wide variation in lithology, surface activities and hydrological regime prevailing in the region. The anion chemistry of the analyzed water samples shows the dominance of SO4 and HCO3 with a minor contribution from Cl, NO3 and F. The observed high values of sulphate in the mine water of the area may be attributed to the oxidative weathering of pyrites. On average chloride is contributing 5% of the total anionic balance (TZ-). Fluoride and nitrate have low concentrations and on average contributing <2% the total anions. The cation chemistry indicates that 79% of the samples are Ca>Mg>Na>K, while the 6% belong to Ca>Na>Mg>K and 1% of Ca>Mg>K>Na. Weathering of rock forming minerals and cation exchange processes normally control the levels of these cations. Concentrations of some heavy metals (Fe, Mn, Ni, Cr) are found to be well above the prescribed permissible levels recommended for the drinking water. The water quality assessment for drinking purposes indicates that most of the mine water having high TDS, total hardness (TH) and sulphate concentrations. This suggests that mine water of the study area is not suitable for direct use in drinking and domestic purposes and needs a proper treatment before its utilization. The assessment of water for irrigation uses show that the water is good to permissible quality and can be used for irrigation uses. However, high values of salinity, %Na, SAR, RSC and Mg-hazard at certain sites restrict its suitability for agriculture uses. Keywords: mine water; ion chemistry; quality assessment; West Bokaro coalfields

Sep 1, 2012

By S. E. Jackson, L. J. Cabri

Quantitative determination of gold at sub-ppm concentrations in sulphide minerals is an important component of deportment studies for sulphide-gold deposits. Laser Ablation Inductively Coupled Mass Spectrometry (LA-ICP-MS) analysis is preferred for this application because it rapidly and cost-effectively provides spatially resolved (<20 pm), low ppb concentration data for gold and other elements in mineral grains. Recent advances in LA-ICP-MS analysis include the development and application of elemental mapping. Raw signals from multiple line scans or lines-of-spots are deconvoluted and calibrated to generate elemental maps which provide detailed information on spatial variations of gold and other elements within and between grains.

Jan 1, 2011

By M. Rhodes

The Sukari project, which is owned by Centamin Egypt Ltd, is located in southern Egypt, 770 km south of Cairo but close to the Red Sea. The project is the first new gold development in Egypt and was commissioned in the middle of 2009. In 2007, Centamin purchased the CIL plant from the Kori Kollo mine in Bolivia. This plant was originally designed to treat 6.5 Mtpa of oxide ore. The Sukari deposit contains an oxide zone close to surface with a thick zone of mixed oxide and sulphides below this. The sulphides contain relatively coarse pyrite and arsenopyrite with fine <10 µm gold inclusions. Eventually, the sulphide ore will be mined from underground. Metplant Engineering Pty Ltd, a subsidiary of Bateman Engineering Pty Ltd was contracted to design modifications and additions to the Kori Kollo plant to enable it to treat the Sukari ores. The plant was designed to treat the three ore types in stages. Throughput was set to 4 Mtpa, dueto Sukari ore being harder, at a head grade of 1.7 g/t to produce 200 000 oz of gold. The oxide circuit was based on the use of the Kori Kollo plant and the difference with mixed ore was that the oxide circuit would treat flotation tailings rather than ore. This circuit has a leach capacity of 26 000 m3 and residence time of 24 hrs The main feature of the upgraded mixed ore plant was the addition of a flotation circuit to produce a concentrate which would be reground and treated in a separate leach and elution circuit. Ore is crushed in a gyratory crusher and the comminution circuit uses a conventional SABC producing a product with a P80 of 150 microns. The throughput of 580 tph of oxide ore and 500tph of mixed ore was set to match the mills from Kori Kollo, with the addition of the pebble crusher to accommodate the more competent Sukari ore. The flotation circuit comprises a single rougher circuit to maximize recovery. The concentrate is thickened prior to regrinding which is carried out in a tower mill and two SMD mills operating in series. The final product, with a P80 of 12 microns, from the regrind circuit is leached in a CIL circuit with a total capacity of 2 550 m3. Gold is recovered through a conventional pressure Zadra circuit. Tailings from both circuits report to separate tailings thickeners and are pumped to a tailings storage facility. The circuit is designed to maximize the recovery of water. The project lies in one of the driest deserts in the world and a feature of the operation is the use of sea water from the Red Sea. This water is pumped 25 km from the coast.

Jan 1, 2009

By Ricardo Thomé da Cruz

Na produção de aços é essencial garantir maior durabilidade do material refratário em panelas siderúrgicas. A formação de um revestimento protetor (“coating”) de silicato dicálcico (C2S) em tijolos dolomíticos em contato com escórias básicas é fundamental ao aumento da vida útil dos mesmos. As temperaturas solidus e liquidus do C2S alfa puro são de aproximadamente 1.464°C e 2.154°C. Assim sendo, é esperada uma alta fração de sólido nas temperaturas de refino do aço. No entanto, a presença de óxidos como Al2O3, FeO e a fluorita (CaF2) na escória podem acelerar a dissolução do coating pela formação de fases de menor temperatura de fusão. A fim de melhor compreender esse processo, foram preparadas amostras de diferentes composições de fluorita + C2S na temperatura de 1.600°C. Os resultados foram analisados com o auxilio do software FactSage (simulação termodinâmica). Especificamente, foi estudada a influência da formação de fases e da temperatura de formação das mesmas, as quais levam a fusão do coating. Os dados de simulação foram validados através de ensaios em forno de laboratório.

Jul 30, 2018

By Mariana Xavier Milagre

As tensões residuais são geradas, sobre um material em equilíbrio, após a deformação plástica não uniforme causada por cargas mecânicas, térmicas ou mudanças de fase. Falhas estruturais podem ocorrer por uma combinação dos efeitos das tensões de serviço e das tensões residuais o que torna importante a medição e avaliação de como estas afetam as propriedades mecânicas dos materiais. Neste trabalho investigaram-se os valores médios das tensões residuais da fase austenítica de amostras de aço inoxidável duplex UNS S32304 por técnica de difração de raios-x. Acompanhou-se o comportamento do plano 420 com radiação CuKa (?= 1,5419 A ) em difratometro de geometria Bragg-Brentano. As amostras foram tratadas a 600°C com tempos de encharque de 10 minutos, 20 minutos e 8 horas em atmosfera ambiente e resfriamento ao ar e água do mar. Os resultados foram analisados pelo método do sen²? e indicam que as variações microestruturais e térmicas, relacionadas aos diferentes tratamentos, influenciam o valor médio das tensões residuais da fase em estudo.

Aug 8, 2018

A comparison of gold, platinum and sulfide ion selective electrodes was made in this investigation for determination of Eh in solutions containing sulfide ions as a model system. The comparison was made in terms of the accuracy of the measured response, response time, pH dependence, and reproducibility of measurement. In addition, the sensitivity of each electrode towards changes in sulfide ion concentration was measured in terms of the change in measured Eh per decade change in concentration of sulfide ions. On the basis of a detailed investigation of the electrode processes occurring at the surface of gold and platinum electrodes, it was postulated that within the pH range investigated these electrodes respond to changes in the hydrosulfide ion, HS-, concentration in solution. In comparison, the sulfide ion selective electrode is known to respond to changes in the sulfide ion, S-, activity in solution. Although the potentials measured with gold and platinum electrodes were mixed potentials, pretreatment procedures can be used to obtain a signal suitable for process control. For control of sulfide ions in flotation pulps, the use of a gold electrode pretreated at 1.0 V with respect to a standard hydrogen electrode is recommended.

Jan 1, 1990

By Evandro Moraes da Gama

Os solos lateríticos, formados pela ação de intempéries e alteração das rochas como itabirito e suas variações, geram um solo onde sua composição mineralógica, características e granulometria favorecem a produção de um ligante pozolânico quando processado através da tecnologia de calcinação flash. A retirada desses solos para explotação do minério de ferro se faz necessária formando os conhecidos depósitos de estéreis. A tecnologia de calcinação flash (PI 9809941-8) permite transformação desses solos em ligante de alta resistência denominado de metacaulim flash. Esse produto, quando tratado com tecnologia adequada, é transformado no ligante denominado de Metakflex (PI 0604142-6). Nesse trabalho faz-se uma descrição da planta piloto integrada de calcinação de estéreis argilosos, rejeitos e lamas com capacidade de produção de 200 kg/h de Metakflex. A utilização da calcinação flash para o aumento da superfície específica de reatividade de minerais e para a redução da perda ao fogo de minérios de ferro pobres é apresentada. Finalmente, são mostrados resultados preliminares da utilização do aglomerante Metakflex para pelotamento.

Aug 1, 2018

By N. Hamlef

In this study, the effects of heat treatment on phase formation and surface morphology of the Cr-Pt coated system are investigated using X-ray diffraction and electron microscopy techniques. The CrPt andCr4Pt (Cr3Pt - A15 type) phases were formed after heat treatment of the coated samples. Heat treating at 1000°C renders a distinct island coating morphology that is non-continuous in nature. A diffusional model is proposed for this coated system with regards to the surface morphology formation after heat treatment.

Jan 1, 2014

By C Bellia, A Maldonado, S Strong, H Baxter

This paper discusses the technical and cost benefits of alternative data collection techniques used to collect lithological information, obtain laboratory testing samples and perform in situ testing. A comparison between diamond coring and sonic coring techniques is made using data from a recent geotechnical investigation for a final pit slope cut-back. The impacts of the coring method on laboratory strength testing results, material character testing and, ultimately, the mass strength parameters and subsequent slope design adopted are compared. The sonic coring method was chosen out of necessity and enabled the collection of tube samples of a clay unit of interest as well as bulk samples for material character and geochemical testing. The sonic coring generated unexpected degradation of clastic units, while cohesive clay-dominated units were recovered well. The likelihood that disturbance due to the coring method would result in lower than expected triaxial strength results was recognised ahead of time, with surplus samples collected and single-stage triaxial strength testing undertaken. This testing compared favourably with historic three-stage testing, where sample degradation occurred during the later stages. Material character testing of fine-grained, clay-dominated units was comparable with historic diamond core testing, while grain size estimates for more clastic units tended to be finer than previous results. The use of sonic coring over non-cored methods enabled the collection of material texture data, geotechnical properties and a full suite of geochemical analyses. This provided a comprehensive understanding of the lithological and geotechnical character of the rock and soil mass. A high-confidence geotechnical model was developed. The end result was the development of a slope design that was more aggressive than was previously designed (5&#176; steeper inter-ramp angle), which has proven to be appropriate to the conditions following excavation. Overall, sonic coring was a cost-effective means of obtaining additional geotechnical data for the site.CITATION:Baxter, H, Bellia, C, Maldonado, A and Strong, S, 2015. Case study assessing alternative data collection techniques and analysis methods to assist with geotechnical slope design, in Proceedings Iron Ore 2015, pp 419–428 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 13, 2015

By A. Vishwakarma, V. Himanshu, K. Dey

Underground mining is the most feasible method after extinction of shallow depth ore deposits. Longhole stoping method is the most technically advanced method for the faster excavation. In this method, the holes are drilled in the form of ring pattern and explosives are used for the rock breakage. During blasting, the explosive energy sometimes also breaks the non-ore material. The non-ore material gets included in the extracted ore and enhances the ore dilution. Few uncontrollable factors which affects the ore dilution are ore body characteristics, rock quality, insitu stress condition etc. Apart from uncontrollable factors, explosive energy and blast design also plays an immense role in ore dilution. In the blasting practice, the purpose is to effectively utilise the explosive energy for rock breakage. The optimum delay is required so that the blast holes attain adequate free face before the blasting. This paper deals with the optimisation of blast design parameters to reduce ore dilution in underground hard rock mining having narrow vein. The study was carried out using numerical simulation. The explicit dynamics based modeller of Ansys was used for this purpose. The parametric variations in the models were done to optimise the parameters. The burden has been optimised first by varying the width of the narrow vein. The blasts of a ring consisting of single hole were conducted in the model by varying the width of the narrow vein. The damage contour under different parametric variations were analysed. The experimental trial has been also carried out at Zawar Group of Mine, Rajasthan, India. The optimum parameter was decided based on the result of experimental trial and numerical simulation model. The output of the model shows that optimum burden for 3.5 m narrow vein width is 1.12 m and for 1.0 m, it is 1.54 m. This shows that the optimised burden is higher in the vein having lesser width as compared to the greater width. The presence of joints/changed media/interface (between the sidewall and narrow vein) is the major reason behind this. The wave gets reflected back very fast on coming in contact with joints in a 1.0 m narrow vein as compared to a 4.0 m narrow vein. This will quickly convert the compressive wave into tensile wave giving rise to tensile slabbing. Hence proper utilisation of explosive energy will take place for the breakage of rock mass when the width of the narrow vein is smaller. The burden obtained from the experimental trial and numerical simulation models is less than 2.0 %. Hence the numerical simulation based approach can be used for the assessment of the optimum burden for ring blasting in narrow vein under different geomining conditions. This helped in reducing ore dilution and maximization of ore recovery. In the future, empirical relationships may be developed by considering different geological discontinuity, the strength of the rock mass and explosive parameters.

Jan 1, 2024

By R. H. Harrison, D. R. Douslin

The thermodynamic properties H - H° , (H - H° ) /T , S - Sideal , S - S° Fide al F - F° , (F F° ) /T , and activity coefficient Y for perfluorocyclobutane were calculated as functions of temperatures ( 115.22 ° to 350 ° C) and molal density (0.75 to 6.5 moles / liter ) . Improved analytical and graphical correlating techniques are described .

Jan 1, 1964