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By R. L. Crosby

The effect of indium on the solid solubility of calcium and of silicon in magnesium was studied using metallographic, X-ray diffraction, and electrical resistivity techniques. The addition of 2 weight-percent or more of indium reduced the solid solubility of calcium in magnesium by forming a compound containing indium and calcium. Indium additions have no perceptible effect on the solid solubility of silicon in magnesium.

Jan 1, 1963

Improve the reliability and accuracy of subsurface images using constrained tomography with enhanced ray-tracing capabilities. Background Geophysical tomography is a technique for imaging the structure of a rock mass using seismic or radio waves, in the same way that medical CAT scans image human tissue using X-rays. Tomography has found numerous practical applications related to mining, including lithologic and structural characterization, fracture detection and fluid monitoring, void detection, and evaluation of stress state and integrity of mine structures. Problems Two fundamental problems have largely prevented geophysical tomography from enjoying the tremendous success achieved by medical tomography. The first is a consequence of practical limitations on the placement of sources and receivers of wave energy: ideal resolution can be attained only when the region being imaged is entirely surrounded by sources and receivers, so that it is crossed by rays traveling in all possible directions. When such coverage is impossible or impractical, the inversion becomes underdetermined: there id not enough information in the measured data to provide a mathematically unique solution. The second major problem in geophysical tomography is the necessity for detailed ray tracing. Commercial software, as well as previous U.S. Bureau of Mines (USBM) software, employs a ray-shooting algorithm that may be unable to model some ray paths when velocity contrasts are larger than about 100%. These ?shadow zones" result in loss of data and degradation of reconstructed images.

Jan 1, 1994

By A. Wahab Khair

"This paper deals with the description of the capabilities of a unique rotary coal cutting simulator which has been designed and fabricated at West Virginia University. It operates under the simulated mining conditions with in-situ stresses (horizontal and vertical stresses) being applied to a coal block of 18 in. x 15 in . x 6 in located in a suitably designed confining chamber. Cutting drum rotation can be varied from 1 to 40 rpm with the capability of stopping the drum after a predetermined number of rotations. Tests can be performed with four different bit angles, 15, 30, 45 and 60 degrees . A maximum of seven bits could be used in seven different orbits. Various cutting depths up to a maximum of 4 in. is possible.Monitoring devices constitute, Linear Variable Differential Transformers (LVDTs), pressure transducers, cascade Impactors, flow meters, flow controls and drum cutting speed. LVDTs are used to monitor the displacement of the coal block as well as the depth of cut. Pressure transducers are used to monitor the changes in pressure, both due to the thrust and due, to the intermittent cutting nature of the rotary cutting. Flow controls will be used to run the drum at a set rpm between 1 and 40 and to provide a different rate of advance. All the above mentioned devices can be operated and monitored by a fully automated control system. Six-stage cascade impactors are used to determine the mass distribution of dust along the rotation path of the drum. The fracture size, shape and Intensity can be studied by optical microscopy and the dust entrainment by using high speed photography.This equipment will basically be used to study the fracture mechanism in coal, associated with operating and in-situ parameters and further relate It to dust generation and entrainment In underground coal mines."

Jan 1, 1988

By Robert L. Marovelli

The thermal conductivities of six rocks were measured by the transient line source method over the temperature range of -850 to 1,500° F. Close-fitting ceramic probes were used in 0.065-inch-diameter holes drilled through 5-to 6-inch-thick rock specimens. Taconite, granite, quartzite, and basalt were used in the tests. The method yields absolute data and is applicable to both laboratory and in situ measurements.

Jan 1, 1965

By R. E. Stiles

The modified perchloric--EDTA method devised by the Bureau of Mines for the determination of copper in high-grade samples gives results that are more precise and more accurate than those from the classical sulfuric-iodometric method. Although the perchloric--EDTA method is more costly than the conventional method, the savings in time alone largely offsets this difference. Specifically, the modifications wade in the more conventional procedure comprise (1) use of perchloric acid instead of sulfuric acid for dissolution of copper minerals, (2) precipitation of copper as copper sulfide from dilute perchloric acid solution, (3) wet oxidation and dissolution of the precipitated copper sulfide, (4) use of larger amounts of indicator than those employed in the Schwarzenbach method of titrating low-tenor copper solutions with disodium ethylenedinitri10-tetraacetate and murexide indicator, and (5) use of refrigeration to partially stabilize aqueous solutions of the indicator.

Jan 1, 1966

By J. A. Organiscak

Enclosed cabs are a primary means of reducing the silica dust exposure of equipment operators at surface mines. The National Institute for Occupational Safety and Health (NIOSH) has investigated various factor effects on enclosed cab air filtration system performance. Factors experimen­tally investigated were intake filter efficiency, intake air leakage, intake filter loading (filter flow resistance), recirculation filter use and wind velocity effects on cab penetra­tion (inside to outside cab concentration ratio). Adding an intake pressurizer fan to the filtration system was also investigated. Results indicate that the intake filter efficiency and recirculation filter were the two most influential factors on cab penetration .Use of a recirculation filter significantly reduced cab penetration over the intake air filter by itself due to the multiplicable filtration of the cab interior air. Cab penetration was also affected to a lesser extent by intake filter loading and air leakage. Adding an intake pressurizer fan notably increased intake airflow and cab pressure while providing only minor changes to cab penetration.

Jan 1, 2008

By Ryan G. Wade, Mark K. Larson

Researchers at the National Institute for Occupational Safety and Health (NIOSH) are studying the time-dependent response of rock stressed along weakness planes. The objective is to improve mine safety by reducing the number of roof falls that cause injuries and fatalities to miners. Researchers conducted direct-shear tests on mudstone overcored from a coal mine roof. Results showed frictional strength weakens with displacement along the shearing planes. Results of direct-shear creep tests also showed time-dependent deformation. Test measurements were compared to classical analytical models. Results suggest that risk of roof collapse may be decreased through layout and support design to reduce creep rates and thus slow progression toward failure.

By Oliver Bowles

"The American Consul at Guatemala City reports that the Guatemala Marble Mining Company is preparing to operate a marble quarry about 13 miles from the railroad station of Zacapa, which station is a little over 100 miles from Puerto Barrios, the nearest port from which the product may be shipped. The deposit is extensive, and though somewhat broken up in places, great quantities of sound marble are available. It is claimed that the marble is equal in quality to the best product of the Italian Carrara quarries.Access to the quarry by rail is obtained by a spur track of the International Railways of Central America (Ferrocarril Internacional de Centro America) from Marmol, 3 miles south of Zacapa. This spur is about 5 miles long and terminates at the foot of the mountains. A double-track incline cable-way 2000 feet in length has been constructed to bring the marble down the mountain. From the top of the incline to the quarry there is a railway six miles in length over which the rock will be hauled by two side-geared Shay locomotives."

Mar 1, 1920

By G. R. Palmer

The Bureau of mines evaluated the elution of uranyl carbonate from a strong base resin with a mixed carbonate eluant in a fluidized system. The system consisted of a multiple-compartment ion-exchange (MCIX) elution column with a continuous flow of solution, except for short periods when the resin increments were withdrawn. The exchange of uranyl carbonate from the mill-loaded strong base resin with an eluant composed of 1.0 [M] NaaCOs plus 1.0 [M] NH4HCO3 was studied. The effects of solution flow rate, aqueous-to-resin flow ratio, column diameter, compartment height, initial resin concentration, and column length were examined. The experimental data indicate that for the eluant examined, a resin residence time of 240 minutes is necessary to attain 90-percent elution efficiency. Also provided is a technique for sizing an elution MCIX column form pilot plant experimental data.

Jan 1, 1979

By Raymond M. Stateham

Microseismic noise rates and slope movements were measured in an unstable area along the north wall of the Tripp-Veteran pit, Kennecott Copper Corp., Ruth, Nev. Low-noise, wide-band microseismic geophones were located at various points in the wall, and the change in distance across open fractures, resulting from instability, was determined by repeated measurements between fixed points set on each side of the fractures. The microseismic noise rate increased and decreased with corresponding increases and decreases in the rate at which the fractures opened. The microseismic noise rates and changes in width of the fractures show excellent agreement, and the two types of measurements complement each other in monitoring the progress of pit wall failure.

Jan 1, 1971

By D. K. Dysinger

In this U.S. Bureau of Mines study, neodymium metal of 99.8 pct purity was prepared by electrolysis of Nd203 salts dissolved in a molten fluoride electrolyte. The metal was electrowon in a molten state at current efficiencies of 50 to 60 pct. Oxygen and carbon were the major impurities detected in the product. During operation of the small-scale laboratory cell, a number of technical problems including anode effect, low oxide solubility in the electrolyte, high neodymium metal solubility, reactivity of the metal with the cell materials, and back reaction of the metal with the anode gases were encountered. Approaches to improve cell operation and prospects for commercial adoption of the electrolytic production of neodymium metal are discussed.

Jan 1, 2010

By M. B. Shirts

Bench-scale studies were made on a reductive hydrometallurgical procedure to convert chalcopyrite flotation concentrate to copper metal or a readily leachable sulfide. Reductive conversion of chalcopyrite and dissolution of iron and sulfur were accomplished in hydrochloric or sulfuric acid solution by the addition of metallic copper, iron, or lead. Use of metallic copper as the reductant enabled extraction of 95 and 46 percent of the iron and sulfur, respectively. The products were ferrous iron, hydrogen sulfide, and a copper sulfide. Use of metallic iron or lead as the reductant enabled extraction of 95 percent of both the iron and sulfur. The products obtained with metallic iron or lead were ferrous iron, hydrogen sulfide, and metallic copper.

Jan 1, 1974

By Liming Yuan

Three-dimensional computational fluid dynamics (CFD) modeling is conducted to simulate spontaneous heating in a large-scale coal chamber with a forced ventilation system. Spontaneous heating is modeled as the low-temperature oxidation of coal using kinetic data obtained from previous laboratory-scale spontaneous heating studies. Heat generated from coal oxidation is dissipated by convection and conduction, while oxygen and oxidation products are transported by convection and diffusion. The water vapor transfer and the effect of heat of wetting are not modeled. The CFD model is validated by comparing simulation results with test results from U.S. Bureau of Mines experiments conducted in the coal chamber. The model predicts lower temperatures in the early stage but agrees well on the induction time for spontaneous heating. The effects of airflow rate and order of reaction on the spontaneous heating process are also examined. The calibrated CFD model is found to be useful for predicting the induction time for spontaneous heating in underground coal mines.

Jan 1, 2009

By W. W. Weller

Heat-capacity measurements of sodium dimolybdate (Na2Mo207) and sodium ditungstate (Na2W207) were conducted over the temperature range from 51° to 298° K. The entropies of the two compounds at 298.15° K were calculated from the heat-capacity values and were used, in conjunction with other entropy data, to evaluate the entropies of formation of the compounds from their constituent elements and oxides.

Jan 1, 1963

By R. V. Ramani, K. Bode

"IntroductionIn part 1 of this paper, the results of the experimental work in a wind tunnel under controlled conditions were presented. To understand the spatial and temporal behaviour of airborne dust under mine conditions, experiments were performed in the Lake Lynn Experimental Mine of the US Bureau of Mines. The mine airway experiments were designed to study the variations of ambient concentrations along the length of an airway, and the deposition rates and deposition velocities in an airway cross section. Other objectives of the study were to investigate the spatial and temporal behaviour of airborne dust with regard to air velocity and particle density, the size distribution of the airborne dust cloud as it travels in the airway, and the size distribution of the dust particles deposited along the airway. Other objectives of the study were to compare wind tunnel results with In-Mine results, whenever appropriate.Experimental ProcedureLocationA complete description of the Lake Lynn Laboratory Mine of the US Bureau of Mines (USBM) can be found in the US Bureau of Mines Information Circular 8911 (Mattes et al., 1983). This mine provides excellent facilities for dust experiments. The airway dimensions are similar to those of a coal mine airway. The mine has a drift (D Drift, see Figure 1) that extends almost 500 meters without interconnecting airways, stoppings, or bends. The D drift measures approximately 6m in width and 2,25m in height.The Lake Lynn Laboratory Mine· is ventilated by a variable speed, 75 kW (100 hp), 28,3 m3/s (60 000 cfm) blower fan installed on the top of the ventilation shaft. Air velocities of 1, 1,3 and 1,8 m/s, respectively, could be obtained in the D Drift. However, the temperature changes at the surface can cause small variations in air quantities and velocities underground. The low background dust level in the mine reduces the problem of sample contamination from other sources of dust. Extended periods of uninterrupted data collection can also be scheduled. Mine airway parameters which are important for the analysis include the dimensions of the airway and the ventilation data such as the air velocity, and the pressure loss in the drift. All these data were acquired during altimeter surveys which were conducted prior to each of the experiments."

Dec 1, 1995

Develop a curved ray geotomographic program with constraints to counteract non-uniqueness in order to improve the reliability of seismic tomographic imaging of geological structure in mining regions. Background Seismic tomography provides a two-dimensional image (tomographic reconstruction) of the distribution of the seismic velocity in geologic structures using measured travel times of seismic waves crossing the area. It can provide a more complete representation of features be¬tween boreholes than other crosshole processing methods that measure only average properties or borehole logging methods that measure properties only near each borehole. Seismic tomography has many mining applications. They include locating geologic structures of contrasting seismic velocity, detecting fractured regions where the seismic velocity is low, and monitoring solution injected above the water table where the increase in saturation increases the seismic velocity. Thus, tomographic imaging techniques show great promise for detecting and locating geologic hazards that affect the productivity, safety, and environment of mining operations.

Jan 1, 1992

By Howard E. Parkinson

A brief description is given of various Bureau of Mines research activities that have begun since July 1974 and are not being reported on by others at the Third West Virginia University (WVU) Conference on Coal Mine Electrotechnology. An essential feature of the various projects is that they are pragmatic. The projects are applied research and are carried out both by the Bureau in-house research group and by other research groups through contract research. Projects have been directed toward wired-type communications with a special effort to modify the wired systems so as to be more effectively used. The projects are in three groups: Pager phone systems, trolley line phone systems, and guided-wire wireless communications. Also, a brief sketch is given of research that is essential for further developments in mine communications. From the early results of these various projects, the Bureau has good reason to project that there will be improved performance of existing communication systems and that communications will be extended to other individuals working in areas that are excluded from present mine communication systems.

Provide an effective method for "soft" soldering aluminum and aluminum alloys using conventional tin-lead solder alloys and flukes. The Problem In the past, it was virtually impossible to solder aluminum and aluminum alloys using standard tin-lead soldering systems (solder and flux) due to the presence of an aluminum oxide surface film which forms instantly on aluminum and aluminum alloys when these are exposed to air. The tenacious and stable oxide film enables aluminum-base materials to maintain their bright luster. But the film also prevents the required wetting and spreading of solder on the substrate, causing the loss of adhesion between the solder and the substrate. In addition, the heat produced during soldering increases

Jan 1, 1983

To clean coal mine air by developing a low-cost scrubber suitable for belt transfer and similar applications. Approach Design a scrubber operated by water only, with no moving parts. Use conventional water spray nozzles located within a duct to both move and clean the air. Use a droplet eliminator to get the water droplets and mist back out of the airstream. How It Works Conventional scrubbers require a mechanical fan driven by either an electric or a hydraulic motor. They also require water sprays and some type of scrubbing mechanism. The water powered scrubber, however, offers higher reliability over conventional scrubbers since it utilizes the water sprays to both move the air and scrub the particulate from the air. Conventional water spray nozzles are placed near one end of a rectangular duct open at both ends. The sprays are directed towards the far end of the duct where a stationary wave blade water droplet eliminator is located. Movement of the water spray droplets coming from the nozzles generates (by momentum transfer) an air movement In the same direction as the sprays. The volume of air moved Is primarily a function of the duct cross-section size, water pressure and water

Jan 1, 1981

RI 9527. Effective Hazard Recognition Training Using a Latent-Image, Three-Dimensional Slide Simulation Exercise, by E.A. Barrett and K.M. Kowalski. Pittsburgh, PA: U.S. Department of the Interior, Bureau of Mines, 1995. NTIS stock number: PB95-170379. Rl 9531). Computer Modeling and Analysis of The Greens Creek Mine, Admiralty Island, AK, by MJ. Beus and T.J. Orr. Spokane. WA. -U.S. Department of the Interior, Bureau of Mines. 1995. NTIS stock number: PB95-176418. RI 9600. Application of Field Measurements and Computer Modeling to Evaluate Deep Mine Shaft Stability in Northern Idaho, by M, J. Beus, T. J. Orr and J. K Whyatt. Spokane, WA: U.S. Department of the Inferior. Bureau of Minus. 1996. NTIS stock number: PB96-140181. [ ]

Jan 1, 1995