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By L. A. Haas

The degree of reduction of various silica-graphite mixtures was studied in a batch reactor to determine optimum physical conditions for maximizing the carbothermic reduction of silica. The extent of interaction was determined for reactant mixtures in loose powder and briquet forms at pressures less than 0.01 torr and temperatures up to 1,445° C. Molar ratios were varied from 0.05 to 6.5 with maximum reaction at a ratio of about 1.5. The solid-solid reaction did not appear to involve gaseous intermediates. The extent of reaction better correlated with the number of interparticle contacts than with the true surface area of the reactants. Carbonized dextrose was a better reductant than graphite.

Jan 1, 1968

By Kathleen Madland Kowalski

In recent years the issue of human stress response in emergency workers has begun to receive attention. This paper presents a rationale for considering human stress as a significant factor in the management of emergencies It discusses the concept of stress, Critical Incident Stress in emergency responders, and intro¬duces the Critical Incident Stress Debriefing (CISD) process. It is suggested that in a disaster, the CISD process can improve the effectiveness of response teams on site, their turnaround time on site, and post disaster time off the job. This paper, prepared by a US Bureau of Mines research psychologist, offers some ideas to the mining industry in general, mine rescue trainers and more universally, to those responsible for developing emergency management plans.

Aug 1, 1998

By C. W. Owings

Two problems perplex many coal-mine operators and employees. Is coal-mine dust harmful to breathe; and, if so, is it possible to keep the concentration below the danger point? The medical profession is not unanimous in its opinion of the danger of breathing bituminous-coal dust, but there appears to be ample and increasing evidence that coal-mine dust can be harmful if breathed in large enough doses for long periods. The question of controlling the dust at the point of formation is still unanswered in the minds of many in the mining industry. However, results of limited studies conducted by the Bureau of Mines in 9 bituminous-coal mines indicate that a full-shift average exposure of workers should not exceed about 20 million dust particles per cubic foot of air (m.p.p.c.f.) and that concentrations can be held within this limit without too much difficulty. Furthermore, these studies indicated that an exposure in the neighborhood of 40 m.p.p.c.f. should not be exceeded for an individual operation and that it is possible to hold within this ceiling.

Jan 1, 1957

By Frank J. Susko

The U.S. Bureau of Mines is developing a process for removing metals from mining and mineral processing waste streams by precipitation. The precipitation process is accelerated by flocculation when a high molecular weight polymer is added. Infrared (IR) studies were performed on zinc hydroxide [Zn(OH);J, copper hydroxide [Cu(OH);J, and zinc sulfide (ZnS) flocculated with both non ionic and anionic polyacrylamide (PAM) and polyethylene oxide (PEO). The IR data were compared with general trends in the performance of the polymers observed during flocculation. These studies will help to understand the bonding between the precipitate and polymer and indicate the effectiveness of a flocculant for dewatering. Two types of bands showed up on the IR spectra; one type described the interlayer water of the flocs, the other described the organic bonds of the polymers. A general decrease in the areas of the three water bands, hydroxyl (O-H) stretching (3,200-3,500 cm-1), water bending (1,610-1,630 cm-1), and torsional oscillations (600-700 cm-1), indicate interlayer water being driven off, which is a favorable condition in flocculation. Shifts in the O-H stretching band indicate water bridging between the precipitate and polymer. Shifts in the amine (N-H) deformation, carbon-nitrogen (C-N) stretch band (1,600-1,610 cm-1) indicate the amine group of the PAM is involved in the bonding. Evidence suggests that ether oxygen of PEO is also involved in the bonding process.

Jan 1, 1990

By P. Kovalchik, S. Peng, G. Cole, R. Matetic

Previous studies conducted by the National Institute for Occupational Safety and Health (NIOSH) have shown that approximately 90 percent of coal miners and 49 percent of metal/nonmetal miners had a hearing impairment by age 50 (Franks, 1997). Mine workers are exposed to additional noise levels underground due to the reflection of machine-generated noise that would otherwise dissipate in an aboveground setting. Determining the sound-absorption coefficients is essential in modeling the sound field in an underground mining environment. Sound absorption is a measure of the amount of acoustic energy that strikes a surface and is absorbed rather than being reflected. The acoustic environment that mining machines operate in is a critical factor affecting the sound pressure level exposure for mining machine operators. Impedance tube testing is an inappropriate method for determining underground absorption coefficients due to the brittle composition of materials such as coal and slate. Classic absorption coefficient estimation using T60 measurements will not work well in an underground environment because the theory assumes a finite room, a diffuse field and a relatively uniform absorption. None of these assumptions are true in an open-ended mine entry. This paper presents a method using a ray-tracing technique to determine absorption coefficients for underground mines. Absorption coefficients are determined and presented for octave bands from 63 Hz to 8 kHz. The absorption coefficients are essential for determining and predicting potential overexposure to machine operators in different mine environments.1

By David Schlain

This Bureau of Mines report describes a method for electrodepositing titanium diboride from a molten salt bath. Initially, the electrolyte is a mixture of LiBO2, NaB02, Na2 Ti03 , Li2Ti03, and Ti02? The cell is operated at 900° C in a dry, inert atmosphere with consumable anodes of titanium or hot-pressed titanium diboride (TiB2) powder. Agitation of the electrolyte is essential. Current densities may be 6 to 9 amperes per square decimeter (amp/dm2) with titanium anodes and 9 to 30 amp/dm2 with titanium diboride anodes. A current density of 6 amp/dm2 is equivalent to a plating rate of about 35 micrometers per hour. The adherence of the TiB2 deposit varies with the substrate material. It is most adherent on molybdenum and on 4130 steel that has been preplated with copper and nickel, less adherent on nickel, and still less adherent on Inconel and on 4130 steel without the preplate. Cathode and anode reactions are suggested.

Jan 1, 1976

The following methods should be used to protect miners from the adverse health effects of exposure to respirable coal mine dust and respirable crystalline silica: ? Informing workers about hazards ? Establishing written emergency procedures ? Using engineering controls, work practices, and personal protective equipment (including respiratory protection when dust control equipment is being installed, maintained, or repaired) ? Monitoring exposures ? Conducting medical screening and surveillance ? Encouraging smoking cessation ? Maintaining medical records

Jan 1, 1997

By G. S. Scott, G. W. Jones

"INTRODUCTION In the course of the investigation the Bureau of Mines is carrying on to determine the causes, behavior, a. control of mine fires, the detection of incipient heating underground in the mines and above ground in refuse banks has received consideration.Many of the anthracite fires have been active for years and have progressed considerable distances free their original source.Some of the fires are in inaccessible territory, and it is often impossible to determine with any degree of accuracy their exact location or even the veins of coal that are afire, especially when the fire is in the upper strata and when it is impossible to go underground because of flooded conditions or the presence of an irrespirable atmosphere.In such cases, the only means by which the trend of a fire may be ascertained (as a result of any fire-fighting methods that may have been employed) are the sampling, exanination, and interpretation of the gaseous products coming from the fire area. The most important information desired is to know whether the temperature in the heated area is increasing or decreasing and to determine whether a fire that has been sealed is cooling down to normal mine temperatures or is maintaining its heat or is increasing in intensity due to infiltration of outside air.Interpretation of the analyses of gaseous products from refuse banks on the surface also should be of value in combating such fires. Refuse bank fires, with the additional danger of starting an underground fire through ignition of the outcrop, are by no means unknown in the anthracite coal region, and the causes of such fires are not always apparent. In a few cases the causes have been strongly suggestive of spontaneous origin."

Jun 1, 1938

By Donald W. Mitchell, John Nagy, Edwin M. Murphy

Information is presented on remote sealing of a mine passageway through a borehole by five methods : PPnneeuummaattiicc injection of mineral wool and sand, ureaformaldehyde foam , balloons , urethane foam, and caving by blasting . An adaptation of the method using pneumatically conveyed mineral wool was tried in an operating mine . Further research is needed to simplify and to improve the techniques involved , as well as to explore the possibilities of other methods and combinations .

Jan 1, 1964

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Jan 1, 1997

By J. Hyvarinen, A. D. Look

"INTRODUCTION AND SUMMARYElectricity is used extensively in open-pit metal mines to provide illumination, heat, and power to operate hauling and loading equipment, drills, pumps, signal systems, and other machinery. Good installation and maintenance of equipment and power, circuits, are essential to minimize the hazards of shock, burns, and fire.In the 13 years from 1931 to 1943, 20 fatal and 82 nonfatal injuries resulted from the use of electricity in open-pit mines in the United States ; 4/ these figures represent about, 10 percent of all fatalities and 1 percent of the nonfatal injuries. The ratio of fatal to nonfatal injuries from electricity in such mines was very high during this period; the figures show one fatality to every five accidents from this cause.Electricity may cause personal injury through abnormalities in equipment, such as short-circuit, accidental ground, overload, and poor contact; however, each year some fatal electrical accidents are due to persons touching uninsulated ""live wires."" These contact injuries are the result of careless body movements of persons in the vicinity of 'wires at places not normally frequented, or of accidental contact with live circuits when handling metal objects. Electrical hazards can be minimized by the enclosure or elevation of current-carrying parts; ample working space around equipment, adequate insulation, locking switches in the open or closed position under certain conditions, identifying and warning devices, protective grounding, insulating flooring, platforms, or rubber gloves, and proper inspection and maintenance."

Apr 1, 1949

By A. Z. Dimitroff, A. C. Moschetti

An improvised rock- dust disseminator, consisting of a 10-gallon galvanized metal milk can that dispenses rock dust in return air currents by the injection of compressed air has reduced the float dust explosion hazards at the Koehler coal mine, Koehler, N. Mex.

Jun 23, 1964

By C. A. Wilson

The Bureau of Mines started a continuing program to investigate and evaluate analytical techniques to assist governmental agencies to select simple, rapid, reliable methods for crude oil spill identification. Six crude oil samples were analyzed to evaluate gas-liquid chromatography, atomic absorption spectrophotometry, infrared spectoscopy, sulfur and nitrogren determinations, mass spectrometry, nuclear magnetic resonance spectroscopy, and ultraviolet spectrophotometry. Samples were studied from the following selected fields: El Morgan, Egypt; Duri, Indonesia; Minagish, Kuwait; Bachaquero, Venezuela; Gach Saran, Iran; and Prudhoe Bay, Alaska. These samples were chosen to represent high-production fields that are likely to be involved in oceanic transport. Over 50 years of Bureau of Mines analytical research on petroleum served as the basis for evaluation of the experimental results to determine which of the methods are effective techniques to identify crude oil spills. Gas-liquid chromatographic analysis, atomic absorption spectrophotometric analysis, and sulfur-nitrogen determinations are recommended as the most useful of the techniques investigated.

Jan 1, 1975

By G. A. Brady

Seven samples of Pennsylvania anthracite from the Bottom Ross bed were analyzed and tested to obtain data on cleaning characteristics, proximate and ultimate analyses, specific gravity, grindability, heating value, and ash softening temperature. Ash content of the samples varied irregularly from 9.0 to 34.4 percent, the range being narrowed to an upper limit of 14.8 percent ash by removing impurities dense enough to sink in a medium with a specific gravity of 1.90. Ash content of the sink material with specific gravity greater than 1.90 ranged from 56.4 to 80.4 percent; corresponding specific gravities were 2.095 to 2.534. Volatile matter contents were indicated to be higher for the ash-forming minerals than for the pure coal substance in the various specific gravity fractions of a given sample. Specific gravities of anthracites with compa¬rable ash contents but from different locations in the bed varied as much as 0.06. The grindability index increased significantly with increasing ash con¬tent of specific gravity fractions from all the samples.

Jan 1, 1968

By Alvin M. Cummings

"INTRODUCTION During July and August 1943, the Bureau of Mines undertook an investigation of the Trego lead-zinc mine, near the town of Platteville in Grart County, Wis. as part of a general investigation of the zinc-producing area of southwestern Wisconsin. The work was done when every effort was being made to increase the production of metals important to the nation's war program.The Bureau of Mines completed eight churn-drill holes and sampled mineralized faces in the mine workings to determine if further exploitation was justified in an area between the mine and a zone previously drilled to the east.Following the investigation described herein, intermittent operations were resumed. Except where otherwise stated, this report describes conditions only to the time of completion of the Bureau of Mines investigations.ACKNOWLEDGMENTSIn its program of investigation of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. The Mining Division, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual investigative work and prepares the final report. The Metallurgical Division, O. C. Ralston, chief, analyzes samples and performs beneficiation tests.The investigation described in this report was conducted under the immediate supervision of the author and 0. W. Terry, mining engineer of the Bureau of Mines, with the assistance and advice of E. D. Gardner, re¬gional engineer, and E. P. Barrett, district engineer. Final data were prepared under the direction of Paul Zinner, acting chief, Minneapolis Branch, Mining Division.A. V. Heyl, Jr., and A. F. Agnew of the Federal Geological Survey cooperated with the Bureau's engineers and made lithologic studies required during the drilling program.The cooperation of W. N. Smith and O. E. DeWitt of the Vinegar Hill Zinc Co. and Francis Piquette of the Piquette Mining Co. facilitated the investigation to a great extent."

Mar 1, 1948

By James A. West

THE South Asian countries of India, Ceylon, Pakistan, Afghanistan, Nepal, Bhutan, and Sikkim have a large variety of mineral resources; however, in spite of mineral industry growth during 1964, development of resources remained far short of possible development, and, in terms of value of trade in minerals, the area remained a sizeable net importer. India's mineral industry is by far the most significant; its minerals production in 1964 accounted for more than 90 per cent of the total value of all minerals produced in the area. The total value of all minerals produced in South Asia in 1964 was only about 1 percent of the area's estimated gross national product of $55,125 million. Despite the rather small current contribution of minerals to the economy, development of mineral resources figures prominently in plans for the industrial development of the nations of this area.

Jan 1, 1966

By J. Nielen van der Merwe

For the last 3 decades, coal pillars in the Republic of South Africa have been designed using the well-known strength formula of Salamon and Munro that was empirically derived after the Coalbrook disaster. The database was recently updated with the addition of failures that occurred after the initial analysis and the omission of failures that occurred in a known anomalous area. An alternative method of analysis was used to refine the constants in the formula. The outcome was a new formula that shows that the larger width-to-height ratio coal pillars are significantly stronger than previously believed, even though the material itself is represented by a reduced constant in the new formula. The formula predicts lower strength for the smaller pillars, explaining the failure of small pillars that were previously believed to have had high safety factors. Application of the new formula will result in improved coal reserve utilization for deeper workings and enhanced stability of shallow workings.

Jan 5, 1999

By G. G. Morgis, J. J. Forbes

"INTRODUCTION The greatly diversified and increased uses of beryllium and its con& pounds in recent years have focused attention on the health hazards incident thereto. The Bureau of Mines has a fundamental interest in safety and the elimination or reduction of health hazards in the mineral and allied industries, and it recognizes that serious hazards are inherent in the production and use of beryllium and its compounds. This circular presents a review of the literature pertaining to such health hazards but does not describe original research by Bureau personnel. Most of the bibliography has boon either quoted in part or abstracted in an effort to present information in a comprehensive and readable form.In reviewing the literature, differences of opinions wore recognized in the writings of the respective authors, but no attempt was made to evaluate such differences. This presentation was devoted strictly to reporting without editorial comment.SUMMARYAlthough beryllium was known to industry for about 150 years, its toxicity did not present any serious problems in the United States until the advent of World War II, when the increased use of this element and its compounds brought to light several toxicologic reactions occurring primarily in the lungs and skin of workers handling it. The pulmonary effects, characterized as acute pnoumonitis and chronic pulmonary granulomatosis in beryllium workers, are far more serious than the dermatological manifestations.The addition of beryllium to the list of toxic industrial metals has boon so recent that there is still some confusion in the clinical picture. Data on magnitudes of exposure likely to be responsible for the production of disease are not yet adequate. There appears to be no relation between the severity of exposure and the development of cases some of those having had severe exposure have not developed a reaction, whereas those having a slight exposure in some instances have developed a response."

Jul 1, 1950

Investigate the use and placement of lightweight concrete to improve ground control technology in deep mines where deformation occurs under heavy ground conditions and where there is danger of rock bursts. Approach Investigations of lightweight concrete properties and placement methods were conducted in the laboratory and in the field. Three test sections were completed: a monolithic, portal-type structure with integral walls and arch constructed aboveground; an underground test section constructed in a mine drift using plywood forms; and a test section constructed in a mine drift using an air-supported formwork. In the two underground test sections, the light-weight concrete was placed using a piston pump with concrete discharge line. A cooperating mine also used lightweight concrete, in the density range of 25 lb/ft3, to replace timber blocking in a raise preparation structure (the enlarged area across a vein where chutes and manway access arc placed). Other experiments included the use of precast lightweight concrete blocks in situations where ground support was needed, such as fur mine, ventilation doors, stoppings, and barricades.

Jan 1, 1990

By John J. Mulligan

The Bureau of Mines sampled a gold-bearing schist series 50 miles east of Nome near Bluff, a dormant mining camp on the southern shore of the Seward Peninsula, Alaska. Gold is unevenly distributed through a section of a schist series that extends from the coast northward 4,500 feet. In this section the schists dip westward 20 to 38 degrees and have an outcrop width of about 1,000 feet and a normal width of about 500 feet. An intensely fractured zone within the schists averages 0.015 to 0.017 ounce of gold and 0.03 to 0.05 ounce of silver per ton for outcrop widths of 200 to almost 500 feet. The grade of the remainder of the schist series ranges downward to scant traces. Gold eroded from these schists collected in solution channels in metalimestones to form the Daniels Creek placers, which also extend from the beach southward under the sea for an unknown distance. The lode sources of the gold placers elsewhere in the southern Seward Peninsula may be similar schists that occupy a similar position in the metasedimentary series.

Jan 1, 1971