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By Manuel Gomez

A general prediction model for the Hardgrove grindability index was constructed from 735 coal samples using the proximate analysis, heating value, and sulfur content. The coals used to develop the general model ranged in volatile matter from 12.8 to 49.2 percent, dry basis, and had grindability indexes ranging from 35 to 121. A restricted model applicable to bituminous coals having grindabilities in the 40 to 110 range was developed from the proximate analysis and the petrographic composition of the coal. The prediction of coal grindability within a single seam was also investigated. The results reported support the belief that mechanical properties of the coal are related to both chemical and petrographic factors of the coal. The mechanical properties of coal may be forecast in advance of mining because the variables used as input to the prediction models can be measured from drill core samples collected during exploration.

Jan 1, 1970

By BUREAU OF MINES

A complete list of permissible mining equipment, rescue apparatus and gas masks tested prior to January 1, 1925, was published in Bureau of Mines Technical Paper 3761. The present list includes all equipment tested and approved by the Bureau, up to and including January 1, 1926, and supersedes the list issued as Serial 27202 in November, 1925. It covers electric air compressors, coal drills, mining machines, mine pumps, room hoists, switches, electric cap lamps, flame safety lamps, electric hand and trip lamps, flash lamp, methane indicators and detectors, blasting units, storage battery loco- motives, power trucks, self-contained oxygen breathing apparatus and gas masks. The system under which these devices were tested permits the manu- facturer, after his equipment has passed certain tests prescribed by the bureau, to mark his equipment with a seal showing that it has been "approv- ed" by the Bureau of Mines. The tests are designed to insure that the equipment has the minimum requirements for safety in use. The only object of the bureau in making such tests and publishing lists of permissible equipment is to safeguard the lives of workers and to help lessen the hazards of mining.

Feb 1, 1926

By H. B. Humphrey

In the 39 years from 1891 to 1929 , gas and dust explosions in the coal mines of Tennessee caused 413 deaths , or one- third of the fatalities in the mines for that period . Inasmuch as explosions caused but about 15 per cent of mine fatalities for the whole United States for this same period it is evident that the Tennessee coal mining record is by no means good , as far as explosion fatalities are concerned . Since 1926 , Tennessee has had a clear record as to fatalities from explosions ; this fact may be credited very largely to the improved conditions and safer practices in Tennessee's coal mines which have been brought about by the work of the State Inspection Department and of the Southern Appalachian Coal Operators Association directed toward adoption of safety precautions and practices most of which are advocated by the United States Bureau of Mines . Chief among these improvements are the replacement of black powder and dynamite by permissible explosives , improved ventilation , and the installation of rigid methods of inspection for gas . With the present tendency for operations to pass into the hands of responsible and informed management , and with unrelaxed care and inspection , the good record of the past several years should be maintained .

Apr 1, 1931

By E. L. Burwell

Application of the in situ recovery process to oil shale was tested during two field experiments near Rock Springs, Wyo. The results of these tests demonstrate that a self-sustaining combustion zone can be created in an oil shale body, that this zone can be moved through the oil shale, and that the process will produce shale oil. Evaluation of the combustion process by monitoring produced fluids for physical and chemical properties and volumes is described. The material and energy balance obtained is compared with a second evaluation based on extensive coring of the test area after the test was terminated. Several side results of the research are noted such as ground surface heating by underground burning and production of low-to medium-Btu gas during retorting.

Jan 1, 1973

By D. N. Nilsen

The Bureau of Mines is investigating a method to recover Ni, Cu, and Co from low-grade domestic laterites through reduction roasting, leaching, sol-vent extraction, and electrowinning unit operations. The objective of this research is to develop processing technology that can convert low-grade domestic deposits containing critical metals into national reserves. As a part of this research, a solvent extraction system was investigated for the extraction of nickel and copper, followed by the separation and production of suitable electrolytes. Nickel and copper were coextracted from ammoniacal ammonium sulfate leach liquors (pH~9.5) with LIX 64N extractant in a laboratory-size mixer-settler continuous circuit. Three extraction stages resulted in >99-pct extraction of nickel, substantial copper extraction, and essentially no cobalt extraction from leach liquors. A crowd stage reduced the ammonia loading on the solvent by maximizing nickel loading. Residual ammonia was removed from the loaded solvent with a pH-controlled scrub. Nickel and copper loaded on the solvent were separated by selective stripping. Typical nickel strip circuit operation using electrolyte containing 90 grams per liter (g/l) Ni and 11.9 g/l H2S04 yielded >99.9 pct Ni stripped from the solvent in five stages. The copper loading on the recycled solvent was controlled in a copper strip stage using electrolyte containing 25 g/l Cu and 160 g/l H2S04,

Jan 1, 1981

By W. H. Young, R. L. Anderson

"Physical conditions, such as thickness and character of the coal seam, dip or pitch of the seam, depth of cover, character of roof and overlying strata, mine water, etc., affect the productivity in bituminous-coal mining. Thickness of the coal seam being mined is probably the most important single item that determines whether the output per man per day shall be low or high; however, in strip mining the depth of cover or overburden to be moved is of equal importance.Bituminous coal is mined today from seams of exceedingly variable thickness - less than 2 feet to more than 50 feet; however, a large majority of the mines are producing .coal from seams 3 to 6 feet thick. The average thickness of the coal seams mined in the United States has not changed materially in the past 25 years. The average seam thickness for all bituminous-coal mines was 63 inches in 1920 4/ and 65 inches in 19)45. As thick seams have been exhausted in the older fields, other thick seams, have been opened in the newer fields.Productivity increased from 4 net tons per man per day in 1920 to 5.78 in 1945. This 45 percent increase in productivity resulted from increased mechanization. The percentage of underground production represented by coal cut by machines increased from 61 in 1920 to 91 in 1945 Mechanical loading increased from less than 1 percent of underground production in 1920 to 56 percent in 1945, and strip mining increased from less than 2 percent to 19 percent of the total production during the same period."

Dec 1, 1947

By Kyei-Sing Kwong

The U.S. Bureau of Mines investigated the synthesis of advanced ceramics (SiC+AlN, SiAlON, SiC+A1203, and Si3N4+AlN) from natural clays (kaolin, halloysite, or montmorillonite) by an intercalation and heat treatment method. This process includes the steps of refining a clay, intercalating organic chemicals into its layered structure, drying the intercalated mixture, firing the treated structure at certain temperature ranges in controlled atmospheres to form desired compounds, and grinding the loosely agglomerated structure. Focus of this research is to economically process advanced ceramic structures from abundant natural resources. The advanced ceramic phases produced in this simple treatment are homogeneously distributed at the nanostructure level, and may potentially lead to cost effective manufacturing processes. The intercalation of clay was confirmed by X-ray and BET analyses. The evolution of chemical compositions during carbonization reactions and carbothermal reduction was investigated. The characteristics of refined clays and synthesized powders were studied. Advanced ceramic composites/solid solution have been produced from intercalated clays, without the presence of other compounds.

Jan 1, 2010

By John Taber, Robert D. O'Brien

"INTRODUCTION The Bozeman corundum deposit was first examined in May 1944 by an engineer of the Bureau of Mines. In August 1944, the property was re-examined because of a sharply increased war demand for corundum. A small program of trench exploring was undertaken after the second examination. The work was started in October 1944 and was completed in December 1944. This report presents the essential data obtained by the exploratory work.ACKNOWLEDGMENTSIn its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that, they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each exploratory project as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploration work, and prepares the final report. The Metallurgical Branch, R. G. Knickerbocker, chief, analyzes samples and performs beneficiation tests.The field work on the Bear Trap project was supervised by E. W. Newman, district engineer Montana District office. The microscopic examinations and. the grid grain-count analyses of the samples and the beneficiation tests were made at the Bureau's laboratory at Salt Lake City, Utah, under the direction of S. R. Zimmerley, chief, Salt Lake City Division, Metallurgical Branch."

May 1, 1947

By d&apos, Kathleen J. Amico

This summary appears in Minerals Yearbook volumes I and III, which cover mineral production in the United States, its island possessions, the Canal Zone, and the Commonwealth of Puerto Rico, as well as the principal minerals imported into and exported from the United States. The several commodity and area chapters contain further details on production. A summary table comparing world and U.S. mineral production also is included. Mineral production may be measured at any of several stages of extraction and processing. The stage of measurement used in the chapter is normally what is termed "mine output." It usually refers to minerals in the form in which they are first extracted from the ground, but customarily includes for some minerals the product of auxiliary processing operations at or near mines.

Jan 1, 1967

By W. H. Ode

Low-temperature distillation tests at 200°, 350°, and 500° C. were made on a subbituminous coal from Boulder County, Colo., and a subbituminous coal from Weld County, Colo., in connection with a survey of carbonizing properties of American coals and investigations of their chemical and physical properties. The coal represented by the sample from Weld County was reported to give off combustible volatile matter at unusually low temperatures When placed on a fuel bed. The yields of tar and oil and the composition of the gas from this coal, as obtained in the distillation tests, did not confirm this report. These yields and the gas composition of the Weld. County coal differed but little from those obtained from the coal from Boulder County. Both coals yielded tar and gas in amounts considered to be normal for coals of their rank.

Jan 1, 1937

By William J. Campbell

The Federal Bureau of Mines provided five test materials--amosite, short-and long-fiber chrysotile, crocidolite, and nonfibrous tremo1ite--to the National Institute of Environmental Health Sciences (NIEHS) for studies on the biological effects of orally ingested asbestos-related materials. An inter-agency agreement between the Bureau and NIEHS made possible this program to characterize these test materials. The Bureau in turn received support through contracts with the Ontario Research Foundation for the milling of amosite and crocidolite, and with the University of Maryland for microscopic measurements. The five test materials, which were supplied in quantities of 960 to 1,200 pounds each, were characterized by chemical-instrumental analysis for elemental composition, surface area, density, X-ray diffraction, infrared spectroscopy, thermogravimetric analysis, mineralogy, and particle size analyses. Particle size distributions were emphasized because of the current theories relating adverse biological effects to length-width characteristics of durable elongated particles.

Jan 1, 1980

By Eugene T. Sheridan

This circular presents data on individual plants of the fuel-briquet and packaged-fuel industries that responded to the Bureau of Mines annual economic survey and reported production for 1959. The companies named herein represent virtually all producers of processed fuels of mineral origin. A few small companies may not have been canvassed or failed to respond, however, as some plants operate intermittently, and the survey is voluntary. No consideration was given to size of the plant and all plants that reported commercial production were included. Specifically excluded were plants that manufactured briquets from wood charcoal. Fuel briquets and packaged fuel are manufactured solid fuels, fabricated from fine-sized mineral fuels by mixing with binders and compressing into small individual shapes. Briquets usually are produced as small, pillow-shaped pieces, 2 to 4 inches long, weighing 2 to 4 ounces. Packaged fuel consists of 3- to 4-inch cubes, 6 or 8 of which are wrapped in heavy kraft paper to form a package weighing 10 to 15 pounds. The overall size of a popular package is 10-112 x 7 x 3-1/2 inches. Briquets are durable, may be stored outdoors, and shipped and used as bulk fuel. Packaged fuel is fragile, and must be stored indoors to keep it from deteriorating. Whereas briquets are consumed in many areas as a general residential fuel, packaged fuel is more of a specialty item, used at times as a supplement to other fuels. Package fuel is burned without removing the paper and referred to as the "white-glove" fuel.

Jan 1, 1960

By David C. Oyler, Paul B. Stubbs

The Bureau of Mines and United States Steel Corp. are conducting a joint project to monitor formation pressures at a large (23-well) coal- bed gas drainage field near Oak Grove, AL. Three monitor holes were drilled in late 1981, and pressure monitoring began in December 1981. The Bureau of Mines direct method was used to obtain gas content data from cores taken in the monitor holes. Comparison of the 1981 gas con- tent data from the monitor holes with initial gas content values obtain- ed from the production wells in 1977 indicates a 50-pct reduction in ad- sorbed gas content inside the pattern and a 29-pct reduction at one point 500 ft outside the pattern. The combination of pressure and gas content data has also allowed an in situ isotherm curve, relating the formation pressure to adsorbed gas content, to be developed for the area of the production wells. From the current rate of pressure decline (1 lbf/inz per month), the observed changes in gas content, and the isotherm curve, it appears that most of the early gas production came from within the pattern, but since 1981 (and possibly earlier) most of the gas produced has been migrating to the wells from outside the pattern area.

Jan 1, 1985

By W. A. McKinney

A sample of oxidized copper ore from a large deposit located in Pinal County, Ariz., about 50 miles northeast of Tucson, was treated by the Federal Bureau of Mines in a small-scale continuous pilot plant by a procedure which comprised acid curing complemented by water leaching and countercurrent decantation washing in a series of drag classifiers. A feed was prepared by pugging minus 1/4-in, ore with concentrated sulfuric acid and about 10 pct, of eater, followed by curing in batches for about 24 hr. The cured ore was fed continuously to a leach drum, where it was mixed with advance solution from the countercurrent washing system to dissolve the sulfated copper. The pulp was thickened and washed in four Esperanza-type classifiers, using a flocculating agent to obtain rapid settling and thickening. The leached ore pulps thickened satisfactorily in the drag classifiers when about 0.8 lb. of a polyacrylamide flocculant per ton of dry feed was used. Clear overflow liquors were obtained, and classifier rake products containing about 60 pct. solids were produced, As much as 90 lb./hr. of ore was treated in the plant, with a recovery of 60 pct. of the total copper or 80 pct, of the acid-soluble copper when 2 tons of water per ton of feed was used in washing. The acid consumption was 4.3 lb./lb. of copper recovered. On the basis of the maximum feed rate employed and the effective pulp-settling area of the classifiers, a total of 1 sq. ft. of pool area was required per ton of dry feed per day for the thickening and washing operations. The washing efficiency in the test was 95 pct.

Jan 1, 1960

By R. Van A. Mills

This preliminary paper is intended to answer briefly some of the inquiries coning to the Bureau of Mines regarding the so-called "paraffining", of oil wells and methods of preventing and remedying that trouble. The increased difficulties in operation and the losses of production caused by the deposition of gummy and waxy hydrocarbons, commonly called paraffin, in the wells, tubing, other pumping equipment, and in the pores of the productive sands, have long been recognized but the trouble has not been overcome. The nature and causes of the trouble, together with some of the possible methods by which it may be diminished or overcome, are outlined below. Character of the Peraffining Materials. The so-called paraffin that collects in oil wells end in the pores of the oil-producing sands immediately around the wells, is generally made up of amorphous wax or uncracked paraffin, asphalt, or other gummy hydrocarbons mixed with more or lees water, oil, and inorganic silt. Some of the samples of this "paraffin" collected from oil wells in different fields and examined by the Bureau of Mines contain as mach as 20 per cent by weight of water and inorganic silt, whereas other samples are composed entirely of waxy hydrocarbons and oil. The inorganic silt accompanying this "paraffin" is mostly fine sand, clayey materials, common salt and finely disseminated precipitates of calcium and magnesium carbonates. Sulphates of calcium, barium, and strontium are less common constituents of the "paraffin."

Jan 1, 1923

By Everett A. Sondreal

Data are presented on the characteristics of lignites with emphasis on the composition and fusion properties of the ash. Differences in the analyses of commercial-grade lignites are related primarily to variations in moisture and ash contents. Lignite ash is generally characterized by high concentra¬tions of alkaline earth oxides and a greater tendency for retention of sulfur in the ash than higher-rank coals. Composition of ash varies significantly within and between mines. The differences within mines are significant for short distances and may be eliminated under certain circumstances by normal mixing occurring during mining. The sulfur in lignite averages 0.6 percent and is found primarily in the organic or pyritic forms with only a trace of the sulfate. During the stan¬dard laboratory asking procedures, from 60 to 100 percent of the original sul¬fur is retained in the lignite ash. Trace elements, such as uranium and germanium, in the ash from commercial¬-grade lignites are present in low concentrations, but others, primarily copper and silver, are present in specific samples in concentrations approaching those found in some commercial ores.

Jan 1, 1968

By D. R. Tesarik, M. K. Larson, D. K. Denton, J. B. Seymour, R. L. Rains, T. J. Williams

Because backfill has occasionally collapsed into an active working area, posing a hazard to miners, engineers from the Spokane Research Laboratory of the National Institute for Occupational Safety and Health and Hecla Mining Co. installed instruments in a cemented, backfilled, stope-ramp intersection at Hecla’s Lucky Friday Mine, Mullan, ID. The purpose was to measure stress and strain changes in the backfill and reinforcing members during undercut mining. The instruments were monitored for 6 months while three successive cuts were mined below the intersection. Readings showed induced loads up to 3450 kPa (500 psi) in the backfill as stope walls converged 2.5 to 12 cm (1 to 5 in). The backfill then deformed against the top and bottom plates of the 2-m- (6-ft-) long vertical rock bolts installed as reinforcement, producing loads to 177 kN (40,000 lb)on the rock bolts. We hypothesize that a compressive zone was created in the backfill that allowed the backfill to remain stable as long as the compressive zones from adjacent rock bolts overlapped. This hypothesis is presented in graphical form. Of particular interest was the effect of loading on trusses installed to augment the vertical rock bolts and wire mesh typically installed in backfill. Data from the instruments indicate that wall closure perpendicular to the vein induced loads in truss legs parallel to the vein and in the rock bolt driven through the center of the truss, but, because they are designed to function under tension, truss legs perpendicular to the vein supplied in significant support as a result of compressional forces from wall closure. Based on this study, use of trusses was discontinued, and an alternative support system of wood beams and posts was installed as needed to ensure the safety of miners working beneath the backfill in stope-ramp intersections.

Jan 7, 2001

By R. H. Grau, S. B. Robertson, R. B. Krog, T. P. Mucho

Stone mines represent the highest percentage of operating underground nonmetal mines in the United States. With the introduction of stricter Diesel Particular Matter (DPM) regulations, large-opening underground room-and-pillar stone mine operators are faced with implementing one or more alternative methods to reduce concentration levels including: install and maintain an effective ventilation system; install lower DPM emission diesel engines; the adding of DPM filters. The National Institute for Occupational Safety and Health (NIOSH) is actively researching various aspects of fan and stopping designs in an effort to improve the ventilation of these mines. NIOSH has identified and further developed three alternative ventilation methods for use in large-opening underground mines: split-mine, perimeter, and unit-ventilation. This paper describes the implementation of the three methods with respect to their use in mines of various levels of development.

By Richard F. Link

The principal procedures for the statistical analysis of gold assay and other trace-element data depend on applying either the normal frequency distribution or the lognormal frequency distribution. The consequences of applying both methods are examined through reference to example data from United States and South African gold mines. It is concluded that for estimation of average grades, except for certain data with a very high coefficient of variation (ratio of standard deviation to mean), use of the lognormal distribution is ordinarily undesirable because bias may be introduced and little efficiency can be gained. However, if biased average grades can be tolerated, as in the examination of data from surveys in exploration geochemistry, use of the log-normal distribution may be desirable. Various statistical analyses are detailed, and the tables presented to implement the analyses are more complete than those previously published.

Jan 1, 1971

By W. H. Rinkenbach, C. A. Taylor

"Among the recently patented detonating compounds that have been suggested as substitutes for the commonly used fulminate of mercury is the normal lead salt of trinitroresorcin, or styphnic acid. As no data concerning its use or practi¬cability were available, a study of its properties was made in the explosives laboratory at the Bureau of Mines experiment station at Pittsburgh, Pa. This paper embodies the results obtained.Normal lead trinitroresorcinate was first prepared and patented*** by Herz; it probably found some use during the World War, but no record of its performance is available,Preparation of Lead Trinitrpresorcinate.In his patent specifications, Herz states that the normal salt may be obtained in a quantitative way by precipitating a multiple of the equivalent weight of the lead salt of a strong inorganic acid - such as lead nitrate - in the presence of a weak organic acid - such as acetic acid - by heating with a Teak solution of the alkali-metal salts or alkaline-earth salts of trinitroresorcin. Herz gives the following example: 245 grams of dry trinitroresorcinand 290 grams of crystalline sodium carbonate are dissolved in in 18.8 liters of boiling water, to which 77 c.c. of glacial acetic acid is added. The toiling solution is mixed with a boiling solution of 650 grams of lead nitrate in 1.4 liters of water, stirring rapidly; and the mixture is boiled for two minutes, after which it is cooled quickly with constant stirring. The precipitated crystals are then filtered off, washed several times with cold water, and dried."

Oct 1, 1923