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By J. S. Bryner

INTRODUCTION IN the study of metallographic specimens in the electron microscope, there is need for a method of locating the same field in both the light microscope and the electron microscope. This need arises chiefly from the fact that in the electron microscope the magnification and degree of resolution are so much higher, and the field so much smaller than in the light microscope that it is often difficult, if not impossible, to identify positively what is being observed. The difficulty is increased by the fact that, because a transparent film replica of the metal surface must be used in the electron microscope, micro-constituents can be identified not by their color but only by their texture and contours. For these reasons it is desirable to obtain a series of photographs showing the same field in both microscopes in order that the appearance of common microstructures and micro-constituents in the electron microscope may be identified and catalogued for future reference. The need for a method of locating the same field in both microscopes arises also when it becomes desirable to enlarge in the electron microscope for more detailed study a particular interesting structure observed in the light microscope. Using the standard polystyrene-silica1,2 replica technique, in which the silica film replica is fished from the ethyl bromide on a 1/3 in. diam 200-mesh specimen screen, the possibilities of locating a particular area on the film in the electron microscope are rather remote. The desired structure may be obscured by the wires of the specimen screen or unrecognizable at the high magnification. A solution to the problem would be provided if a specially designed specimen screen, containing an opening which could be absolutely identified and quickly located in the electron microscope, could be fastened to the silica film replica in such a position that the desired field on the specimen would be located at the identifiable opening in the specimen screen. The design for such a specimen screen, a method for producing it, and a technique for fastening it to the silica film replica are described below. DESCRIPTION OF METHOD The Specimen Screen A simple design for a specimen screen containing an opening easy to identify and locate in the electron microscope is one with two lines of openings at right angles in the form of a cross. Such a screen is shown in Fig I. The opening at the center of the cross is identified easily and can be located quickly in the light microscope and in the objective image of the electron microscope. The specially designed specimen screens for this work were produced in quantity by electroforming. On both sides of a polished strip of copper 1 X 3 X 1/8 in., twenty patterns of the cross of openings were punched with a diamond point micro-hardness tester, using a load of magnitude

Jan 1, 1948

By C. Dean Starr

The physical basis of the equation correlating electrical conductizlity and temperature coefficient of resistance of solid solution alloys has been inzlestzgated and the nature of the constants evaluated. It is shaun that the same form of correlation is valid irrespective of the magnitude of the temperature coefficient. However, the effect of therma1 expansion and change in resistivity with temberature nust be considered when the magnitude of the temperature coefficient of resistance is near zero. In a comprehensive literature survey conducted at the Armour Research Foundation in 1950, it was found that a linear relationship exists between the electrical conductivity, K, and the temperature coefficient of resistance, a, for solid solution alloys. This was expressed by the equation where B, a constant, depends on the solvent metal but not the solute. A continuing investigation by Hansen, Johnston, and Parks showed this equation was generally appropriate for Cu, Ag, Au, Pd, Pt, and Co base binary solid solution alloys as well as for many ternary alloys of copper over a range of conductivities and temperature coefficient of resistances from 0.02 to 0.60 reciprocal pohm cm and-0.00015to0.004Q per 0 per "C respectively. Eq. [I] was not always valid for alloys that exhibited a change in state (magnetic to nonmagnetic) or for alloys that had a temperature coefficient of resistance near or below zero. For example, in nickel alloys, a simple linear curve as predicted by Eq. [l] was not obtained when the conductivity was plotted against the temperature coefficient of resistance. Hansen suggested that deviations observed were caused by transitions from a ferromagnetic to a nonmagnetic state. Subsequent and more extensive data by ronin on Ni-Mn alloys confirmed Hansen's postulate. While both states independently showed a linear relationship between K and a, the value of B was different for the two states. In some copper and gold base alloys, as well as the platinum and palladium alloys investigated by Hansen, the conductivity did not extrapolate to zero at zero a as demanded by Eq. [I]. This deviation can be readily corrected by simply adding a constant to Eq. [I.] whence Eq. [2] shows the K decreases as a decreases but that K has a positive value when a = 0 which is observed for commercial solid solution alloys as well as the experimental alloys tested by Hansen. While other methods of correlation of electrical properties have been made such as the one by Starr and Wang3 who found a linear relationship between resistivity and temperature coefficient of resistance for Ni-Cr-Al-Cu alloys, the data, in general, can also be correlated by a form of Eq. [2]. Thus, Hansen's empirical equation has considerable merit. The objective of this paper is to determine the physical basis for this equation and to examine the region near zero a in more detail. ELECTRICAL CONDUCTIVITY VS TEMPERATURE COEFFICIENT OF FU3SISTANCE The resistance of a metal or alloy is defined as

Jan 1, 1963

By A. T. English

X-ray dif action techniques were used to investigate ordering and domain coalescence for the B2 (CsC1) superlattice in this alloy. Essentially complete disorder is obtainable by drastic quenching. isothertmal ordering occurs very rapidly at temperatures between 565° and 680°C, only a few seconds being required for development of substantial long-range order. A very fine antiphase dormain structure, found in samples annealed for short times, undergoes coalescence with further annealing. Domain "size" is found proportional to (t)1/2 . This Yate law can be derived by adapting the formalism of Hillert's analysis 01- metallurgical grain growth. For this Purpose the material is descvibed in terms of a "Swiss-cheese " structure, consisting of two multiply connected, mutually intertwined domain volumes. The observed activation enevgy for coalescence, 70 kcal per g-atom, agrees with an estit~lated value ,for volume diffusion in disordered rrzaterial. It is suggesled that the experimental value vejlects the substantially disordered environment of mobile vacancies located in the moving antiphase domain boundary. The alloy Fe-Co-2V is bcc below about 900'C and orders into a B2 (CsC1) superlattice below about 730c It has important applications in magnetic components, including many requiring extensive cold rolling.* example, Marcinkowski and Brown6 observed a re1atively small as-quenched domain size of about 250Å in B2 Fe3A1. Since there appear to be no published data on domain coalescence in B2 alloys, this process was studied in detail. MATERIALS AND EXPERIMENTAL TECHNIQUES A commercial high-purity alloy, nominally 49 Fe-49Co-2V, was obtained from the Arnold Engineering Co. in the form of cold-rolled sheet 0.004 in. thick. Samples were annealed for 1 hr at 800°C in dry H2 to produce disorder and quenched into iced brine. They were then annealed in a nitrate-nitrite salt bath for various times at temperatures between 525° and 625°C. Estimates of the LRO parameter S and the APD size D were made using established X-ray diffraction techniques. Superlattice peaks are best observed using CoKa radiation, for which the value of (fFe-fCo) is maximized. Peak-to-background intensity ratio was improved by filtering CoKß from the incident beam to eliminate sample fluorescence, and by using a pulse-height analyzer. The LRO parameter S was computed from the ratio of integrated intensities I 100/I 200- Owing presumably to systematic errors associated with the presence of crystallographic texture and X-ray extinction, only rough agreement was obtained between experimental and theoretical (absolute) intensity ratios. For this reason certain experimental refinements (e.g., use of balanced filters) were considered superfluous and were omitted. Emphasis was placed on maximizing intensity in order to reduce the time taken to accurately determine the contour of the very small (loo), peak. This was done by point counting 105 counts at appropriate intervals. Background intensity averaged about 1200 cps.

Jan 1, 1967

Oregon State Agricultural College, School of Mines, Corvallis, Ore Available publications of the old Bureau of Mines and Geology of Idaho have lately been distributed through the School of Mines of Oregon State College As the School of Mines was abolished in the summer of 1932, all of the bulletins and publications available have been turned over to the State College Library for distribution. At present plans have not been completed for further distribution For information on available publications, address: Director of Libraries, Oregon State College, Corvalhs, Oregon

Jan 1, 1933

Engineering Experiment Station, University of Arkansas, Fayetteville, Ark. W N Gladson, Dean and Director The Engineering Experiment Station has published a number of bulletins, only a few of which are of particular interest in this directory: Bulletin 3, Arkansas coal or oil for domestic heating; 4, Road materials of Arkansas, 5, A study of Arkansas coals, 6, Portland cement materials in Arkansas; 11, Natural gas versus Arkansas coal for house heating. Circular 3, Short cuts to combustion efficiency with natural gas Address the Engineering Experiment Station for any of these publications.

Jan 1, 1933

By G. S. Hume

The production of petroleum in Canada is relatively small in proportion to the amount of oil consumed. Production figures are given in Tables 1 and 2, which show that the production in Alberta for 1934 was more than for the whole of Canada in 1933. The production of natural gas for Canada is shown in Table 3, In Turner Valley, the largest producing gas and oil field in Alberta, seven naphtha wells from the Paleozoic limestone and one crude oil well from Lower Cretaceous strata were completed during the year. Six-

Jan 1, 1935

By Ahmad Saberian

Five salt samples 20 to 40 cm tall, sealed on all sides except one, were exposed to a series of dissolution tests in various brine solutions and at different temperatures. Solvents were in the 50 to 96% saturation range and the temperatures varied between 40°F and 150°F. The collected dissolution data sets for vertical salt surfaces were analyzed and three were selected to be used for developing a general relation. After various curve fitting efforts, an empirical relation for salt dissolution rate as a function of brine temperature and salinity was developed.

Jan 1, 1985

By H. K. Livingston

A TECHNIQUE has been developed which makes it possible to determine the spreading pressure of liquids and solids, for simple systems. Data for surface tensions, interfacial tensions, spreading pressures, and contact angles for water, heptane, and silica are tabulated. These results can be applied to the evaluation of capillary rise and displacement pressure in a petroleum reservoir. Appropriate equations are presented and the application of these equations is discussed. The presence of surface-active components affects both capillary rise and displacement pressure and also seems to influence the rate of fluid flow.

Jan 1, 1942

By Richard E. Ellwanger

Methods of utilizing flocculents as settling and filter aids for mineral processing slurries are reviewed. Broad chemical classifications and techniques for proper dilution, multiple addition, and combination treatments are discussed. A variety of custom built and commercially available systems for makeup and delivery of flocculents to the application points are in use throughout the mining industry. Those concepts which, in the author's opinion, are particularly important to the successful makeup and we of flocculants are presented in relationship to the available makeup and feed systems. Actual industrial applications are included in the presentation.

Jan 1, 1982

AS you have been able to observe, I have up to the present demonstrated as, well as I knew how in writing the art of casting- and the methods of making moulds and of baking them; then the arrangements of the furnaces for melting the materials, including those made for melting by reverberation of flames or with bellows and charcoal, and the hearth, basket, ladle, and other similar instruments customary in such operations. Now I wish to show you how to bring to their conclusion the works for which these instruments are made, and show

Jan 1, 1942

By Richard Klimpel

In this paper various formulae are developed which can be used to estimate stream flow rates or weight ratios given information on the stream components. The type and level of experimental error present in the stream component analyses does have an important bearing on the numerical values (and reliability) of the weight ratios calculated by the various formulae. A simple but theoretically sound method is shown for selecting appropriate estimation formulae for any given engineering operation. The derived formulae are applied to sets of experimental classification data for illustration purposes.

Jan 1, 1980

By Angelus S. C. Owili-Eger

This paper discusses a model for groundwater quantity prediction at operating sections of underground mines. The approach involves the development of a mathematical model for the movement of water through an integrated (unsaturated-saturated) flow domain within a definable watershed. The model is programmed for the IBM 370/168 computer using the method of finite difference approximation coupled with a finite element analysis. The conceptual and computational aspects of the model have been validated with both experimental and field data and applied to an active coal mining operation located in central Pennsylvania.

Jan 1, 1977

By J. A. Herbst, D. W. Fuerstenau

An analysis of the kinetics of dolomite grinding in a dry ball mill reveals that the following approximations apply for the parameters of the batch grinding model: (1) the size discretized selection functions are proportional to the specific power input to the mill, and (2) the breakage functions can be taken as invariant. These approximations are shown to provide the basis for accurate predictions of product size distributions obtained for several mill speed, ball load, and particle load combinations within the normal ball mill operating range. The engineering implications of these findings are discussed.

Jan 1, 1974

By Erik G:Son Odelstjerna

ALTHOUGH the Swedes have not taken as prominent a position in the open-hearth as in the Ressemer industry, the successful development of which in Sweden has been described by Prof. Åkerman, in a paper read before the Institute,? nevertheless our work with the Siemens-Martin method may possess some interest, even for countries outside our own, and especially for the United States, where the charcoaliron industry competes with that of Sweden for the first rank in extent and importance. I take the liberty therefore of giving in

Jan 1, 1895

By P. J. Connors, William J. McCormick, F. B. Olender, Jerome F. Sheldon, Donald T. Mylar, Edgar T. Gregory, Owen S. Roberts, H. Colijn

A quiet revolution has taken place in the conveyor belt industry. Man-made materials, improved production facilities, better splicing techniques and emphasis on repair and maintenance have all contributed substantially to lowering material handling costs for the mining industry. Formerly the rubber industry had only cotton for a belt carcass and tree grown rubber for the protective cover. Monofilament rayon, with desirable elongation and elastic properties, was the first synthetic fiber to be used in place of cotton. But wet strength and other limitations restricted its use, and the conveyor belt industry turned to nylon.

Jan 3, 1972

By AIME AIME

WHEN H. I. Smith joined the Institute back in 1908, he was an instructor in mining and metallurgy at Penn State the college from which he had graduated the year before with a B.S. degree. He had not gone far afield for his education, for he was born, February 15, 1984 at Finleyville, Pa., a small village some fourteen miles south of Pittsburgh and without doubt famous chiefly as H. I.'s birthplace. The summer that he graduated he took a trip to the copper mines Arizona and Mexico and en route worked for four weeks for the Portland Gold Mining Co. at Cripple Creek, Colo., as a mucker and trammer. The next summer he roamed farther afield mines and metallurgical works in Europe. Wishing to see more of Arizona, he left the Penn State faculty early in 1909 and went out to Wenden in that State to become mining engineer and assistant superintendent of something called the Corona Copper Co., with 72 mining claims and a one-mule-powered whim for a hoist. When that job folded he helped build the Santa Fe railroad from Parker. Ariza., to Danby Cialif., and then came back to Pennsylvania to enter Government services as a junior mining engineer with the Bureau of Mines.

Jan 1, 1943

By K. R. Crocker

PRIMARY blasting at the open pit of the Cananea Consolidated Copper Co. has been developed to meet several conditions peculiar to the operation. Mining at Cananea is not confined to the open pit but is in conjunction with the underground mine which has been in operation for many years. Several old stopes included in the pit area were filled with waste obtained in stripping for the pit. The main haulage tunnel for the underground ore passes directly under one section of the pit and at present is but 180 ft below the pit floor. The pit as originally laid out called for an overall final pit limit slope of 60°. However, the upper 275 ft - a fairly soft oxidized capping, was carried at a 50° slope and the lower benches, which constitute 750 ft in combined height, are being mined to an over-all final slope of 60°.

Jan 6, 1950

By J. L. Wyatt

THE strain sensitivity, K, a property of metals defined as the unit change in electrical resistance per unit strain, was measured for commercial purity titanium wire to determine its usefulness as a strain gage material. A Kelvin double bridge, accurate to 0.000001 ohm, was used to make measurements from 0 to 1 pct total strain. A positive value of 0.17 for K was found. This compares with 2.15 for constantan and 3.5 for cold-worked invar, two of the more common strain gage materials. The effect of temperature also was determined. It was found that a change in temperature of 30°F caused the same resistance change as 1 pct strain. It is therefore concluded that titanium would have utility as a strain gage only if the thermal fluctuations in the specimen could be controlled to a high degree and in applications of very large total strain.

Jan 1, 1953

The income of the Institute is derived from dues, subscriptions to MINING AND METALLURGY and sale of publications. These sources are fortunately supplemented by the interest from invested funds now amounting to over $500,000, a considerable portion constituting endowments for especial purposes. Aside from the medal funds the principal endowments are the James Douglas Fund for support of the Library, the Rocky Mountain Fund and the Seeley W. Mudd M.emoria1 Fund. The income from the two last named is available for the support of research and a variety of other purposes. It is allocated by the Board of Directors upon recommendation of standing committees in each case. An active effort is being made to increase the endowments of the Institute, it being felt that unusual opportunities exist for research and public and professional service through the organization and at a minimum of expense.

Jan 1, 1932

By John F. Abel

The following quotation is from "Guidelines for evaluation of undergraduate curricula in geological engineering, mineral processing, and mining engineering" prepared by the Committee on Education of SME of AIME. "The objectives of the Engineers' Council for Professional Development (ECPD), as delineated in its constitution, are: (a) To promote and advance all phases of engineering education with a view to the promotion of the public welfare through the development of the better educated engineer and engineering technician." (Italics added.) The problem is that no one has as yet seriously developed a method of supplying engineering technicians. There were great hopes that the expansion of junior colleges would help satisfy this need. Sadly, they have not; and it appears they are unwilling or unable to supply the need for mineral engineering technologists. Apparently, the junior colleges cannot afford staff for such courses, even when the colleges are located in mining districts.

Jan 1, 1971