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By Steven G. Jansto

Carbon content and continuous casting parameters affecting solidification behavior, such as super heat, mold level fluctuation, heat transfer, fine grain chill zone depth and other process solidification parameters directly influence the surface and internal quality of the steel strand. The carbon content, resultant fine grain chill zone depth, the equiaxed-columnar transition zone and the strain energy are the primary drivers that govern hot ductility behavior. These factors influence the propensity for crack formation during the unbending section in the continuous casting process. Elements such as microalloys exhibit secondary or tertiary root causes for crack formation and are not the primary crack formation root cause. This solidification research identifies that the traditional hot ductility as measured via the percent reduction in area (%RA) at elevated temperature grossly overstates the minimum ductility required to assure crack-free casting of microalloyed steels. The strain at the ultimate tensile strength exhibits a very high correlation coefficient with strain energy while an extremely low correlation coefficient is exhibited with %RA.

Oct 30, 2017

By Raúl Daniel López

Ternium-Siderar steelmaking has been focused in permanent improvements and process optimization. At present the Slab Continuous Caster N°1 has been totally transformed after 20 years of uninterrupted work. The authors of this paper summarize and comment on aspects which were the main changes and place emphasis largely on those technological developments in which they have been active during that period. Productivity and quality have been our goals during the last 20 years; it has led us to improve process and to achieve better control tools. In the development of this presentation, the authors will put special emphasis on the explanation of those works that were made following their own experiences through the technical personnel who belong to the staff of the company.

Jul 30, 2018

By Simon Chiartano

A global reflection on the design of blast furnace main runner was investigated in this paper. TRB Company used its skills and expertise to understand what the best option for this sensitive component is, including some innovative tools: intelligent block design for safety lining, thermal & thermomechanical numerical simulation, immersive measurement by thermocouples, IR thermal camera, 3D laser scanner.

Oct 1, 2019

By Paul Pugsley

The need for dimensional measurement of products has always been there, now with the industry 4 push to further understand measure and to record process parameters is more important than ever. This applies to both flat and long products, camera systems have always provided the method to measure, stereo Linescan cameras for flat products and innovative applications using 2D and Linescan cameras for long products. Instrumentation will become more important to producers enabling processes to be better controlled and understood, that aim being to make the production process understandable more repeatable and less reliant on operator influence. Primetals Technologies Ltd offer solutions for all types of products.

Oct 30, 2017

By Priscilla Pessin Coppo

The prevention of dental enamel wear has particular relevance for preventive and restorative purposes in dentistry. The wear damage can increase due to salivary disorders and/or parafunction (bruxism); antagonists incisal surfaces become flat and coincident. This study aims to investigate the wear behavior and the related mechanisms in sliding pairs of conformal incisal enamel, with similar values of hardness and fracture toughness, with different applied normal loads and lubricated conditions. Bovine incisors, under pin on flat configuration, were tested in two lubrication condition (dry or with natural saliva) and two applied normal loads (8 and 16 N). The worn surfaces were investigated by 3D profilometry and SEM. The analysis of worn surfaces indicated mechanisms of brittle fracture, but with different severities. Under a normal load of 16 N and dry condition, wear is controlled by a brittle process: microcracking with flake-like wear particles, which results in high friction coefficient (> 0.85), wear rate and wear volume. On the other hand, under a normal load of 8 N and natural saliva, wear took place in the interprismatic region, with consequent exposure of prisms and fracture in localized regions. In this case, the friction coefficient was 16% lower and the wear volume was one order of magnitude lower. Under 8 N and natural saliva, the wear was greater than in the dry condition, probably due to tribochemical reactions.

Jul 31, 2018

By Daniel Carvalho, Marcos Viana, Leonardo Demuner, Herbert Castro

Intensive process and technology improvements related to the BOF converter — the key process to increase steel plant productivity and stability — have been performed at Ternium Brazil. This paper details the road map for process developments and investments in equipment technology, as well as the results achieved. The main topics of this development are the process control and optimization systems, slag forming model, oxygen blowing pattern, end-of-blow point control and slag carryover control. The outcomes of this development are improvements in the reblow rate, end-of-blow oxidation, direct tapping, slag carryover, slopping ratio, metallic yield and lining life.

Oct 1, 2019

By Carlos Gonzalez-Rivera

An alternative cooling curve analysis method focused on the experimental determination of the latent heat of phase changes and phase transformation kinetics is proposed in this work. The method analyses the cooling process of a metallic sample, initially liquid that is contained into a cylindrical metallic mold, both of known weight, thermally isolated at its top and bottom. The method is based on an energy balance associated with the experimental measurement of the temperature change of the sample and the mold during their cooling process. From the numerical processing of the cooling curves, are obtained approximate values of the acting global heat transfer coefficient as a function of temperature in order to describe quantitatively the energy exchange of the metal/mold system with its surroundings. These relationships and other experimental data are used to process the cooling curve of the sample and the mold during solidification, in order to obtain the latent heat of solidification.The method was applied experimentally to zinc and tin of commercial purity, initially liquids and contained into stainless steel molds in order to determine its ability to measure the latent heat of solidification. The obtained results suggests that this method shows a good potential to characterize the solidification of metals.

Oct 30, 2017

By Zhisong Chai, Wei Xu

Q&P steels undergo continuous multiple processes, including hot rolling, intermediate heat treatment, cold rolling and continuous annealing etc. The inheritant effect of initial microstructure could affect the final microstructure and mechanical properties of Q&P steels. In this work, effects of different hot rolled microstructure/texture on the final microstructure and properties subjected to Q&P process were investigated in Fe-0.38C-1.58Mn-1.6Si system. Different initial microstructures were generated combing different TMCP and cooling strategies. The microstructure and texture of hot rolled materials were characterized in detail. The hot rolled material was subsequently processed by intermediate annealing, cold rolling and continuous annealing. The comparison reveals great effects of the initial hot rolled microstructures, i.e. inheritance effect. The faster reverse transformation would lead to more sufficient austenitization and it would greatly weaken the inheritant effect of the initial microstructure. Although the difference of final phase fraction for different initial microstructures was not significant, the inheritance effect was mainly reflected in the effect on austenite morphology. For the mechanical properties, no obvious difference in strength was shown for the samples with different initial microstructures after Q&P heat treatment, but there was fluctuation in elongation.

Oct 1, 2019

By Günther Staudinger

Danieli Linz Technology has been honored at 4.1.2013 with the first contract for the exchange of a 350 t BOF converter for ArcelorMittal Poland Dabrowa Gornicza on a turnkey basis. This paper describes the new design features of this converter based on the development of a new Danieli converter suspension system. The issue was to install a new converter (incl. trunnion ring, suspension system and bearings) with maximum volume but keeping most of the existing equipment unchanged. So, the big tilting drives on both sides had to be reused and the existing foundation, pedestals as well as the bearing distance had to be maintained. Further on the welded coreequipment (vessel shell, trunnion ring, pedestals, slag shields, etc.) was manufactured in-house within the pressure vessel division of Danieli Thailand. Due to the huge dimensions of these parts the delivery had to take place in parts which had to be welded together on site under full production conditions of the steel plant. But also the erection had to be applied under this condition. Additionally the main support bearings, parts of the screening (doghouse) as well as an upgrade of the existing relining machine had to be delivered.

Jul 29, 2018

By Jens Kempken

A competitive landscape pressurizes the steel producers business, zero defect requirements from customers forces the operators for additional efforts in process control and quality management. The so called quality related cost, which include also rework, cost for downgrading or even scabbing of material is already a remarkable lever in a plants profitability breakdown. The introduction of advanced state of the art grades in the product portfolio requires already a budgeting for the expenses for R&D and quality management. PQA has been developed as a process and quality management software solution next to existing level 2 or level 3 automation systems. It is focusing on the analysis of process data, equipment information, in line quality measurement devices and trend analysis to obtain an answer whether the process is according to definition and expectation and whether the intermediate or final product can be shipped for further processing as prime material. Advanced analytics which are linked to an expert know how based configuration identifies deficiencies in the production and processing process. An intelligent, state of the art quality rating system evaluates tolerable deviations. PQA comprises the software platform including the database, data configurator and collector from the different sources in the production process and units. The core element of the platform is the knowledge based expert know how package defining process and quality determining fundamentals. The paper describes the structure of the software package, it gives insights on the expert know how package, process and quality evaluation and points out the customer benefits, cost reduction, improvement yield, customer satisfaction increase. The link to recent operational references is given.

Oct 30, 2017

By Michael Windhager

UltimaTM rolls have been designed for intermediate and finishing stands of rod and bar and small and medium section mills. The rolls and rings are spun cast, with a highly alloyed working layer and a tough nodular iron core. Microstructure and hardness level can be adjusted over a wide range, which allows us to adapt the rolls to differing rolling conditions. After introducing the UltimaTM concept, this paper will describe the results of UltimaTM rolls achieved in various mill applications, like finish rolling of rebar, and slitting. Special emphasis is given to performance gains when using UltimaTM rolls, compared to standard rolls. This paper also examines the impact of UltimaTM rolls on mill and roll shop productivity.

Jul 30, 2018

By Davide Onesti

Electrode regulation is the technology at the heart of the AC and DC Electric Arc Furnace. As such, in the last decade it underwent continuous improvement to maximize the EAF performances, in terms of process efficiency, machine utilization and operator safety. Given this background, Danieli Automation’s efforts in the field of electrode regulation have been focused on fast response to scrap cave-in, compensation of supply variations, automatic resonance detection, transformer protection, dynamic regulation of the electrical and chemical set-points, coordination and control of slagging and foaming agents, arc irradiance supervision. An extensive analysis of operator utilization and feedback was also carried out to develop an innovative system HMI. In this field, the choice of the variables shown to the user is the key aspect to allow a prompt process evaluation by the operator, who can refer to a condensed set of useful data. This paper will describe the innovative features and embedded models of the electrode regulation module (Q-REG+) and the supervision HMI, together with the effects of their application on EAF process efficiency and system usability.

Oct 30, 2017

By Jorge Madias

Pin holes as a surface defect, and blow holes as an inner defect, occur in billet / bloom / beam blank casting, particularly for Si-Mn killed steel cast with metering nozzle and oil lubrication. If they are present in abundance or have a large size, they may originate defects in the rolled products. Their characteristics, factors behind their formation, as well as usual processing conditions that promote their occurrence are discussed. Finally, the evolution of these defects during reheating and rolling is analyzed, with industrial examples.

Aug 16, 2017

By Fernando Velazquez Guzman

Titanium is an alloying element used to refine grain size in steel and improve its physical and mechanical properties. In some stainless steels it is used to increase the resistance to corrosion by the precipitation of titanium carbides or carbonitrides. Its alloying performance is highly variable and depends largely on the stage of the secondary metallurgy process when it is added. Furthermore, the addition method (wire injection or direct addition) has a remarkable influence in secondary refining. This paper describes the tests performed in vacuum degasser (VD), with a highly compacted and encapsulated Ferrotitanium wire (FeTi HC). The yield of titanium in steel increased from 52% to 89%. Moreover, the consumption of the highly compacted Ferrotitanium was optimized.

Oct 30, 2017

By Washington Martins da Silva Júnior

In stamping process, sliding between metal sheet and forming tool leads to wear of tool surface. Maintenance of stamping tools involves polishing the tool edge, or, in case of severe damage, replacement of the tool. Hard coatings have been applied on the stamping tool surfaces in order to reduce the maintenance cost causing a great economic impact in metal work industry. In this work, CrAlSiN coatings were applied by PVD onto SRV2W tool steel. The coating toughness was avaliated by the critical load in scratch tests. The following coating parameters were analyzed: 1- substrate surface finishing process; 2- coating architecture (multilayer or gradient); 3- chemical composition of the coating. AlSi concentration varied from the substrate/coating interface to the surface. Coatings were 3 µm thick. Scratch tests were carried out using a Vickers indenter. The applied normal load was varied from 0 to 13 N for a scratch length of 5 mm. In order to study the effect in the toughness, the substrate roughness was controlled by the finishing process before PVD coating. Samples subjected to polishing presented highest critical loads. Gradient coatings presented higher critical loads than those with a multilayer architecture. Coatings with higher concentration of AlSi near the surface supported higher loads before failure.

Jul 31, 2018

By Antonio Esposito

Saving energy and reducing resource’s consumption by minimizing emissions are today great challenges in the coking industry worldwide. In order to achieve satisfying results, equipment as well as technology should be continuously improved and designed to minimize the energy requirements and to maximize the recovery of materials and energy. The sensible heat in coke pushed out of oven chamber takes up 35 ÷ 40 % of energy consumption of coke oven. Usually the coke thermal energy is lost during traditional coke wet quenching, necessary to reduce the coke temperature for the storage and the following use in steelmaking processes. BPSL CDQ project is a sample how Paul Wurth’s technology allows to reach the energy saving goal and offers an alternative to traditional quenching. With the adoption of Coke Dry Quenching process, a considerable amount of this sensible heat in the coke can be recovered by producing steam; its production depends on various parameters, some of them battery related (Volatile Matters in red hot coke) and others CDQ system related (coke burning losses, superheated steam characteristics (i.e. P,T)), greatly depending also on boiler efficiency (heat exchange efficiency, insulation of the boiler itself, air leakage, etc.). The adoption of CDQ process reduces also the water consumptions in comparison with traditional quenching.

Aug 16, 2017

By Felipe Beluche Lima, Caio Augusto Silva Santos

Brazil is the largest producer of crude steel in the Americas by BOF process and many challenges come along with the increasing market demand. In the BOF, a tubular wall hood structure has been showing premature failures related to the overlay welded tube technology placed in the hood wall. The main root causes were: thermal fatigue at 1800°C, hot spot formation, high heat-affected zone (HAZ) leading to susceptibility of stress cracking, carburizing corrosion and superficial wearing. Based on that, co-extruded tube technology (named composite tube by Sandvik) was the alternative chosen to enhance hood performance without compromising BOF process. In order to rises safety and productivity, composite tube has 100% metallurgical bond assuring stable expansion, high heat exchange efficiency, better corrosion resistance and less rough surface finishing. It was highly suggested to many others mills due to similar and already existing reported cases.

Oct 1, 2019

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the ex-service condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 52 to 224 MPa producing rupture times varying from 5 to about 3950h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results obtained on a similar plate of the same material in the virgin condition.

Aug 16, 2017

By Cermets

Ti(C,N)-based cermets offer good high temperature strength, perfect chemical stability, excellent wear resistance, and relativly better machinability. In the present work, the tribological behaviors of Ti(C,N)/SiC sliding pairs lubricated in water and seawater were evaluated using a ball-on-disk tribometer. The experimental results show that a relatively low friction coefficient (about 0.025) can be obtained when lubricated with artificial seawater at the sliding speed of 200 mm/s, while the date is about 0.2 in purified water. The wear surface profiles and the lubricants collected after running-in process for the high/low friction conditions were compared. In addition, the effect of salt molar concentration of the lubricant on the Ti(C,N)/SiC friction properties was investigated. It was found that the smooth and flat surface is the premise to gain the low friction. At the same time, the proper concentration of silica colloid, which is affected by the salt ions, is also an essential one. Moreover, the high sliding speed (200 mm/s) is beneficial to achieve low friction.

Jul 31, 2018

By Salete Martins Alves

The future lubricants must be more environmentally adapted, with a higher level of performance lower total life cycle, cost than currently used lubricants. Environmental friendly, the biodegradable alternatives are available for a large variety of mineral oil based lubricants. Vegetable oils are the major source of these base fluids, although they have lower thermal and oxidation stability and even worse low-temperature behavior than mineral oil. These physical and chemical properties can be improved by chemical modification. The aim of this study was to evaluate physicochemical properties and film formation from modified vegetable oils. The vegetable oil was chemically modified by epoxidation reaction with acetic and formic acid using sunflower oils. Viscosity, iodine value, density, acidity value and thermal stability were determined for epoxidized oils. The film formation was analyzed using a HFRR tribometer. The results showed that epoxidized vegetable oils had excellent properties to be used as lubricant, and their tribological performance is higher than mineral oil.

Jul 31, 2018