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By D. C. Yates, G. V. Jolliffe

In the five coalfields of Staffordshire, there have been some 43 incidents of spontaneous fires and heatings which have required special attention in the past ten years. This total excludes incidents in the Thick Coal Seam of South Staffordshire, which was worked until 1967, and which was subject to an almost continuous series of heatings. The incidents have been classified to show the sites of occurrence, the contributory factors which may have caused them and the treatments applied to them. The remedial techniques, as practised in Staffordshire, are dealt with in detail, with particular reference to standard methods of stopping-off. Precautionary measures taken are described, including a "liability to spontaneous combustion" classification of all seams, and the setting up of an emergency organization with emergency stocks of materials and equipment. The paper is concluded by a few words on the organization and control at the time of an incident.

May 23, 1905

By Paul D. Merica

This year of 1926 marks the 40th. anniversary of nickel mining in Canada. Although the first nickel mine of the Sudbury basin was discovered in 1883, it was not until 1886 that the Canadian Copper Company was organized and actually began to mine copper-nickel ore from the Lady McDonald, Stobie and Evans mines. The intervening years have witnessed some exceedingly interesting nickel history, particularly interesting and gratifying as well to Canadians. Forty years ago, at the inception of Canadian nickel mining, the world's consumption of that metal was about 1000 tons per annum and this was supplied largely from New Caledonia ores refined in France. This nickel was used principally for the production of nickel-silver, coinage alloys, and for nickel-plating. No processes were then known for refining the Sudbury ores nor for the separation of copper from nickel. Consequently, the pioneers in Canadian nickel mining faced the double problem of finding a method of treating their ores, and of finding a market for the nickel when and if they could extract it.

Jan 1, 1926

By Henry F. Hebley

THE solid fuel industry, especially that branch represented by bituminous coal, is gradually becoming aware of its ? paramount importance in a world where there is an ever increasing demand for the products of a mechanical age. In practically every process of manufacture, the necessity for energy in some form is being multiplied. Some of that prime energy is derived from water power-hydro-electric schemes, flood control schemes, etc. - but often the electrical energy thus developed is generated at great distances from the load centres, requiring long transmission lines with consequent transformer and transmission losses. A few plants have harnessed the tidal power of the seas and one has harnessed the energy of the wind in a modern manner. All of these schemes are dependent on certain natural geographical, hydrographical, and physical advantages of terrain, as well as an adequate area of consumption of the energy developed. If flood control is the primary object, then power generation is a by-product; and the economics of large capital expenditure on power generating equipment must be considered in that light.

Jan 1, 1945

By H. M. Thorne

Oil shale, a potential source of products presently obtained from petroleum, is found in many countries. The most extensive known deposits from the standpoint of potential shale oil in place are those in Brazil and the United States of America. Mining methods used for oil shale range from open-pit operations for shallow deposits to room-and-pillar and longwall techniques for deposits with thick overburdens. Oil shales from different sources vary greatly in the amounts and types of organic and inorganic constituents. By retorting, the organic material is converted to oil, gas, and coke. The largest percentages of oil are obtained from materials having the highest hydrogen content. Over 2,000 retorting systems have been patented, but only a few have been used industrially, and no single process seems best for all types of shales or economic conditions. Shale oils have different characteristics, depending on the source rock and method of retorting. They contain large quantities of olefinic hydrocarbons and more oxygen, nitrogen, and sulfur derivatives of hydrocarbons than most petroleums. Consequently, petroleum refining methods usually must be modified for shale oil. This is particularly true in catalytic processing. Hydrogenation, even under mild conditions, improves shale-oil refinability. Several byproducts may be obtained from both the retorting and refining steps,

Jan 1, 1964

By R. W. Stahl

An award is a form of recognition given for superior performance in a special field of endeavor. Each year awards are given by the Joseph A. Holmes Safety Association and the National Safety Council to mineral industries' mines, quarries, and plants that have worked a specific number of man-hours without a lost-time injury. These awards have a dual significance in that they prove that efficiency can be attained without injury to persons. Safety awards do not result from luck or good fortune but do result from sincere desire coupled with sufficient effort and cooperation to achieve a desired goal.

Jan 1, 1963

By A. J. Forney

Recent experiments used catalysts of plate assemblies in synthesizing high-Btu gas and gasoline indirectly from coal. A gas with a heating value of 925 to 943 Bt-: per cubic foot has been prod u la the hot-gas-recycle pilot plant from synthesis gas (3H2+100) with lathe turnings used as catalyst in the first reactor, and assemblies of parallel sprayed plats of nickel in the second. Solid plates made of Raney nickel, and steel and aluminum plates sprayed with Raney nickel or nickel oxide were tested. Those catalysts had very low resistance to gas flow; 90 percent lower than nickel granules used in previous experiments. In a single stage of synthesis thee nickel plates were only partially successful. Although the heating values of the product gas ranged from 856 to 941 Btu per cubic foot, the carbon monoxide content of he gas was above 0.1 percent. Both steel and wrought turnings were tested in single-stage synthesis, but the conversion of hydrogen and carbon monoxide was too low to attain the desired heating value of 900 Btu per cubic foot in the product gas. Assemblies of plates thermally sprayed with fusel iron were tried in an experiment to make gasoline. A gasoline yield of 52 percent (of the hydro¬carbons produced) was obtained using a 1H2-10O feed These sprayed assemblies were in service for 1,500 hours, the longest that this type of catalyst has been used. When a second reactor containing Raney nickel catalyst was added in series with the first reactor, complete utilization of the feed gas was obtained because in addition to the liquid product, a high-Btu gas with a heating value of 800 Btu per cubic foot was made.

Jan 1, 1965

By Frank G. Snyder, Paul E. Gerdemann

The Southeast Missouri lead district, located about 70 miles south of St. Louis, embraces four important sub-districts and several minor ones. The important sub-districts, in order of discovery, are Mine La Motte, the Old Lead Belt, Indian Creek, and the Viburnum Lead Belt. Descriptions that follow are of geology and ore deposits of the Old Lead Belt. The ore deposits are stratiform in character and are localized in a narrow carbonate bar and algal reef environment on the flanks of exposed Precambrian of the St. Francois Mountains. Ore structures include a variety of primary depositional features such as pinchout zones, disconformities, ridge structures, reefs, and submarine gravity slides. Faulting, prior to and during ore deposition, "prepared" the host rock and strongly fractured areas are mineralized much more intensively and extensively than unfractured parts of the same sedimentary structures. The deposits are epigenetic in character. Mineralization is believed to have occurred at the time that post-lower Ordovician faulting took place. The mineralizing solutions are believed to be concentrated brines from adjacent basins that moved out of the basins during faulting, uplift, and erosion of the St. Francois positive area.

Jan 1, 1968

The negative effects of pyrite and pyrrhotite on thiosulfate gold leaching have been investigated. Possible remedies to reduce some problems are discussed. In a gold bearing pure silicate ore, 92% of gold could be extracted within 3 hours using a solution containing 0.2 mol/L ammonium thiosulfate, 0.9 mol/L ammonia, 30 - 300 ppm copper sulfate and 8.6 ppm dissolved oxygen at pH 10.26. The thiosulfate consumption was 7.1 kg/t under these conditions and could be further reduced to 3.5 kg/t by decreasing the dissolved oxygen to 0.3 ppm. Addition of 16% pyrrhotite or pyrite into the silicate slurry led to a decrease in gold extraction by 2% or 9% respectively and an increase of thiosulfate consumption by 11 kg/t or12.8 kg/t respectively in three hours. Several adjustments, such as increasing copper ion and ammonia concentration and reducing the dissolved oxygen level to 0.3 ppm resulted in increased gold extraction and lower thiosulfate consumption despite the presence of these sulfides.

Jan 1, 2005

By H. W. Wainwright

.1. The purification pilot plant and the equipment, solution, and gas cycle used for removing hydrogen sulfide and carbon dioxide are described. 2. As sulfur recovery is necessary in any large Fischer-Tropsch plant, pilot-plant runs were made at 300 p.s.i.g. to study the efficiency of tri-ethanolamine solutions in removing selectively hydrogen sulfide from gases containing varying amounts of carbon dioxide. 3. Aqueous solutions of TEA of 20, 30; 35, and 50 percent were investi¬gated. Data indicate that 30 to 35 percent is the optimum concentration if both selectivity and economy are considered. Slightly better selectivity is obtained with the.20 percent solution, but steam consumption is greater owing to the higher solution rates. Results from our pilot plant runs indicate that a 50 percent solution not only produces an acid gas of lower hydrogen sulfide content but also requires high solution rates to effect hydrogen sulfide purification. 4. Data from 37 runs using TEA are presented in tabular form. In addition, the data are correlated and presented in three sets of curves. By using these curves, it is possible to calculate the compositions of the purified and acid gases for various raw gas mixtures. 5. In cooperation with the Southern Natural Gas Co., investigations were carried out at 300 p.s.i.g. on the simultaneous removal of hydrogen sulfide and carbon dioxide, from gases using various concentrations of diethanolamine. 6. Data from 17 runs employing 20, 30, and 40 percent DEA are reported in both tabular and graphic form. 7. A comparison of the data from one DEA run made at 200 p.s.i.g. with those from the runs operating at 30O p.s.i.g. shows float the absorption capacity of the solution, and, hence, the steam requirements per gallon are about the sage for both pressures. .The only real advantage of the higher pressure is the additional volume of gas that can be treated. 8. The quantity of steam needed to reactivate fouled TEA and DEA solutions increased as the reactivator pressure was increased about 1,0 to 1.1 pounds of steam was required for each gallon of circulating solution when the reactivator was operated at 5 p.s.i.g. 9. A curve is included that shows the effect of the hydrogen sulfide con-centration in a lean 35 percent TEA solution on the hydrogen sulfide content of the purified gas and on steam consumption for reactivation. 10. Both TEA and DEA reduced the organic sulfur content of the raw synthesis gas considerably. Analyses of the lean amine solutions showed a gradual build up of sulfur compounds, indicating that the compounds formed by the amines and organic sulfur do not break down under the ordinary operating conditions of the reactivator. 11. Considerable operating difficulty was encountered in the pilot plant owing to foaming of the amine solutions. Laboratory experiments in which the effectiveness of certain antifoam agents was studied showed Alkaterge C to be most promising for the particular conditions studied.

Jan 1, 1952

By Andrew St. Amant

This report reviews the first three "investigative and concept generation" phases of the referenced contract, and details task performance of Phase IV. This last phase integrated the most promising concepts from Phases I, II, and III into a prototype detailed design which was manufactured, and then tested on a mine locomotive. The concepts developed during the first three phases provided "Improved Pole Tracking," automatic "Rapid Pole Retraction" in the event of dewirement, and servo-operated "Remote Pole Repositioning" on the trolley wire. The Appendix of this report supplies detailed information for the design and construction of the prototype system which is comprised of an RCB (Remotely Controlled Base subassembly), an RCL (Remote Control Lever subassembly) and an SAU (Servo Amplifier Unit) subassembly.

Jan 1, 1980

By WILLETT G. MILLERS

GENERAL RECEPTION COMMITTEE.-Willett G. Miller, Chairman; F. G. B. Alan, Hon. Frank Cochrane, Eugene Coste, Thomas W. Gibson, Cyril W. Knight, J. C. Murray, 0. N. Scott, Alan Sullivan, J. B. Tyrrell, J. W. Wells, A. B. Willis. COBALT RECEPTION COMMITTEE.-Arthur A. Cole, Chairman; Will. Ask with, R. W. Brigstocke, Robt. Bryce, Fred Coombs, M. I. Culbert, I. R. Drummond, J. W. Evans, A. Ferland, F. N. Flynn, E. L. Fraleck, S. R. Heakes, Joseph Houston, D. L. Jemmett, I. R. Jones, Major Leckie, Capt. Jack Leckie, R. W. Leonard, W. H. Linney, Alexander Longwell, Frank Loring, Murdock McLeod, John Martin, D. B. Rochester, W. E. Running. COBALT RECEPTION COMMITTEE (Ladies).-Mrs. A. A. Cole, Mrs. A. Edwards, Mrs. R. Jennings, Mrs. S. H. Logan, Mrs. A. Longwell, Mrs. H. F. Marsh, Mrs. J. Smith. SUDBURY LOCAL COMMITTEE.-Mayor L. O'Connor, Chairman; S. Fournier, Secretary; A. H. Beath, W. J. Bell, F. B. Bennett, D. M. Brodie, J. S. Buchanan, F. C. Busby, Wm. Chalmers, R. Dorsett, W. A. Evans, John Frawley, J. S. Gill, A. B. Gordon, J. G. Henry, T. N. Kilpatrick, Major Leckie, Chas. McCrea, John McLeod, Wm. McVittie, R. Martin, R. S. Mitchell, J. H. Morin, J. A. Orr, James Purvis (President Board of Trade), C. R. Reid, Major Smith, W. W. Stull, J. F. Templeton, S. E. Wright. The first session, held in the Banquet Hall of the King Edward Hotel, was called to order Tuesday, July 23, 1907, at 2.30 p.m., President John Hays Hammond presiding. Prof. Willett G. Miller, chairman of the General Committee, introduced Alderman J. J. Graham, who, in behalf of the City of Toronto, extended a hearty welcome to the members and guests of the Institute. To this welcome, President Hammond replied in a few well-chosen and hearty remarks. In the hall in which the session was held there was exhibited a fine, full-length, life-size portrait of Dr. Rossiter W. Raymond, in 1871 Vice-President and acting President, in 1872, 1873 and 1874 the elected President, in 1876 and 1877 Vice-President, in 1883, by appointment of the Council, and for the last 24 years by annual election, Secretary, of the Institute. Dr. James Douglas, of New York, N. Y., on behalf of numer-

Sep 1, 1907

By lchiro Aoi, Hideo Nakae, Makoto Yoshida, Makoto Ishino

"The influence 6f gravity on the microstructure of unidirectionally solidified Cu-Pb monotectic, Ag-Si and Fe-C eutectic alloys is studied. In order to examine the influence of gravity in a lg environment, both the upward (opposite to direction of gravity) and downward (direction of gravity) unidirectional solidifications are carried out. The results are as follows: (1) For the upward solidified Ag-Si eutectic alloy, the eutectic Si continuously grows. On the other hand, in the downward solidified Ag-Si alloy, the Si grows discontinuously and disperses into the ex-Ag matrix. (2) No morphological difference in the eutectic growth is observed between the upward and downward solidified Fe-C eutectic alloys. (3) In the case of the upward solidified Cu-Pb monotectic alloy, a banded structure, which consists of Pb-rich layers and Cu-rich layers, is observed. However, such a banded structure -is not observed in the downward specimen. (4) The banded structure is not found in the upward solidified Cu-Pb-0.05 mass % Al and Cu-Pb-0.1 mass % Al alloys. In the Cu-Pb-0.05 mass% Al alloy, a fibrous -L 2 phase grows continuously parallel to the growth direction at low growth rate. Only 500 mass ppm addition of aluminum induces the morphological change of the monotectic L2 phase.IntroductionThe influence of gravity on the solidification of eutectic and monotectic alloys has been investigated in microgravity environments [l-9]. The purpose of these studies was to obtain a homogeneous microstructure of eutectic or monotectic alloys, most of which alloys tend to solidify with macro-segregation under gravity. However, in most of the previous experiments, e.g., in free fall systems, in aircraft or in space laboratories, the growth rate was too high to realize a planar solid/liquid interface. This would be due to the limited time for solidification. Thus, it was difficult to examine the influence of gravity on the planar coupled growth of the eutectic or monotectic alloy. In this study, both the downward U.D.S. (unidirectional solidification by gravity) and upward U.D.S. (opposite direction to gravity) are carried out in order to examine the influence of gravity on the coupled growth in a lg environment [l0, 11]. In the case of the downward U.D.S. using the current Bridgman method, the molten alloy must be confined between the crucible and the solid."

Jan 1, 2000

By Guichao Wang, Geoffrey M. Evans, Graeme J. Jameson

"In this paper we present a new method for studying the detachment of particles from bubbles in a rotating turbulent eddy. The eddy is formed in a wall cavity in a two-dimensional water tunnel with transparent walls. When water flows through the tunnel, a vortical flow field develops in the cavity. The properties of the eddy can be modulated by changing the free-stream velocity of the water in the tunnel. Bubbles are pre-loaded with one or more particles in a fluidized bed flotation device located beneath the vortex cavity. Loaded bubbles are released one at a time into the cavity, and the motion of the bubbleparticle aggregate is studied using a high-speed video camera. The diameters of the particles and the bubbles, and the number of particles initially attached to the bubble, can be varied. The trajectories taken by the bubbles are quite complicated. In some cases, the bubble moves to the centre of the eddy, and particles rotate around its axis. If the rotational speed is sufficient, particles may detach due to centrifugal force. However, other modes were observed, including inertial detachment due to rapid changes in direction of the surface of the bubble, because of changes in trajectory of the bubble as a whole, or because of pulsations and oscillations of the bubble surface. Clusters of bubbles held together by particles were seen to form and reform. In the traditional explanation for the detachment of particles in flotation cells, it is assumed that particles detach from bubbles rotating in an eddy due to centrifugal force (Schulze, 1977). Although the conditions assumed in Schulze's theory may exist, it is only one of a range of phenomena that can lead to the detachment of particles from bubbles in a turbulent vortex.INTRODUCTIONThe recovery of particles by flotation methods is dependent on the particle size. The recovery in the existing flotation machines reaches a peak for particle size, typically in the range of 20 to 100 µm. This size range varies as a function of the particle’s properties (type and composites). For coarser particles, the recovery drops very quickly (Gaudin, Groh & Henderson, 1931; Jowett, 1980). If the upper size limit can be increased for flotation, dramatic savings in the grinding energy can be achieved."

Jan 1, 2016

By Sabine Knott

The thermodynamic properties of four liquid ternary zinc alloys, Au-Sn-Zn, Ag-Sn-Zn, AI-Sn- Zn and Cu-In-Zn were measured with an electromotive force (emf) method at three or four cross-sections with an constant X:Sn or Cu-In ratio. At the Au-Sn-Zn and AI-Sn-Zn system calorimetric measurements were also carried out in order to compare the integral enthalpy of mixing from the direct measurements with the data of the emf measurements, which were derived by Gibbs-Duhem integration.

Jan 1, 2003

By Hans Lundberg

Magnetic methods have been used for more than three hundred years in prospecting for magnetic ores. More recently magnetic methods have been used for finding salt domes and studying certain geological formations. A number of instruments have been developed and substantial improvements made as to their sensitiveness and accuracy. Papers and articles written on magnetic methods are generally elaborate and technical, and the average prospector finds it difficult to obtain the necessary information as to how to operate the simple magnetic instruments to the best advantage. The miner's compass, dip needle, and inclinator are, indeed, very useful instruments and are easy to handle, and a great deal of valuable information can be gained if the instrument is properly operated and the results correctly interpreted. The lack of knowledge of the fundamental principles, however, has caused a great deal of disappointment. Other and more elaborate geophysical methods have recently come into the limelight, and the prospectors seem to have lost a great deal of interest in the dip needle. This is much to be regretted, because magnetic methods have a particular field of use. The present article is an attempt to help the prospector regain interest in the magnetic instruments and to show the use and application of a simple magnetic survey. If the prospector expects some useful help in his work, he must, of course, know the instrument, know how to take the readings, and know how to plot and interpret the observations.

Jan 1, 1929

By A. Galvan

High rate compressible media filter (CMF) tests produced exceptional total suspended solids (TSS) removal at hydraulic loading rates ranging from 97.8 to 122.2 m/h. The compressible media is manufactured from a robust resin fiber that can withstand low pH and temperatures up to 149 °C. The media porosity can be varied by applying compression onto the media. At 40% compression, the CMF can remove particles greater than 4 μ. Three synthetic test-samples were generated by Hazen Research Inc., (Golden, Colorado) to simulate the copper Pregnant Leach Solution (PLS), Raffinate and Electrolyte solutions used for the testwork conducted at their facility. The preliminary results showed that the CMF was very effective in removing TSS without the use of chemical conditioning from the above test-solutions with efficiencies of 98%, 97%, and 96%, respectively. Given the remarkably high hydraulic loading rates, the industrial equipment footprint would be minimized appreciably over conventional clarification and alternative filtration systems.

By K. Ono

A new process for extraction of titanium metal from its oxide is demonstrated. In this process, row material to be reduced is titanium oxide synthesized from ilmenite. The reducing agent is the Ca+CaCI2 two-phase mixture. TItanium is elaborated in the medium consisted of liquid Ca, Caq and solid TI02 at the temperature range 1200 to l300K by means of mixing mechanically the ingredients in the reactor into a smooth paste. Fluidity of the feed which enables continuous scheme depends on the CaCl2 content. The oxygen level of the reduced titanium is the range 500 to 1000 mass ppm varying with the operational conditions. The Ca+CaCI2 reducing agent is taken out from the electrolysis of CaC12 at 11401(, and this CaCl2 is produced by aqueous chemistry conversion using Cl2 gas recycled from the electrolysis.

Jan 1, 2001

By D. M. Ramsey

HIGH-INTENSITY magnetic separation as now practised in the commercial treatment of a large variety of industrial minerals is a com-paratively recent development, having had its practical beginning about ten years ago when it became necessary to devise more effective methods for the purification of the electric furnace abrasives and refractories-silicon carbide and fused aluminium oxide. The fundamentals of magnetic separation are, of course, very well under-stood; bur while very, very old in principle, the process has, in recent years, been developed to a point of far greater usefulness than heretofore. In fact, until the development of the high-intensity process,. magnetic separation was limited largely to the removal of tramp iron? with magnetic pulleys and the removal of the very highly magnetic portions of industrial minerals by means of horizontal conveyor-belt-type separators. All magnetic separation processes depend for their success on the fact that various materials are kinetically influenced to a greater or lesser degree by the force that we speak of as 'magnetism'. We have now come to regard 'magnetic separation' and 'high-intensity magnetic separation' as two different and distinct methods. However, both depend upon the reaction of a particle when placed in a magnetic field. The common types of magnetic separators quite generally operate on the principle that a magnetic particle can be lifted by a powerful magnetic force from a stream of material moving on a belt or other type of conveyor. The application of the force removing magnetic material by this scheme is directly opposed to the force of gravity and is, therefore, limited to sub-stances of a relatively high order of magnetic susceptibility, such as metallic iron and magnetite. Until a few years ago, one very important principle was almost entirely overlooked. Practically every substance is susceptible to some extent, at least, to magnetic attraction, and by the application of a magnetic force great enough, and properly applied, separations of materials heretofore considered 'non-magnetic' can be accomplished.

Jan 1, 1937

By T. Ahokainen, J. Pitkälä, J. L. Xia, A. Jokilaakso, J. Vaamo

"The aim of the present paper is to use the two CFD codes to model the two phase flow in a water model ladle with central gas injection. The codes examined are CFX and Phoenics. An Eulerian two phase model is used and predictions are compared against the experimental data available. The results show that the codes can reasonably well predict the gas-liquid plume in the ladle, and predictions are generally in a good agreement with experimental data. However, differences do exist in predicting the gas volume fraction and velocity profiles. The results should be interpreted most carefully and cautiously, because they are very sensitive to the boundary conditions and dependent on the models for the physical phenomena involved. IntroductionSubmerged gas injection has widely been used in the metallurgical industry for more than a century. At the present, the use of gas is most effective in steelmaking industry where the advantages of the gas injection have already been long well understood. Effective mixing, large contact area between reactants, easy modifications and flexibility of the processes are the most important advantages. Disadvantages include refractory wear, blocking in the tuyeres, and splashing. These disadvantages can be reduced and advantages further improved by studying the flow phenomenon in process vessels. However, it is difficult to study flow in a real vessel because of the high temperatures and physical and mathematical modelling is therefore increasingly used in the process development work."

Jan 1, 1999

By R. F. Favreau, Patrice Favreau

"Ever since we have started to assist those responsible for blasting with blast simulation studies, we havebecome aware of an interesting aspect, namely that in 90 % of cases we are asked ‘‘Can you seek ablasting method which gives better fragmentation than the method which we use now’’. But after a visit to the site, and the evaluation of the fragmentation obtained with their present blasting method, it very often becomes evident that it is the ease of mucking and not the fragmentation which requires improvement. Hence we then proceed to do a simulation study the results of which are improved mucking rather then more fragmentation, and those responsible for the blasting always become very satisfied."

Jan 1, 2017