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By Yonghong Qin, Songbo Ma, Qi Zhang, Peng Gao, Jianwen Yu

Herein, the coal-based reduction was proposed to utilize the ferronickel slag of Jingchuan company. An excellent index with metallization rate of 99.22%, iron grade of 77.91%, and iron recovery of 92.79% was obtained at carbon addition coefficient 2.0, reduction temperature 1573 K, reduction time 60 min, the particle size of coal and ferronickel slag − 2.0 mm, and CaO content 15%. The 2FeO·SiO2 was reduced to Fe and SiO2 with the increase of temperature. The CaO could promote the reduction of iron oxide. Most of the sulfides (Fe, Cu, Co, and Ni) in the sulfonium were reduced to metal. The reduction degree increased with the reduction time and reduction temperature. The higher reduction temperature represented the higher peak value of reduction rate and the shorter time of reaching the peak value. The isothermal reduction process included three stages: early stage, middle stage, and late stage. The mechanism function were f(α) = 1/2(1 − α)3, f(α) = 3/2(1 − α)4/3[(1 − α)−1/3 − 1]− 1, and f(α) = 4(1 − α)[− ln(1 − α)]3/4, respectively. The activation energy of three stages was 183.498 kJ·mol−1, 420.077 kJ·mol−1, and 656.619 kJ·mol−1, respectively.

May 24, 2022

By Nikhil Dhawan, Shrey Agrawal

Feldspar, a low-alumina, and abundantly available aluminosilicate source, is explored in this study to extract aluminum and potassium values. The sample comprises lamellar layers of microcline and albite with quartz containing 17.4% Al2O3, 9.67% K2O, and 66.3% SiO2. Mechanical (milling) and thermal (alkali and acid baking) activation are investigated, followed by HCl leaching. The milling treatment up to 6 h is inefficient in phase dissociation and results in ~ 40% Al and K dissolution. The alkali thermal treatment yielded 80% Al and 71% K extraction. Direct precipitation of the dissolved Al and Si values yielded alumina purity of ~ 29%, and silica gelation separated SiO2 and improved alumina product (94% purity, 71% recovery). Acid baking yielded 98% pure alumina precipitate; however, Al and K extraction were limited to ~ 45% and 65%, respectively. The microwave-assisted alkali treatment was optimal with 800 W and 10 min processing conditions yielding 80% Al and 71% K recovery with 2.26 kWh/kg alumina of thermal energy consumption. The final product contains γ-alumina with a specific surface area of 87 m2/ g. Keywords Feldspar · Alumina · Potassium ·

May 18, 2022

By HONGWEI YANG, Lili Zhang

The oxidation behavior of copper smelting slag under non-isothermal conditions was studied by thermal analysis. The results indicate that the copper slag is mainly composed of fayalite ( Fe2SiO4) and magnetite ( Fe3O4). The oxidation behavior can be divided into two reaction stages with the increase in temperature; the first stage is the oxidation of fayalite to magnetite, and the second stage is the oxidation of magnetite to hematite. The two reaction stages cannot be strictly separated; that is, the reaction of fayalite is not complete, and magnetite has begun to transform into hematite. Based on the TG (thermogravimetric) curves, the ABS (Achar–Brindley–Sharp–Wendworth) differential and the Coats–Redfern integral methods were employed to investigate the oxidation kinetics of copper slag during the continuous heating process. The oxidation of fayalite into magnetite and amorphous silica phases occurs mainly in the temperature range of 673 to 1083 K. The activation energies calculated by the two methods are 193.69 and 195.52 kJ mol− 1, respectively. The reaction is consistent with Avrami–Erofeev equation, and the mechanism of oxidation is random nucleation and growth. The oxidation of magnetite to hematite occurs at 1083–1303 K. The activation energies are 308.79 and 328.77 kJ mol− 1, respectively. The mechanism conforms to the Jander equation and is controlled by the two-dimensional diffusion.

May 16, 2022

By Emily Sarver, Cigdem Keles, Jonathan Gonzalez, Nishan Pokhrel, Lizeth Jaramillo

This paper presents a case study of respirable dust characterization in a thin-seam coal mine in southern West Virginia. Samples were collected in various locations within the mine and analyzed using scanning electron microscopy with energy-dispersive X-ray (SEM-EDX), thermogravimetric analysis (TGA), and Fourier transform-infrared (FT-IR) spectroscopy. The study found high non-carbonate mineral content, particularly aluminosilicates and silica, in the dust. The results indicate that fine aluminosilicate particles may interfere with SEM-EDX analysis, leading to an underestimation of coal content. The findings highlight the importance of using multiple analytical methods to accurately characterize respirable coal mine dust.

May 5, 2022

By Neha Shukla, Nikhil Dhawan

The current study examines the extraction of rare-earth elements from trichromatic phosphor of discarded tube lights via baking processes. The Y2O3: Eu3+ (YOX) and BaMgAl10O17: Eu2+ (BAM) phases completely decomposed during acid and alkali baking with > 90% Eu and Y extraction. Prior, selective acid leaching of the YOX phase enhanced the acid baking process at a lower temperature (< 230 ℃). Feed acid baking showed a maximum 87% Tb, 36% La, and 17% Ce extraction at 500 °C, 0.5 h, 1 ml/g H2SO4, and alkali baking yielded 16.1% Tb, 86% La, and 73% Ce at 300 ℃, 0.5 h, 50 wt.% NaOH. The acid baking of the acid-leached phosphor yielded 72% Tb, 95% La, 63% Ce, ~ 95% Y, and Eu extraction at 300 °C, 0.5 h, 1.05 mL/g H2SO4. Lower Tb extraction during the acid baking of acid-leached phosphor can be attributed to the formation of Ba3Tb( PO4)3 and BaTbO3 phases. Insoluble Si3Tb5 phase formation and partial decomposition of CeMgAl11O19: Tb3+ (CMAT) phase in the alkali baking route leads to lower Tb extraction. The acid baking process is suitable for extracting Tb, Eu, and Y, whereas the alkali baking process is suitable for La and Ce. The thermal analysis of phosphor and flux interaction depicts that alkali baking is less energy-intensive than acid baking. In comparison, the one-step acid baking process and the two-step alkali baking process yielded desirable extraction results (87% Tb, total RE (rare earth) 78.5% and 50.4% Tb, total RE 59.3%). The product yield in the acid and alkali baking route of feed, acid-leach phosphor is 36%, 29%, and 39%, 28.2%, respectively, with ~ 98% mixed rare-earth oxide purity.

May 5, 2022

By Shi Wang, Hongbin Liu, Meiliang Wei, Wu Liu, Xiaojun Wang, Yuxian Ke, Xuepeng Song, Tiejun Tao

The study investigates the influence of water migration on the fluidity of fresh cemented paste backfill (CPB) with and without flocculant under variable shear rates. The research utilizes nuclear magnetic resonance (NMR), rheological tests, and scanning electron microscopy (SEM) to analyze water migration, rheological properties, and microstructure evolution. The findings reveal that water migrates to more stable states as shear rate increases, and the addition of flocculant enhances water migration and increases shear stress and apparent viscosity. The study establishes relationships between water content and rheological parameters, providing insights into the flow characteristics of fresh CPB for pipeline transportation.

May 4, 2022

By X. Chen, F. An, H. Chen, Z. Wang

The bottom drainage roadway plays a crucial role in preventing coal and gas outbursts by using underground gas drainage methods. Therefore, it is essential to select the ideal position of the bottom drainage roadway. In this paper use a combination of geological data and numerical simulation to study the ideal position of the bottom drainage roadway, we taking the gas drainage of the first workface of No. 3 coal seam in the Yuxi coal mine in China as an example. The geological study showed a limestone marker layer at an average vertical distance of 14 m from the first mining face. Using this marker layer, the bottom drainage roadway could be excavated without the risk of accidentally exposing the coal seam, and less crosscutting borehole drilling from the bottom drainage roadway would be required. Based on the needs of gas control, the layout of the bottom drainage roadway was selected as an external stagger type. Combined with the numerical simulation results, when located 20 m outside of the mining workface ‘footprint’ on the horizontal projection, the bottom drainage roadway was a sufficient distance from the stress concentration area during mining of workface 1301, which facilitated roadway maintenance. Furthermore, the length of the crosscutting boreholes is also relatively short, which reduces the amount and cost of drilling. The results of this study are expected to provide a reference for the selection of an ideal position of the bottom drainage roadway in field engineering.

May 2, 2022

By S. Sekhar, S. Bhargava, A. K. Godugu, J. L. Porathur

Cemented backfilling has enabled underground hard rock mines to extract orebodies more safely with improved ore recovery. It is important to estimate the minimum required strength parameters for a backfill mix by optimizing the binder percentage to enable cost-effective and safe stoping operations. We conducted three-dimensional numerical modelling to study the effect of various stoping parameters on the stability of a free-standing backfill wall. A Mohr-Coulomb material model was used for the backfill material and the rock-fill interface. A strength reduction technique, excluding friction angle, was employed to arrive at a minimum stable strength value for the backfill. For a given combination of strength values, the stability state of the backfill wall could be demarcated using a displacement and yield zone tracking method. The numerical modelling results are compared to some earlier theoretical models. From the simulations, a predictive equation is developed to predict the required strength parameters for a backfill mix to ensure a stable free-standing wall. Examples are given of the successful use of the predictive equation at some underground hard rock mine sites in India.

May 2, 2022

By Ed Revoort, Robert Schippers

In Rotterdam in the Netherlands the project ‘De Zalmhaven’ is being developed. The project consists of the realization of houses, parking facilities, two residential towers of 70 m and a residential high rise of 215 m. An artist impression for the project is given in figure 1. For the high rise a new development in the use of large diameter, drilled piles with a steel casing has been successfully utilized. In this article the installation method of 65 m long steel drilled piles in two consecutive sections is presented. The settlements for the building (and the influence on its surroundings) have been analyzed in detail using 3D Finite Element calculations, which will also be discussed. Finally there is focus on the results of settlement measurements carried out during construction in relation to the settlement prognosis.

May 1, 2022

By Stuart Hardy, Xiangbo Qiu

The South Bank Place project comprised the redevelopment of the iconic Shell Corporation headquarters in Waterloo, located on the Southbank of the River Thames in central London. The site was originally developed in the 1950’s and due to the monitoring of the underlying Bakerloo Line tunnels by the Building Research Station it has become a seminal case history for the long term swelling behaviour of London Clay. The redevelopment, undertaken by a joint venture of Canary Wharf Group and Qatari Diar, included demolition of the existing building (with the exception of the main towers) retention of the existing basement structure and the construction of eight new mixed use buildings, up to 31 storeys in height. The foundations for the new buildings varied according to the building height and the below ground constraints. Two of the buildings are partially founded in reused under reamed piles that were installed as part of the original 1950’s development. The paper describes the novel methodology developed to assess the re-use of the under reamed piles which builds on the guidance published by CIRIA and the BRE for straight shafted piles. The paper also describes the physical investigations and numerical analyses undertaken as part of the assurance process and the procurement of latent defect insurance by the client.

May 1, 2022

By Dipl. -Ing. (FH) Thomas Schmitt, Dr. Melvin England

Foundations in Geneva are difficult and expensive due a large overlayer of clay and silt above competent bearing material in the moraine. Common foundation schemes use deep barrettes or bored piles, first passing large, weak layers of soil before finally reaching acceptable, solid moraine with reasonable values of skin friction and end bearing resistance, thus requiring further deep penetration for the necessary length for load transfer in the moraine. Depths of more than 60 m (200 ft) in Geneva are common in this region. At the Onyx-Project Geneva Implenia Foundation Company also encountered these circumstances. Despite usual solutions Implenia referred to an old and well known, but still intelligent and in today’s words smart, efficient and economical solution. Using small shafts, passing the large layers of clay and silt, ending with the pile toe in the underlaying moraine with a belled or underreamed base was the technic adopted to save drilling time, reduce spoil and concrete, so finally reducing the CO2 footprint. Piles with enlarged base (“belled” or “underreamed”) are reported at the beginning of the 20th century, for example at Chicago, which has a quite similar geotechnical structure as Geneva with the need of deep foundations. The first pile base enlargements were built in hand-dug caissons with wood lagging and steel ring bracing. In the 50s and 60s piling works were more and more mechanized, driven by the development of more powerful cranes and specialized drill rigs. Additionally the first tools for mechanized base enlargement were invented around that period. This report describes the project situation at Geneva, the drilling and enlargement technique of the pile base, the verification of the design values with an in-situ bi-directional load test and the smart execution by reduction of CO2 and costs.

May 1, 2022

By Terzis D. PhD, Katterbach M.

While awareness around the environmental impact of existing grout materials and chemical binders is increasing rapidly, biotechnologies are growing traction as sustainable alternatives in groundwork operations. Herein we present the principles and application methods of bio-grouting. The term is used to describe a system which is based on soil, groundwater or marine enzymes which are able to catalyze the production of calcite replicating a natural phenomenon. The system’s end result are mineral crystalline bridges which act as binders to improve the geotechnical properties of soils. This paper presents a comprehensive description of bio-grouts, their underlaying mechanisms contributing to mineralization as well as environmental considerations. With their water-like rheology, bio-grouts have a wide application range and are minimally invasive, requiring only very limited injection pressures. The equipment is the same as that used in conventional cement grouting, and the reactant components are worldwide available or easily suppliable, which explains why bio-grouting has nowadays become a valuable and sustainable alternative towards efficient soil treatment. Recent developments in the last years have allowed to further increase the applicability and efficiency of bio-grouts to ultimately bridge the gap between research and practice. A case study is illustrated in this paper showing the successful implementation of bio-grout for the stabilization of weakly cemented sandstone to safeguard an adjacent road segment in Switzerland

May 1, 2022

By Jack Taggart, Chris Barker

Pile load testing strategies for large infrastructure projects and multi-phase building developments have historically justified cost and programme benefits for undertaking advance preliminary and working pile load testing. However, more recently piling and pile load testing strategies have included assessment of the embodied carbon to understand and present the carbon savings that can also be achieved. This paper gives an overview of the factors contributing to carbon and emissions in the construction of bored pile foundations and presents the methodology taken in assessing embodied carbon as part of the pile load testing strategy for a multi-phased building development in London. Potential embodied carbon savings for various bored pile types and load testing strategies are discussed alongside alternatives and other considerations including pile re-use and carbon offsetting to inform continual improvement for future projects.

May 1, 2022

By Marcel Bielefeld, Joost Bakker, Rob van Dorp

Pile load testing can be performed by a static, rapid or high strain dynamic (generally designated as dynamic) testing method. The static load test is often considered the “gold standard” of testing with the other methods merely ‘alternatives’. However, the rapid load test, as a quasi-static test, has all the positive elements of the static alternative: the direct measurement of loads and displacements. Moreover as stress wave phenomena have no influence, the interpretation of rapid load test results is more straightforward than that of dynamic testing, and also independent of the person performing the interpretation. This paper will explore the Rapid Load Testing method and illustrate the advantages and limitations through a case study in Rostock, Germany

May 1, 2022

By Packer M. L

Residual load development in driven precast piles has been widely researched in recent decades, however, cast-in-situ piles are often falsely assumed to be unaffected by this mechanism. In contrast to driven precast piles, driven cast-in-situ (DCIS) piles require adequate time prior to loading for the concrete hydration and curing processes to occur. The concrete-soil interaction is complex with several processes influencing the strains within the concrete pile after installation. DCIS piles are of particular interest given that residual loads can be developed during both the driving and casting phases. This paper present four instrumented end-bearing DCIS piles in which temperature and strains were monitored from installation, with the objective of identifying the processes contributing to the measured strains prior to testing. Strain gauges at all depths recorded a net compression and compressive strains continued to increase up to the commencement of load testing. Residual strains in the test piles were interpreted to be influenced by temperature (concrete and ambient soil and air temperature), consolidation of soils due to dissipation of excess pore water pressure, and swelling from absorption of groundwater. Several residual load interpretive methods are evaluated with the Siegel and McGillivray (2009) approach being consistent with the skin friction full mobilisation theory of the Unified Design method. The full-scale field tests presented herein provide a unique opportunity to examine DCIS pile behaviour, particularly given the lack of presently available published studies on these pile types.

May 1, 2022

By Scott White, Pishun Tantivangphaisal, Andrew Bell, Chris Barker

There has been considerable advancement in recent years in the tools, both software and hardware, available to allow efficient digitalization of site records during the construction of geotechnical works. Whilst these tools have excelled at replacing handwritten records, the ability to use digital records to validate design and construction requirements in real time or even within reasonable timescales has generally been limited to the development of bespoke ‘prototype’ project specific solutions. This paper describes the development and implementation of an industry standard design schedule and the benefits of the broad adoption of a single database schema for data recorded on geotechnical sites. The former has brought significant improvements and automation of the design process, whilst the latter has enabled the validation of the constructed works against design intent in almost real time. Further details of the standardized design schedule, already publicly available in the UK through the FPS, examples and lessons learnt from implementing digital site record systems on live projects are presented herein. The utilization of cloud computing technology and complex algorithms linking plant/rig instrumentation with design data can further automate construction sites using IoT (Internet of Things) best practices. The authors will share their experience of the recent deployment of a digitalized design-to-construction record system, give recommendations for future development and a call for an industry wide drive to finalize and adopt the AGS Piling data schema.

May 1, 2022

By Bastian Hoffmann, Christian Moormann

The paper presents results of an experimental study on the axial load bearing behavior of vibratory driven full displacement piles in comparison with impact driven and cyclic quasi-static installed piles in dense sand. The test setup and the measurement devices used to this end are explained. Subsequently, the results of the axial loading like load settlement curves are shown and the impact of the installation method is interpreted. The results presented in this work are mainly based on three installation methods: test series one investigates axial behavior of vibratory driven piles, test series two describe the same cyclic pile installation process but without dynamic influence wherein a special test setup developed to install the piles cyclic quasi-static in the soil was used. A third test series carried out using the conventional impact pile driving method served the purpose of not only comparing the results against vibratory driving, but also aided in isolating the effects of dynamics inherent to the vibratory driving process.

May 1, 2022

By J. E. De Waele, J. J. Lee, M. J. Mulheron, Luke R. Deamer

There is increasing demand for geotechnical contractors to commit to carbon reduction, net zero or science based targets. A lot of focus has therefore been placed on using low carbon materials and low emission rigs. However, whilst these are ways to help reduce carbon, there is a need to look beyond just substituting materials and fuels to meet net zero. Using the IEMA carbon hierarchy, there is a need to first look at eliminating and reducing emissions, before considering substitute materials. For example, in geotechnical designs, this may mean considering using ground improvement or reducing the number of piles, before considering using low carbon cements. Equally, for remaining emissions, this hierarchy means considering carbon negative products to offset emissions, such as ground source heat pumps. This hierarchy can also be applied throughout geotechnical contractor organisations. For example, considering video conferencing for meetings, before considering public transport or using an electric vehicle. This article explores the carbon hierarchy and how it can be applied to all areas of a geotechnical contractor’s business. Only through embedding this hierarchy across the business can geotechnical contractors achieve the step change required to meet net zero.

May 1, 2022

By Luca Pingue, Regine Jagow-Klaff, Franco Muratore, Carlandrea Albonico, Damiano Frontini, Rudolf Wernecké

This paper describes an artificial ground freezing (AGF) application carried out to ensure both watertightness and structural support for the safe excavation of four cross passages of the Forrestfield Airport Link (FAL) project in Perth. The line will deliver 8.5 km extension of the existing urban rail network connecting the growing eastern suburbs of Perth with the existing suburban rail network. The proposed soil improvement technique is adopted as a smart alternative to jet grouting from the surface since the use of heavy equipment with long vertical mast was not allowed due to the line underpassing an airport in operation. In this paper, details of the challenges and lessons learned during both design and construction phases are given. Furthermore, it is described the geometry and the installation of freeze pipes in presence of a massive steel frame, ventilation system and slurry pipes of the tunnel boring machine (TBM) in operation. It is also illustrated the web monitoring system to allow key personnel to follow in real time the development of soil temperatures, tunnel convergences and ground surface deformations as well as changes in the interaction between international parties involved due to the COVID-19 pandemic.

May 1, 2022

By Remco Offenberg, Marcel Bielefeld, Martijn van Delft

The question of the continued suitability of existing foundations arises when the function of the superstructure changes. This can occur when the superstructure is replaced or when the existing structure is expanded, leading to higher loads on the existing foundation. Quite often it is a challenge to define the suitability (with respect to integrity, bearing capacity or both). The lack of information on the existing foundation (such as pile dimensions, installation records, original soil investigation, design calculations, etc.) makes it frequently seemingly impossible to assess whether the foundation or foundation elements can be re-used. The paper outlines the tools available to an engineer to evaluate existing foundation piles for potential re-use. The paper illustrates the application of these tools through a few case studies from The Netherlands, including the evaluation of a 400 years old bridge foundation to address increasing traffic loads.

May 1, 2022