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By P. P. Gregory

ESTIMATION of re- serves in prorated sand fields has been discussed by S. A. Judson, H. D. Easton, Jr., and W. A. Schaeffer, Jr., in a paper that appears in Vol. 114 (1935), of the A.I.M.E. TRANSACTIONS. The purpose of this present paper is to extend the investigation to prorated flush limestone fields and to outline a method of procedure in determining the amount of oil originally in place and the amount of oil that can be recovered from such fields. Although it is possible to use the decline curves to estimate the amount of recoverable oil in certain limestone fields that are allowed to produce the oil at or near capacity production, such a method cannot be used in fields under severely restricted production rates. The problem is exceedingly complex due to fluctuation in the allowable rates of oil production over a wide range and at frequent intervals, and especially because of the heterogeneous nature of the reservoir itself. A well completed in a large solution cavity, capable of producing great quantities of oil per day, may be offset by a well of very limited capacity. Also, it is di5cult to arrive at an average figure for porosity in a given limestone reservoir due to abrupt variations in the character of limestone, in many instances even between two ad- joining wells. It is a safe statement that uniformity of porosity and permeability in limestone reservoirs .is nonexistent. It is evident, therefore, that the method of estimation of re- serves on the basis of per-acre content can give only approximate results.

Jan 1, 1935

By Fan Yang, Meigui Yi, Lan Xiang, Zhuoying Yang

This paper reported the calculation of the reaction heat in titanium-bearing blast furnace slag (abbreviated as TBFS)-H2SO4 system based on estimation of thermodynamic data of CaTiAl2O6 by mechanical mixture model. The thermodynamic analysis indicated that CaTiAl2O6 was more stable than the corresponding ternary oxides as CaO·TiO2, CaO·Al2O3, and Al2O3·TiO2. TBFS-H2SO4 system was highly exothermic since all of the reactions involved in the system were exothermic. For example, the increase of temperature from 25 to 200°C led to the increase of the release of the reaction heat in TBFS (100.0g)-H2SO4 system from 181.28 to 189.73kJ. Eighty-five to 90%of the reaction heat in TBFS-H2SO4 system was contributed by the reactions among CaTiAl2O6, CaTiO3, CaMgSi2O6, and H2SO4.

Feb 1, 2021

By G Ferguson a, P Carrasco, P P. A Dowd

International codes of practice offer broad definitions with respect to the classification of resources in terms of risk. Specific guidelines and protocols, to analyse sample data, carry out geostatistical appraisals, develop geological models and finally estimate and classify resources, are not addressed. Neither are detailed requirements for engineering mineable reserves from estimated resources. In addition, international codes of practice fail to distinguish between types of deposit, other than in broad terms, as for example, The AusIMM JORC Code (JORC, 1999) which makes reference to diamond and coal deposits. The objective of this paper is therefore to set in motion the process of specifying detailed protocols, acceptable to the international community, for the assessment, reduction and management of risk associated with the development and extraction of mineral deposits. Ordinarily, the main risks and issues encountered during the process of estimating resources and subsequent conversion to reserves, encompass:failure to understand relevant geological controls of mineralisation; validation of grade interpolation; optimism in geotechnical appraisals of dilution and stability and the consequent selection of inappropriate mining methods; metallurgical modelling of minerals and contaminants reporting to concentrates; appraising the hydraulics of heap leaching and the numerous factors that can affect recovery; difficulty of managing metal price cycles and changes in regulations within the constraints of long-term mining plans; and development of better evaluation techniques for mining ventures. Uncertainty is inherent in estimation and engineering work, and its identification, reduction and management should be a fundamental goal of all involved in the mining industry (Figure 1). Variability may be reduced by:following internationally accepted practices for the collection, manipulation and analysis of geoscientific data; and verifying that the procedures actually performed meet the associated standards. Increasing amounts of data will also reduce uncertainty, but only if the procedures used to collect and appraise such data follow the relevant procedures. It is thus the aim of a series of papers in preparation, Beniscelli et al (in prep), to put forward detailed guidelines, for:project sponsors û to provide a global view of the work and documentation needed to support requests for funding various phases of project development and budget approvals; geologists û to indicate a checklist of the requirements and standards for the exploration and estimation of resources; and engineers and economic analysists û the protocols for characterising, modelling, engineering and evaluating the extraction of reserves. It is therefore hoped to encourage the development of consistent standards for declaring reserves within the mining industry. Data from projects and operations will be utilised to illustrate the benefits of adopting a rigorous approach to estimating resources and engineering reserves, Beniscelli et al (in prep).

Jan 1, 2000

By L. A. Nazarova, M. Vandamme, L. A. Nazarov, R. I. Rodin

"The paper describes a new method of interpreting the “canister test” data for the quantitative estimation of gas-kinetic parameters of coal bed based on the developed model of gas emission from coal sample placed in a sealed container. The model accounts for grain-size composition of the sample, initial gas content S, as well as coefficients of diffusion D and mass transfer ?. The inverse coefficient problem is formulated to find S, D and ??from the data of pressure measurements in the sealed container. It is shown that the inverse problem is uniquely solvable if the pressure is dropped during the experiment. The method has been tested using the data from an underground coal mine in the Kuznetsk Basin.Based on the poroelastic model of a coal bed and Khristianovich’s concept about origination and evolution of the filtration zone F in the neighborhood of a degassing borehole the authors considered the corresponding direct problem on rock mass geomechanical state. It was offered interpretation method for data on pressure measurements in a plugged degassing borehole allows evaluation of the diffusion coefficient, the horizontal component of natural stress field and parameters of F. The related inverse problem of the mixed type is formulated, and the cost function is constructed. The analysis using synthetic input data has shown that the cost function has a number of local minimums arranged on the same straight line, one of the minimums being the inverse problem solution. INTRODUCTIONPre-mine degassing is an integral part of coal mining. It allows mitigation of induced accidents in mines (coal and gas outbursts, rock bursts) (Guide, 1990; Malyshev & Airuni, 1999; Seidle, 2011) and also furnishes an alternative and ecology-friendly energy source—methane (Rice, 1997; Nambo, 2001). Choosing an optimized pattern of degassing boreholes, as well as estimating degassing time and amount of gas recovered requires data on gas-kinetics indices of coal beds out of which the key parameter is a gas content S. According to the latest guidelines for coal mines in Russia (Ruban et al, 2012), mining is allowed if S in a coal bed section is under 7 kg/m3."

Jan 1, 2015

By Ratnakar Singh, Raj Kishore, Kisor Kumar Sahu, Ranjeet Kumar Singh, Ganesh Chalavadi

The Falcon concentrator is capable of separating minerals in fine size classes based on their differential density. Separation of mineral particles depends upon the fluid flow characteristics and relative movement of particles in a fluid. In the present study, a fluid flow characteristic inside the Falcon concentrator was established through experimentation and modeling. The Falcon concentrator has two fluid entry points: (a) Fluid entering through gravity assisted feeding system and (b) Fluid entering through the fluidized hole on the concentrator wall. In order to identify the role of fluid entering the concentrator, a tracer was injected into the system. As per the tracer based experimentation, it was established that fluid entering through the gravity based feeding system is responsible for thin flowing film formation in the stratification zone where particles are stratified based on their relative density. The momentum balance and continuity equations were simplified for a high centrifugal force field, and the fluid velocity profile was estimated inside the thin flowing film. Estimated fluid flow profiles will help to simulate the particle trajectories inside the Falcon concentrator. The influence of rotational speed, fluid flow rate, and cone angle on the fluid velocity profile were investigated. Fluid thickness over the concentrator wall is also estimated, and it is typically of the order of ~150–200 μm.

By C. Bazin

The fundamental error associated to the sampling of heterogeneous ore particles is unavoidable and can only be minimized by an adequate selection of the sample mass and/or size reduction of the sample before division into sub samples for testing or assaying. The preparation of ore batches to carry out the mineral processing evaluation of an ore is a sampling process. The fundamental error associated with the division of the ore into batches is responsible for the differences in the composition of the batches. This paper attempts by various means to assess the reproducibility of the gold content of test batches prepared from a gold ore sample. The results of the investigation shows that for fine gold grain sizes the variability in the composition of the batches is less than that predicted by Gy?s formula and that the gold grain size is a strategic information in the assessment of the gold content variability of test batches.

Feb 23, 2014

By M. Pötsch, A. Kluckner, P. Söllner, W. Schubert

"The in situ block size is a key parameter in the geomechanical characterization of rock masses. It describes the fracturing of the rock mass and thus is a measure for the degradation of the rock mass strength. Several classification systems use the in situ block size. For instance, the Geological Strength Index (GSI) requires the “blockiness” and joint surface condition factor as key input parameters. The “blockiness” has recently been related to the in situ block volume (Cai et al., 2004). Due to the limited information about the internals of a rock mass, it is not possible to determine the in situ block size directly. Currently, the in situ block size is determined by calculations using oversimplified models, vague estimations or, due to the lack of relevant information, it is neglected. As remote measurement systems have become available for rock mass characterization, a more comprehensive record of discontinuities can take place. Measurements can be performed on exposed rock outcrops and in particular on tunnel faces and walls, delivering the location, orientation, spacing and persistence of discontinuities at an arbitrary number and locations. An estimation of the in situ block size at the same level of sophistication is still not available. This paper aims at examining the relationship between visible and measureable information at the rock surface, and the in situ block size. Three-dimensional block model simulations were performed using the block model engine of the distinct element code 3DEC. Initial investigations focussed on the minimally required observation area in order to obtain reliable block size distributions. Based on a representative volume element, a reference distribution of the block area at the observation area for a specific discontinuity system was determined. Subsequently, the size of the observation area was decreased stepwise and each new distribution was compared to the reference distribution. For all analyzed systems, it turned out that the mean block area must be smaller than 1% of the observation area to achieve a reliable block size distribution. Further simulations focussed on discontinuity systems with three non-persistent sets. The results were compared to the formula proposed by Cai et al. (2004). A transformation factor T was introduced which replaces the persistence terms in Cai et al.’s proposed formula. The factor describes the correlation between block volumes generated by persistent and corresponding non-persistent discontinuity sets. The simulations included the variation of the discontinuity set spacing, persistence, and orientation. The mean and additionally the 25%-, 50%- and 75%-quantiles of the block size distribution were analyzed. Examining all values for the transformation factor the distribution can be described by a power function with a negative exponent. The function depends on the persistence only. Finally, the results of random simulations were compared to the analytical formula using the transformation factor. The predicted mean and selected quantiles show a good agreement with the simulation results. It gives a comprehensive picture about the block size distribution in discontinuity systems with three non-persistent sets."

Jan 1, 2015

By Mark Van Dyke, Gamal Rashed, Khaled Mohamed, Timothy Barton, Morgan Sears

"The unconfined compressive strength (UCS) of coal is an important parameter that controls the stability of coal ribs in underground mines. Estimation of the UCS of coal units composing the rib is required for conducting the rib stability assessment technique. This technique requires conducting large numbers of conventional UCS tests in a laboratory, which are expensive and time consuming. The research work outlined in this paper examines the use of indirect strength estimation methods—the point load test (PLT) and the in-situ Schmidt hammer test (ISHT)—for evaluating the intact strength of coal. The conventional UCS test was conducted on 80 coal specimens from 10 different coal seams for eastern coals. For each coal seam, the PLT and the ISHT were compared with the UCS test results to establish a correlation between the strength indices from the PLT or ISHT and the UCS. Moreover, to simplify the estimation of the UCS, a correlation between the megascopic coal lithotype and UCS was established.INTRODUCTIONBased on Mine Safety and Health Administration (MSHA) reports, rib failures have resulted in 17 fatalities, representing 52% of the ground-fall fatalities in underground coal mines in the United States over the past decade (MSHA, 2018). In an attempt to control rib failures in underground coal mines, the National Institute for Occupational Safety and Health (NIOSH) is working on developing a coal rib stability rating technique to provide a quantitative means to characterize the stability of coal ribs and to provide guidelines for early selections of rib support. The unconfined compressive strength (UCS) of coal units composing the ribs is one of the key input parameters required to estimate coal rib stability. The UCS of coal is an important parameter that controls the resistance of coal ribs to fracturing and slabbing. Direct determination of the UCS is time-consuming and expensive. Moreover, the UCS may be limited to testing only the strong coal samples since the weak or highly cleated samples might not survive the transportation and the preparation process (cutting and grinding). Therefore, alternative methods have been tested to indirectly find the intact strength of coal, such as the point load test (PLT) and the in-situ Schmidt hammer test (ISHT). The acronym ISHT refers to Schmidt hammer tests that were conducted in-situ on coal pillar ribs, while the acronym SHT refers to tests that were conducted on small scale blocks of coal."

Jan 1, 2018

By Salustio s. Guzman

The standard .free energies of formation of tin chlorides were estimated with reviewed and estimated basic thermodynamic data, and measured reversible potentials for the disproportionation of tin dichloride into metallic tin and tin tetrachloride. Values for cºp, Sº, Hº?-Hº 298, -(Gº - Hº298) /T,.Hºf, Gºf, and log Kp are given in tabular form, these estimations are compared with estimations reported in the literature.

Jan 1, 1985

By Hojong Kim, Isehaq Al-Nafai, Kwadwo Osseo-Asare

The standard Gibbs free energy of formation (ΔGo f, 298) of bastnasite, (Ce, La, Nd, Pr)FCO3, was estimated using four different methods. The obtained average values were − 1589.5 kJ/mol for CeFCO3, − 1599.5 kJ/mol for LaFCO3, − 1589.1 kJ/mol for NdFCO3, and − 1595.4 kJ/mol for PrFCO3. The value for cerium bastnasite, CeFCO3, was used to construct a potential vs. pH (Eh-pH) diagram to investigate the stability relations of cerium bastnasite. The diagram shows that CeFCO3 is stable in neutral to basic conditions (pH ~ 6.5–11).

By Yazn Khasawneh Ph. D. P. E., Will Tjaden, Spencer E. Ness P. E., Mohammed Nasim Ph. D. P. E.

Wind turbine components undergo many loading cycles during their operational life. Additionally, wind turbines may undergo extreme loading conditions from natural hazards, mechanical failures, or emergency stops. Current design practice for the foundations of wind turbines accounts for these complex loading conditions through a simplified pseudo-static approach based structural loading combinations. A rotational stiffness for the foundation is estimated from the pseudo-static analysis and then compared to an acceptable minimum rotational stiffness provided by the turbine manufacturer. These minimum rotational stiffnesses are based on dynamic analysis of the tower and nacelle system with the foundation represented as linear springs. This approach provides a reasonable approach to the foundation design but does not accurately capture the true dynamic performance of the entire soil-foundation-tower-nacelle system. This becomes especially important for pier-type foundations, which are being more commonly used to support modern and future generations of larger turbines. Additionally, the dynamic performance of the foundation will vary as the adjacent soil undergoes a large number of loading cycles of varying strain magnitudes. In this study, the full turbine-tower-foundation-soil system was modeled using finite element methods. An advanced non-linear soil constitutive model and dynamic loading time histories were used to investigate changes in stiffness of the soil, and the possible impact on the dynamic response of the system. Results were compared to conventional design methodologies with the goal of reducing foundation capital costs while avoiding increases in O&M costs and which can lower the LCOE of wind energy.

Oct 1, 2022

By D. H. Dueñas Tapia, Laura R. A. Huallpa, Laime L. Alarcón

Este trabajo se basará en datos obtenidos en el campo y también analizados en laboratorio, que serán interpretados y analizados para dar conclusiones y recomendaciones. Es necesario realizar un estudio Geológico, Geoquímico y Petromineragráfico del yacimiento de Oro orogénico (mesotermal) en la comunidad de Ccapana- Ccatca-Quispicanchi-Cusco.

May 1, 2008

By Edmundo Alfaro, Álvaro Ordoñez

La presencia de Las Tierras Raras o Rare Earth Elements (REE) y de metales alcalinos (Rb, Cs y Li), como elementos estratégicos, son de gran interés en el mundo por su empleo en nuevas tecnologías. Por trabajos y reportes de prospección geológica realizados por el INGEMMET durante los últimos años se ha evidenciado la presencia de aquellos elementos estratégicos en la zona sur del país. Por ello, el presente trabajo se orienta a presentar una investigación preliminar con minerales de la zona sur occidental de la región Arequipa.

Sep 29, 2023

By Geraldo Lúcio de Faria

Os aços IF são livres de elementos intersticiais, como o C e o N, na matriz ferrítica. Estes elementos são controlados no processo de refino na aciaria, a partir da aplicação de técnicas de desgaseificação a vácuo, juntamente com a adição de elementos estabilizantes, como Ti e Nb. Durante a fabricação e em algumas aplicações dos aços IF, como por exemplo soldagem, a transformação de fase austenita?ferrita e o efeito dos elementos de liga na sua cinética têm forte influência na microestrutura final.Neste contexto, este trabalho caracterizou microestruturalmente e comparou as cinéticas de transformação de fase de dois tipos de aços IF com composições químicas diferentes, sendo eles o IF-Ti e o IF-TiNb. Por meio dos resultados obtidos, foi possível concluir que o aço IF-TiNb, como fabricado, possui uma microestrutura mais refinada devido à presença do Nb e seu papel na laminação controlada do aço. Além disso, observou-se que as temperaturas críticas Ar3 e Ar1 do aço IF-TiNb são sistematicamente menores do que as temperaturas medidas para o aço IF-Ti. Como a fração dos elementos microligantes em solução sólida é muito pequena, atribui-se este efeito à diferença no teor de Mn dos aços estudados, que parece potencializar o refino de grão na etapa final de resfriamento da chapa de aço laminada.

Oct 30, 2017

By André Oliveira Galon, Caio Vaccari Silva, Victor Bridi Telles, Raphael Mariano de Souza, Felipe Fardin Grillo, José Roberto de Oliveira

Neste trabalho foi estudada a influência da granulometria de CaO adicionada ao processo de desfosforação, temperatura e teor de FeO da mistura desfosforante na aglomeração de partículas sólidas na escória. Para isto, foram realizados testes laboratoriais em sete condições experimentais distintas, bem como a análise de imagens via software Quantikov, para medir a aglomeração, além de análise termodinâmica computacional. A granulometria, temperatura e porcentagem de FeO se mostraram parâmetros relevantes na aglomeração da escória de desfosforação e a análise de imagens mostrou-se uma ferramenta útil para a obtenção destes resultados.

Oct 1, 2019

By Danilo Fontes Ferreira

O presente trabalho estudou o comportamento de uma liga de titânio ASTM-F67Gr1 frente à corrosão e à tribocorrosão em meio fisiológico. Para a realização desta pesquisa foi desenvolvido um aparato experimental capaz de impor simultaneamente um desgaste mecânico e corrosivo às amostras testadas, visando avaliar o comportamento tribocorrosivo. O meio corrosivo selecionado foi a solução de Ringer. A partir de curvas de polarização potenciodinâmica foi possível obter os parâmetros eletroquímicos necessários à realização dos ensaios de tribocorrosão bem como comprovar a excelente resistência a corrosão do titânio na solução de Ringer. A partir dos ensaios de tribocorrosão foi constatada a influência da velocidade e da carga aplicada, no fenômeno de tribocorrosão. Os resultados evidenciaram uma maior influência da velocidade no incremento da corrosão e da carga aplicada no incremento da sinergia, durante o desgaste tribocorrosivo.

Aug 16, 2017

By Francisco Alberto Marreiros da Rocha Filho

No processo de laminação a quente ocorre ocasionalmente a perda de ductilidade a quente que pode causar o fenômeno denominado como “abertura de cabeça” da barra durante a sequência de passes. Essa perda de ductilidade a quente pode ser severa e causar interrupções no processo produtivo. Esse fenômeno pode estar associado a diversos fatores entre eles: composição química do aço; defeitos presentes no tarugo; condições do processo de laminação; e temperatura do aço durante o processo, principalmente nos passes de desbaste e intermediários de laminação. No processo em estudo, a perda de ductilidade a quente ocorre associada à laminação de vergalhões a partir de tarugos oriundos diretamente do lingotamento contínuo. O presente trabalho tem como objetivo avaliar a influência da temperatura e da microestrutura formada ao longo do processo na perda de ductilidade a quente das barras através de um exame comparativo entre os vergalhões laminados com e sem o uso da etapa de reaquecimento.

Oct 30, 2017

By Daniella Gomes Rodriguesr

"As mudanças que ocorrem ao longo do recozimento na microestrutura e textura foram observadas no aço inoxidável ferrítico estabilizado ao nióbio, tipo ASTM 430 por meio de Difração de Elétrons Retroespalhados. As amostras deformadas foram recozidas com uma taxa de aquecimento de 23,5°C/s. O recozimento foi interrompido nas temperaturas de 780, 830 e 880°C para acompanhar a evolução da microestrutura e textura. Os resultados mostraram que a nucleação dos novos grãos ocorre preferencialmente nos contornos de alto ângulo. No estágio inicial da recristalização a fibra g é dominante na fração recristalizada, com as componentes 111121, 1111 ,1 2 mais intensas. Na fração não recristalizada a fibra a foi mais intensa. No progresso da recristalização as componentes 11112 1 e 1111 ,1 2 permanecem predominantes, a fibra g torna-se dominante em detrimento da fibra a."

Jan 16, 2018

By Fernanda Borba Simões

Na produção de biocombustíveis a partir de óleos vegetais produzidos via craqueamento térmico-catalítico, é realizada a desacidificação do produto final para sua viabilidade, podendo ser efetuada pela adsorção. Os adsorventes são diversificados e vão desde zeólitas até o uso de resíduos industriais. Este trabalho buscou testar a lama vermelha previamente ativada quimicamente e termicamente como adsorvente de ácidos graxos livres presentes no gasóleo leve produzido a partir do craqueamento do óleo de palma com índice de acidez inicial de 55,1257 mg de KOH/g. A lama vermelha foi utilizada em cinco condições: seca sem tratamento, ativada quimicamente (pré-tratada a 400°C/2h) por solução de HCl a 37%, de H2O2 a 4%, de HCl a 1,5 M e de KOH a 1,5 M. Na cinética de adsorção, a lama vermelha ativada por solução de HCl a 1,5 M mostrou-se mais eficiente que os demais adsorventes, pois reduziu o índice de acidez do biocombustível de 10,7574 mg de KOH/g para 9,1752 mg de KOH/g no tempo de 50 minutos. Quanto à eficiência dos adsorventes restantes, no que tange a desacidificação, apenas a lama vermelha seca e a ativada quimicamente por KOH a 1,5 M apresentaram remoção dos ácidos graxos livres perceptíveis.

Aug 16, 2017

By Marcio José Cuccolo Rosales

A soldagem por brasagem a vácuo promove a união de materiais dissimilares com alto valor agregado. Este trabalho visa estudar a interação química do nitreto de boro hexagonal (h-BN) na interface de ligação brasada do par Kovar®/h-BN. As variáveis de processo são determinantes para formação da junta brasada metalurgicamente estável. O trabalho estuda a molhabilidade do h-BN quando em contato com ligas de adição do sistema eutético Ag-Cu durante a solidificação. Foram conduzidos ensaios no h-BN a fim de caracterizar sua aplicação no sensor de posição do feixe de elétrons (BPM) do projeto do Sirius, e as propriedades que influenciam o seu processamento durante a brasagem, como coeficiente de expansão térmica e molhabilidade superficial. Os ensaios de brasagem com a liga Ag-Cu-4,5Ti, mostraram boa molhabilidade e espalhamento na superfície, favorecendo a formação da junta sem descontinuidades. As reações na interface são complexas no sentido de formação de novas fases e intermetálicos e, influenciadas pela seleção dos materiais, que possuem diferentes temperaturas de fusão e coeficientes de expansão térmica. Os resultados indicam que a seleção da liga com Ti, que é o elemento de ativação, promove a interação na superfície do h-BN com os demais materiais da junta.

Oct 30, 2017