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By A. Andreas, E.H. Wells

The oil and gas industry of New Mexico recorded notable progress ill 1935. More wells were brought in than in any previous year, and important new discoveries were made. The total number of completions was 340, of which 260 were oil wells, 8 were gas wells and 72 were dry holes. The total oil production was 20,228,947 bbl., an appreciable increase over the 1934 production of 16,636,804 barrels. Many of the wells completed in southeastern New Mexico were acidized. This treatment proved highly effective in increasing the capacity of the wells, the resulting potentials usually being two to ten times as large as before acid treatment. In the Lea County fields in which proration was entirely on an acreage basis, the tendency of many of the operators was to complete their wells according to best conservation practice rather than to obtain the largest possible potential. Much remedial work was done in the Hobbs, Cooper, Jal and Eunice fields, and with excellent results. At many of the wells high gas-oil ratios were greatly reduced and encroaching waters shut off by setting packers. Several companies carried on pretentious geophysical campaigns in the southeastern part of the state. The location of the Amerada discovery well in the Monument field was based on geophysical surveys. The New Mexico Oil Conservation Commission, established by the 1935 Legislature and consisting of the Governor, the Commissioner of Public Lands and the State Geologist, began to function in May. Production in the state thereafter was based on orders issued by the Commission. Proration in the Hobbs field, which had been provided for since July, 1930, by successive proration agreements signed by all operators in the field and approved by the State Geologist, was continued by the Commission by giving approval to the current proration agreement,. A plan of proration for the other Lea County fields that had been in offect since early ill 1934 was adopted. 111 September, 1935, the Commission approved a. proration agreement for the Artesia-Jackson-Maljarnar area in Eddy and Lea counties that had been agreed upon by

Jan 1, 1936

By E. H. Wells, A. Andreas

The oil and gas industry of New Mexico recorded notable progress ill 1935. More wells were brought in than in any previous year, and important new discoveries were made. The total number of completions was 340, of which 260 were oil wells, 8 were gas wells and 72 were dry holes. The total oil production was 20,228,947 bbl., an appreciable increase over the 1934 production of 16,636,804 barrels. Many of the wells completed in southeastern New Mexico were acidized. This treatment proved highly effective in increasing the capacity of the wells, the resulting potentials usually being two to ten times as large as before acid treatment. In the Lea County fields in which proration was entirely on an acreage basis, the tendency of many of the operators was to complete their wells according to best conservation practice rather than to obtain the largest possible potential. Much remedial work was done in the Hobbs, Cooper, Jal and Eunice fields, and with excellent results. At many of the wells high gas-oil ratios were greatly reduced and encroaching waters shut off by setting packers. Several companies carried on pretentious geophysical campaigns in the southeastern part of the state. The location of the Amerada discovery well in the Monument field was based on geophysical surveys. The New Mexico Oil Conservation Commission, established by the 1935 Legislature and consisting of the Governor, the Commissioner of Public Lands and the State Geologist, began to function in May. Production in the state thereafter was based on orders issued by the Commission. Proration in the Hobbs field, which had been provided for since July, 1930, by successive proration agreements signed by all operators in the field and approved by the State Geologist, was continued by the Commission by giving approval to the current proration agreement,. A plan of proration for the other Lea County fields that had been in offect since early ill 1934 was adopted. 111 September, 1935, the Commission approved a. proration agreement for the Artesia-Jackson-Maljarnar area in Eddy and Lea counties that had been agreed upon by

Jan 1, 1936

Alder, John W., Student, Mass. Inst. of Tech Cambridge, Mass. '38 Allen, Charles F Mines McFarland, Cal. '34 Anderson, Norman John, Student, South Dakota School of Mines Rapid. City, S. D. '32 Ansel, Gerhard, Student, Mass. Inst. of Tech Cambridge, Mass. '34 Arakelian, Haig Mark, Student, Inst. of Tech Cambridge, Mass. '34 Archer, George K., Student, Colorado School of Mines Golden, Colo. '34 Arnot, Paul H. 608 S. Acacia St., Compton, Cal. '31 Asel, Philip R., Student, Colorado School of Mines Golden, Colo. '32 Augenthaler, Robert L., Student, New Mexico School of Mines Socorro, N. M. '32 Augustine, Robert W. Address Wanted. '32. Austin, Robert B., Student, Univ. of Idaho Moscow, Idaho. '34

Jan 1, 1934

By Robert A. Cummings, Francis S. Kendorski

The behavior of the rock mass during block caving affects the production of the mine and dictates the loads and deformations placed on required drifts. Traditionally, the drifts used are massively reinforced and buttressed against very high and erratic mining- induced abutment loads or swell muck loads, resulting from undercut- ting. Extensive field investigations in numerous block caving mines in the porphyry intrusive environment, coupled with models developed for tunneling and longwall coal mining, have allowed the development of a unified hypothesis for ore bodies of various degrees of competence. In general, the hypothesis incorporates several sequential steps in the driftlrock mass deformation history, each with characteristic magnitudes, duration, and areal extents depending on ore body competence. 1. Prior to initiating caving, but subsequent to drift development, the rock mass and drift are in a state of near-equilibrium. Zones of stress concentration have stabilized, as for a tunnel. 2. For a newly undercut panel, the rock mass and drifts directly beneath the undercut respond by dilating towards the void created, and undergo a release of compressive strain that manifests itself as tensile failures. 3. For adjacent areas, the rock mass is compressed as the load is shed from the undercut level.

Jan 1, 1983

By F. T. Davis

The annual review of mineral dressing was the subject of considerable discussion at the MBD meeting in New York last February. Because the amount of material now being published is so imposing, it was generally agreed that reviewers should try only to cite the items of importance. In order to conserve even more space, it was agreed to omit bibliographies. In reading these reviews, and those of the past two or three years, one is impressed by the advances in materials handling, the enlargement and the advances in automation of unit process equipment. Although there has been development of a variety of new concentration principles in flotation, magnetic separation, et al., the design of these principles into new plants has not been widespread. The probable reason is that the plants being built today are so large and costly that few are able to face the risk of any significant degree of experimentation. There are exceptions to this; for example, some of the chemical processes, but these are usually because there was no conventional process available. This situation should change in time as the ores amenable to our conventional methods become depleted.

Jan 2, 1967

By A. W. Mitchell

Barite occurs as bedded and vein-type deposits in Nevada along a north-northeast trending zone that Parallels the Antler orogenic belt. The Nevada bedded deposits presently supply 85% of domestic barite production, used primarily as a weighting agent in the petroleum drilling industry. The ore bodies are controlled structurally and stratigraphically along regional and local structural breaks in siliceous eugeosynclinal rocks of lower to middle Paleozoic age. Evidence for the origin of the barite includes sedimentary and hydrothermal features, indicating that localization probably took place along fractures in the sea floor.

Jan 1, 1982

By Luis A. Fierino, M. Ashraf Mahtab

This paper reviews the background of, and solution techniques for, the major geomechanics problems affecting caving operations, including prediction of cavability, defining size distribution of or fragments, stability and support of production openings, and control of rock bursts and subsidence. Further research is also suggested in the solution of the various geomechanics problems.

Jan 1, 1984

Jan 1, 1953

By E. Ackerman, L. Y. Tu, S. C. Sun

The use of ultrasonics in forming emulsions is not new. As early as 1927 Wood and Loomis' reported preparation of emulsions with ultrasonics. In 1935 Rschevkin and Ostrawskyz described the use of great ultrasonic power in producing fine emulsions of various oils and paraffin in water. Recently Oyama and Tanakahmployed ultra-emulsification to increase the effectiveness of sodium ethyl xanthate in flotation of chalcopyrite and galena. An emulsion is a two-phase system consisting of two incompletely miscible liquids, the one being dispersed as finite droplets in the other. The dispersed liquid is known as the internal or discontinuous phase, and the surrounding liquid is termed the external or continuous phase. There are two types of emulsions; one is oil-in-water (O/W) and the other water-in-oil (W/O). The word oil refers to the liquid other than water. Circumstances exist in which the emulsion type is not clearly defined, and the internal and external phases both contain portions of the opposite phase. This is said to be a dual emulsion. Among the many hypotheses', 6v proposed for the formation of emulsions, the Bancroft's adsorbed film or double interfacial tension theory is widely accepted. Bancroft ""educed that in the process of emulsification the interfacial tension between oil and water is lowered by the formation of an emulsifying film, which contains the adsorbed molecules and/or ions from the emulsifying agent and the two liquids.

Jul 1, 1955

By Ashbel Welch

Ashbel Welch, Lambertville, N. J.: Dr. Dudley has given the wear of steel rails under four different conditions. He arrives at the conclusion that the softer rails, or those that from their composition ought to be softer, wear better than the harder. But there is another condition which has an important bearing on the subject, and should not be overlooked,—the weight on a wheel. With the lighter weights of the past, the softer rails may have worn best; with the heavier weights of the future, the harder may wear best. Weights will probably be increased up to the capacity of steel to bear; then doubtless the harder steel will wear best. A leaden rail with ten pounds on a wheel might carry millions of tons, but with one hundred pounds on a wheel, it would be destfoyed by a few thousand tons. So in the days of iron rails, my experience was that the softer rails under light machinery stood better than some of the harder; but under heavy machinery the softer were much the most rapidly destroyed. It is doubtless the same with steel. The pounding motion of the wheels loosens or spreads the particles of a thin film of steel; the pull lengthwise on the rail de-

Jan 1, 1881

By John Patek

KNOWLEDGE of the relative floatability of silicate minerals is increas-ing in importance as flotation is being applied to the concentration of nonsulfides. Many silicates are in themselves commercial products amenable to concentration by flotation. Moreover, the selective flota-tion of other nonsulfide minerals, such as cassiterite, depends largely upon the floatability of associated. gangue silicates. Differences in floatability existing between the various silicates have not been suffi-ciently appreciated; for example, the feldspars that differ greatly in floatability have generally been merely treated as "feldspar." It was the purpose of the work described in this paper to determine by experi-ment the differences in floatability between silicates; to investigate the causes for such differences, and to discover a means of predetermining approximate floatability without the necessity of experimentation.

Jan 1, 1934

Would you briefly describe how you chose the minerals industry and reflect upon some of your earliest experiences? I wish that I could say that I had a well-formulated career plan early in life and that mining engineering was always foremost in it, but I cannot, In fact, I was quite indecisive before I finally chose my life's vocation. But in another respect, I am glad my career unfolded in the manner it did because it gave me a better insight into advising others on career opportunities. Probably the greatest problem confronting our youth, and the one I find preys upon their minds the most, is their inability to select a career path early in life. This indecision frequently has a deep psychological effect upon them and they become down on themselves. Therefore, it fortifies them somewhat to learn that others who have become successful in their careers had difficulties choosing a career path early in life. However, while assuring young people that an early choice is not absolutely essential for success, I caution them to work toward as early a decision as possible.

Jan 3, 1979

By Joseph Hartshorne

The attention which this process has attracted, especially in Europe, has led me to believe that members of the Institute would be interested in a report of the progress which has been made in the year and a half that has elapsed since my paper on the subject was read at the Colorado Meeting of this Institute. As already described in that paper (Duns., xxvi., 380), this process is a modificatioii of the open-hearth steel manufacture, whether acid or basic, collsistillg essentially in the division of the charge between two furnaces, one of which is charged about two hours earlier than the other, and tapped into the other after the charge in the latter has become fluid, the slag of the first bath being removed from it during the transfer. This description still remains true as far as it goes, but further experience has demonstrated that circumstances will very materially modify the relation of the two furnaces to each other, and the character of the work done in each of them. The function of the primary furnace has become more clearly and entirely that of doing the rough work of desiliconiziug and dephosphorizing, while that of the second or finishing-furnace has become almost entirely that of decarburizing and finighing the heat. To indicate these developments and their results is the object of this paper. In order to avoid needless repetition, I shall try to accomplish part of this object by giving a short resume' of what has been published elsewhere on this subject since my former paper was read. This will at least enable those interested to study the matter for themselves from original sources. Since that time the following papers have been read and published: " The Bertrand-Thiel Process of Making Steel," by Percy C. Gilchrist (Cleveland Institution of Engineers, Session of 1896-

Jan 1, 1899

By M. A. Scheil, S. L. Hoyt

About three years ago eight standard steels were prepared for the cooperative investigation of methods for oxygen analysis, sponsored by the Iron and Steel Division of the American Institute of Mining and Metallurgical Engineers and by the National Bureau of Standards. A preliminary report of the results was made at the annual meeting of the A.I.M.E. in February, 1936. † This report showed the reliability of vacuum-fusion methods and further brought out certain advantages of the fractional vacuum-fusion method. The results obtained by the authors with the latter method will be discussed here, with some comments on the procedure for those who are interested in determinations of gases in steel. Some additional comments are offered on the use of the polarizing microscope for identifying the inclusions in the steel to check and amplify the findings of the fractional vacuum-fusion analysis. For details of the fractional method, see the paper by L. Reeve1. Degassing the Crucible One of the sources of error in vacuum-fusion methods has been the blank gases evolved from the graphite crucible after preliminary out-gassing. We have used 1750" C. as the outgassing temperature. This gives a base pressure at that temperature of less than 0.030 mm. after one hour and of 0.004 mm. on dropping the temperature to 1575" C. At lower extraction temperatures the base pressure is 0.001 mm. at 1050" C., 0.002 mm. at 1170" and 0.003 mm. at 1320' C. Because of the size of our induction coil we are limited to this temperature, although it 'would be advantageous to use 1950" to 2000" C. Hamilton2, after outgassing at 1850" C. for 100 min., was able to reach a base pressure of 0.001 mm. for a temperature of 1700' to 1725" C. This would give a blank corresponding to less than 0.00015 per cent 02 and 0.00005 per cent H2. Chipman and Marshall outgas at 2000" C. for one hour by using a special construction

Jan 1, 1937

By J. N. Hobstetter

It is widely believed that the nucleation of phase transformations in solid metals is accomplished by some type of local atomic fluctuations in the parent phase which arise from spoutaneous difiusion in the metal or alloy system. Under appropriate conditions, these fluctuations are believed to be stable in the sense that the free energy of the entire system is lowered if the fluctuations, or nuclei, grow. Under other conditions they are thought to be unstable in the sense that the free energy is lowered if they redissolve. The criterion for stability is usually taken as the size of the fluctuation. This view has been rationalized by Beckerl in terms of the free energy released by the volume of the nucleus and the free energy associated with the formation of a new surface surrounding the nucleus. The qualitative result of this reasoning is shown in Fig I where the changes in free energy for the surface and volume effects are plotted together with their sum against the radius of the nucleus. There is evidently always a critical size r, beyond which the release of free energy which is proportional to the volume always dominates the increase of free energy which is proportional to the surface area. Borelius2 has also attempted to rationalize the stability criterion for binary alloys, but in terms of the internal concentration of the fluctuations. He has found that, if surface energies are entirely ignored, the fluctuation must still reach a critical concentration if it is to become stable and avoid subsequent dilution. Although the Borelius theory fails to predict many observed nucleation phenomena such as the vanishing of the nucleation rate at the critical temperature, the major premise must certainly be valid. In this paper a reconciliation of the Becker and Borelius views is made by means of a search for nuclei which are at once stable with respect to both size and internal concentration. The increase in free energy per mole accompanying the formation of a nucleus which is just stable, AF., is independent of the path whereby the nucleus is brought into being. It is thus appropriate to seek critical nuclear attributes without reference to the fluctuation mechanism. The rate of nucleation, however, cannot be treated without a detailed understanding of the exact fluctuation process which produces stable nuclei. In this and succeeding papers the purpose will be to find the size, shape and internal concentration of the stable nucleus which is formed with a minimum increase in free energy in a wide variety of systems. The Nature of the Nucleus It is necessary ti have rather detailed knowledge of the nature of a nucleus if AF, is to be computed. Fortunately, enough facts are known or suspected about the nucleus to make possible a detailed analysis. X ray diffraction studies have shown

Jan 1, 1949

By Nicholas J. Grant, Chih-Chung Wang

TO phase of the Ti-0 system has the structure of NaCl and has a wide range of solid solubility.' In the course of studying the Ti-Cr-0 ternary system, binary alloys were made of iodide titanium and high purity TiO,. It was found from X-ray studies of the binary alloys that a transformation of the TiO appears to take place at a temperature near 925°C. Evidence of this phase change is best seen in Fig. 1. Fig. 1A shows the X-ray spectrometer pattern (CUKa radiation) of an alloy of 25 wt pct 0 corresponding to the stoichiometric composition of TiO.

Jan 1, 1957

Jan 1, 1967

By Nev A. Gokcen

PUBLISHED data on the solubility of nitrogen in liquid manganese are widely discordant. Ochsenfeldl observed that a Mn-N alloy with 3.6 pct N consisted of solid and liquid phases at 1260°C but at 13 00° to 1340°C the solid phase disappeared and the liquid contained 0.1 to 0.13 pct N. In contrast Saito's measurements at approxhately 1400°C yielded an average value of 0.97 pct N. Sieverts3 volumetric method is not suitable for the determination of gas solubility in manganese because the liquid metal vaporizes readily and condenses in the cooler parts of the apparatus where it can absorb large amounts of nitrogen. The purpose of this investigation was, therefore, to determine the solubility of nitrogen in manganese accurately in the range of 1273" to 1500°C. The experimental method used in this study was as follows. Electrolytic manganese of 99.9 pct purity, and weighing 50 g, was melted in a pure alumina crucible placed in a tubular furnace. Temperature was measured with a Pt-10 pct Rh thermocouple and controlled within ± 5°C. Pure nitrogen was bubbled through the melt for 1 hr at constant temperature and then a sample was taken by sucking the metal into a 2-mm clear silica tube and immediately quenching in water. The sample was broken into small pieces and found to be sound to the naked eye. The entire sample was then dissolved and the resulting solution was analyzed for nitrogen by the well-known solution-distillation method. The experimental results are presented in Fig. 1. All the nitrogen solubility data refer to 1 atm of nitrogen pressure; hence the observed values are slightly corrected by using Sieverts' equation when the atmospheric pressure differed more than 5 mm Hg from 760 mm, and further, in the case of the runs at 1500°C the correction arising from the presence of Mn vapor has been made. (Cf. Eq. [3]). Scattering in the data is within ±5°C in temperature measurement and ±3 pct in total nitrogen analysis. The straight line in Fig. 1, correlating the percentage of dissolved nitrogen, %N, with the inverse temperature in OK-1, can be expressed by:

Jan 1, 1962

By F. J. Hurst

The rapid expansion of the phosphate fertilizer industry in conjunction with the projected shortage and spiraling price increase of uranium has greatly renewed interest in wet- process phosphoric acid as a significant source of uranium. Two attractive solvent extraction processes for recovering uranium from the acid have recently been developed and tested through bench-scale at Oak Ridge National Laboratory. One of the processes has been successfully tested on a pilot-plant scale at phosphate plants; the second process, which offers several potential advantages, still needs additional testing. The merits of each process are discussed.

Jan 1, 1978

By H. Becke, D. Stolnitz, D. Flatley, W. Kern

Zinc difhsions in gallium arsenide having surface concentrations as low as 5 x 10'' atoms per cu cm have been attained. A multiple-difhsion sequence is employed during which zinc enters the gallium arsenide from a silicon dioxide film in a solid-to-solid diffusion step. The technique is illustrated for the case of a zinc surface concentration of -1 x 1017 atoms per cu cm and a junction depth of 1.2 p. Radiotracer measurements of -0.1-p layers of gallium arsenide are used to delineate the resulting profile. A diffusion coefficient for zinc in pyrolytically deposited silicon dioxide is reported. ZINC is frequently used as an acceptor impurity in gallium arsenide. As examples, p-n junctions are formed using zinc-diffused layers in solar cells, lasers, and varactor diodes. For these purposes surface concentrations of 10'' to over loz0 zinc atoms per cu cm are desired and readily obtained from a vapor source. Diffusion of zinc into gallium arsenide to yield surface concentrations of about 1017 atoms per cu cm, however, is more difficult. For instance, oldstein' reports that large changes in the vapor density of zinc produce only small changes in surface concentration. Such low surface concentrations are necessary in forming the diffused base of a gallium arsenide double-diffused n-p-n transistor in order to obtain an adequate emitter efficiency. An alternative approach to zinc diffusion which can provide reduction in surface concentration of several orders of magnitude is the introduction of the diffusant from a solid source. This can be conveniently accomplished by using oxide films of the type generally employed for selective diffusion masking. Such oxides also serve to prevent the dissociation of the gallium arsenide surface at the high temperatures of diffusion. DIFFUSION PROCEDURE Fig. 1 illustrates the diffusion sequence which is employed for obtaining zinc surface concentrations in the range from 5 x lom to 1 X 10" atoms per cu cm. The description of technique will be given for the instance of -1 x 1017, which is typically utilized in double-diffused gallium arsenide transistor investigations at this laboratory. Tin- or germanium-doped gallium arsenide wafers drawn from crystals grown by horizontal Bridgman or Czochralski techniques are used, with bulk concentrations ranging from 1 to 3 X 10" carrier atoms per cu cm. Each wafer is chemically polished on the (iii) arsenic face using a mixture of five parts concentrated sul-furic acid, one part water, and one part 30 pct hydrogen peroxide at room temperature, followed by rinsing in deionized and quartz-distilled water. Pyrolytic silicon dioxide was chosen as the oxide coating because of the high quality of the films obtainable, the ease of their preparation, and the excellent control over film thickness and uniformity.

Jan 1, 1964