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By Nobuhiro Shinihara, Makio Naito, Keizo Uematsu, Tadashi Horta, Hiroya Abe, Masataro Okumiya

"A significant variation of strength was noted in silicon nitride ceramics made through the powder compaction processing with minor processing changes. The relevance of the fracture strength to the microstructure was examined in these ceramics. In the examination of microstructure, the ceramics were made into thinned specimens, and their internal structures were observed with an optical microscope in the transmission mode. This technique can distinguish a difference in microstructure associated with the minor processing changes. The strength of all ceramics examined in this experiment was qualitatively correlated with the -pore size distribution in the specimens. Clearly, the elimination of these detrimental defects will enhance the reliability of ceramics.IntroductionIn ceramics made through powder processing, a variation of properties is often encountered [l ,2]. This brings a major problem on producing reliable and cost-effective ceramics. The variation is often ascribed to the changes in the characteristics of defects. However, there is no clear evidence f\)r this explanation due to the lack of an adequate tool for identifying the defects determining the properties. Details of the origin of the variation have still been poorly understood.A new technique is very promising for clarifying the origin of the variation [3,4]. This has very high potential in detecting minor differences in structure for .engineering ceramics. With this technique, ceramics are made transparent with its thinning down to about 50 µ m and their internal structures are observed with various types of optical microscopes in the transmission mode. The characteristics of the defects determined through this approach were found to be directly related to the strength of the ceramics [4-6].The objective of this study is to clarify the ongm of fracture strength of silicon nitride ceramics. This material is representative of high performance ceramics, and the origin is of great practical interest. For this study, silicon nitride ceramics with minor changes in processing condition were prepared. Specific feature focused in this study is the difference of large pore structure determined with the new technique and its relevance to the strength of the silicon nitride ceramics."

Jan 1, 2000

By G C. Reed, J M. Murray

During more than 100 years continuous mining of the lead-zinc orebody at Broken Hill, an immense amount of geological data has been collected about shear zones related to the orebody. The challenge to current mine geologists is to synthesise and interpret these data sets in a way that is applicable to production demands. Precise knowledge of the locations of major shear zones is important not only for the determination of ground conditions but also to develop an understanding of ore remobilisation along these structures. Traditionally, geological information has been collected from drill core and back and wall mapping underground, and interpreted on sections that are approximately 20 m apart. The recent introduction of MaptekÆs Vulcan software has enabled the shear zones to be modelled in three dimensions. The new three-dimensional shear models have been combined with seismic data from the Southern Cross area. The seismic data is collected from a microseismic monitoring system installed in the Pasminco Southern Operations in August 1996 (Rauert and Tully, 1998). The addition of seismic information to the shear zone models has led to a greater degree of certainty about the shear zone locations and has provided information about shear zones in areas yet to be drilled.

Jan 1, 2000

By Erik M. Westerberg

The Soilex Pile combines a slender shaft, for quick and easy installation, with an enlarged pile toe, for high capacity. The key component is the Expander Body, which is inflated by injecting cement grout when in position. The latest development in the Soilex Pile System results in a reduction of the total cost of Soilex Piles, in many cases values that are competitive with pre­cast concrete piles and displacement piles. Soilex Piles can now be installed on top of a bearing soil layer, instead of 3 to 4 m into that soil as previously required, further minimising the ground disturbance. Soilex Piles achieve high capacity in relatively loose soils, with ultimate loads typically between 1000 and 2000 kN in a sand with CPT qc = 5 to 10 MPa or SPT N= 10 to 20. It is possible to pre-load and proof-load all piles with dynamic testing up to 2000 kN or using built-in jacks, thereby verifying the capacity. The vibratory installation method, which is extremely quick and causes very little soil disturbance and noise, is exemplified by two case histories.

Jan 1, 2000

By M. Grodner

Underground excavations exhibit different hangingwall conditions in response to varying geotechnical and mining situations. These differences need to be quantified so as to accurately determine the effectiveness of the mining and/or support strategies. A useful tool for the quantification of these differences is hangingwall profiling. Two methods of hangingwall profile measurement are described?termed irregular and periodic methods. Several data analysis techniques are reviewed for these methods and the suitable ones are discussed in detail. For irregular data the suitable techniques are the determination of the length, the average of the profile and the average absolute deviation from the mean of the profile. All of these techniques as well as determination of the moving average of the height and examination of the spectral image of the profile can be successfully applied to regular data. The effect of preconditioning on the hangingwall is discussed as an example and it is quantitatively shown that it results in improvements of conditions. The techniques described allow the engineer to quantitatively identify the appropriate support type or mining strategy and thus represent a valuable decision-making tool. It is suggested that these techniques should be employed on a routine basis by the rock engineers on the mines as part of their geotechnical classification, as well as support manufacturers to quantify the effectiveness of various support types.

Jan 1, 2000

By Thomas M. Barczak

The decade of the 90's brought an unprecedented increase in the development of innovative technologies to provide more effective and easier to install roof support in underground mines. To facilitate the application of these technologies to improve mine safety. National Institute for Occupational Safety and Health (NIOSH) developed the Support Technology Optimization Program (STOP). STOP is a windows based software program that provides mine operators with a simple and practical tool to make engineering decisions regarding the selection and placement strategy of these various standing roof support technologies. This program includes a complete data base of the support characteristics and loading profiles obtained through safety performance testing of these supports at the NIOSH Safety Structures Testing Laboratory. Support design criteria in the form of the required support load density at a specified convergence can he established from four options: ( 1 ) a data base of measured ground reaction data from various mines or ground behavior information inputted by the user. (2) determination of loading requirements based on a detached roof block or rock failure height. or (3) criteria based on the current roof support system, and (4) arbitrary criteria set the by user. Using these design criteria, the program will determine the installation requirements for a particular support technology that will provide the necessary support load density and convergence control. Optimization routines are also available to determine the most efficient support design for a user specified support installation- In addition to these performance measures. STOP can be used to compare material handling requirements and installation costs. Comparisons among the various support technologies are easily made including graphical analysis of relevant support parameters. This paper describes the STOP and its application to optimize standing secondary roof support systems.

Jan 1, 2000

By K. Severin, B. Flanigan, P. Marion

“Plutonic-related” gold deposits in Interior and SW Alaska (Tintina Gold Belt) vary significantly in size, grade, vein/deposit morphology, depth of emplacement, distance from causative pluton and metal association. Metal associations such as Au-Bi and Au-As-(Sb-Hg) are a good empirical indicator of depth of emplacement and distance from causative pluton and have been used successfully in exploration. Results from a variety of analytical techniques also suggest a phenomenological cause for these metal associations, e.g. gold and bismuth have linked metallogenesis at high temperatures and thus are best correlated at deposits that are deep and/or close to causative intrusions.

Jan 1, 2000

By Hitoshi Iijima, Fumitaka Tsukihashi

"Fine powder of tantalum is used as materials of electric condenser. It is important to control the distribution of particle diameter of tantalum fine powders for the commercial use. In this study, fine powders of tantalum were produced by reducing tantalum chloride vapor with hydrogen gas at 1673 and 1773K. The tantalum chloride vapor was reduced with hydrogen and the produced fine particles of tantalum were collected to observe the distribution of particle diameter. The effects of reaction temperature, partial pressure of hydrogen gas and vaporization temperature of tantalum chloride on the distribution of particle diameter and reaction efficiency of reduction were determined. The mechanism of reduction reaction of tantalum was discussed.IntroductionThe ultra fine powder shows various different physical properties from that of bulk materials. Therefore, the application of ultra fine powder to various fields such as magnetic material, electric material, catalyst, etc is anticipated. The control of shape of powder, size distribution, property of agglomeration, purity is required for the practical use of ultra fine powder. Although the ultra fine powders of ceramics are produced by various methods, the ultra fine powder of metals are produced by the evaporation in gas atmosphere, plasma evaporation process, chemical vapor deposition process, and reduction and precipitation in liquid phase depending on the metal and productivity. The chemical vapor deposition process has features that pure metal powder can be obtained and the control of the distribution of powder size is easy. [1,2,3,4,5]"

Jan 1, 2000

By Paul F. Ph. D. Ziemkiewicz, Courtney D. Black

According to the American Coal Ash Association, 105 million tons of coal combustion products (CCP) were produced by the power generating utilities in 1997. Of that total, 1.68 million tons were used in mining applications (ACAA, 1997). Results have ranged from the environmentally beneficial to neutral and, in some cases, detrimental. Twenty years ago coal ashes: bottom and fly ashes constituted nearly all CCPs. With the shift to new emission control technologies at power plants, however, large volumes of new products are being generated. Many do not lend themselves to traditional ash applications such as cement formulation. Many CCP disposal sites are not documented with reliable pre and post application monitoring. In this report we discuss types of CCP, their relevant characteristics and the mining environment. We have attempted to identify a range of documented applications and to draw conclusions about their environmental effects including benefits and adverse impacts.

Jan 1, 2000

By Raj P. Singh

Applications of cementation in the recovery of metal ions from process solutions have been known for a long time. Cementation reactions involve electrochemical precipitation of a noble metal from solutions of its salts on a more electropositive metal which, in tum, progressively dissolves. For example, addition of zinc metal powder in a solution containing zinc and cobalt ions would allow for the precipitation (separation) of cobalt according to the following chemical reaction. This paper pertains to the recovery of cobalt from cobalt process solutions via a cementation reaction on aluminum shavings (metal scraps from cans etc). Specifically, we report on the characterization of cobalt process solutions, a by-product obtained from cobalt chemicals, and the kinetics of cobalt, nickel and manganese cementation from process solutions on aluminum shavings.

Jan 1, 2000

By Dale Ramsey

Emulsion explosives have become the product of choice for many blasting applications and are not limited to just extreme wet hole conditions or special application environments as in the past. Today’s novel emulsion technology has evolved over many decades, allowing a great diversity of formulations, Emulsion explosives can be effectively designed to produce very high energies, cap sensitive high explosive cartridges to bulk blasting agents, with varying viscosities, stable VOD’s, excellent water resistance, long shelf life and sleep time. They are also conducive to the mixture of emulsion, An/F0 blends in varying proportions and are amenable to any type of sensitizer. The key to a stable, reliable and consistent emulsion formulation is the careful mixing of the internal phase, which consists of a solution of oxidizer salts suspended as microscopically fine droplets, with the surrounding continuous fuel phase. There are few blasting applications today where some form of an emulsion explosive cannot fit the application. In massive, hard rock, dense, tightly jointed and fine grained rock types, the emulsion explosives are the best choices in creating new fracture networks for good fragmentation with a few alternatives. In such environments, emulsions with expanded drill patterns often result in better economics than the use of straight AnLFo. This paper will cover emulsion formulations, sensitizing options, product testing, material handling, and blast optimization, Emulsion explosives characteristics have also proven to reduce adverse environmental effects such as noxious fumes, ground vibration, and airblast while still remaining cost effective.

Jan 1, 2000

PURPOSE: Evaluate practical technological advances in level-dependent hearing protectors and inexpensive personal acoustic monitors. RESEARCH SUMMARY: The results of previous NIOSH research show that miners develop hearing loss much more quickly than nonoccupationally noise-exposed individuals and that miners experience a greater severity of hearing loss than would be expected for nonoccupational noise-exposed persons of the same age and gender. Using hearing thresholds at 4,000 Hz as an indicator, coal miners experience hearing loss 2.5 to 3 times greater than would be expected for persons not exposed to occupational noise. At age 50, 90% of coal miners and 49% of metal/nonmetal miners were found to have a hearing impairment. In comparison, only 9% of a nonoccupationally exposed control group had a hearing impairment at age 50.

Jan 1, 2000

By J. van Deventer

Testwork was done with two different adsorbents, Dowex-Minix gold-selective resin and activated carbon, to detemine their relative performances with regard to gold recovery from clarified low-grade solution employing a fixed-bed operation. The mill discharge from the milling-in-cyanide operation at a Witwatersrand gold mine was used as feed to the adsorption columns. A small amount of gold was leached during the milling process, so that this solution simulates, to a certain extent, a low-grade solution representative of a heap-leach operation. A speciation of the feed solution was done to establish which metal complexes were present in the milling-in-cyanide solution. This information was necessary to interpret metal loadings on the resin, as base metal cyanide species and their respective charges have an effect on the final gold loading capacity of the resin. Equilibrium isotherms were established for both adsorbents to estimate the rate of adsorbent flow anticipated for this specific feed solution. Breakthrough profiles were obtained at two different superficial linear velocities for each adsorbent. Mass transfer zone heights determined from the test work and the elution/regeneration time requirements were used to size a 150 m3/h full-scale plant for both adsorbents. A counter current configuration of adsorption columns, using three columns, should be suitable to recover gold effectively and to produce an effluent with a gold concentration below 0.01 mg/l. Based on the results obtained from the breakthrough tests, a preliminary techno-economic comparison was done between the resin-in-solution and carbon-in-solution options for the recovery of gold from low-grade solutions. This study indicated that the capital expenditure for a carbon-in-solution plant would be about 33 percent higher than that of a resin-in-solution plant. The operating expenditure for a resin-in-solution plant is expected to be only 60per cent of that for a carbon-in-solution plant. Keywords: resin-in-solution, carbon-in-solution, heap leach.

Jan 1, 2000

Tonnage and grade are the principal reported components of mineral resource estimates but tonnage is a derivative of two more fundamental estimates; volume and bulk density. Typically, most of the effort in a resource estimation study is directed towards grade and volume, yet poor application of bulk density data to resource models can result in significant biases. The impact on tonnage estimates is easily recognised but poor density estimates may also introduce subtle biases into the grade estimates. Methods for measuring bulk density have been discussed previously. This paper focuses on the manipulation of bulk density data and the extension of bulk density from essentially point measurements to block estimates within resource models. Bulk density is a continuous, geologically controlled, spatial variable and should be treated as such. Issues such as combining data from multiple sources, sample support and the interdependence of bulk density and grade estimates must be resolved. The statistical and geostatistical techniques used for grade estimation are, under the right circumstances, equally applicable to bulk density. The importance of bulk density needs to be recognised. With robust raw data and correct estimation procedures, better estimates of bulk density can be obtained and both local and global tonnage and grade estimates can be improved.

Jan 1, 2000

By S DeKruijff

The Mount Isa Mines Copper Mine in Mount Isa started producing copper in 1966. The Copper Mine gradually increased production rates to nearly six million tonnes per year. Over the last three years the mine has been in a gradual ramp down due to the reduction of primary ore sources and head grade. The majority of ore sources are predominantly in pillar retreat sequences bounded by multiple fill masses. There also a substantial lower grade resource delineated to the south of the main orebody. These remaining ore sources present significant engineering challenges to obtain a safe and cost-effective extraction. Stope designs have become increasingly complex and require additional engineering and operations input and analysis. This paper describes the major planning and operational challenges and issues associated with the stope design and extraction of an orebody in the later stages of mine life.

Jan 1, 2000

By Bert Allard, Åsa Sjöblom

The River Vormbäcken is the recipient of treated AMD from the Kristineberg mine site, northern Sweden, where mining of a complex sulfidic ore has taken place since 1940. Parts of the river flow through different kinds of wetlands. The changes in metal concentrations and water chemistry that occur upon passing these wetlands have been studied by analysis of water chemistry data from a number of stations along the river collected during 11 years of monthly sampling. It is concluded that the impact and functioning of wetlands cannot be elucidated from chemistry data alone. Future studies including e.g. reconstructed water flow are needed.

Jan 1, 2000

By Giuliana A. Zelada

This paper reports on a study of 43 compression load tests (five fully instrumented) and ten pullout tests of auger cast-in-place (ACIP) piles in sand. Eight design methods reported in the literature were used to predict the measured pile capacities. Ultimate load capacities of the ACIP load tests were determined using two different definitions of ultimate capacity and compared with predictions. Load transfer behavior was determined from a study of the fully instrumented pile tests and compared to predicted values. Recommendations are made regarding the design approach most appropriate for these foundations and the best procedure for estimating ultimate capacity from pile load tests.

Jan 1, 2000

By P K. Smith, N G. Corner, R J. Ryan, D C. Arne, F P. Bierlein

The Reefton Goldfield has produced 67 t of gold from mesothermal vein gold deposits in metasedimentary rocks of the Greenland Group (Cambrian-Ordovician). The Globe-Progress deposit contributed 13.2 t (418,000 oz) of this total, predominantly from quartz veins. Recently a resource of 14 Mt at 1.96 g/t Au (27.5 t or 882,300 oz of contained gold) has been delineated at Globe-Progress in quartz vein remnants and disseminated within adjacent sedimentary rock, much of which has been locally brecciated. The breccias consist of quartz vein and sedimentary wall rock fragments set in a matrix of clay ærock flourÆ and sulphide (arsenopyrite plus minor pyrite and stibnite). Gold, closely associated with sulphide, is disseminated within the breccia. Disseminated gold also occurs in massive siltstone and sandstone adjacent to the quartz veins and breccias. Exploration drilling at Globe-Pogress, and several other Reefton prospects (e.g. Capleston, Merrijigs, Big River and Alexander River), has intersected zones of disseminated arsenopyrite carrying up to 20 g/t more gold. These mineralised sediments commonly have little or no megascopic quartz and or carbonate veining. There is little visible indication of former primary or secondary permeability for the passage of hydrothermal fluid and deposition of gold. However, porosity and permeability were formerly present in inter-granular pore spaces and microveinlets now filled with quartz, carbonate and K-mica. The Fosterville gold deposit in Victoria bears many similarities to the Globe-Progress deposit at Reefton, in terms of age, host rocks, hydrothermal alteration and mineralisation style. Many ofthe disseminated deposits in Nova Scotia, including deposits at North Brookfield and Moose River (Touquoy Zone), have similar characteristics to the Reefton disseminated mineralisation, but commonly have abundant pyrrhotite and some deposits have disseminated metal alloy grains of complex metallurgy.

Jan 1, 2000

By Karen Bolm, Floyd Gray, Ailiang Gu, Kerry Caruthers, Carlos Velez, Laurie Wirt, Douglas M. Hirschberg

Understanding sources of dissolved metals and transport characteristics of acid drainage is needed to assist land-use strategies in mineralized regions, particularly in the semi-arid southwestern United States. Water- quality samples were collected from mined and un-mined parts of the Patagonia and southern Santa Rita Mountains of southern Arizona from streams, springs, seeps, adits, alluvial wells, and bedrock wells. Water quality during base-flow conditions was compared with that *of runoff samples from infrequent winter and summer storms. The largest fraction of annual discharge in these ephemeral streams consists of storm runoff, although springs provide a steady source of low discharge base flow to numerous intermittent perennial reaches. Several abandoned mines in the northern Patagonia Mountains contribute acid and heavy metals to streams. During base-flow conditions in mineralized areas, natural springs and intermittent stream reaches produce acidity but the volume is typically low and acidity is often diluted or neutralized down gradient. Overland runoff contains low concentrations of dissolved metals and moderate acidity, however, stream waters were strongly acidified and metal-laden from contact with abundant pyrite-bearing stream sediments derived from erosion of waste-rock material in and along the sides of the stream channel.

Jan 1, 2000

By Yasuo Kudo, Wu, Hayato Sato, Hiroshi Nakazawa, Shouming

"In order to recover copper from a waste nickel condenser powder, bioleaching experiments were carried out using Thiobacillus ferrooxidans in a shaking flask. The content of nickel and copper in the waste nickel condenser powder in this study were 8.0% and 3.5%. X ray analysis showed the peak of barium titanate. In the preliminary study using metal nickel and copper powders , the dissolutions of nickel and especially copper were accelerated with the addition of ferric iron in the bioleaching of nickel and copper powders while not in the absence of ferric iron. Ferric iron oxidizes both metals, and Thiobacillusferrooxidans oxidizes ferrous iron resulting from the oxidation of metals, whereby the dissolutions of metals proceeds. The dissolution rates of nickel and copper increased with increase in the concentration of ferric iron in the bioleaching of the waste nickel condenser powder.1. IntroductionNickel condensers rejected from manufacturing plants are crushed and landfilled. Waste nickel condensers contain nickel and copper and could be considered as nickel and copper ores. Since the capacity of landfills is diminishing, it is required to recycle metals of waste nickel condensers in order to reduce the amount of wastes landfilled. Conventionally, metals in the waste were recovered by dry metallurgy after the incineration.Nickel has been refined by solvent extraction - electrowinning method (SX-EW method). Recently the amount of copper refined by SX-EW method has increased (Takahashi, et al. 1994). This method is cleaner and consumes less energy than conventional methods. Nickel dissolved well in acid solutions, but copper is not. If copper is leached efficiently from a waste nickel condenser powder, SX-EW method will be applied to recover copper from them"

Jan 1, 2000

By Guillermo Silva

A novel, ultra-low density explosive composition, particularly suited for wall control and other applications requiring customising of the explosive’s energy output, has been developed. Being reactive in nature, the low density explosive enables the controlled dilution of dry blasting agents from their nominal densities down to values slightly less than 0.10 g/cm3. The product has been detonated at densities of 0.07 g/cm3 in diameters as small as 50mm under confined conditions, using a 227 g (l/2 lb.) primer. Recorded velocities of detonation ranged between 1200 m/set and 2200 m/set for densities between 0.07 and 0.2 g/cm3. Theoretical velocities ranged from 1700 m/s to 2500 m/s for the same density range. The low density explosive was insensitive to initiation by a blasting cap which is a desirable feature for transportation purposes. Mixing of the product with ANFO has been accomplished with minimum segregation making it suitable for applications where reduction of pressures are necessary.

Jan 1, 2000