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By André Carlos Silva

Dewatering stage is among the most important industrial unit operations, and is wide adopted in many different industries, due the fact that a large portion of industrial products is produced using suspensions of solids in liquids. Nowadays the mineral processing tailings disposal is a big problem due the environmental degradation produced. The phosphate rock processing in Anglo American Phosphate Brazil, situated in Catalão/Go/Brazil, generates around 180 t/h of tailings for a plant feed of 480 t/h (approximately 37,5% of the processing plant feed), with 5 to 10% of solids and approximately 14% of P2O5. Nowadays the tailings are sent direct to the tailings dam. The present work proposes the paste production using with the tailings from phosphate rock processing plant divide in two different stages. The first one composed by the free settling of the material in presence of industrial flocculants in a graduated cylinder with 2.0 L of internal volume for one hour, in the same way it must occur in conventional thickeners. After that time, the clarified liquid was drained and the remaining pulp was sent to the second stage consisting in the tailings vacuum filtration. Ten different flocculants and nine different filter media were tested. The found results were satisfactory for paste tailings production with solids percentage around 65%.

Aug 8, 2018

By Kelen Juliane Mucelin

In order to better understand the tribological behavior of self-lubricating materials, Fe-Si-C matrix composites containing solid lubricants added during the mixing step were studied. The samples were produced by conventional powder metallurgy route, presenting total contents of 5%, 7.5% and 10% in volume of h-BN and graphite mixtures as solid lubricants. The composites were evaluated in terms of tribological properties, under reciprocating sliding conditions, and mechanical properties by using tensile tests. Additionally, the wear scars were characterized by Raman spectroscopy and scanning electronic microscopy. Higher total contents of solid lubricants greatly increased scuffing resistance however decreased mechanical properties. Furthermore, increasing h-BN contents reduces both properties. These results confirmed the applicability of such sintered composites as self-lubricating parts, reaching values up to 7000 N.m for scuffing resistance combined with ultimate tensile strength of 220 MPa.

Jul 31, 2018

By Uwe Wilhelm

Pittini Group has contracted Danieli in 2011 for the supply and replacement of the existing EAF at Ferriere Nord Plant in Osoppo. This was a very challenging project: giving the fact that the Meltshop was operating already under very high performance level, there were many elements involved for the project to improve (reduce the amount of charges, promote highest possible chemical energy utilization, allow best optimization on existing transformer power, modification on Drop Out box and Water Cooled Duct, Hydraulic System for EAF, Scrap Bucket design to fit to new EAF with existing loading and transport system, Automation System Review and Upgrade) as well as limitations of the existing installation (limited space, lifting capacity building and cranes and the required solutions for fast shell and roof exchange). All furnace parts, as well as installation engineering, were developed and discussed carefully with the Customer to either provide proven and reliable concepts, but also to define solutions for fast installation/maintenance access and quick exchange for offline turnaround. In the end, from disassembly of existing equipment up to the first heat of the new furnace, only 38 days were necessary. First heat was made on January 24th 2013, on the 6th production day 32 heats where produced at nominal design capacity and 28 days after start up 100,000 t liquid steel have already been produced.

Jul 30, 2018

By Flavia de Paula Vitoretti

Pelletizing of iron ore fines is an important process used to produce high quality of raw materials for the subsequent reduction processes in the ironmaking industries. The process involves the production of green pellets and subsequent induration on a traveling grate furnace to promote inner partial melt and agglomeration which confer physical and metallurgical proprieties appropriated to the subsequent reduction processes. The pellets are produced with addition of charcoal to improve efficiency in the reduction processes. The lignin coal from sugarcane straw is an alternative source to replace the charcoal or coke in the self reduction of pellets. This work focused on the influence of biomass on the chemical kinetics parameters inner agglomerate pellet structure under industrial process conditions of the travelling grate furnace due hot gas flows within the pellets.

Aug 1, 2018

By Pablo Bruno Paiva Leão

The present work is based on the characterization of nonmetallic inclusions in Ti stabilized ultra-low carbon steel, produced in a large steel mill. Due to a large incidence of submersed valve clogging in a continuous casting, the study is important in order to know the characteristics of the inclusions which are causing the problem. Total of 24 heats were sampled in the tundish and manually analyzed with a scanning electron microscope. The results revealed that 98.65% of the 3183 inclusions analyzed were solid in steelmaking temperature and 66.54% were alumina. The solid inclusions of alumina have low wettability for the iron bath, showing a high tendency of agglomeration in the submersed valves, affecting the castability. It has been concluded from the results and literature that some alternative measures such as the application of the treatment with calcium, precautions to avoid steel re-oxidation and the total or partial replacement of the pre-deoxidized element; would reduce the obstruction problem.

Oct 30, 2017

By Giulio Rodrigues Altoé

Environmentally correct composites, made from natural fibers, are among the most investigated and applied today. In this paper, we investigate the mechanical behavior of epoxy matrix composites reinforced with continuous fique fiber, through bending tensile tests. Specimens containing 0, 10, 20 and 30% in volume of fique fiber were aligned along the entire length of a mold to create plates of these composites, those plates were cut following the ASTM standard to obtained bending tests specimens. The test was conducted in a Instron Machine and the fractured specimens were analyzed by SEM, the results showed the increase in the materials tensile properties with the increase of fiber amount.

Aug 16, 2017

By Saulo Brinco Diniz

O alumínio e suas ligas por apresentarem uma série de vantagens, são largamente utilizados em diversas aplicações. O que mais reduz o campo de sua aplicação é sua baixa resistência mecânica, porém esta pode ser modificada através da adição de determinados elementos de liga e de processamentos termomecânicos adequados. Este trabalho teve como objetivo estudar a evolução microestrutural de uma liga de alumínio 7475-T7351 processada por laminação cruzada, e posteriormente submetida ao tratamento térmico de recozimento a 500ºC para recristalização, com tempos de encharque de 15, 30, 60 e 120 minutos. De acordo com os resultados apresentados, pode-se observar que a completa recristalização ocorreu entre os tempos de 30 a 60 minutos de encharque no tratamento térmico.

Oct 30, 2017

By Claudio Pereira Diogo

A lot of galvalume/aluzinc steel sheet was furnished to a metallic roof manufacturer intended for tile fabrication. But, according with the roof manufacturer, that coils develops a different superficial aspect during processing. The purpose of this work was to provide an explanation for the appearance of the observed surface on one side of the coils. In order to find out the origin of the problem, mechanical and microstructural characterization tests were done at INSPEBRAS with the support of a partner laboratory. The results are described in this paper with their analysis and conclusions.

Aug 16, 2017

By Gerhard Finstermann, Ichiro Maeno, Takehiko Saito, Hironori Shimogama, Konrad Krimpelstätter

Automobile manufacturers are developing Electrified Vehicles with light steel body structure designs that reduce mass and therefore greenhouse gas emissions over the vehicle’s entire life cycle. This raises the demand for the production and development of Advanced and Ultra High-Strength Steels (AHSS / UHSS) and Electrical Steels with increased permeability and reduced core loss to improve energy conversion efficiency. To meet this requirements the steel market is tending towards new generations of AHSS with improved formability (3rd generation AHSS) and high-silicon steels with higher strength and thinner products. With this growing demand for advanced high-strength steels and electrical steels, producers are faced with a unique and interesting challenge in producing materials that strain or exceed the capabilities of existing mill equipment and automation designed to produce low- to medium-carbon sheet. While specialty steel producers have known for decades how to process special high-strength steels and thinner gauges, this equipment typically does not offer the yield and productivity desired by the market, necessitating innovation in re-engineering existing equipment to meet the market demands more economically than new construction. In the case of cold rolling, this can be supported through variable roll geometries, more effective roll-gap lubrication technologies, application of strip heaters (Warm Rolling) to reduce risk for edge crack propagation and strip breaks as well as continuous rolling managed by state-of-the-art automation technologies.

Oct 1, 2019

By Dr. Steven G. Jansto

The market demand for reduced fuel consumption and CO2 emissions in the automotive, energy and construction sectors have further increased the demand for new and advanced higher quality microalloyed grades produced via TMCP. The technological integration of the process and physical metallurgical advancements of value-added niobium (Nb) microalloyed thermo-mechanical controlled process (TMCP) steels continue to be developed and is an important element for these more demanding end user requirements and cost-effective steel production. The reheat furnace process step has a profound effect on the TMCP performance, final hot rolled steel quality and mechanical property consistency during the production of hot rolled steels. The uniformity of heating applied across the entire width, thickness and length of the slab or billet is essential in the successful achievement of consistent customer properties regardless of the chemistry. The resultant ferrite grain size in the final hot rolled product is significantly governed by the initial prior austenite grain size. However, the transition from laboratory melted and TMCP hot rolled heats to the production scale is often quite challenging. Aberrations in the reheating process step at the industrial furnace are often the root cause of mechanical property quality issues. These combustion process metallurgy parameters connect directly to the resultant TMCP product quality and is defined as Combustion Metallurgy

Oct 1, 2019

By Christian Overhagen

In bar and wire rod mills, rolling procedures featuring three- and four-roll technologies are state-of-the-art to produce high-quality long products. While a rolling model for the three-roll process including an equivalent pass method was already presented by the author, pass design methods are dealt with in the current work. The geometry of the rolled product and roll grooves are described mathematically using functional contours, allowing geometric-numerical methods to be used for manipulation and deformation simulation of the rolled product. For a given pass, the output section is constructed using these methods. Roll force, torque and rolling power are calculated using the mathematical rolling model presented before. Interstand tensions are discussed as influencing parameters on the force, torque and power demands, as well as on the section shape. A mathematical model for the influence of interstand tensions on lateral spread is incorporated in the model. To complete the pass design model, elastic mill stand feedback is considered in terms of a fixed elastic modulus for each rolling stand, the elastic feedback and therefore cross-sectional variation due to elastic mill spring being calculated iteratively from the roll force by application of the Gagemeter equation. The interaction of section height and width faults due to elastic mill spring and spread variations is analyzed in detail and the consequences for the roll pass design are shown.

Oct 1, 2019

By Tiago de Abreu Siqueira

CO2 geological storage is one of the current technologies developed worldwide to reduce industrial emissions of carbon dioxide to the atmosphere. Two main mineral types of deep geological reservoir could be contemplated for CO2 storage: sandstone reservoirs and carbonaceous reservoirs. Geochemical reactivity of a dolomite-calcite mineral compound and magnesite pure mineral was studied with a set of nine experiments per crushed mineral phase with two saline solution and with mQ water and three temperatures: 50°C, 90°C and 150°C. Experiments were performed in batch reactors with 250 bar of CO2 partial pressure during 24h to assess the effect of temperature and salinity in constant CO2 pressure. Solid characterization was performed by XRD and solution analysis by ICP-OES. Acidification of solutions due to CO2 dissolution in water is the main source of reactivity in the system. Proton concentration increases and causes partial dissolution of initial dolomite, calcite and magnesite and release of Ca2+ and Mg2+ cations in solution. Bicarbonate anion (HCO3) concentration also increases due to CO2 dissolution in water and carbonate minerals dissolution. Temperatures of 90°C and 150ºC increase the kinetic of reaction and the dissolution of minerals and cations release in solution. New carbonate crystalline phase precipitates as a Ca, Mg solid solution between dolomite and calcite pure poles.

Aug 8, 2018

By Paulo Conceição, Carlos Sampaio, Carlos Petter, Ariane Kuerten

The Sensor Based-Sorting technology is an emerging technology applied in mineral separation and concentration. The technique consists in using a method known as Dual Energy X-ray Transmission sorting (DE-XRT). The particle's position over the conveyor belt was evaluated and, despite de variability of results, shows that there is no a position with greater accuracy on the sensor's reading. Results obtained indicated that DE-XRT sorting technology was able to significantly reduce the mass and the ash content of the ore feed, being an interesting option for reduction of costs and improvement of coal quality in beneficiation plants.

Oct 3, 2019

By Franco Gandin

With increasing demands for highly performing and at the same time efficient and running-costs saving vacuum-degassing equipment, dry mechanical pumps have been confirmed a proper choice to completely fulfill the expectations of steel-making companies worldwide. Regarding the production of both special carbon steel and stainless steel grades, the usage of mentioned pumps allowed reaching simultaneous remarkable results from different viewpoints in various Danieli worldwide installations (treating up to 200 t of liquid steel). As a matter of fact, in front of the replacement of a widely spread and renowned technology such as steamejector pumps with the recently developed technology embodied by the dry mechanical pumps, well-established metallurgical performances in terms of carbonhydrogen- nitrogen-sulphur removal have been repeatedly attained while meeting at the same time the client’s expectations concerning, for example, running-costs and push-button availability. Additionally, thanks to the very flexible, modular, redundant and maintenance-friendly equipment design, random problems occurring to the singular mechanical pumps can be easily solved without affecting the VD-VOD plant availability and metallurgical performance. With a particular regard to the VOD process, a very short overall process-time has been repeatedly performed (averagely less than 58min under-vacuum time at ChMP1) while guaranteeing the expected required quality of the final refined stainless steel. Moreover, in several VOD installations (ranging from 6 t up to 110 t of liquid steel) an efficient automatic process control such as dynamic pressure-regulation during oxygen-blowing has been attained thanks to the controllable variable-speed drives with which each mechanical pump is provided.

Aug 17, 2017

By Tiago Bristt Gonoring

Este trabalho estuda a redução de pós de hematita de alta pureza (com Fe2O3> 99,00% e tamanho de partículas

Aug 1, 2018

By Aline Lima da Silva

The reduction in SOFC operating temperature due to recent development in materials and fabrication techniques enables the use of ferritic stainless steels as interconnects for SOFCs. Ferritic stainless steels offer many advantages over traditional ceramic interconnects, such as higher thermal and electronic conductivity, as well as relative ease of fabrication. However, the formation of chromium oxide on ferritic stainless steel results in an increase in ohmic resistance and can lead to the loss of cathode catalytic activity (due to Cr volatilization, with cathode poisoning). The oxide growth depends on several factors, such as steel composition, temperature, oxygen partial pressure. In this way, knowing the phase stability, the oxidation behavior of the material and the oxidation kinetics is of great interest. In this context, a thermodynamic study of the oxidation of ferritic stainless steel 430 under oxidizing atmosphere (cathode), at the temperature of 750ºC, is carried out. As one can see, the thermodynamic system can be very complex, involving several phases (chromium oxide, (Fe,Cr,Mn)3O4 Spinel, iron-chromium oxides, etc.). The effect of oxygen partial pressure and alloying elements on phase distribution is evaluated. Thermodynamic modeling is compared with experimental results from literature.

Aug 8, 2018

By Patrik Bloemer

Reliable and accurate furnace bath level data during the melting process is invaluable for good decision making and furnace optimization, while obtaining such information rapidly and safely on a regular basis is of paramount importance. This paper shows how a melting process problem was identified as a concern, how a solution was sought and how a real-time measurement system was tested by simple modification to an existing temperature sampling manipulator. Also how, with furnace power on or off, taking reliable hot heel, fill and running levels could be used to assist melting control, aid decision making and improve safety.

Jul 30, 2018

By Andrew Salach

Experimento laboratorial avalia desgaste em rodas e trilhos de PR’s. Chegou-se a conclusão de que rodas com elevada dureza economizam desgaste de rodas e de trilhos.

Aug 16, 2017

By Henrique Silva Furtado

This paper presents the results obtained on the exchange of an original old blow charge model for a new up-to-date state of art global model, employing optimization techniques and process modelling, and, the results obtained in terms of fluxes consumption reduction and the introduction of user friendly tools and practices.

Aug 17, 2017

By Mariana Sizenando Lyrio, Weslley Luiz da Silva Assis, Harison da Silva Ventura, Gabriella Maria Silveira de Sá, Paulo Rangel Rios

Nesse trabalho, simulações computacionais de transformações de fase são realizadas para analisar situações em que a nucleação e a velocidade de crescimento não são homogêneas no material. Os resultados foram comparados com modelos analíticos de Rios e Villa. A microestrutura e a cinética microestrutural das transformações são obtidas e analisadas para casos em que há um mesmo gradiente de velocidade e diferentes gradientes de núcleos. O principal resultado é que a cinética de transformação e a microestrutura são afetadas da mesma maneira para as diferentes quantidades de núcleos, embora o gradiente de velocidade seja o mesmo. Na microestrutura foi observado que na parte inferior os grãos são maiores enquanto que na parte superior os grãos são menores, como consequência da densidade de núcleos e da velocidade de crescimento. Todas as simulações computacionais apresentaram um bom acordo com os modelos analíticos.

Nov 4, 2019