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By T. T. Campbell

A survey of the literature eras made covering the use of aqueous non-aqueous, and fused-welt systems for the electrowinning or electroplating of molybdenum metal. The survey was prepared in order to provide background for further investigations directed toward the electrodeposition of pure molybdenum metal from either aqueous or nonaqueous mediums. While a thorough effort was made to cover all available references, a critical review was not attempted nor does this survey pretend to be exhaustive in nature.

Jan 1, 1955

By W. W. Adams

During the calendar year 1927 the United States Bureau f Mines conducted, for the third consecutive year, a safety contest among more than 250 mines and quarries. Aside from its underlying purpose to promote safety, the object of the contest was to learn which mine or quarry had completed the year's work with the smallest proportionate loss of time from accidents to its employees. Competing companies were grouped into five classes, namely, anthracite mines, bituminous teal mines, metal mines, nonmetallic mineral mines, and quarries and open-pit mines. To the winning company in each group was awarded the bronze trophy "Sentinels of Safety," the gift of The Explosives Engineer magazine. The winner in each group was the mine or quarry whose record showed the smallest loss of time from accidents in proportion to the total amount of time worked by 411 employees. This proportion is designated the "accident-severity"3 rate; it indicates the number of days of disability resulting from personal injuries per thousand man-hours of work performed by all employees. Each company's standing was determined by the Bureau of Mines from detailed records furnished by the contestants. Records of the leading companies were made known to a committee of seven men well known to the mining industry but not connected with the Bureau of Mines. This committee selected the winning companies in accordance with rules governing the Competition. According to the contest rules, the competition for the trophy was restricted to mines employing at least 50 men underground and to quarries and open-pit mines employing at least 25 men in the pit. As several plants fell below these figures during the year, their records could not be considered in connection with the award of the trophy. Figures covering these plants are, however, included in the attached tables.

Jan 1, 1928

By G. M. Martinez

A cell concept adaptable to large-scale electrowinning of zirconium metal from zirconium tetrachloride was investigated by the Federal Bureau of Mines. Tests were made in twin cells, each 12 inches in diameter by 33 inches long. Electrowinning was performed in one chamber from which the electrolyte was transferred after electrolysis to the other chamber where it was renewed by the introduction of ZrC14 by direct sublimation. The formation of a salt plug in the connecting pipe provided a seal between the chambers. Optimum electrolyte composition, with respect to quality of the metal product (91 pct meeting ASTM standards except for the oxygen content) and current-carrying capability (about 350 amp) was determined to be 16.7 wt-pct NaF-83.3 wt-pct NaCl mixture plus ZrC14 equal to about 3 wt-pct zirconium. A twin-cell design incorporating the unit operations covered by this investigation is proposed.

Jan 1, 1976

By Gregory P. Cole, Jeffrey Shawn Peterson

The Pittsburgh Research center3 conducted research to study and improve electrical fault detection on coal mine direct-current (dc) trolley systems. A suspended trolley line delivers power at voltages of 300 or 600 V dc to the haulage equipment and other loads. Roof falls or other accidents may force the trolley line down so that an electrical fault current may flow between the trolley line and rail. This fault current could result in localized heating, arcing, and perhaps fire. Such faults are not always preventable by the existing circuit protection because the current magnitude is well below typical operating levels of the trolley system. The research discussed in this report studies the applicability of computerized signal analysis techniques to solve this problem. Tests were conducted at cooperating coal mines. Measurements were taken during normal loading of the trolley system (light, intermediate, and heavy traffic), during induced fault conditions (arcing and bolted faults), and during transitions between the two. These data were then used to train and test a microprocessor-based fault detection algorithm. Later, field tests of the detection algorithm found that it correctly classified the state of the trolley system greater than 95% of the time.

Jan 1, 1997

By N. F. LeJeune

For a number of years the Bureau of mines has conducted semi-annual surveys to determine the changes in the characteristics of the motor gasoline being sold in the United States. The Bureau of Mines surveys, from April, 1917, to January, 1943, indicated a progressive decrease in the end point range. The survey for July, 1923 showed an interruption in this progressive decrease. This interruption, as shown in Table 1, in the line marked "Difference," was apparently a definite one, for the data obtained in the surveys of July, 19233, January, 19244, and the present one, apparently substantiate it. The figures in Table 1 were obtained by averaging the end points of the least volatile and most volatile samples of gasoline. For example, of 850 samples analyzed in 1919, the 10 per cent (85 samples) having the highest end points and the 10 per cent having the lowest end points were grouped, and the end points of each group averaged. These averages are represented in the table as the "Maximum 10 per cent" and the ?Maximum 10 per cent," respectively. The same scheme was used on the succeeding surveys.

Jan 1, 1924

By N. C. Tomoeda, W. D. Bensema, J. W. Adams

Measurements of surface magnetic field noise were made at various locations over the Geneva Coal Mine near Price, Utah, on June 12, 1973. The locations selected were on the surface over emergency locator beacons underground at depths between 350 meters (1150 ft .) and 488 meters (1600 ft .) . The surface terrain where these measurements were made was mountainous, and access was difficult. There were no power lines within several miles, and the weather was clear; therefore, the magnetic noise levels were about as low as will normally occur. Results of measurements of distant sferics indicate rather sharp cutoff frequencies below which broad- band, impulsive noise is attenuated. The mechanism of propagation for this noise above the daytime cutoff frequency of 3500 Hz and the nighttime cutoff frequency of 1700 Hz is deduced to be a waveguide formed by the D or E layers of ionosphere as an upper plane and the earth as a lower plane. The measurement systems used are similar to those used earlier. The technique is to record broadband, analog signals, digitize the data, and use a fast- Fourier transform to obtain spectral plots. This tech- nique is novel in that it can measure simultaneously all magnetic field energy within a limited portion of the spectrum for a limited time, and, after processing, reproduce the events occurring in that time interval in great detail .

Jan 6, 1974

By Robert H. Merrill

A method of determining the strength of a mine roof layer in place is described in this report. The method was tested on a limestone roof layer 50 feet wide, 100 feet long, and 20 inches thick. In place measurements were accomplished by introducing air under pressure into a separation between the layer and the overlying roof, and as pressure was increased, the corresponding strain and deflection of the roof layer were measured until the roof failed. The ultimate strength of the roof agreed with the tensile strength of the roof rock (modulus of rupture) as determined in the laboratory; the modulus of elasticity as measured in place did not agree with the laboratory-determined values; the deflection and tensile strain in the layer in place showed good agreement with the theory of a body-loaded beam clamped at both ends. This procedure for determining the strength of a mine-roof layer is safer and less costly than successively widening a roof to failure. For example, it would have been necessary to mine the room to a width of 114 feet and a length of 228 feet to produce failure in this roof layer. The method is not necessarily limited to limestone; any thinly bedded rock type can be tested by this procedure when there is an open parting over the mined area.

Jan 1, 1958

By W. Bruce Montgomery

Manganese oxides occur, with some iron oxides, in small scattered lenses on property controlled by the Columbia Manganese Co. (1943) near Evington, Campbell County, Va. The company mined some manganese ore during 1917 and 1918. A preliminary examination in May 1942 indicated the possibility of finding additional ore. On August 21, 1942, the Bureau of Mines began prospecting to verify the continuity of the ore exposures. Work on this project continued until February 5, 1943. Prospecting and development work included shaft sinking, crosscutting, drifting, trenching, and test-pitting in six separate areas indicating two types of deposits. The most predominant type is a wide brecciated area in which occur lenses or pockets of nodular manganese oxides. The other type is characterized by more of a vein structure, including thin layers of manganese oxides.

Jan 1, 1949

Develop technology that can reduce the dust exposure of a mine worker at the tailgate end of the longwall face by providing him with a clean split of air. Approach Use the jet spray air mover (JSAM) developed under a Bureau of Mines contract (refer to Technology News No. 117 for details on the development), to clean a small portion of the face air and to discharge the clean air behind a brattice partition. How It Works At most longwalls, air flows along the face from head-to-tail. Most of the airborne respirable dust generated along the face during mining is transported to the tailgate with the airflow. Any miner required to work at the tailgate is exposed to this dust. The only practical means of removing airborne respirable dust is with a scrubber. Simplicity and size made the JSAM the best choice for cleaning a portion of the tailgate air. The scrubber has no moving parts and is operated by water at low flow rates (<10 gpm) and fairly high pressures (250-500 psig). Many longwalls have sufficient water systems to supply the JSAM with adequate water pressures and flow rates. Also, the JSAM&apos;s size (4&apos;x 2&apos;x 1&apos;) allows it to be hung on one of the tailgate&apos;s shields or at some other convenient location. A clean split can be maintained at the tailgate by discharging the cleaned air behind a brattice partition at the work area. This should effectively seal off the clean air from the dusty air and provide the tailgate worker with a less dusty work environment.

Jan 1, 1983

By N. A. C. Smith

One of the most important considerations in any manufacturing industry is the production of stable material, that is, material which will not change in quality before it reaches the consumer. The manufacturer of gasoline, the refiner of crude petroleum, is handicapped in this respect by the varying nature of his raw material, but as far as it is commercially practicable, he has endeavored to improve his product, and in most cases he has been eminently successful. It sometimes happens, however, that a gasoline that is apparently normal when first made, will In time deposit small quantities of a gummy substance. The present Investigation was undertaken in the hope that it would throw some light on these gums and indicate how their formation might be prevented.

Jan 1, 1922

By McHenry Mosier

This paper describes come mechanical raid electrical signal systems in common use in Metal-mine shafts, together with several distinctive systems that indicate or control the origin of the signal. The latter systems remove the hazard of the movement of the cage from one level in response to signals from another. Previous publications of the Bureau of Mines have covered several meritorious installations One of the best signal systems for deep shafts is at the Homestake mine4/. A successful installation of an induction system in the Lake Superior mining region permits signaling as well as telephoning from cages at rest or in motion5/. El Potosi mine uses a variation of the three-wire electric system6/. A mine in Utah has developed a system of the double trolly-wire type, in which the cage attendant may signal from a moving cage7/. At present no system of the sine-shaft signaling employing radio is available.

Jan 1, 1939

By M. L. Whisman

Several commercial processes for reclaiming used lubricating oil were duplicated on a laboratory bench scale. Laboratory tests were selected and in some instances modified to determine the physical properties of each oil produced. In addition, the hydrocarbon composition of some samples was determined using a liquid chromatographic technique, and compared with the composition of new oil in order to determine the severity of the re-refining technique. Selected samples of reprocessed oil were reformulated with an additive package for further estimates of quality as determined by wear, corrosion, foaming, and oxidation stability tests. Additionally, several samples of commercially re-refined oil and new oil were obtained and physical properties were determined for comparative studies.

Jan 1, 1974

By D. S. Kingery

The control of coal dust on coal tipples and cleaning plants has not been given the consideration that is afforded underground dust hazards. This apparent oversight is undoubtedly due to the general opinion that coal-dust accumulation in tipples or cleaning plants does not present the same type of hazard that it does underground. That this opinion is at least in part a fallacy has been proved many times, and the Bureau of Mines has on record many examples of explosions in tipples and cleaning plants.3/ In addition to this explosion hazard, coal dust is considered by sonic authorities to be injurious to the health of individuals exposed to it.4/ Obviously, it reduces visibility and contributes materially to accident hazards and the discomfort of the employees. Several companies have recognized this dust hazard and the advantages derived from controlling it; consequently, they have installed equipment to allay and control the dust on, their cleaning plants and tipples. The object of this paper is to. Summarize briefly some of the methods new in effect.

Jan 1, 1943

By Fun-Den Wang

Finite-element structural analyses were performed to determine the stress distribution and displacements around a single rectangular coal mine opening in a multilayered rock system. The effects of changes in mechanical properties of roof and coal layers, roof layer and mine opening geometry, horizontal-to-vertical load ratio, and structural geologic features on the stress distribution about the opening were studied. Variability in the stiffness and relative thickness of the immediate roof layers can produce a considerable difference in the stress distribution about the opening as compared with that of a homogeneous material. Changes in opening width and horizontal-to-vertical load ratio have different effects on the stress distribution about the opening depending on the composition of the roof layers. In general, where a stiff layer exists in the roof at the surface of the opening, the stresses are higher in the roof and ribs around the opening. Horizontal changes in facies in the roof layers produced by structural geologic features can also greatly alter the stress distribution about the opening compared with the simple layered cases.

Jan 1, 1974

By C. Q. Cupps

Rate of gas diffusion in reservoir oil has been investigated in an effort to explain the variation in oil characteristics observed in the Weber Sandstone reservoir, Rangely field, Colorado. Coefficients of gas diffusion were determined experimentally for the Rangely oil system and used in a mathematical simulation of gas diffusion during the probable life of the Rangely reservoir, estimated at 65 million years. The simulator involved solution of Fick&apos;s law for diffusion in two dimensions by the method of finite difference and successive over-relaxation. The results show that continuing gas diffusion is a logical explanation for the variation in oil characteristics at Rangely and that the pattern of gas distribution by diffusion in an asymmetrical reservoir will not conform to structural contours as originally proposed.

Jan 1, 1971

By J. G. Walters

In a survey of the coking properties of United States coals, the Bureau of Mines has accumulated data on more than 500 coals and blends tested by the Bureau of Mines-American Gas Association (BM-AGA) method.4/ The importance of these tests depends upon the fact that a greater number of different coals has been tested in this apparatus than in any other of similar scale, thus permitting comparison of the carbonizing properties of many coals. Evaluation of BM-AGA results with respect to industrial data supplied by member firms of the American Gas Association was one of the first objectives in developing this test apparatus and procedure. Early data showed that, de-pendent upon BM-AGA carbonizing temperature, BM-AGA and commercial results agree closely.5/ Because of limited data, statistical relationships were not established at that time.

Jan 1, 1959

By A. J. Barry

Five makes of expansion-type shells and two types of bolts (mild-steel and high-strength) were used in 30 tests made in sandstone and shale roof, The results show that the anchorage obtained in both the sandstone and shale were stronger than either type of bolt. That is, the yield loads of both bolt types were exceeded before excessive anchor slip occurred. A relationship for evaluating the anchorage effectiveness of 3/8-inch-diameter, expansion-type bolts is presented. A comparison of test results indicates that the anchorage effectiveness of 5/8-inch- and 3/4-inch-diameter expansion-type bolts did not differ appreciably.

Jan 1, 1957

By Fun-Den Wang

A two-dimensional plane strain analysis by the stiffness matrix method was used to analyze two basic pit slope configurations. The magnitudes and the directions of stresses are given for a V-shape and for a flat-bottom pit with the slope angle varying from 30° to 90° at 10° intervals, Stress effects due to irregular pit configuration or to in-situ forces are discussed. Equations of similitude for gravity loading are given. Expressions are also given for the stresses at the toe as a function of slope angle. Procedures are given for finding the stresses in any geometrically similar pit slope of different dimensions and material properties from the stresses and equations presented in this report. Numerical results show that the V-shape pit slopes have lower stresses than the flat-bottom pit slopes; hence, they are inferred to be more stable.

Jan 1, 1970

By Launa G. Mallett, Dana Reinke, Charles Vaught, Michael J. Brnich

As mines become safer and major disasters fewer, the number of experienced emergency responders is decreasing. This decrease will create a gap in response expertise which could have serious ramifications during future mine disasters. While working toward safety goals which may make emergency response obsolete, it would be reckless not to acknowledge that the potential for disaster still exists and that the protection of miners in such circumstances must remain a priority. The Mine Emergency Response Interactive Training Simulation (MERITS) is a computerized mine emergency simulation that meets a variety of needs. It allows personnel in leadership positions to test their knowledge and skill. Groups of individuals composed of representatives from mining companies, labor, and government agencies can practice working together during the simulated mine emergency much in the same way an actual emergency would require. An individual could also run the program to enhance his or her response skills. With this training tool, responders will be able to learn from their mistakes before facing situations with potentially catastrophic consequences. This paper discusses MERITS and its use in providing command center training.

By J. J. Henn

A process is evaluated for recovering metallurgical-grade manganese are from the low-grade manganiferous iron ores of the Cuyuna Range, Minnesota. The process, developed by the Bureau of Mines, employs high-temperature sulfatization of the are to form manganese sulfate and reduction of the are to convert the iron to a magnetic oxide. The roasted ore is water-leached to dissolve the manganese sulfate, which is then separated from the leach residue, is crystallized, and is calcined to produce the manganese product. Iron is recovered from the leach residue by magnetic separation, and is pelletized and calcined to produce byproduct iron ore pellets. The fixed capital cost for a plant yielding a product containing 100 tons of manganese per day is $19.6 million on a mid-1970 basis when the raw are contains 4.84 percent manganese. The estimated operating cost of the plant is $211 per ton of contained manganese. Graphs are included to show the effects of ore cost and varying manganese content of the raw ore on the estimated operating cost.

Jan 1, 1972