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By R. A. Beall

As part of an ongoing program to develop high-quality materials with improved performance and service lives, and to conserve critical minerals, Bureau of Mines, U.S. Department of the Interior, researchers studied the process of hot-rolling metals, alloys, and composites in vacuum. First, a comprehensive review of the literature is presented, including the advantages and disadvantages of using vacuum. Next, details of hot-rolling titanium, chromium, and molybdenum-iron bimetal are given. Finally, the design of new equipment is described. At this time, it is uncertain whether hot-rolling metals in vacuum will gain commercial acceptance in the future.

Jan 1, 1979

The oxidation of zinc vapour plays a very important part in the operation of the Imperial Smelting Process. The kinetics of the reoxidation of zinc vapour by carbon dioxide and water vapour onto quartz and zinc oxide substrates is qualitatively understood and this pertains to the conditions found as the gases are being transferred from the furnace to the splash condenser. However, re-oxidation also occurs in the shaft of the furnace where the solid substrates are sinter and metallurgical coke. It was found that there was a threefold increase in the rate of oxidation on sinter, compared to quartz and a 30 to 300 increase in rate on the coke. This was attributed to the high surface area offered by these materials.

Jan 1, 2003

By C. F. Johnson

Nearly all of the sulphur produced in the world today is converted to sulphuric acid and 49 % is used in the manufacture of fertilizers. In the last few years we have seen the beginning of another chapter in the volatile history of sulphur as the severe shortage of 1963:-67 has been transformed into present-day surplus. Prospects for further aggravation of this situation in the years ahead seem assured. In 1970, western world production showed a rate of increase of 4 -5%, which 1S somewhat less than that of 8% for the period 1963-1967. The rate of growth of consumption dropped considerably in 1968 when the demands of the fertilizer industry fell. During the same period of time, wide-spread demands have been set in motion for a clean environment which indicates that a fundamental change in sulphur supply, demand, and even sources, is likely to result from this upheaval. The sale of sulphur by Poland to the western world has increased and for 1970 was estimated at over one million metric tons. In the next few years, increase in Canadian sulphur supply will stern from two sources;

Jan 1, 1972

By V. Sheikhzadeh, M. Saghaeian, R. Hejazi, A. Abazarpoor

Green pellet strength including drop number and green compression is highly depended on particles size and shape. The used grinding method, ball mill or high pressure grinding roll (HPGR), directly vary the particle size and shape. Considering mode of pellet crack, green pellet is composed of particle-binder-moisture system. Different type of forces existed in such a system to create a stable green pellet: solid particle interaction, magnetic, binding and cohesive forces in the interface of particle-moisture. The pellet failure can occur at solid-liquid interface and/or through liquid phase. Pellet crack occurs when crack passed through entirely the plane failure. In this research, the effect of particle size and shape of pellet feed on green pellet strength has been investigated. It was deduced that green pellet strength highly improved by increase of specific surface area. The drop number and green compression strength of pellets prepared by HPGR was higher than ball mill. It was found that the main reason responsible for this difference was the particle shape. Capillary force is responsible for part of pellet force and improves by decrease of particle size. Also more elongated shape of HPGR particles resulted in higher capillary force due to thinner interface layer between particles. The less circular shape of particles lead to improvement of capillary force as can be occurred for HPGR particles. The rougher shape of HPGR particles resulted in higher wettability of particles and better diffusion of water among particles. In fact the rougher particles means lower connection angle. Aspect ratio of particles was of great importance of crack growth because the required energy of pellet failure increases directly. The required energy for pellet failure increases by increment of particle aspect ratio. The relationship among crack failure force, roughness and aspect ratio has been modeled considering 3 shape descriptors.

Jan 1, 2018

By F. Y. Kang

Graphite with layers structure is easily to form graphite intercalation compounds (GICs) by means of intercalation reactions due to the weak cohesion force among carbon layers, van der Waal?s interactions. By controlling the oxidation-intercalation, high quality exfoliated graphite with low residual sulfur content and MClx-GICs (M=Fe, Co, Ni, Cu, Zn) powder for electromagnetic wave absorbing and shielding materials have been invented. The expansion volume of expandable graphite can be larger than 160 mL/g while the residual sulfur content is less than 800 ppm. The MClx-GICs powder can shield infrared ray and laser completely up to 15 min. We have also in-vented exfoliated graphite for heavy oil adsorption and mild-expansion exfoliated graphite for anode materials in lithium ion battery by controlling the intercalation/de-intercalation. The exfoliated graphite can adsorb heavy oil up to 80 g/g, it also exhibits better performance than commercial active carbon in sewage treatment. The mild-expansion exfoliated graphite as anode material shows high capacity of 370 mAh/g and good cycle performance.

Jan 1, 2014

By Fathi Habashi

Nitric Acid has been used for over 50 years in the uranium industry and in phosphate fertilizer manufacture. Its application in the treatment of sulfide concentrates is relatively recent. A review of recent developments is given.

Jan 1, 1999

By V. Sheikhzadeh, M. Saghaeian, R. Hejazi, A. Abazarpoor

"The morphology of pellet feed is known to influence several properties of iron ore pellets, including drop number, compression strength and reduction properties. The effect of grinding method on the particle size, specific surface area and particle shape of an iron ore concentrate has been studied. Grinding methods considered were ball mill and high pressure grinding rolls (HPGR). 5 different samples (Blaine= 1800, 1900, 2000, 2100 and 2200 cm2g-1) were used to compare the size, shape and specific surface of particles for each grinding methods. Particle size was meticulously examined by sieve analysis, laser sizing and image analysis. In samples ground by ball mill, it has been observed that the fraction of particles <10µm increases from 39% to 46% as the Blaine number increases from 1800 to 2200 cm2g-1. For HPGR samples, corresponding figures are 41% and 49% respectively. It is evident that for samples ground by HPGR, the fraction of fine particles is higher than that of those ground in the ball mill. To measure the specific surface area of particles, Blaine and BET were used. A higher real surface area was observed from HPGR treatment in comparison to ball mill grinding, provided by a higher porosity, cracks, roughness and new surfaces. Shape factor of particles was determined using three descriptors: circularity, roughness, and aspect ratio. It was also observed that particles produced by HPGR were more elongated, less circular, and rougher than those processed by the ball mill. 1. INTRODUCTION Particle size and shape are important parameters that can significantly affect mineral processing plants and pelletizing plant performances (Brozek and Surowiak, 2007). It has also been proposed that green pellet quality is directly related to the amount of fine particles in a pelletizing plant (Dwarapudi et al., 2008; Umadevi et al., 2008; Gul et al, 2014; Van der Meer, 2015). Particle size distribution and specific surface area (SSA) are also key factors that can control the quality of green and fired pellets. Processing circuits generally reduce the fines fraction to lower than the required specific surface area (SSA). It is therefore necessary to regrind concentrates to produce suitable pellet feed for further treatment in the balling and firing steps [1, 2]. Two main methods are used for re-grinding of concentrate; high pressure grinding rolls (HPGR) and ball mill. Given the different forces used to reduce size in these methods, it is expected the shape of particles will be different (Pourghahramani and Forssberg, 2005)."

Jan 1, 2018

By Jeffrey H. Welsh

The Bureau of Mines studied the use of computerized, continuous, remote monitoring systems for safety from power system faults in underground coal mines. In this report the need to improve protection against power system faults is documented, and types of faults are identified. The relationship between mine safety regulations and computerized, continuous, remote monitoring is analyzed.

Jan 1, 1983

By Marco Zurco, Claudia M. Mendez, Alicia E. Ares, Carlos E. Schvezov, Carlos M. Rodriguez

"Zinc-Tin alloys were solidified in horizontal form and the obtained results were analyzed. During solidification the distribution of temperatures were measured by using thermocouples located strategically along the length of the samples. From the measured temperatures the following parameters were derived; the local temperature gradient, the cooling rate and the velocities of the liquid and solids fronts. Comparing the structure of the samples and the values of these parameters it was found that the temperature gradient reaches minimum values of as low as - 0.6 °C/cm, and velocities of the fronts of around 0.1 cm/s. In addition, the grain size was measured along the samples. The results are presented and discussed in the frame of the results previously obtained for other alloys.IntroductionGenerally solidification leads to two types of grain morphologies: columnar and equiaxed. The origin of each one has been the subject of numerous theoretical and experimental researches in the field of metallurgy for many years [1-7]. The columnar-to-equiaxed transition, CET, is considered as an object of high technological relevance with respect to the directional solidification of metallic alloys. This structure transition may be sharp or gradual and it has been reported to be dependent on thermal conditions associated with the casting process, including melt convection, heat transfer coefficients at the metal-mold interface, growth rates, thermal gradients, cooling rates, transport of solute, alloy composition, melt superheat, mold temperature, mold design, casting size, casting geometry, and the concentration of nucleating particles. As a consequence, it is critical for industrial applications to understand the physical mechanisms which control this transition during solidification. Many studies highlight the importance of the relative growth of the equiaxed and columnar grains and develop expressions or numerical procedures to describe a criterion for the CET. A number of experimental investigations reported in the literature suggest that the CET occurs when GL in the melt reaches a minimum critical value [5-7]."

Jan 1, 2012

By A. P. Liu

Semi-industrial test on fine products of Meishan dressing plant was carried out with type RP80/25 high pressure roller mill produced by Homburg Corporation of Germany, and the influences of such factors as energy consumption, water containing, throughput and circulating load on rolling effect were investigated. Closed circuit experiment result showed that Meishan iron ore could be suitable for powder grinding with high pressure roller mill, and energy consumption of the operation was declined by 25%~30%, which was favorable for energy-saving, increasing production efficiency and improving grinding effects. According to above experimental results, this paper put forward the technical proposal of application of high pressure roller mill in Meishan, and pointed out some technical problems which needed to be settled urgently in technology disposal.

Jan 1, 2014

By Bhagyadhar Bhoi, Chitta Ranjan Mishra, Hara Prasanna Mishra

"In the Sukinda Valley of Orissa, India, the total quantity of nickel ore reserves comprising of both lateritic and chromite over burden(COB) have been estimated at around 231 million tonnes containing 0.3 to 0.9% Ni. While mining of one tonne of Chromite ore, around 6-7 tonnes of chromite over burden are removed. These overburden materials are disposed as waste materials, which causes lot of environmental hazards and ecological imbalance. India imports a large amount of nickel and ferro-nickel to meet its growing demands in various sectors. For import substitutions, efforts have been made to produced ferro-nickel from the lean deposits of nickel bearing lateritic ores/ chromite over burden materials by reduction roasting followed by magnetic separation and then the nickel rich magnetic fraction is smelted to produce ferro-nickel. It has been possible to produce ferro-nickel of grade varying from 4-25% nickel.IntroductionDuring mining of chromite ore, large quantities of overburden materials are being generated. The materials amount to approximately 10 million tones per year contain around 0.3-0.9% Ni, 0.02-0.06% Co, 20-50% Fe and 4-9% Cr2O3 depending upon the location and the depth of the mine. These materials presently do not find any application for the extraction of nickel due to lack of a suitable technology. The materials are also unsuitable for ferro-nickel making because of their very high iron to nickel ratio. The country is seriously looking for a suitable technology to utilize these resources as its entire domestic requirements of nickel is met though imports. In this connection, a systematic approach has been made at the Institute of Minerals and Materials Technology, Bhubaneswar to develop a process for ferro-nickel making from this indigenous resource."

Jan 1, 2011

By William Petruk

The primary requisite for a successful extractive metallurgy operation is to grind an ore fine enough to liberate the minerals so that they can be concentrated, or to expose mineral surfaces so that the minerals can be leached. The ease or difficulty of liberating or exposing the mineral grains is dependent upon the mineral textures such as grain size, crystallinity and bonding between mineral grains. In particular, mineral grains with straight grain boundaries and a weak bonding to other minerals are easily liberated and readily concentrated into high grade concentrates. In contrast mineral grains that have re-entrant boundaries and are strongly bonded to their neighbours are not easily liberated and will not produce high grade concentrates, even with regrinding. Similarly, inclusions that occur along fractures and grain boundaries can be readily exposed and leached. Whereas minute random inclusions in large grains will not be liberated or exposed unless they occur along planes of weakness.

Jan 1, 1995

"The research aimed at solving the problem of measuring instantaneous local physical quantities for multiphase flows in mineral processing, which are common in minerals industry and with significant challenges. Due to the lack of proper measurement tools currently in minerals industry, multiphase flows (such as in flotation cell) are treated as in a “black-box”. It is crucial to develop measurement technique by which the acquired processing data can be used for process optimization and control. By measuring the conductivity distribution across a measurement area, Electrical Resistance Tomography (ERT) has been adopted by many researchers to monitor and investigate many processes involving multiphase flows in other industry sectors. A compact ERT probe was built and then used to measure the conductivity distribution within a few flotation machines. In a flowing foam flotation column, the results showed that ERT can accurately measure the change of liquid content (high conductivity fluid distribution). In another part of work, based on the Green-Kubo relations, ERT can measure turbulence via the fluctuation of conductivity caused by bubbles moving through the measurement area, changing the density of the fluid. The tests with the Metso 3 m3 RCS flotation cell were also carried out for turbulence measurement under different air rates and impeller speeds. The results of flotation cell from ERT measurement showed that varying impeller speed had more pronounced influence than changing air rate. When impeller speed is increased, the size of the high turbulent zone increases. ERT is a powerful technique that has the potential to be used for a wider range of applications. The future work will be carried out with more case studies and expanded to more processes such as leaching process, high temperature flows in further downstream production chain (steel making process and alloy manufacturing process).INTRODUCTIONMultiphase flows constitute a majority of the naturally-occurring and industrially-relevant flows, especially in mineral processing. Some of the measurement techniques have been used for the study of fluid characteristics. Optical techniques such as Laser Doppler Anemometry (Kyselaa et al., 2013) and Particle Image Velocimetry (Nobach and Bodenschatz, 2009) can produce accurate measurement results with high spatial and temporal resolution, but their applications are limited to transparent flows. Hot wire probes (Amini et al., 2013) have high spatial and temporal resolution in turbulence quantification, but they are susceptible to environmental factors."

Jan 1, 2018

By X. M. Chen

The selection of leach reagent mainly according to the ratio of useful mineral to gangue in mineral raw material and the structure of mineral raw material. Besides that the price of reagent, the capability of reagent decomposing mineral and its causticity on equipment is also supposed to be in regard. On common conditions, the scandium content in mineral raw material is low, even Sc concentrate of specimen-Yunnan rare earth ore which contain Sc used in this experiment only is 148 g/t. Moreover, in enlarging scale experiments the content of scandium in leach liquid is only 3.6g/t, meanwhile various and complicated impurity existing in it. At present, both domestic and abroad has succeed in enriching scandium from vitriol solution, while enriching scandium from hydrochloric acid only has been studied in some minority units, which is not reported to be practical in industry. Therefore, this item offer a new research issue on Sc?s extract, which is as well as the task of this research. Spectrum analysis, chemic component analysis and scandium content have been made in main mineral measurement on rare earth with Sc in the paper. Based on characters of sample, select hydrochloric acid, vitriol and nitric acid as leach reagent and make different blueprints to accomplish the experimental research about selecting leach reagent. In the aspect of rare earth leach scandium leach density is researched, leach liquid to solid rate, leach temperature, leach time, leach granule rate and leach solution. This experiment claims that in the optimal experimental ambience, leach rate of vitriol is 58.18%, the leach rate of nitric acid is 50.73% and the leach rate of hydrochloric acid is 59.34%. Among them, hydrochloric acid has the best effect, therefore this experiment choose it as the leach reagent.

Jan 1, 2014

By V. J. Ramirez, A. M. E. Noguez, M. J. Navarrete, B. G. Salas, N. T. Robert

"The close die forging stress in truncated conical cavities is evaluated with dimensional analysis. Five dimensionless groups are proposed from the process variables in order to simplify the forging stress determination. These groups are experimentally related and graphically expressed. This methodology can be used to predict the actual forging stress in industrial close die forgingThe use of the dimensionless groups allow to comprise more cases than the presented here, provided similar geometries and operational conditions.Introduction.Closed die forging is essentially a plastic deformation inside a two piece mold (forging die) with the inverted shape of the actual forging geometry. This plastic deformation will always be the result of a compressive stress. There are theoretical models which include complex calculations for the analytical determination of stresses (1, 2, 3, 4). Results of these calculations are approximate, requiring generally ulterior tests to obtain the true operational conditions(5).In this paper, it is presented a simplified approach to the actual compression stress needed in the forging. A well known tool in engineering: the Buckingham's Pi theorem in conjunction with dimensionless groups and a working piece scale model is used. Dimensional analysis will give the dimensionless terms needed to experiment with a selected scale model geometry to make the stress determination. The results presented demonstrate the reliability of this methodology."

Jan 1, 1997

By Ted H. Eyde

Nearly 17 years ago a major producer of synthetic zeolites started an extensive exploration program for natural zeolite deposits which resulted in the discovery of over 170 occurrences in the western United States. A few years later several of the other producers and consumers of synthetic zeolites also started similar exploration programs. Since then, small quantities of natural zeolite minerals have been produced from at least 12 deposits in the United States. Of these the Bowie deposit, about 13 miles north of Bowie, Arizona, is the most important,having produced over 5,000 tons of vitric tuff zeolitically altered to the mineral chabazite and minor amounts of the minerals erionite and clinoptilolite. Mining Districts and Mineral Deposits of Arizona compiled by Charles A. Mardirosian, Consulting Geologist, estimates the value of the total production from the Bowie deposit at a very conservative $2,000,000. Unfortunately, none of the companies responsible for the discovery and the initial production of natural zeolites made any effort to develop the high volume, low cost applications of this unique mineral raw material. Instead, they developed only the high unit value uses to supplement their existing synthetic molecular sieve product lines. With the producers of synthetic zeolites thinking in pounds and not in tons, further development of natural zeolite deposits stagnated for over a decade.

Jan 1, 1974

By T. Gonzales

Magma Metals Company operates an Outokumpu Flash Furnace, four Peirce-Smith Converters and two Anode Casting Wheels supported by six Anode Vessels. Process gasses from the Flash Furnace and Converters are treated in a two train/double contact sulfuric acid plant. Sulfur capture for the smelter is +98%. The new flash furnace was commissioned on July 7, 1988 and has processed over three million tons of sulfide concentrate without a major rebuild. Magma has gained unique experience in the operation of the flash furnace at high oxygen enrichments with low off-gas dust loadings. New procedures have been developed to maintain secondary material generation at equilibrium and for maintaining metallurgical control of operating parameters. This paper describes all the procedures, operation control parameters and operating philosophy that has allowed Magma to achieve superior performance.

Jan 1, 1992

By B Tutmez

Determination of stress-strain behaviour of rocks plays a crucial role in understanding the response of rocks during loading. However, it is a tedious, expensive and a time-consuming process to obtain such characteristics both in the laboratory and in situ. On the other hand, non-destructive testing methods such as ultrasonic velocities can produce a reliable and fast solution to indentify state of strain and stress in rocks. The present paper aims to provide insight into the relations amongst ultrasonic wave velocities, amplitudes and deformability properties of porous siltstone under compressive loading. For this purpose, pulse (vP) and shear wave velocities (vS) along with amplitudes (AP - AS), and applied loads with resultant strain were measured simultaneously so that response of siltstone to compression can be evaluated. In addition, initial vP and vS were recorded at the beginning of each test to calculate dynamic elastic properties of the specimens. This provided a comparison between static and dynamic elasticity properties of siltstone. Crack damage associated with the onset of dilation was also investigated. The results showed that there is a non-linear logarithmic relation between velocities and stress-strain level for siltstones.

Sep 26, 2011

The viability of physico-chemical purification methods such as selective flocculation for separation of two components having similar chemical composition and same crystal structure but different surface properties is demonstrated. Loss of selectivity was observed in a dolomite-dolomite mixture with Polyethylene Oxide (5 million molecular weight) as the flocculant. Hetero-flocculation was minimized using a low molecular weight PEO (MW -105) as the site blocking agent (SBA). Near complete separation was achieved at pH 10.5 at 100% recovery level.

Jan 1, 1993

By O Arafat, R E. McIvor, K M. Bartholomew

It is well known in the industry that good classification system performance is vital to efficient ball mill circuit performance. But what is meant by good classification system performance, and how is it achieved? Unfortunately, the perceived complexity of classification systems, and the day-to-day time demands placed on the practicing metallurgist, all too often put the low-hanging fruit of classification system optimisation in the ‘I’ll do it later’ basket. Additionally, lingering confusion about basics such as the relationship between circulating load ratio and ball mill circuit performance makes the optimisation objective seem nebulous to both plant metallurgist and designer.Some of this confusion can be eliminated by taking a step back from the overwhelming detail of sharpness of separation curves, circulating load ratios, cyclone feed pressures, vortex and apex sizes etc, and focusing on the purpose or function of the classification system – to apply mill power to particles that need further size reduction! The classification system efficiency (CSE) metric captures how well the classification system is performing its function with two quick and easy size distribution analyses.Once CSE is understood and implemented as the optimisation criteria, well-tested methods for improving CSE can be implemented and quickly measured at plant scale to give confidence that the right change was made.This paper will describe CSE and how it is measured in practice. Next, a guide for improving CSE through manipulation of design and operating variables in the classification system will be provided. Examples and case studies will illustrate the gains in ball mill circuit efficiency that can be achieved by maximising CSE.CITATION:Bartholomew, K M, McIvor, R E and Arafat, O, 2018. A guide to maximising ball mill circuit classification system efficiency (CSE), for operators and equipment designers, in Proceedings 14th AusIMM Mill Operators&#39; Conference 2018, pp 553–558 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018