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By W. J. Boone

Experimental determinations were made of vapor-liquid equilibria data for a helium-nitrogen-methane system. A mixture composition was chosen to approximate the crude helium to be produced Or conservation that will eventually be further refined to obtain pure helium. Although there are publications of studies of the vapor-liquid equilibria of helium-nitrogen, helium-methane, and nitrogen-methane binary systems, there is little indication of work done on the ternary system of helium-nitrogen-methane. The experimental data presented in this report supplement the information available for the binary systems. The equilibrium vapor-liquid data and equilibrium vaporization coefficients are presented in tabular form. Graphs are employed to show an extensive amount of the data.

Jan 1, 1963

By Y. Chengxian, F. Yaorong, Xinzhe. L.

Many factors about the HIC (hydrogen-induced cracking) resistance of pipelines are discussed in this paper. The main factors that influence the ability of HIC are environmental and material factors. The chemical compositions, non-metal inclusions and microstructure are discussed in detail, while a group of tests on HIC resistance are done according to varying C, S, Mn and P contents in pipeline steels, different experiment time and different strength to the coupon. It is concluded that decreasing the amount of C and S can obtain good HIC resistance; the test time has an effect on the different microstructure of X70; microstructure is the most sensitive factor for the initiation processes of HIC.

Jan 1, 2005

By D. Pawelus, J. Butra, R. Debkowski, M. Szpak

Impact of horizontal stresses on stability of underground workings in mines is a very important issue in underground mining. Identification of the initial state of stress in the rock-mass should be one of the main actions taken into account while designing and carrying out the mining activity in underground mines. The paper presents the tests on three dimensional stress pattern in Polish copper mines, owned by KGHM Polska Miedz S.A. Group, carried out in 2012. The research program covered 7 measuring stands in two mines; their average depth was about 1000 m. The main aim was to identify the values and directions of horizontal stresses in order to optimize the extraction and to improve the safety. The overcoring method with the use of CSIRO HI type probe was applied. The paper also describes the measuring technique which was developed for the purpose of specific mining and geological conditions of KGHM mines, taking into consideration the natural hazards encountered there as well as technical and operational capabilities with regard to drilling equipment. The experience gained during the underground measurements and the issue of making such measurements in underground copper mines in Poland are presented in the paper. The stress patterns obtained during the underground measurements are of application importance for the process of designing the spacing of mine workings and improving their stability and mine support selection.

Jan 1, 2015

By Frame Ritzert, Dennis Keller, Vijay Vasudevan, David Arenas

"An investigation was conducted to describe topologically close packed (TCP) phase instability as' a function of composition in the advanced ·Ni-base superalloy Rene N6. TCP phases are detrimental to overfill high-temperature performance of Ni-base superalloys because of their brittle nature and because they deplete the Ni-rich matrix of potent solid solution strengthening elements. Thirty-four variations of polycrystalline .Rene N6 determined from a design-of-experiments approach were cast and homogenized at 13 l5°C for 80 hours followed by exposure at 1093°C for 400 hours to promote TCP formation. The alloys had the following composition ranges in atomic percent: cobalt 10.61 to 16.73, Mo 0.32 to 1.34%, W 1.85 to 2.52%, Re 1.80 to 2.11%, Ta 2.36 to 3.02%, Al 11.90 to 14.75%, and Cr 3.57 to 6.23%. Physical and chemical characteristics of all microstructures obtained were described using various analytical techniques. From these observations, a mathematical description of TCP occurrence (s and P phase) was generated for polycrystalline Rene N6.IntroductionNi-base superalloy single crystals represent the state-of-the-art for turbine engine airfoil application as they offer the best balance of properties to allow for the high operating temperatures required: for efficient engine operation.1 Current trends in alloy design take advantage of improved creep rupture strength with the addition .of higher levels of refractory elements. 2 In .particular, the addition of significantly higher levels of Re in third generation superalloys is key for both microstructural stability and creep rupture strength. 3 While the presence of the refractories is thought to provide strength benefits from solid solution hardening, a tendency for alloy instability in the form of topologically-close-packed (TCP) phases or secondary reaction· zone (SRZ) ·phenomena accompanies the high refractory content. 3 The formation of these phases in sufficient amount is detrimental to the overall high temperature performance of Ni-base superalloys because of their brittle nature and because they deplete the Ni-rich matrix of potent solid solution strengthening elements.4 The tendency for a particular composition to form TCP may not be immediately known since the precipitation of TCP phases in Ni-base superalloys is nucleation controlled, thereby requiring long times at elevated temperatures to precipitate. 5 They preferentially nucleate along the octahedral planes of the Ni-base superalloys, usually in areas of refractory metal enrichment at grain boundaries or inside dendrites.5-6 In Rene N6, two closely related TCP phases, a and P, have been observed.2"

Jan 1, 1998

By J. M. Skeaff

As much as 100% of the gold and 67% of the silver in a sulphur-bearing hydrometallurgical leach residue have been transferred to copper metal at copper smelting temperatures by dissolving the partially calcined residue in an iron-bearing slag maintained in equilibrium with the liquid copper metal and matte phases. The precious metals can then be recovered by conventional refining techniques. Copper can be recycled at least four times without any detrimental effects on gold and silver transfers and recoveries. Apparent copper recovery in the .process can be over 100% because of the copper content of the residue. Based on slag analys.es, the overal1 recovery of gold in the copper metal and matte phases varies from 94% to 100% under all conditions investigated. On the? same basis, silver recovery varies .from 9S% ?to 99% under optimum conditions, but is only 4S% to 73% under other, less attractive conditions. Unaccounted for silver losses of' about 30% make it difficult to determine the major factors affecting ?silver transfer and recovery. A method for implementing the technology on a commercial scale at a Canadian copper/zinc smelter has been proposed. A preliminary economic assessment and comparison of the proposed pyrometallurgical process with conventional cyanidation indicates that either process is economically attractive for recovering gold and silver from leach residues. Although the capital costs are higher, the pyrometallurgical process is simpler, has higher recoveries, lower operating costs and no .potential environmental problems related to cyanide disposal.

Jan 1, 1989

By G. V. Sullivan

This report summarizes the results of a preliminary study concerning manganese extraction from low-grade dolomitic materials from the Philipsburg district in Montana by the Dean-Leute ammonium carbamate process. Studies were made to determine the relationship between the variables involved in treating these materials by a roast-leach process and the amount of manganese extracted. The variables studied were the roast temperature, the roast particle size, the molar ratio of NH3 to CO2 in the leach solution, the liquid-solid ratio in leaching, the leach time, and the size of the particles being leached. The roast-leach studies were statistically designed, and the experimental results were evaluated by an analysis of variance.

Jan 1, 1962

By K Johnson, G Morrison, N Lisowiec

The Mount Wright gold deposit is located near the town of Ravenswood, ~90 km south of Townsville, in north Queensland. The deposit has been mined by underground methods since 2006. It produced approximately 138 koz Au in the 2011 - 2012 financial year and has a total endowment of approximately 1 Moz Au. To facilitate near mine exploration, a re-logging campaign of 600+ diamond and RC drill holes was recently conducted, resulting in a revised three-dimensional (3D) geological model and improved understanding of the ore controls and the mineralised system. The deposit is within a Permo-Carboniferous breccia complex approximately 350 m diameter and more than 1200 m deep. It consists of early peripheral granite-rich breccia, polymict breccia, a rhyolite spine and a late tuffisite (fine-grained milled breccia) pipe. The rhyolite spine is approximately 60 m + 250 m + at least 1200 m deep and is zoned with massive, flow-banded and breccia phases that are in part gradational with the other breccias. There is extensive sericitic alteration centred on the tuffisite and rhyolite units and fading out into the shallower and peripheral polymict and granite-rich breccias. There is also a broad pattern of metal zoning with elevated Pb-Zn ¦ Ag in the upper 400 m, Au-Cu-Bi below 400 m fading out below ~850 m, and a poorly defined deep Mo-W-Te-Sb anomaly. The majority of the Au ore is between 400 and 850 m below the surface in the rhyolite spine. Below this, Au mineralisation is less coherent, and more localised in the margins of the rhyolite and in the adjacent tuffisite. The developing model is that the ore is not confined to or necessarily directly genetically related to the rhyolite spine, but is driven by other phases of intrusion that also generated the tuffisite pipe. This model is being used to generate additional drill targets away from the present mine development.CITATION:Johnson, K, Morrison, G and Lisowiec, N, 2013. Advancing near-mine exploration with an updated geological model for the Mount Wright gold deposit, Queensland, in Proceedings World Gold 2013 , pp 469-478 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Sep 26, 2013

By M Ind, B Usher

Environmental regulators are increasingly adopting risk-based approaches to protect aquatic ecosystems. The Australian and New Zealand Environment and Conservation Council (ANZECC) and the Agriculture and Resource Management Council of Australia and New Zealand (ARMCANZ) (2000) introduced a risk-based approach to water quality guidelines that use decision frameworks to adapt water quality guidelines to local environmental conditions. Environmental quality objectives are no longer a simple ‘pass or fail’ number such as restricting total suspended solids (TSS) concentration to a specified limit for a particular rainfall event. This approach ignores spatial and temporal variability and the complexity of aquatic ecosystems. The risk-based approach establishes levels where adverse effects may occur. If these objectives are not met, further risk-based investigation is undertaken to assess the potential impact to the ecosystem. Klohn Crippen Berger (KCB) developed a dynamic simulation to predict the variability of sediment discharges, which is applicable for risk-based impact assessment of aquatic ecosystems. The application of the methodology over the life of a mine site is illustrated using a proposed South Pacific mine.The site location is in extremely rugged terrain with a high annual rainfall of approximately 4.7 m. There were two major sediment ponds proposed to reduce sediment discharges. A sediment and hydrology model was developed in Goldsim to provide daily estimates of run-off flows and sediment concentrations. A modified algorithm based on the Australian water balance model was created and incorporated into the Goldsim model and calibrated using recorded field data.The sediment module was developed based on a Revised Universal Soil Loss Equation (RUSLE) assessment, an annual prediction of soil loss over a catchment. A land-use type erosion vector was developed for different land-use types and for each of the subcatchments, a subcatchment erodibility vector was calculated. This vector and the daily rainfall erosivity factor were used to estimate the daily soil loss. The estimated soil loss and the modelled run-off yielded predictions of daily sediment concentrations. Finally, a sediment settling module was used to predict the daily efficiency of the sediment ponds and hence discharged sediment concentrations.The results of this modelling form the first part of a quantitative risk-based assessment into suspended solids impacts. The second part is the assessment of the effects of these predicted TSS concentrations on aquatic ecology. As part of the feedback-loop required in a risk management framework, if the environmental quality objectives are not met then further management decisions and actions may be required to reduce the risks presented by suspended solids. This may include modifications to: the mine-development plan; construction techniques and scheduling; processing techniques; rehabilitation strategies; or hard-engineering solutions such as sediment basins or flocculation.The Goldsim water-balance model provides a quick and efficient method of testing potential remedial actions on predicted sediment loads and concentrations. In combination with a cost-benefit assessment, options for reducing sediment releases from the mine site can be effectively and quantitatively compared thereby providing mine operators with a basis for decision-making. Regulators can also be satisfied that potential impacts to aquatic ecology have been comprehensively assessed and the necessary management decisions have been initiated to limit risk to the environment.CITATION:Ind, M and Usher, B, ?2014. A dynamic sediment simulation to predict the variability of suspended solids concentrations over life-of-mine for application to a risk-based environmental assessment, in Proceedings Life-of-Mine 2014 , pp 191–204 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 16, 2014

By N. P. Mabasa, N. Naudé, A. M. Garbers-Craig

An improved methodology is presented for assessing the economic feasibility and effectiveness of recycling MgO-C and Al2O3-MgO-C refractory bricks, which are widely used in the steelmaking industry. Since approximately 28 Mt of refractory bricks are discarded each year, it is logical to recycle them. When furnaces and ladles are relined, the spent refractory bricks become mixed up, and need to be sorted before recycling. This study examined the use of a hand-held X-ray fluorescence analyser (HH-XRF) to distinguish between spent oxide-based and oxide-carbon-based refractory materials, with special emphasis on spent MgO-C (MC) and Al2O3-MgO-C (AMC) bricks. HH-XRF analysis was conducted on 18 oxide-carbon refractory bricks as well as on MgO-chromite and bauxite-based refractories. X-ray diffraction, reflected light optical microscopy, and scanning electron microscopy with energy dispersive spectroscopy were used to characterize the MgO-C and Al2O3-MgO-C bricks to confirm the accuracy of the HH-XRF analyses. This study also underlined the importance of calibrating the HH-XRF analyser for the refractory bricks to be sorted. The HH-XRF was successful in distinguishing between the different oxide-carbon-based refractory bricks both before and after cleaning. This result is important as it proves that HH-XRF provides a method whereby spent MC and AMC bricks can be sorted quickly and reliably.

Jan 26, 2023

By X Tian, J Forster, A Olmsted, E R. Bobicki, M Goldbaum, D Boucher, C A. Pickles

As the global demand for metal values expands, it becomes increasingly important to create more sustainable mining operations. Consequently, considerable research and technology development is required to produce processes which are both more energy efficient and have a minimal environmental impact. One potential technology is the utilisation of microwave pre-treatment to reduce the energy requirements in comminution. Microwaves can preferentially heat the valuable mineral phases in an ore and the resulting differential thermal expansion leads to the formation of microfractures along the grain boundaries. As a result of the preferential heating, ore competency is reduced, mineral liberation is enhanced, a coarser grind size can be employed, and plant throughput can be increased. Furthermore, microwave pre-treatment can be combined with advanced ore sorting, to decrease the quantity of gangue material processed downstream and hence reduce tailings production. Previous studies on the microwave treatment of ores over the last 30 years have mainly been limited to low power bench-scale studies and there is a paucity of information on pilot and/or commercial scale studies. In the present research, the microwave heating behaviours of over 40 ores have been studied at the bench-scale. These results were used to generate a database, from which a unique classification system was developed. This system was used to rank the amenability of any given ore for microwave pre-treatment. This knowledge can be employed to predict the performance of the ores in the high-power pilot scale tests and thus can be used as a pre-screening tool. The effects of high-power microwave pre-treatment on grindability and liberation were reported. Additionally, the ore sorting potential was evaluated using a combination of X-ray transmission (XRT) and microwave infrared (MW/IR).

Aug 24, 2022

By Pedro Cunha Alves, Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Julio Aníbal Morales Pereira, Antônio Cezar Faria Vilela

Consideráveis esforços vêm sendo realizados para aumentar o desempenho das operações metalúrgicas e a qualidade do aço produzido. Nesse sentido, o papel das escórias no processamento do aço tem se tornado de muita importância. Com o objetivo da otimização das escórias, numerosos estudos têm sido conduzidos para uma melhor compreensão do efeito da composição química e demais propriedades da escória sobre a viscosidade, bem como, sua influência sobre o controle da limpeza inclusionária. Também se tem observado uma evolução das técnicas experimentais de laboratório que são empregadas para a investigação estrutural e medidas das propriedades físicas das escórias. Essa evolução e investigação são fundamentais, inclusive, para o ambiente prático da indústria do aço.

Oct 1, 2019

By E. Oraby, S. Garcia, A. Thurgood, D. Bertoldi, G. O’Malley

Mining and Process Solutions (MPS) most advanced process, GlyCatTM is the only process that can be easily adapted to existing cyanidation plants in the market today whose real advantages over cyanidation are when treating copper containing ores, concentrates or tailings. With such complex material, GlyCatTM requires 70-90% less cyanide addition to achieve the same precious metal extraction. However, GlyCatTM is not simply cyanidation with added glycine. It is a completely different process where the solution chemistry and conditions needed to effectively leach the precious metals are quite different. Downstream however, the process is largely unchanged as the recovery of the leached gold and silver uses existing known processes such as conventional activated carbon or zinc cementation (Merrill-Crowe process). Another advantage is lower SCN, OCN, WAD and no free cyanide in the effluent which can substantially reduce cyanide detoxification requirements and decrease the OHS and ESG risk of the operation. This paper outline some of these differences and presents testwork, piloting and process examples to highlight the advantageous of this new process over conventional cyanidation.

Feb 1, 2023

By Wei Qu, Yongsheng Song, Xingyu Liu, Wenjuan Li, Shuang Liu, Guiying Zhou, Bowei Chen

The Pb,Sb,Zn multi-metal sulphide ore is processed in sequence of beneficiation of jamesonite, sphalerite . Due to relative large amount of collector (xanthate), activator (CuSO4) and regulator (lime) during different flotation stage, the flotation wastewater from sphalerite beneficiation stage can’t be directly recycled to the first lead flotation stage. In this paper, the flotation wastewater from sphalerite beneficiation stage was treated by Ozone and BAC technology, results showed that when the influent concentation of COD and copper ion were 850 mg/L, 10.48mg/L respectively, the Ozone and BAC technology could effectively treat such type of water. In the treated wastewater, the COD is 60mg/L, copper ion concentration is 0.023mg/L, pH is 7.0, which satisfy the need of Pb,Sb-Zn preferential floatation separation process. After recycle of the treated wastewater to Pb,Sb floatation circuit, qualified Pb,Sb concentrate and Zn concentrate were obtained.

Jan 1, 2014

By J. G. Groppo

Froth flotation technique is an effective and efficient process for recovering of ultra-fine (minus 74 pm) clean coal. Economical dewatering of an ultra-fine clean coal product to a 20 percent level moisture will be an important step in successful implementation of the advanced cleaning processes. This study is a step in the Department of Energy's program to show that ultra-clean coal could be effectively dewatered to 20 percent or lower moisture using either conventional or advanced dewatering techniques. The main focus of the pilot plant study was on proof-of-concept testing of a dewatering technique for a fine clean coal product. The coal industry is reluctant to use the advanced fine coal recovery technology due to the non-availability of an economical dewatering process.

Jan 1, 1997

By Wen Xuan

Concentrados ?midos de minério de ferro podem se congelar durante o inverno e ficarem presos nos vagões de transporte, dificultando o descarregamento e a operação. Este problema vem sendo observado nas minas de Kryvyi Rih, Ucrânia e Mont-Wright, Canadá, onde o minério de ferro possui respectivamente 10,5% e 3,5% de umidade e, durante os invernos rigorosos, as temperaturas podem chegar a valores abaixo de -20°C. Nestes locais, uma grande quantidade de energia e tempo tem sido gasta para aquecer e descongelar os vagões. Este artigo mostra que polímeros superabsorventes, como o poliacrilato de sódio, podem evitar o congelamento e facilitar as operações de descarregamento e manuseio, além de possuír fácil aplicação, sendo eficientes quando aplicados apenas no fundo dos vagões, sem a necessidade de se misturar o polímero com o concentrado de minério de ferro.

Aug 17, 2017

By Ricardo José Gonçalves Costa

A estabilização do aço inoxidável ferrítico ASTM 409 na aplicação em sistemas de exaustão de automóveis é cada vez mais exigida em função do aumento das garantias e de desempenho neste sistema, particularmente em temperaturas mais elevadas dos gases de escape. O Ti é um dos elementos mais utilizado como estabilizante da estrutura ferrítica. No entanto, teores elevados deste elemento pioram as condições de lingotabilidade durante a produção do aço, aumentando a sua suscetibilidade a problemas de qualidade superficial. Desta forma, a dupla estabilização com Ti e Nb é uma solução para reduzir o teor de titânio. Assim, o objetivo deste trabalho foi investigar o efeito da adição de Nb na microestrutura por meio da comparação entre o aço ferrítico estabilizado ao Ti (409H) e bi-estabilizado ao Ti e Nb (409S). Os resultados deste trabalho mostraram que o aço 409S é afetado diretamente pela microestrutura mais deformada após laminação a quente em relação ao aço 409H, gerando maior força motriz para recristalização no recozimento final.

Aug 17, 2017

By Alexsandro Marcio da Silva

Com o objetivo de prover informações precisas, coesas e em tempo real aos gestores da Diretoria da Usina Presidente Vargas (UPV) para a tomada de decisões, foi criado o projeto para Gestão de Indicadores de Desempenho em Tempo Real com o foco no processo produtivo e performance das áreas de Laminação (a quente e a frio), Zincagem e Folhas Metálicas. O projeto foi desenvolvido em fases, onde cada fase contemplava um determinado número de equipamentos, áreas e plantas, com visualização em drill down. Utilizando os conceitos de Data Visualization e Operational Intelligence, foi possível integrar e centralizar as informações de diversas fontes de dados, tais como, PIMS, MES, LIMS, ERP, Supervisórios, PROCOM's e entradas manuais. Padronizar as informações de controle do processo produtivo entre os gestores facilita a identificação de problemas e suas causas, e permite analisar simultaneamente várias áreas e plantas. Exibir em tempo real perdas operacionais em decorrência de desvios de processo, torna o processo de tomada de decisão mais rápido e assertivo, contribuindo para a melhoria da performance dos equipamentos, redução de riscos de falhas, e além disso aumenta a vida útil dos equipamentos e otimiza a monitoração dos processos.

Jul 30, 2018

By Ana Paula Gonçalves Chaves

A pesquisa relativa ao transporte ferroviário no Brasil tem se intensificado nos últimos anos visando principalmente a melhoria no desempenho do par roda-trilho. Isso se deve a demanda de se transportar cada vez mais carga por eixo visando uma redução no custo de transporte. Através de mudanças na microestrutura do material ou de mudanças na composição das ligas utilizadas na fabricação pode se aumentar a resistência do par roda-trilho. Neste trabalho foi analisada a influência de diferentes microestruturas (puramente perlíticas e perlíticas-bainíticas), obtidas através de tratamento térmico por dilatometria, nas propriedades de um aço alto carbono similar ao utilizado em rodas convencionais classe C destinadas a implementação pesada com altas cargas e baixas velocidades. Foram realizados tratamentos isotérmicos em dez temperaturas diferentes para um aço eutetóide. As análises incluíram técnicas metalográficas (definição de fases presentes e distância interlamelar da perlita), ensaios mecânicos de dureza e ensaios magnéticos (saturação magnética e ruído de Barkhausen).

Aug 17, 2017

By Thomas Schanz

Current steel market conditions require small investments only to lower operational cost. SMS Concast has developed new products which optimize continuous casting process cost for long product steel production. This paper describes a selection of three products. All three systems are patented (patent pending for CONDRIVE). CONSAFE, a non-radioactive mould level measurement system for reliable mould level measuring on open stream casting CCM’s; CONSTIR-MWS, an improved control software for electromagnetic stirrers which lowers energy cost by 35%; CONDRIVE, a brand new oscillation drive system which provides the features of a hydraulic oscillator, however with a cost efficient electric drive.

Aug 17, 2017

By Secretary of the Interior

"INTRODUCTION The Bureau of Mines Synthetic Liquid Fuels Program again forged ahead during 1952, and important technical advances led the way to improved methods of converting coal and oil shale into liquid fuels. Marking the eighth year of activities under this program, the past 12 months brought a new domestic industry nearer realization.The increasing demand for gasoline and oil and the rising cost of finding new petroleum, coupled with America's growing dependence on imports and the unsettled international situation, have continued emphasize the importance of the Bureau's Synthetic Liquid Fuels Program. Oil, the indispensable material of wartime, likewise has critical importance in peacetime, touching as it does the life of every individual. Supplementing petroleum with synthetic liquid fuels will not only conserve this Nation's petroleum reserves but also will bring into greater use its tremendous reserves of coal, as well as the vast deposits of oil shale for which no other practical use has yet been found.The Bureau of Mines Synthetic Liquid Fuels Program is one of the most important and far-reaching of the Government's research projects. Through development, of commercial synthetic liquid fuels, the United States can obtain oil products from its great inland reserves of coal and oil shale to supplement petroleum in any quantity that may be necessary, consistent with economic and other requirements, such as national defense. The use of raw materials from such deposits would be of highest importance in wartime, when shipping lanes are menaced by the enemy. The Synthetic Liquid Fuels Program of the Bureau of Mines and research efforts of industry have advanced American technology to the point where it is now possible to begin the design and construction of prototype plants. Certainly, significant improvements will be made as the program continues, but this prospect in no way alters the fact that the start of prototype plants should be encouraged. These plants, as the first step in the development of a synthetic fuels industry, would serve a threefold purpose:"

Jan 1, 1953