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By L. J. Kane

While analyzing synthesis gas produced from coal, the Bureau of Mines found that conventional procedures for naphthalene determination were difficult and time consuming. The Bureau developed a rapid and sensitive turbidimetric procedure, which requires only simple instruments and hence can be used in plant-control laboratories. The gas is passed through a saturated aqueous solution of picric acid at 3° to 4° C. whose turbidity is then measured at room temperature. A dispersing agent is added to prevent coagulation of the suspension on warming. Only about 1 mg. (0.015 grain) of naphthalene need be absorbed, and precision and sensitivity are a few ten-thousandths of a grain, or a few hundredths of a grain per 100 cubic feet. The determination can be completed less than 10 minutes after absorption. INTRODUCTION One of the functions of the Branch of Coal Gasification, Bureau of Mines, Morgantown, W. Va., is to develop economical methods for manufacturing, from coal, a mixture of hydrogen and carbon monoxide for producing hydrogen, methane, and other gaseous fuels. This raw gas may contain many impurities, including naphthalene. This impurity is usually determined by first forming naphthalene picrate in a water solution of picric acid, separating the picrate, and titrating the unreacted picric acid or the picrate itself.

Jan 1, 1957

By M. J. Beus

The U.S. Bureau of Mines is conducting investigations to improve design methods for mining volcano-genic massive-sulfide (VMS) type deposits in environmentally sensitive regions. This study was conducted at the Greens Creek Mine, which is typical of many VMS-type deposits throughout southeast Alaska, and served as a case history for computer modeling and structural analysis. Results indicated that the finite-element design method provided reasonable comparisons with both the anticipated regional stress regime and the measured deformational response of the underground accessways. Investigators concluded that reasonable accuracy can be expected for stability analyses of proposed mine design scenarios at this mine using the results of this preliminary study.

Jan 1, 2010

By Fred G. Hewett

The Cassiar orebody is located in a sill-like serpentinite body intrusive into the Devonian-Mississippian sedimentary rocks of northern British Columbia. Subsequent intrusion of the Cassiar batholith formed the McDame synclinorium and produced chrysotile asbestos. Present information indicates an orebody of approximately 16,277,000 tons amenable to open-pit mining, but continued diamond drilling will be needed to accurately define total tonnage and grade. A program has been developed at the mine to provide the required information on a daily basis, and work is continuing on more effective dollar-value prediction methods.

Jan 1, 1978

By Marcelle A. Hauseux

"The Turgeon Lake granite lies 5 miles north of Baie Johan Beetz, Quebec, at the eastern margin of the Grenville Province. The rocks are classed as granites, granulites, quartzites, biotite schists and gneisses, and amphibolites. The granite's uraniferous character is manifested by phosphuranylite, uraninite, and metamict .zircons associated with magnetite. Field anomalies occur in irregular pods, conformable with the tectonic foliation, in bands roughly paralleling sedimentary bedding. Associated features diagnostic of uraniferous granite are smoky quartz, brick-red feldspar, magnetite and a coarse to pegmatitic grain size. The granite is chemically and physically heterogeneous. Metasediment-granite contacts are diffuse or sharp, and usually conformable to bedding. The regional foliations within all rock types are coherent, and sedimentary structures are often preserved within both metasediments and granite. Autometasomatism probably was a strong granitization agent.A uranium reconcentration into fold-axial zones from original sediments which have been highly granitized during at least two phases of folding is suggested from the available data."

Jan 1, 1977

By John P. Powell

A comprehensive study of the effects of hydraulically fracturing water-flood wells in Oklahoma has been made by the Federal Bureau of Mines. This report presents results of that study and an analysis of some of the factors governing the results of fracture treatment on waterflood properties. Originally, hydraulic fracturing was used to stimulate oil production from old wells producing by primary methods, and its application to water-flooding was regarded with skepticism by most producers. However, since 1953 the number of fracture treatments of both oil and input wells in waterfloods has increased steadily. Hydraulic-fracture treatments in waterfloods have generally been successful in stimulating production from oil wells and increasing the rate of injection into input wells. Hydraulic fracturing has enabled several producers to turn probable failures into economically successful projects.

Jan 1, 1961

By M. Misra

Improved liberation and flotation of kerogen from eastern oil shale were accomplished with high-temperature grinding and a1 so with the addition of fuel oil during the grinding stage. Liberation measurements indicated that possible coalescence and aggregation phenomenon of kerogen particles during grinding may reflect this behavior. Additionally, ultrasonic treatment of the rougher concentrate prior to cleaning improved the quality of separation.

Jan 1, 1984

By A. Visnapuu

High-grade synthetic rutile has been produced in the laboratory from domestic ilmenite concentrates by a new carbonyl process. The ilmenite was first reduced to convert the iron oxides to metal and then treated at temper-atures over 1000 C in high-pressure carbon monoxide (CO) to convert the iron to the pentacarbonyl. Rapid carbonylation was achieved in the presence of small quantities of selected promoters. Maximum iron removal occurred at temperatures between 110° and 130° C at CO pressures from 1,000 to 1,400 psig. Iron pentacarbonyl appeared as liquid and vapor in the reactor and could be removed by gravity flow and vapor transport. More than 90 pct of the iron was extracted in 2-hr experiments at pressures of 1,000 psig and above. The Ti02 product is porous owing to the removal of the iron, has the rutile crystal structure, and is suitable for chlorination. Waste disposal problems associated with the process would be minimal because the iron pentacarbonyl can be decomposed to produce iron powder or pellets for sale and CO for recycling.

Jan 1, 1973

By Muhammet Mustafa Kahraman

Despite technological advancements and organizational adjustments, lost time accidents are major issues in occupational safety. However, there is very limited work that focuses on variables influencing days lost as a result of occupational accidents. In this study, decision tree and artificial neural network methods were used as machine learning techniques to investigate the impact of factors on accident lost day duration. Degree of injury, worker age, and worker activity were found to be the top three variables impacting loss of time from work. It was also identified that the mining method, location, and nature of injury had a moderate influence on duration lost due to occupational accidents. However, worker experience and ore type did not have any significant impact on the duration, which is an unexpected result. These results confirmed that some accident factors that might have a large influence on the number of mine accidents can be less critical when it comes to accident lost day duration.

Feb 3, 2021

By R. Mattos, E. Calcina, G. Quispe, S. S. Kanchibotla

During blasting, rock breaks and moves but standard grade control practices do not adjust ore waste boundaries to cater for blast movement. Rock movement resulting from blasts can result in mischaracterization of grade boundaries resulting in ore loss and dilution. Ore loss takes place when ore is mischaracterized as waste and sent to waste dumps, and dilution occurs when waste is mischaracterized as ore and sent for processing. Las Bambas operations of MMG Peru, realized the economic impact of blast movement on ore loss and dilution and adjust ore boundaries using limited blast movement measurements. This is a step in the right direction but has limitations for everyday application. This paper discusses the advantages of disadvantages of current blast monitoring techniques and introduces an operational tool to estimate polygon movements for different blast designs and confinement conditions. Blast movement estimates from this new tool have been compared against the estimates from the current tools for several production blasts and the results were quite promising.

Mar 2, 2022

By Donald L. Katz

FIFTEEN years ago Dr. Manning published a paper in "Petroleum Development and Technology" on '.Fundamental Research Relating to Petroleum." He tabulated for several industries "the proportion of their present success which can be fairly attributed to the application of information and processes obtained by scientific research," giving petroleum a score of 7 compared to 100 for the electrical and coal-tar industries. Today the petroleum industry as a whole and the producing groups both have raised their score beyond the majority and are climbing toward the top. Present practices are being developed both by fundamental research and the application of the research method in field operation.

Jan 1, 1941

By R. R. Wells

As a part of the strategic mineral program, examining engineers of the Bureau of Mines collected samples several manganese properties in Colorado. As all of the ores were too low-grade to be acceptable to manufacturers of ferromanganese, beneficiation studies were required .to determine the amenability of the ores to concentration. Manganese in the form of impregnations in sedimentary beds is found in the Denver plains area a few miles east of the Rocky Mountain front. Deposits are reported to occur intermittently over a distance of more than 200 miles. The manganese oxides occur in beds of conglomerate or arkosic sand, generally accompanied by limonite. The Manganese and iron oxides,, however, usually are found in separate layers. Three samples were submitted for beneficiation tests, two samples from Buckley Field bombing Yang, Arapahoe County, and one from near Franktown, Douglas County.

Jan 1, 1952

By T. T. Read, T. L. Joseph, F. H. Royster

In a preliminary study of the beneficiation of iron ores conducted by the Bureau of Mines, one of the authors (T. T. Read) found it necessary to ascertain, if possible, how much effect a decrease in the silica content of an iron ore has upon the cost of making pig iron from the ore. In the beneficiation of iron ores the most important impurity to be removed is usually silica, and the amount that can be expended on a beneficiation process to reduce the silica content of the ore is obviously determined by the amount of increase in the value of the ore after beneficiation. The price that can actually be obtained for a beneficiated ore is, of course, a matter of negotiation between the seller and the buyer, but since the relative value of different grades of iron ore must be chiefly based upon the cost of making pig iron from them, an approximation as to the effect which decrease in the silica content of ore has upon the cost of snaking pig iron is an important guide in estimating what probable average gain will result from subjecting an ore to a beneficiation process. A search of the literature failed to reveal any detailed statement on this important topic, but fortunately the data are at hand to permit making an approximate calculation of the probable effect. For the purpose of the calculation assume three iron ores with the following composition (natural):

Jan 1, 1924

By G. W. Jones

Explosion hazards that may exist when air becomes polluted with combustible gases and vapors are extremely dangerous, particularly if the volume of gaseous atmosphere is large, and an explosion under such circumstances could do tremendous damage to persons and property. The hazard is even greater if explosive mixtures are confined under high pressure, as the pressure could increase to tremendous proportions just before the container would rupture. Because of its interest in safety in the mining and allied industries, the Federal Bureau of Mines has investigated the flammability (explosibility) of various types of combustible atmospheres and published its findings. The explosibility of natural gas has been studied, and the limits of flammability have been determined and published. Other investigations have shown how explosions of natural gas-air mixtures may be prevented by the addition of nitrogen and carbon dioxide.

Jan 1, 1949

By G. L. Gates

The Bureau of Mines in cooperation with the City of Long Beach) Calif.) studied some physical factors effecting the deposition of barium sulfate scale in oil-well rotary pumps. Freshly formed barium sulfate was obtained by combining sulfate in sea water with barium from a barium chloride solution. The rate of scale deposition was measured quantitatively by weighing the pump impellers and diffusers. The results of the tests showed that coating the impellers with plastic significantly reduced the rate of barium sulfate deposition.

Jan 1, 1967

By A G. Dempster, B McKeown, S Saydam, J Coulton

The mining industry has undergone a profound and transformative shift in recent years, driven by the rapid advancement of emerging technologies such as automation, digitalisation, and electrification. These technological innovations have not only revolutionised operational efficiency and productivity but have also introduced an imperative need for new and innovative approaches to conducting mining activities. Specifically, the mines of the future face a new series of complex challenges when planning and developing greenfield or brownfield mining projects in the 21st century. These challenges include greater operational depths, higher seismicity levels, higher rock temperatures, increased environmental constraints and sustainability requirements, a higher degree of interoperability, lack of skilled workforce, and the need for sustainable and eco-friendly mining practices. Consequently, there is an essential need to formulate novel strategies and robust planning methodologies that re-evaluate how mines are planned, executed, and managed, from the early exploration stages to the post-mining era and the consequent uses of mine sites. This research focuses on identifying the factors influencing the implementation of modern technologies, such as autonomous machinery in mining operations, and their impact on mining method selection and longterm mine planning. The findings underscore a crucial need for a paradigm shift in how mines are planned and developed, going beyond mining method selection, which primarily focuses on geological and economic factors, and must evolve to incorporate the multifaceted implications of modern mining operations.

Sep 1, 2024

By Hebbard GJ

Vertical crater retreat mining is being used at Zinc Corporation, Limited and New Broken Hill Consolidated, Limited for pillar recovery between previously mined and filled stopes. In order to increase productivity in the older lead lode areas of the mine, particularly in the lower grade sections around the keel of the orebody, score form of longhole stoping was considered necessary.Due to poor ground conditions in the country rock surrounding the ore and the requirement to provide sane wall support during mining, primary VCR mining has been utilised in these areas.At Zinc Corporation, several stopes have thus far been mined by a hybrid longhole stripping - VCR method.

Jan 1, 1985

By Leland E. Paulson

The Grand Forks Energy Research Center and Commonwealth Edison of Chicago jointly conducted tests in which 400 tons each of subbituminous coal and lignite were dried in a commercial scale dryer, oil sprayed and cooled, then shipped in open-top rail cars from Pekin, IL to Grand Forks, ND and stockpiled. Cars containing raw coal and dried coal that had not been oil sprayed were also transported for comparative purposes. The tests were conducted in August and November of 1974. The subbituminous coal was dried from 26 to 16 pct moisture and the heating value was upgraded from 8,420 to 9,650 Btu/lb. The lignite was dried from 39 to 22 pct moisture and its heating value was increased from 6,420 to 8,300 Btu/lb. Before loading subbituminous coal was cooled to 115° F and sprayed with oil at a rate of from 2 to 6 gal/ton. Similarly, lignite was cooled to 85° F and oil sprayed at rates of from 1 to 2 gal/ton. Both shipments arrived in Grand Forks with a minimum of difficulty. The subbituminous coal was subjected to 2 inches of rain during transit with no change in average moisture content. The cars containing dried and oil treated coal had less material lost to wind than either cars containing raw or untreated dried coal. With both dried lignite and subbitnminous shipments, a moderate increase in temperature was measured during transit. With the subbituminous shipments, ignition occurred near poorly fitted bottom dump doors, but was limited to a very small area. The dried lignite was shipped when ambient temperatures were below freezing, and frozen coal was noted around the edge of the car. At Grand Forks, the coal was stockpiled using proven techniques and has remained stable to this date.

Jan 1, 1975

By E. H. Denny

In discussing safety in Colorado metal mines there are two important points for metal -mining men to consider , namely , the direct and indirect cost of accidents and the possibility and means of preventing accidents . For statistics on Colorado metal - mine accidents , reference has been made to published reports of the United States Bureau of Mines on metal- mine accidents from 1919 to 1927. This period was considered because only with the year 1919 are complete figures on nonfatal accidents available and because these years represent postwar activities ; 1927 is the last year for which the U. S. Bureau of Mines has published accident statistics . During the nine -year period 1919 to 1927 , inclusive , 153 metal miners were killed by mine accidents in Colorado and 5,035 miners suffered lost - time injuries . The accidentfrequency rate of number killed per 1,000 300- day workers for this nine - year period was 4.68 as compared with the general average of 3.26 for all the metal mines of the United States for the same period . In other words , the fatality rate in the metal mines of Colorado for this nine- year period averaged 40 per cent higher than that of the metal- mining industry in the United States generally . In 1924 and 1926 the Colorado metal mines had a better accident record than the average of those of the United States , but 1927 was a bad accident year and the State Bureau of Mines figures for 1928 and 1929 showing respectively 18 and 23 men killed in and about the metal mines indicate a continuing relatively high death rate from accident . The cost of accidents to the miner for the period 1919 to 1927 can be estimated from the accident figures just given . The United States Bureau of Mines as well as other authorities assess 6,000 days lost time for every fatality and every permanent total disability . These authorities have also agreed that a permanent partial disability costs 800 days lost time to the worker over his working lifetime , that lost time injuries of less than 14 days average about 6 days lost time and lost time injuries not involving permanent disability but having loss of more than 14 days average 32 days lost time . On this basis the Colorado metal miners have suffered in nine years a gross loss of 1,214,146 days , or , at $5 per day , $6,070,730 . The miner receives about one -ninth of this amount in compensation so that the net loss to the metal miner in Colorado for this nine - year period was about $5,400,000 .

May 1, 1930

By G. Mark Aylmore

Various processes have been developed using a combination of elevated temperature and chemical treatment processing to recover Li from silicate minerals. To facilitate further process development, a comprehensive understanding of the deportment of Li and associated minerals in ore bodies is essential to allow the industry to predict the response of ore reserves to metallurgical treatment options. This paper describes results from the integrated use of the John de Laeter Centre’s state of the art analytical and mass spectrometry techniques to characterise a selection of Li bearing ore bodies and determine their amenability to potential processing options for the extraction of Li. The mineralogy, mineral associations, and liberation characteristics of ore-bearing and gangue minerals were characterised using a combination of the TIMA and XRPD studies. The Li content and distribution within minerals were defined using LA-ICPMS and field emission scanning electron microscopy techniques (EBSD, ToF-SIMS) and atomic probe microscopy.

By W. E. Wallace, V. Castranova, F. Saus, D. Bates, C. A. Hill, V. Vallyathan, M. J. Keane

"Two in vitro systems are being developed to model initial stages in the interaction of respired dusts with the acinar region of the lung. Incubation of quartz and kaolin with dipalmitoyl glycerophosphorylcholine, a major component of pulmonary surfactant, suppresses the prompt C)1otoxicity of both dusts as measured by in vitro enzyme release from pulmonary macrophages or assay by erythrocyte hemolysis. Additional data is presented to quantitate the detoxification of quartz and kaolin by dipalmitoyl lecithin. Subsequent incubation of lecithin treated dusts with phospholipase enzymes results in partial to complete restoration of the assayed cytotoxic potentials, dependent on the lipase activity applied, the incubation time, and the mineral. Restored cytotoxic potential is due to removal of the prophylactic lecithin surface coating and/or due to residual lysolecithin which is produced by the partial enzymatic digestion of lecithin. Data is presented on the contribution of each mechanism to the restored toxicity. Again, this is dependent on the mineral used, the lipase activity applied, and digestion time. Additionally, a system is under development to challenge pulmonary macrophages in culture with native and surfactant treated dusts. A preliminary test of the dipalmitoyl lecithin - quartz rabbit pulmonary macrophage system is presented to illustrate the method.IntroductionRespirable quartz dust exposure is known to cause librotic lung disease; respirable clay dust exposure is less likely to do so as indicated by epidemiologic data on occupational exposures and by animal model studiesP·7) The hypothesis that damage to pulmonary macrophages in the acinar region of the lung by respired dusts is an early event in the disease process requires consideration because kaolin clay and quartz dusts are comparably cytotoxic to pulmonary macrophages in vitro.(3•9)"

Mar 1, 1989