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By Francis R. Redfern

Newton's method of solving a nonlinear equation is employed to develop a least-squares acoustic emission source location method in which the spatial residuals of the location equations are minimized. These residuals, related to the distances from the least-squares source location perpendicular to the surfaces described by the location equations, permit location error to be estimated to first order along the spatial axes. The solutions obtained by this method are the best spatial solutions to the location equations in the least-squares sense. Also presented is a procedure by which the geometrical control of a transducer array can be evaluated using the rate of change of source location with fractional velocity change.

Jan 1, 1982

By W. E. Robinson

Sixty samples, selected from a 2,300-foot core of the Green River Formation in Colorado, were studied to ascertain differences in the structure of the organic material present in the oil shale samples. Emphasis was placed upon relating differences in the aromatic content of the insoluble kerogen and the alkane content of the extractable material obtained from the selected samples. The methods used in determining these differences consisted of fractionation of the soluble material, carbon and hydrogen analysis, volatile material determination, carbon residue determination, oxidation rate determination, and infrared analysis. In general, it was concluded that the organic material in this core does vary in chemical structure and that same of these variations resulted from factors related to depth of burial. Other observed changes in structure of the organic material were not depth-dependent and resulted from other factors such as source material variations, biological alterations, or ecological differences.

Jan 1, 1971

By G. M. Molinda, J. P. Ulery

Since 1970, abnormally high methane emissions have been observed in eastern sections of the Federal No. 2 Mine operating in the Pittsburgh Coalbed in northern West Virginia. The nature and volume of these emissions indicate a source other than the coalbed. An investigation was undertaken to delineate probable methane sources. Gas well information and stratigraphic correlation of corehole data indicates that a sandstone directly above the main coalbed is an additional source of methane emissions. The sandstone body appears to be an ancient stream channel, infilled with fine-grained sand and organic matter. Coalification of the organic matter produced methane as a byproduct. Additional methane presumably migrated into the sandstone unit from the subjacent coalbeds. The methane became trapped in the porous clasticunit by the surrounding impermeable strata. Mine development near this unit creates a significant pressure gradient, triggering abnormal methane emissions into the mine along naturally occurring fractures. Pre-development methane drainage of the sandstone could be accomplished by completing vertical boreholes along its trend.

Jan 1, 1984

By R. L. Montgomery

Heats of solution of cerium metal and cerium (III) chloride in hydrochloric acid were measured. The standard heat of formation of the aqueous cerium (III) ion at 25° C is -166.1 ± 0.3 kcal/mole. Heats of solution of cerium (III) chloride in hydrochloric acid are consistent with the existence of a complex CeC1++ having a stability constant of 1 and a heat of complexing of 5.4 kcal/mole.

Jan 1, 1962

By H. A. Doerner

Tellurium is a silver white solid with metallic luster, the e17atal.line torm being ver., brittle aud e.g,s!ly powdered. It has a specific gravity of 6,27, melta at 45a0c. and boils at red het, giving off a. golden 1ellow vapor when air 11 excludei. When heated in air, telluri'UiD burns with a bl\te name tinged with green, and evolves wh1 te vapors ot tellurium dioxide. An amorphous form of tel­lurium, obtained by red.uction and precipi ta.tion from so).ution, haa II specific gr1.vity ot 6,015, and when heated ia cho.nged to the cry:.,talline variety. Telluri,a 11 insoluble in water, c&rbon diaiJ.phido, or h;rd.rochl oric acids, but it 11 41a-1olved bJ nitric or concen t1·ated. sulphi.U·ic acid. It 1..oea not tamiah in moiet ah•• 11 ree11tant to alkaline solutions, e,;:ctpt concentrated KOB, but it 11 cliaaolvecl by tuaed. &lkl 1••. I ts 11.to!!lic weight h..'l.a been the "J.Ubject ot mch controverq, bu\ t.he value 137 .5 :.a bl!ten generally accepted, Tho chflmietr:, of tellurium ia eim1lar to that ot IUlphur. It tonne throo xid.ee TeO, To02, and Te0 , al10 tellur14ea, t•llurite,, and. tellur1.t11, A number of halide compoWld.1, a 3iulph1de, and. a .ulpbat.e are known.

Aug 1, 1922

By R. V. Ramani, R. Stefanko, G. W. Luxbacher

TEST DECK – ALTMETER SURVEY WITHOUT PLTTMETER TEMPERATURE CCRRECTION DATA INPUT

Jan 1, 1977

By R. E. Mussler

Electrowinning of copper from chloride solutions in a diaphragm cell was studied by the Bureau of Mines. The copper powder product was shaken periodically from the cathode and removed from the bottom of the cell. The effects of copper concentration, brine concentration, copper chloride species, and cell voltage were investigated. Power consumption of 1.1 and 2.1 kW-hr/kg were obtained with cuprous and cupric chloride solutions, respectively.

Jan 1, 1975

By D. S. Kingery

The practice of using doors to control main ventilating currents in bituminous-coal mines is common throughout the industry. When doors are erected in pairs to form air locks, they are usually accepted as satisfactory by both State and Federal coal-mine-inspection agencies. A review of the contributing factors in recent methane ignitions showed that interrupted ventilation (often caused by doors latched open, destroyed, or damaged) was the principal cause of methane accumulations that subsequently were ignited.

Jan 1, 1958

By Donald I. Kurth

This Bureau of Mines report describes the development and application of a computer model of aquifer hydrology associated with in situ leaching of uranium. The model provides uranium resource developers with a simulation of leachant flow characteristics in a preproduction or pilot five-spot leaching operation. Various types of aquifers are modeled using closed form solutions of the partial differential equations describing the change in fluid head (pressure) as the leaching operation is carried out. User-supplied descriptive input consists of aquifer, well, and leachant flow characteristics. Numeric and graphic outputs such as isopressure, iso-velocity, and isotime contours are available. A typical application is shown.

Jan 1, 1978

By David A. Benjamin

In 1989 and 1990, the Bureau of Mines conducted a mineral resource investigation of the 122,000-acre Trinities study area, located in the Trinity Mountains of south-central Idaho. No identified mineral resources were delineated during this study. There are 58 lode mining claims within the area. Five localities contained elevated metal concentrations which may indicate precious metal mineralization at four localities and molybdenum-precious metal mineralization at another. Four of the five localities appear to form a northwest trend through the center of the study area. Twenty-eight individual sites contain anomalous concentrations of gold, silver, bismuth, molybdenum, and beryllium.

Jan 1, 1991

By M. J. Ackerman, C. R. Waine, W. M. Merritts, L. P. Mokwa

Tests were conducted in the Pocahontas No. 4 coalbed in southern West Virginia to determine if successful degasification techniques, developed during an earlier study in the Pittsburgh coalbed, would be effective in removing methane from those usually more gaseous coals. Specially designed long-hole drilling equipment and Bureau of Mines continuous recording devices were used to measure the quantity and methane content of the ventilating air during the investigation. Infusions were made with water at normal waterline pressures ranging from 200 to 220 psi or at pump pressures ranging from 400 to 650 psi. Results of the tests showed that methane emissions from free-flow bleeder holes were as much as 131 cfm. Infusions of some of the holes increased the methane emission from other holes and from the exposed coal surfaces near the working areas as much as 1,540 cfm. The methane content in the main return-air currents after infusion was reduced more than 86 percent of the amount recorded before tests were made.

Jan 1, 1963

By H. E. Powell

The selective recovery of nickel and zinc from a waste phosphate solution by solvent extraction was investigated by the Bureau of Mines as part of a broad program to recover valuable metals and compounds from industrial wastes, and to reduce the associated land and water pollution caused by dumping these wastes. The waste, which resulted from the phosphation of automboile bodies, yielded 99 percent of both the nickel and the zinc by extraction with dinonyl naphthalene sulfonic acid (DNSA) and di-2-ethylhexyl phosphoric acid (EHPA), respectively. Dilute sulfuric acid was used to recover the metals and regenerate the solvents.

Jan 1, 1970

Synthetic dawsonite [NaAl(OH)2C03] has been prepared with crystallinity similar to that of dawsonite found in oil shale deposits of the Piceance Creek area of Colorado. Optimum experimental conditions were as follows: Na/Al atomic ratio, 43; temperature, 175° to 200° C; pCO2, 15 psig; and reaction time 5 hr. Chemical and spectrographic analysis revealed that the synthetic dawsonite was of high purity and Has essentially stoichwmetric. Similarity of the synthetic to natural dawsonite, demonstrated by X-ray diffraction, infrared spectrophotometry, and electron microscopy, suggests its suitability as a standard.

Jan 1, 1972

By Daryl E. Radcliffe

Ninety-seven roof bolts were instrumented with strain gages and resin-grouted in three areas of the Bear coal mine, Somerset, Colo., by the Bureau of Mines. Measurements taken with these instruments indicate roof support is achieved through a combination of point suspension and resistance to vertical and horizontal stresses caused by localized shearing in the roof. The localized shearing results in bending of the bolts, yielding due to high vertical stresses, and the transfer of high loads to the bolt head or plate.

Jan 1, 1980

By Arnold M. Lansche

Domestic Production.-Domestic production of white arsenic, AS,03, was derived entirely as a byproduct of smelting arsenic-containing copper ores by The Anaconda Company at Anaconda, Mont., and American Smelting and Refining Company at Tacoma, Wash. The Anaconda Company discontinued production of white arsenic in 1965. Arsenic metal was not produced. Consumption and Uses.-Most of the white arsenic produced in 1965 was consumed in manufacturing lead and calcium arsenate insecticides.

Jan 1, 1966

By Manuel Gomez

The purpose of this study was to evaluate the feasibility of using statistical response surface regression analysis to predict the sulfur and ash distributions and the washability characteristics of coal along a seam in advance of mining. Prediction equations were developed with experimental data from channel, bench, and core samples from the Pittsburgh coal seam in Greene County, Pa. It was not possible, with the available experimental data, to construct mathematical models to predict ash and sulfur concentrations between sample points. In the authors' opinion, however, the good agreement between experimentally determined and predicted values at given sample points demonstrates the usefulness of the method. More input data, such as geologic information, seam characteristics (rock-to-coal ratio), petrographic analysis, and chemical data, would perhaps make it possible to predict sulfur and ash concentrations and washability characteristics between sample points.

Jan 1, 1970

By J. D. Sargent

Selenium might be described as a paradoxical element, being a metal or a nonmetal, a conductor or nonconductor, amorphous or crystalline, colorant or decolorant, and a hydrogenator or dehydrogenator. Selenium was discovered in 1817 by the Swedish chemist, Berzelius, while studying flue dust from the lead chambers of the sulfuric acid works at Gripsholm, Sweden.

Jan 1, 1954