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By D. R. Tesarik, R. W. McKibbin

Material properties affecting slope stability were measured in a large 50-year-old, partially consolidated rockdump located in an active open-pit mine. Field tests included single-ring infiltration and density. In addition, a nuclear depth-moisture gauge was used to measure water content in six stainless-steel-cased drill holes on the crest and an upper bench of the rock dump. Precipitation, evaporation, wind speed and direction, and temperature data were collected at a weather station installed on the dump’s crest. Laboratory tests included particle-size distribution, specific gravity, Atterberg limits, and water content. By measuring material properties of a rock dump presumed to be stable, the safety of miners working on or at the toe of old rock dumps constructed of similar material and located in a similar climate can be assessed.

Jan 1, 1999

By d&apos, Kathleen J. Amico

THIS SUMMARY is shown in volumes I and III of this series on mineral production in the United States (including Alaska and Hawaii), its island possessions, the Canal Zone, and the Commonwealth of Puerto Rico, and on the principal minerals imported into and exported from the United States. For further details on production, see the several commodity and area chapters. A summary table comparing world and U.S. mineral production also is included. [ ]

Jan 1, 1960

By Larry P. Jackson

As part of the current research effort in shale-oil chemistry conducted by the Federal Bureau of Mines, reduced chlorophyllins were prepared and pyrolyzed in an effort to identify the role of plant pigments and their decomposition products in the nitrogenous compounds found in the product of oil-shale pyrolysis. The properties of the chlorophyllin pyrolysates were related to the composition of the reduced chlorophyllins with particular emphasis on the amount and types of nitrogen compounds formed. A comparison based on the types of nitrogen compounds present was made betvJeen shale oil and the chlorophyll in pyrolsates. In order to make this comparison, a sample of shale-oil light distillate was separated into polar and nonpolar fractions, and a careful examination of the polar fraction was conducted to obtain an accurate picture of the types of nitrogen compounds present. The information gathered from these studies was used to evaluate reduced chlorophyllin as a model of oil-shale kerogen insofar as the production of nitrogen compounds was concerned. The results indicate that the reduced chlorophyllin does yield nitrogen products which are directly related to the nitrogenous compounds in shale oil, and it therefore represents a good model of shale-oil kerogen.

Jan 1, 1975

By V. R. Miller

The Bureau of Mines has developed a technique to separate and recover the three major components, Pb, Zn, and Cd, from lead smelter flue dust. This research was conducted as part of the Bureau's effort to reduce environmental conflicts and occupational hazards associated with mineral-processing operations and to recover valuable constituents in emissions and effluents. The laboratory process utilizes sulfation roasting of the flue dust followed by water leaching to extract over 95 pct of the cadmium and zinc. Ninety-nine percent of the cadmium was recovered from solution by cementing with zinc dust, and zinc was electrowon from the resulting solution after purification. Zinc electrolysis was carried out in a 1-liter cell at 35° C with a cathode-current density of 8 A/dm2 in a solution containing 65 g/l Zn++ and 180 g/l H2S04, Current efficiencies of 80 pct were obtained. The leached residue consisted largely of PbS04, which was converted to PbC03 and leached with H2SiF6 to produce PbSiF6 electrolyte. Ninety-five percent of the lead contained in the residue was converted to electrolyte. Lead was electrowon from solutions containing 70 gil Pb++ and 90 g/l H2SiF6 using a lead cathode, Pb02-coated titanium anodes at 28° C, and a current density of 1.6 A/dm2. Current efficiencies approaching 92 pct were obtained. Accessory minerals such as cobalt and nickel were separated into purification residues and liquor.

Jan 1, 1982

By H. B. Cooke

In connection with its researches on the crude petroleums of the United States, the Bureau of Mines has made a particular study of apparatus for the distillation of hydrocarbon mixtures. While this study is still incomplete it has already resulted in the development of considerable laboratory and semi-plant equipment, motet of which has been described in various publications of the Bureau. The laboratory apparatus (Hempel distillation) and method gives satisfactory comparative results in the laboratory examination of crudes and have been found applicable to crudes of all types, but the agreement of laboratory and plant distillations is not as close as might be desired. This is due, in part, to limitations in size and construction of the laboratory apparatus. Some refiners claim that the Bureau of Mines' laboratory method (Hempel distillation3) for distilling crude petroleum, does not show the full gasoline content of the oil, while others have stated that it indicates more gasoline than can be obtained from the crude commercially. This difference of opinion among refiners results largely from the great variation in stills used and methods of operating them. The Bureau's experience has shown that crude oils from different fields vary widely in character; in fact, that it is not yet possible to classify crude's adequately on the basis of their Down chemical and physical characteristics. As a result of the differences that exist among crudes, and of the difficulty of designing refinery equipment, no standard practice has yet been adopted for the commercial distillation of petroleum, and ma" types of stills are used in the refineries of this country. Although many factors enter into the design of equipment and the development of commercial practice in refining of crude oil, there

Jan 1, 1924

By Jamie Girard Dwyer, Edward McHugh, Stanley Miller, Jeffrey Whyatt

This user's guide covers the operation of a suite of three computer programs-Bplane, Bstepp, and Bwedge. These programs can be used to evaluate the potential for plane shear, step-path, and wedge failures along the crest of a slope bench. Such failures reduce the width of a catch bench and may compromise the bench's ability to catch rolling or sliding material before it reaches miners working below. The Bplane and Bwedge programs address sliding of blocks defined by continuous planar joints. The Bstepp program examines sliding of blocks defined by more complex failure surfaces that include steeply dipping cross joints and may even include breaks across small bridges of intact rock. The programs are applicable to jointed rock masses where the joints are small relative to the overall slope and form a number of sets with uniform statistical characteristics within a slope sector. The theoretical basis, application, and operation of these programs are described.

Jan 3, 2007

To reduce accidents associated with transporting, installing or maintaining mine conveyor belts by providing easy-to-use tools for use in specific tasks. Approach The Bureau of Mines, through a re-search contract, developed three devices for use on conveyor belt systems 1) for use in moving and positioning conveyor components. 2) to reduce spillage and clean-up around conveyors, and 3) to lessen the maintenance of the belt system. The Saucer Skid Moving conveyor components using runner nose 1-beam skids is a simple task when the direction of travel parallels the beams. However, when the unit is moved sideways or around corners for final positioning, the web of the beam scrapes the floor with a bulldozing effect. Many strain and sprain injuries hap-pen when mine workers drag the skids into position at this paint. To minimize such injuries, the Bureau of Mines developed a saucer skid five feet in diameter with rounded sides and a flat bottom. Its design incorporates eight reinforced ribs with holes so the component may be secured to the skid, and eight exterior eyelets to which towing chains may be attached. The skid can be easily moved in any direction because its rounded sides slide over the mine floor rather than drag across it.

Jan 1, 1984

By T. T. Campbell

This report describes the development of new electroplating baths from which tin-nickel alloy plate was deposited. Although tin-nickel plate can be deposited from an aqueous ammonium bifluoride bath, the corrosive nature of this bath has served as a deterrent to its use. The Bureau of Mines felt that more general acceptance of this new alloy plate would follow if neutral or alkaline baths could be developed. Promising results were obtained from electrolytes containing both tin and nickel chlorides dissolved in triethanolamine-hydrochloric acid or in ethylene glycol hydrochloric acid baths. Current efficiencies close to 100 percent were obtained with these baths. Research revealed that tin-nickel plate could be produced from organic solvents or from mixed aqueous-organic electrolytes. The composition of the alloy deposit - 65 percent tin and 35 percent nickel - was found to exhibit the same single-phase structure that is obtained from the commercially accepted fluoride-type bath.

Jan 1, 1959

By E. Morrice

Gadolinium, dysprosium, and yttrium are difficult to electrowin as high-purity liquid metals because of their high melting points (>1,300° C). Samarium metal is difficult to prepare directly by electrolysis because the metal reacts with the electrolyte. In this Bureau of Mines study, the rare-earth metal was electrodeposited on a solid manganese, chromium, or iron cathode to form a low-melting alloy. The alloy was then vacuum distilled to separate the rare-earth metal from the ferrous metal. A typical samarium metal product, obtained as the distillate from vacuum distillation of a samarium-iron alloy, contained 150 ppm oxygen, 80 ppm carbon, and 50 ppm iron as impurities, Gadolinium metal, obtained as a residue from the distillation of a gadolinium-chromium alloy, contained 300 ppm oxygen, 200 ppm carbon, and 100 ppm chromium.

Jan 1, 1969

By Ernest R. Rodriguez, Allen D. Look

"INTRODUCTION The underground mine of the Miami Copper Co. has operated since 1927 without a fatality from blasting or the handling of explosives. To improve safety and efficiency, electrical blasting has been used exclusively since 1934. During the period January 1, 1934, to December 31, 1948, inclusive, over 4,000 tons of explosives were used to produce 60,925,071 tons of ore with 896,760 feet of development footage and 2,591,788 square feet of undercut area.The purpose of this paper is to recount the company's precautions to insure safe handling of explosives at this operation, where safety involves careful planning rather than ""trial and error.""GENERAL INFORMATIONThe Miami Copper Co. operates on underground mine in a large, low-grade, Porphyry copper deposit near Miami, Ariz. The deposit contains numerous fractures and planes of weakness, which contribute to ease of working the ore bodies by the block-caving method of mining.An individual stope-caving method is used with stoles 150 feet by 200 to 300 feet and 30- to 50-foot pillars between stapes. After the stope is undercut, the ore is drawn through the draw raises on the grizzly level, and thence through the transfer raises to the ore chutes on the haulage level.Access to the mine is by four active shafts, three of which are primarily for ventilation. No. 5 shaft is used for both hoisting and service. There are four operating levels in the mine. The elevations of the grizzly levels are governed by the contour of the bottom of the ore body and therefore vary in different locations in, the mine.Grizzly levels are on the 850, 900, and 975 levels. The 1,000 level is the haulage level. This mine operates in very low-grade ore and requires economical handling of large tonnages safely and efficiently."

May 1, 1950

By F. E. Brantley

Optimum autoclaving conditions were determined for separation of iron and manganese values from pregnant leach liquor produced in extracting manganese from low-grade umber are. The umber was leached with a synthetic anolyte similar to a recycle solution, used in manganese electrolysis cell operations, that had been renewed with ferrous sulfate and sulfuric acid. The equipment used and results obtained are presented for the several conditions employed. The kinetics of the separation were studied. Rate equations were derived for the formation of solid ammonium-manganese sulfate, (NH4)2 Mn2 (S04)3.

Jan 1, 1968

By Gertrude N. Greenspoon

Legislation and Government Programs.-The Occupational Safety and Health Administration (OSHA) held public hearings in early 1975 on proposed standards for exposure to inorganic arsenic. The findings obtained at the hearings will be considered to promulgate emission standards. Domestic Production.-Arsenic trioxide (As203) was produced domestically only at the Tacoma, Wash. copper smelter of ASARCO Incorporated. Production data cannot be published. Output rose 9% over that of 1974, shipments were less than half those of 1974, and stocks rose 31 %. Production of arsenic metal, begun by ASARCO in August 1974, continued in 1975.

Jan 1, 1977

By A. C. Fieldner

The Bureau of Mires in its investigations of gas masks for use in mines and allied industries has studied and developed various types of masks for protection against noxious uses and furies that may be present in atmospheres encountered in mines, metallurgical works, chemical and other industries. As a result of these investigations, the Bureau issued a schedule5 of tests under which manufacturer who voluntarily submit masks for examination and test, are issued an approval certificate for masks that meet the Bureau's specifications. In the Bureau's schedule, masks arc classified by types of gases removed, as type A masks for protection against acid gases; B; organic vapor; C, ammonia; D, carbon monoxide; E, smoke, dust, and mist; F, special gases; combination types, and type N, for protection in air against all gases, vapors, and smokes. The purpose of this paper is to describe the physical and chemical tests that were conducted on a type N mask, the protective principles and construction of the essential elements of the canister and attachments, and the uses and limitations of this type of mask. The mask tested is known as the all-service mask, manufactured by the Mine Safety Appliances Co., Pittsburgh, Pa;, and was approved (approval No. 1403) by the Bureau on July 1, 1924, for protection from all classes of poisonous vapors, gases and smokes in air.

Jan 1, 1925

By S. W. Lambert

In this Bureau of Mines investigation, production was monitored for 1 year at over 30 coalbed gas-drainage boreholes located in Alabama, Pennsylvania, and West Virginia. Results indicate that the quality of data gathered from such wells can be improved greatly if potential problems are anticipated and prevented in the early stages of well production. Major water-monitoring problems include solids buildup, freezing, the presence of gas in surface waterlines, and improper pumping interval settings. Such problems may be avoided by incorporating in the original well design waterline filters, sand screens, separator tanks, and systems to automatically control pumping intervals. Problems related to measurement of coalbed gas flow include large quantities of water vapor contained in the gas, especially during winter months; freezing and subsequent obstruction of flow; sudden, uncontrolled release of gas pressure; and solids buildup in metering equipment. The installation of commercially available items, such as filters, separators, and insulation, and the thoughtful application of a basic knowledge of coalbed gas reservoir characteristics will prevent most production-monitoring problems.

Jan 1, 1978

By Ivan F. Avery

PRODUCTION of carbon black decreased 4 percent in 1961. Output in the major producing States of Texas and Louisiana decreased 1 percent and 8 percent, respectively. Production of channel black continued downward, declining 10 percent in 1961 compared with 9 percent in 1960. Furnace black production also decreased 3 percent from 1960. Total domestic sales, however, increased 2 percent, Sales to most major consumers increased, but sales to the ink industry decreased 10 percent. Producer's stocks decreased 5,083,000 pounds during the year. Exports decreased 4 percent. SCOPE OF REPORT Carbon black is a very pure grade of quasi-graphitic carbon; particle diameters range from 50 to 5,000 angstrom units. Annual reports were submitted to the Bureau of Mines by operators of all commercial plants in the United States.

Jan 1, 1962

By C. E. Hennig

On January 1, 1960 there were 310 petroleum refineries in the United States, with a crude-oil capacity of 9,901,424 barrels daily, according to the Bureau of Mines' annual survey. Compared with a year ago, this represents a net decrease of three in the number of refineries and an increase of 81,578, barrels per day in crude-oil throughput capacity. Continuing the trend to fewer units with greater individual throughput, the capacity of the average refinery in the United states increased during 1959 from 31,373 barrels per day to 31,740 barrels per day. Compared with the previous year, total crude-oil capacity of refineries on January 1, 1960 was lower in the Appalachian No. 1, Other Rocky Mountain, and Texas Gulf refinery districts. All other districts showed slight increases in capacity. At the beginning of 1960 the industry had under construction facilities that would increase the crude-oil capacity in the United States by 70,947 barrels per day. This was the smallest capacity increase under construction at the beginning of the year since 19460 Included in this construction of additional capacity were two new refineries, one in Michigan and another in Hawaii. In addition, the industry was constructing facilities to replace 50,250 barrels per day of existing crude-oil capacity.

Jan 1, 1960

By T. O. Llewellyn

The Bureau of Mines conducted laboratory batch beneficiation tests on a waste granite sludge from New Hampshire to determine the feasibility of recovering a reusable silicon carbide product. The granite sludge responded to attrition scrubbing, desliming, and flotation in either alkaline or acid circuits using fatty acid as a collector. Recovery of over 80 percent of the contained silicon carbide at grades of up to 96 percent SiC was obtained.

Jan 1, 1975

By T. M. Barczak

Many of the support concepts currently used in the United States originated in South Africa. These products include the Hercules Crib1, Propsetter, MX Prop, Rocprop, and Spider Prop. Another recent development has been the introduction of hydraulic prestressing units, such as the Jackpot system, to various U.S. standing support systems. Several other prop-type supports with similarities to systems used in South Africa are in use in U.S. coal mines. Some exciting new developments that improve the installation and yield performance of props are also underway. In addition to prop-type supports, crib-type supports and single-unit systems such as the Can support are also frequently utilized in longwall tailgates in the U.S. The goal in U.S. support development is to enhance roof support capability while alleviating material handling barriers to reduce injuries associated with support handling and installation. Support products are generally full-scale tested at the National Institute for Occupational Safety and Health (NIOSH) in the unique Mine Roof Simulator load frame. The performance testing protocol is designed to simulate the full range of load conditions that occur in underground mining to identify the performance deficiencies and limitations of the support products. Once the products complete the performance evaluation, they are implemented into the NIOSH Support Technology Optimization Program (STOP). STOP is a window’s based software program that was developed by NIOSH for facilitating the design of standing roof support systems. STOP has become an industry standard to compare the performance capabilities and facilitate the application of these support products into various mining conditions. The purpose of this paper is to provide an overview of the support design and application philosophy in the United States.

By F. J. Smith, W. A. Gallagher, C. A. Herbert

"INTRODUCTION A fire started about 10 a.m., November 10, 1947, at the Kings mine, Princeton Mining Co., Princeton, Ind., about 1,800 feet inby the main shaft bottom on the main west haulage road at a point estimated to be 2 miles from the faces of the main west entries. No lives were lost, as 27 men escaped from the mine after a series of explosions, which necessitated sealing the mine on the surface. This information circular shows"" how adverse conditions might be overcome, when reopening a sealed mine, by expert planning and close cooperation on the part of various organizations. Conditions found in the mine after it was reopened were comparable to the worst that had been anticipated, yet the mine was recovered with comparatively little difficulty and a minimum of risk. The open workings in the mine covered a vast area, but most of the mine resumed production of coal after being sealed for only 37 days.The information contained herein also points to the desirability of adhering as closely as possible to a predetermined schedule of operations."

Feb 1, 1949

By R. Blickensderfer

Test equipment that simulated frictional impacts between coal-cutter bits and mineral inclusions at a coal face during operation of a continuous coal mining machine was used by the Bureau of Mines in the laboratory to study the incendivity of impacts between various rocks, metals, and hard-metal alloys in an explosive mixture of air-7 pct natural gas. Quartzitic sandstone was found to be the most incendive of several rocks tested. Limestone concretions from a coal seam, known locally as "sulfur balls," sparked furiously but were not incendive. Among the metals tested, the type of steel used in commercial coal-cutter tools was the most incendive material tested. A l7-4PH stainless steel was less incendive and appears to be the most promising high-strength steel alloy, reasonably economical, for use in coal-cutter bits. Some hard-metal alloys, primarily titanium and zirconium diboride composites, were also evaluated as possible replacements for the conventional cobalt-bonded tungsten carbide used in the tip of coal-cutter bits. The metal-bonded diborides were generally less inc endive but more brittle than the conventional tungsten carbide. Carbonitride coatings on tool bits were also tested but found to have no advantage. The source of ignition during frictional impact between metal and rock was studied. Immediately after impact, a yellow flash was observed and a smear of metal near its melting point occurred on the rock. This hotspot on the rock, rather than the yellow flash or sparks or metal fragments, was observed to be the cause of the ignition.

Jan 1, 1974