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By Leon Lorenzen, Trevor J. Britz, Pierre J. Van Zyl, Ellis R. Els

Enhanced granulation of UASB granules was tested on pilot scale with two different test reactors (about 5 litres capacity each). Sludge from a local sewage works was used, with peach cannery effluent as carbon source. Cyclic motion of the reactor contents, and a daily replenishment of feed material create the necessary stress conditions for enhanced growth. Sizable granules, bigger than 0.5 mm, were produced within 20 days. Of the two reactors tested, the reactor equipped with a horizontal agitation shaft proved more effective.

Jan 1, 2003

By M. Gonzalez Fernandez

"Commercially introduced in 2004, the SAGDesign™ test has today proved its efficiency for sizing SAG mills for a wide variety of ores, from very soft to very hard ones. The interest of building a model using the SAGDesign™ test specific energy is the introduction of such a model into a complete process simulator making it possible to predict a complete material balance. The developed model compares the required specific energy with the energy provided by the mill. This energy calculation is derived from the Austin Power Formula. The specific energy provided by the test is corrected, using various parameters, such as the Ball Mill Work Index, to take into account the true operating conditions, the feed and product sizes. The core of this model allows the determination of the product d80 using the mill geometry, its operating conditions and of course the SAGDesign™ test results. To be included in a simulator, the model must also predict the overall size distribution of the SAG mill discharge. Assumptions to answer this point are presented here. The model has been implemented in the USIM PAC simulator. It is used either to predict the product size distribution for a given SAG mill, but also to size a SAG mill for getting a required reduction ratio. INTRODUCTION Over the last few years several types of new comminution machines have been introduced in the market. The most notable newcomer was the HPGR (Morley, 2006). But, even when these machines have some advantages, they have not earned the trust of the mining industry. That is why the established technologies still being the first choice. And, in comminution, that first choice are SAG and ball mills. The design of ball mills has been well understood for a long time. The Bond Ball Mill Work Index is the standard test which helps to describe the ore in terms of energy requirements for milling. Unfortunately, the development of an equivalent test to characterize the ore subject to SAG milling has taken some time. As of today, several tests are available in the market, like the MacPherson test, the MinnovEX SAG Power Index (SPI™), the JK Drop Weight Test, the SMC Test® and the SAGDesign™ test (Verret et al., 2011). The SAGDesign™ test, developed by John Starkey in Canada in the early 2000s (Starkey et al., 2008, 2015), has become one of the standards to assess the grindability of an ore in a SAG mill. One of its advantages is the reduced sample mass needed to perform it, hence, the reduced cost. The second one is that the output of the test is straightforward, it is the energy required to grind the ore between two sizes. Because of this energetic approach, the results provided by the test can be directly applied to size a new mill or to assess the performance of an existing mill."

Jan 1, 2018

By M. Ito

The authors have developed the RETAC jig (a modified TACUB jig) and have reported that the RETAC jig can separate relatively low density particles such as plastics. To further improve the separation ability, a hybrid jig (a RETAC jig with an air bubbler under the particle bed), which can separate plastics having similar specific gravities by the differences in the wettabilities of the particles was developed. Surface modification of plastics with similar wettability enabling separation in the hybrid jig and the effects of wettability control of the plastics using reagents are reported.

Sep 1, 2012

By Crasta Jeason, T. Sreenivas, M. Narasimha

The subtle nature of the flow inside the hydrocyclone has encouraged development of mathematical models for predicting its performance, which are widely used in simulation of comminution circuits. But most of the models available are based on single average feed density. But the feed to hydrocyclone classifier is generally mixture of particles of different densities. This effect of varying density of feed particles on performance of hydrocyclone has been reported in literature. Further investigation of the effect of multi component feed on the performance of hydrocyclone is the objective of this work. This work involves experimental work to study multicomponent behaviour in various size cyclones. The performance of hydrocyclone for feed mixture of magnetite and quartz has been studied. The effect of presence of magnetite, a high density material on efficiency of separation of quartz has been analysed. It was observed that the effect of component interaction increases with feed solids concentration leading to an increased cut-size for a given optimum cyclone conditions. Based on the multi-component exiperiments available in literature, a concept for modeling the performance of hydrocyclones is proposed. A set of semi-empirical model equations for cut-size, sharpness of separation are presented. An attempt to validate the new hydrocyclone model on multi-component behaviour is made.

Jan 1, 2014

By Anuttam Patra, Romain Bordes, Andreas Fredriksson, Tommy Karlkvist, Krister Holmberg, Kota Hanumantha Rao

The present investigation aims to develop and distinguish mineral specific reagents with two functional groups for use in flotation of calcium containing minerals. For this purpose, a series of dicarboxylate-based surfactants with varying length between the carboxylate groups (one, two or three methylene groups) were synthesized. As reference, a surfactant with the same alkyl chain length but with only one carboxylate group in the polar part was synthesized. The adsorption behavior of these new reagents on pure apatite and calcite mineral surfaces was studied using Hallimond tube flotation, FTIR and ? potential measurements. The relation between the adsorption behavior of a given surfactant on a specific mineral surface and its molecular structure over a range of concentration and pH values, as well as the region of maximum recovery were established. It was found that one of the reagents, with a specific distance between the carboxylate groups, was much more selective for a particular mineral surface than the other homologues synthesized. This selective adsorption of a given surfactant to a particular mineral surface relative to other mineral surfaces as evidenced in flotation studies is substantiated by ? potential and infra-red spectroscopy data.

Jan 1, 2014

By S. Banisi, Seyyed Omid Mousavi, Alireza Ghasemi

Discrete Element Method (DEM) is extensively used to simulate the behaviour of particles in various processing units. This method is based on modelling the forces acting between particles in any contact and consequently calculating the new position of particles. The high number of elements and numerous equations needed have made the required computation time very long even using computers with very fast processors. The required computation time mainly depends on the time step. If the time step is chosen very short, the computation time will significantly increase. On the other hand, if the time step is chosen very long, the simulation will be in error due to not fully observing the contacts. In DEM calculations, the time step is chosen as a fraction of the collision time. In this research, a relationship was proposed between the contact time fraction and the error of simulation. In other words, to select the time step in addition to physical parameters, the accuracy of the simulation was also accommodated in the frequently-used relationships. The simulation error was defined as the relative difference between the initial restitution coefficient and the restitution coefficient obtained after simulation. The required time steps to arrive at the simulation error of 5% were calculated for two common contact force models namely, Hertz-Mindlin and linear spring-dashpot. The simulation was performed for two particles with radius of 3 cm, elasticity modulus of 210 GPa, Poisson's ratio of 0.3 and relative velocity of 0.5 m/s. The required time steps were found to be 2.3 and 0.19 µs for the Hertz-Mindlin and the linear spring-dashpot contact force models, respectively. Results showed that with a scaling-down the modulus from 210 GPa to 2.1 MPa, the required time steps for the Hertz-Mindlin and the linear spring-dashpot contact force models, with an equal simulation error, increased by 100 and 316 times, respectively.

Jan 1, 2014

By Claudio Bisso, Javier Vargas, Charles Lozano

"This paper summarizes the activities performed to predict SAG milling throughput at Minera Esperanza. Having highly reliable geometallurgical models aided by the new computer tools and specific metallurgical testing to rely on has become a major issue in recent times due to their impact on the business. Minera Esperanza’s SAG throughput model was constructed by characterizing the ore feed and operational parameters of the plant. Producing a robust model required satisfying number of requirements for the parameters used for both the ore and the plant as follow: 1) geologic and geometallurgical characterization parameters; and 2) parameters of a plant running at the rated production under optimum operating conditions. Obtaining these parameters required increasing the quantity of samples and metallurgical testing through drilling campaigns, mapping the drill holes and putting samples through various comminution tests while sampling all operational flows at the plant to obtain the metallurgical information for the operational parameters. The information was entered on the JKSimMet software to enable a throughput model to be developed to output SAG mill throughput predictions that are very close to actual throughput figures, i.e., accurate within a range of 2% on a monthly basis."

Jan 1, 2014

By T. Fujita

A high-grade fluorite ore is converted into hydrogen fluoride to produce many kinds of materials containing fluorine. Recently, it is becoming necessary to use low-grade fluorite ore due to the depletion of high grade ore. The low-grade fluorites usually have impurities such as SiO2, P, CaCO3 and arsenic. The most impurities such as SiO2, CaCO3 and P can be removed by using flotation method. However, the removal of arsenic is difficult, and the arsenic contamination decreases the hydrogen fluoride production percentage. The novel technologies for processing low-grade fluorite ore are urgently needed, in order to lower the arsenic concentration to less than 100 mg/kg. In this study, the removal of arsenic from low-grade fluorite ore has been investigated by means of an autogenous grinding using tower mill in sulfuric acid aqueous solution and 0.3 mm zirconia balls in water. The nano grinding in water can prevent the dissolution of 0.3 mm size zirconia balls as grinding media by sulfuric acid solution. Experimental results showed that the arsenic concentration was reduced from 260 mg/kg to 90 mg/kg and CaF2 recovery reached 90% by this process.

Sep 1, 2012

By H. Mengbing, A. Potokin, A. Usov

"Revealed and analyzed in the study are the ways of significant perfection of specific characteristics of the equipment, such as use of high-frequency voltage transformation to create a charger; use of pulse transformers, with core made of materials with high magnetic permeability, in pulse generating circuits; as well as use of special ways to produce voltage pulses with a short front. The experiments have proved the possibility to adapt these technological solutions for electric-pulse installations, and suggested on this base is a strategy of further development and application of electric-pulse technologies. The different applications joint work schemes of voltage sources with two levels voltage and energy in electric pulse technologies are investigated. The possibility of increasing energy efficiency of destruction is shown."

Jan 1, 2014

The multiphase reactive flow in process equipments, e.g., fluidized beds, involves complex coupling among flow, heat/mass transfer and reaction kinetics over scales ranging from molecules, sub-particle eddies up to equipments. Conventional two-fluid model (TFM) ignores the effects of meso-scale structures, and hence is not suitable for describing the intrinsically multi-scale heterogeneity within multiphase systems. To be consistent with the meso-scale structures, we proposed a structure-dependent multi-fluid model (SFM), and closed its drag force by invoking the stability condition defined in the energy-minimization multi-scale (EMMS) model. The SFM reduces to the conventional TFM if homogeneous distribution is assumed within each grid, and reverts to the original EMMS model if it is used to describe steady state, global behavior of a fluidized bed. The multi-scale computational fluid dynamics (CFD), which is characterized by coupling of TFM and EMMS drag coefficient, can then be viewed as a simplified solution of the SFM. We demonstrate that the SFM significantly improves the accuracy and at the same time enables higher efficiency by allowing for much coarser grid used than in TFM. Recent application of it in 3D, full-loop, transient simulation of industrial processes, e.g., fluid catalytic cracking, coal combustion, gasification, kaolinite clay calcinations, shows its advantages in helping design and troubleshoot multiphase process equipments. Keywords: meso-scale, SFM, multiscale, CFD, simulation, structure, EMMS, multiphase

Sep 1, 2012

By V. Z. Kozin, E. A. Bekchurina, P. S. Volkov, Yu. P. Morozov, A. S. Komlev

"The current sampling systems of ore flows or concentrates are based on the method of cross sections in point sampling and the method of scooping in reducing. The limited number of point samples in sampling and microsamples in reducing lead to big random and probable systematic errors. The paper defines the principles of sampling, which assure the absence of systematic errors and also provides calculation formulas of probable errors in sampling methods of cross and longitudinal sections as well as in samples preparation. The article sets the fundamental laws of sampling: the dependency of minimal mass of gross sample and number of point samples from mass of point sample in sampling from heterogeneous body; the dependency of a sample minimal mass from lumps’ size in preparation of carefully mixed samples; the dependency of point samples’ dispersion from duration of control period. The paper introduces the fundamental notions: lump variance; probable systematic error; methodical error. It also provides a solution of outstanding sample correct application in analysis results calculations. In application of automatic analyzers, mounted in material flows, the probable error connected with sampling, is calculated by the formulas for carefully mixed sampling bodies. The paper describes the developed and introduced sampling systems on the base of combined application of cross and longitudinal sections methods in sampling and preparation of samples. The advantages of this equipment are compactness, reliability, simplicity in service and operation, and for pulps it is adaptability in pipelines. Application of the developed equipment entirely excludes probable systematic error. The new systems of sampling and preparation of samples are introduced at 25 concentrating plants. Introduction of the developed systems at sampling balance points of concentrating plants allowed double reducing balance deficiency."

Jan 1, 2018

By T. B. M. Himawan

In this study, effect of thiosulphate and oxidation using oxygen were studied in arseno copper ore flotation. Single mineral study of chalcopyrite and tennantite in regard to the aforementioned techniques was also studied. Zeta potential, XPS, contact angle and floatability of single minerals were conducted for each treatment to understand the mechanism. It was revealed that the separation is best conducted in alkaline condition at where there will be interaction between thiosulphate and the mineral surface as well as the formation of hydroxide species in the oxidation using oxygen. From zeta potential of both thiosulphate and oxidation conditioning, it can be found that the reactivity of tennantite is much higher rather than chalcopyrite resulting higher rate of depression on both techniques as shown from contact angle and floatability of each mineral after treatment. XPS spectra confirmed qualitatively and quantitatively the existence of species responsible for the depression of each conditioning techniques. As for the copper ore flotation test, it is the oxidation using oxygen provides best performance after 60 minutes of oxidation. Keywords: tennantite, chalcopyrite, arseno copper ore A, thiosulphate, oxidation using oxygen

Sep 1, 2012

By Sarthak Kaushik

Zeta potential measurements show that the isoelectric point of crandallite, in aqueous solution of 10-2 N sodium chloride is at about pH 5.5. Measurements of turbidity confirm the point of zero charge or crandallite. Calcium ions specifically adsorbed on the surface and thus changed the zeta potential and turbidity. From the measured data, it is confirmed that starch acts as a flocculent for crandallite. Oleic acid, which is a collector used in phosphate ore processing is weakly adsorbed on the surface of crandallite. This results in hydrophobic coagulation of particles resulting in a lower turbidity.

Sep 1, 2012

Dielectrophoresis is a separation technique that uses a non-uniform electrical field to separate particles on the basis of their permittivity. There are many areas of mineral processing that might benefit from the application of dielectrophoresis. These include: coarse removal of gangue, recovery of ultrafine particles, upgrading of flotation concentrates or simply as a laboratory analysis technique. In order to determine the potential value of dielectrophoresis to the mineral processing industry, the response of composite particles was investigated. The electrical properties of composites involve complex relationships between the shape, distribution and permittivity of the individual grains within the rock. The relationship between mineral composition and dielectrophoretic force was measured on single particles from two ore types. The results were used to populate a model that could predict the separation characteristics of the ore. The insights gained from this model separator allowed potential applications of the technology to be examined and their performance evaluated.

Sep 1, 2012

By P. K. N. Raghavan

Bauxite is the principal source for the production of aluminum metal which has gained tremendous importance over the years due to its versatility as a metal capable of substituting almost all of the non-ferrous metals, non metals like wood, plastics, fibre glass, etc. and even steel in many applications. 90% of the high purity alumina needed for the production of this wonder metal in the world comes from bauxite. Even though alternate methods have been developed to produce alumina from non bauxite sources, owing to the high capital and operating costs involved, Bayer process still retains the superiority among all the methods by virtue of its simplicity and favourable economics. Bauxite continues to be the perfect ore for alumina production and its remarkable utilization makes it the most important non-ferrous ore. Most of the Alumina Refineries in the world process different types of bauxite and that too from varied sources. The technology employed in the Alumina Refineries depends on the Bauxite processed, with an ultimate view to produce alumina of required quality in the most efficient manner. Bureau of Indian Standards (BIS) and Indian Bureau of Mines (IBM) had from time to time put forward bauxite specifications for metallurgical and other applications. However, these are found no fully based on alumina technology, present developments and availability of different types of bauxite in the country. The aim of this paper is to provide scheme of metallurgical grading of Indian Bauxite based on the background of alumina processing technologies and availability of various types of bauxite in the country. Efforts are made here to evaluate beneficiation techniques for central Indian Bauxite from the point of view of alumina production. Keywords: bauxite beneficiation, digestion, alumina, gibbsite, bohemite, diaspore

Sep 1, 2012

By K. C. Corin

It is well known that the grinding circuit plays a crucial role in flotation. The effect of pulp chemistry during grinding is often overlooked. It is believed that the surface properties of the minerals can be adjusted during flotation rather than during grinding. However, recent development in surface analysis techniques (TOF-SIMS, XPS, and AES etc.) have proven that the hydrophilic iron hydroxides formed at the mineral surface during grinding make it difficult for collector adsorption, which may result in poor grades and recoveries of the valuable minerals. This study investigated the effect of the pulp chemistry conditions during milling and the subsequent effects on flotation performance of an Nkomati ore. The results have shown that there was approximately 10 % increase in Ni recovery, when the ore was ground at a dissolved oxygen (DO) concentration of 0 ppm (DO-0) in comparison to no gas control during the grinding stage. However, when the pH was changed from 9 to 11, no gas control resulted in a 20 % decrease in the Ni recovery compared to only 5 % decrease in the Ni recovery at DO-0. A noteworthy observation is that controlling a combination of DO and pH during grinding is of critical importance for better floatability and selectivity for such a system. It also became clear from this study that the presence of oxygen is critical to the consumption of xanthate, which is consistent with the general literature. It has been established that grinding at lower DO levels/redox potentials (Eh) in the presence of xanthate significantly improves the flotation performance of the valuable minerals.

Sep 1, 2012

By Anatoly F. Usov, Vyacheslav A. Tsukerman

"The Russian scientists have developed a new energy saving method for an efficient destruction of the sturdy and hard materials (rocks, ores, frozen soils, concrete blocks ets.) - the Electric Pulse Discharge method of materials destruction (EPD). The detailed researches of a broad circle of problems connected to development EPD-disintegration of materials of a various nature and area of use are executed. The electrical and power characteristics of process, physical fundamentals of selectivity of a breakdown and destruction are investigated, the means of electric pulse splitting and refinements of materials are developed, the technological efficiency of disintegration of industrial minerals estimated.One of the most important characteristics of the EPD-disintegration of ores is the high selectivity of destruction, which provides a large ratio of useful minerals' grains opening, and at the same time, it destroy them less. This ensures in the subsequent stages of beneficiation of ores considerable increase of the extraction and improving the quality of concentrates.The technological tests of various industrial minerals have shown a possibility the EPD-disintegration, as a process that provides the best efficiency of disclosure of useful minerals in all types of ores. Technological and economic efficiency of the method of ore beneficiation is the highest for difficult beneficiated ores with rather low extraction by existing methods. The increase of extraction in this case can reach several percents. As a rule, at a EPD-disintegration the disclosure of mineral grains happens in earlier stages of material comminution than at a mechanical comminution, and with less damage of products. This promotes a simplifying the process of ore preparation and for reducing the power consumption."

Jan 1, 2003

By M. Brennan, A. Majumder

"The mineral processing research community has devoted enormous efforts to the modelling of mineral separators over the last 50 years. While many efforts have been made to use only fundamental physics as a basis for the models, fluid flow patterns in separators are not simple while the motion of particle swarms through fluids is extremely complex.One of the simplest separators is the sluice, in which separation takes place in a flowing film a few millimetres thick. The particles are suspended by turbulent eddies and motion relative to the fluid takes place in so-called hindered settling mode.In an effort to test the extent to which fundamental fluid mechanics can provide a prediction of particle separation, a study on a simple parallel-sided sluice has been carried out using glass beads at various particle concentrations and flow rates.The actual particle separation taking place was compared to predictions made by first describing the fluid flow by a modified ‘law of the wall’ model.Particle concentration distributions were described using Hunt’s sediment transport model, assuming the particle eddy diffusion coefficient to be the same as that for the water. Settling velocities were calculated using either the Richardson and Zaki or Brauer and Thiele models. The latter takes into account particle size and density distributions and solids volumetric concentration.The resulting predictions of particle separation are remarkably good, even though the model does not model the local settling velocity in the slurry."

Jan 1, 2003

By D. G. Hulbert

"Mineral processes are complex operations that have been modelled, controlled and simulated by diverse technologies. A review is given of some models of mineral processes in the literature. A new variation of a dynamic process model of flotation is presented. Process models, describing real and relevant physical variables, give a good understanding and good qualitative simulations, but can sometimes require prohibitively difficult and extensive parameter estimations. Process control is usually best done on operational plants by the fitting of system models, which can home in on the plant?s observability, controllability and optimisation. System models can be of a form amenable for use in appropriate techniques for controller design and implementation. The control of milling circuits is discussed in some detail. While simulators use models to predict dynamic or steady-state information, part of their strength lies in their ease of use and their ability to test different types of specifications. Some results are given for a flotation circuit simulator that can be made to solve virtually any permutation of specifications.INTRODUCTIONThe development and application of appropriate technology can lead to better operation of mineral processing plants in industry, so that substantial benefits can be obtained from improved throughputs, efficiencies and product qualities. This paper addresses some of the principles and methods used in the quest for the development and exploitation of such technology. Although the design of processes is often the motivation for modelling and simulation, this paper also targets the use of modelling and simulation for the control and optimum operation of mineral processes. The two processes given the most attention here are flotation and milling.Technologies used in mineral processing range from simple to very complex. Simple technical principles, such as mass and component balances, can yield some simple and effective strategies for modelling and control. However, minerals in particulate form have such complex physical and chemical properties that there appears no end to the complexity that emerges, as more and more factors are taken into consideration in the pursuit of better results and understanding. The situation is aggravated by the complexity of mineral processing plants, which have spatially variable conditions within process units, and complicated interactions between these units."

Jan 1, 2003

By Peter J. Scales

The recovery of water for re-use in minerals processing is an important issue in the reduction of water use in mining, as is the dewatering of tailings to reduce the propensity of ?wet? tailings dams. It is common in these dewatering operations to use thickeners whereby polymeric flocculants are combined with the dilute feed to the thickener to aid sedimentation and the subsequent consolidation of particulate materials. Thickeners are the workhorses of water recovery and tailings dewatering and although the basics are well understood, there is still no ability to reliably predict the throughput and underflow density from a thickener based on traditional sedimentation tests and flux analysis. The reasons for the discrepancy between full-scale operations and predictions based on laboratory tests are numerous, including difficulties in mimicking the flocculation conditions experienced in the field and the shear conditions in the thickener. The latter effects are little understood and hard to quantify and include effects due to flocculated aggregate densification, complimentary shear and compressional effects and aggregate break-up. Developing a set of test protocols to quantify the effects of densification, shear in compression effects and aggregate breakup and the subsequent contributions of each to compressional dewatering in a thickening environment has been completed for a simple model polymer flocculated particulate suspension. The data and analysis shows that aggregate densification is a dominant contributor to the difference between observed and predicted behavior based on laboratory tests. A major consideration in the analysis is the fact that common thickener operations are permeability limited and although the various effects are all important, the one that results in the fastest water release is dominant. Of interest also are the shear rate, concentration, and time dependence of the aggregate densification process. A basic model of the process has been developed along with network yielding tests conducted using rheometry. Keywords: compressional dewatering, gravity thickening, rheometry, aggregate densification, raked batch settling

Sep 1, 2012